CN110358630A - A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette - Google Patents
A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette Download PDFInfo
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- CN110358630A CN110358630A CN201910553195.5A CN201910553195A CN110358630A CN 110358630 A CN110358630 A CN 110358630A CN 201910553195 A CN201910553195 A CN 201910553195A CN 110358630 A CN110358630 A CN 110358630A
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- spicy
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to technical field of tobacco processing, and in particular to a kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette.Clear spicy tobacco aromaticss of the present invention, be made of the raw material of following mass percent: 20%-30% Chinese prickly ash bud-leaf, 30%-60% perilla leaf and 20%-40% touch perfume (or spice), in cigarette preparation process, organic solvent dissolved with the clear spicy tobacco aromaticss is uniformly sprayed on pipe tobacco, when the additive amount of clear spicy tobacco aromaticss accounts for the 0.01 ~ 0.1% of pipe tobacco weight, cigarette smoke can be enriched, effective flavouring effect is played to cigarette products, the extract can also assign cigarette unique note, prominent cigarette characteristic, it is whole to promote cigarette interior quality.For the extract as tobacco aromaticss, effect is obvious, has good application prospect to the cigarette products with distinctive style, is suitable for cigarette industry metaplasia and produces.
Description
Technical field
The invention belongs to technical field of tobacco processing, and in particular to a kind of clear spicy tobacco aromaticss, preparation method and
Application in cigarette.
Background technique
Tobacco aromaticss are the important components during cigarette brand is cultivated, and protrude the personalized style of cigarette product
Important means, while reducing coke tar in cigarette, the fragrance matter of the tobacco being present in tar inherently can inevitably be damaged
The problem of losing, the style and features such as cigarette flavor loss, sense organ degree of comfort decreased caused to weaken, and natural perfume material has note only
It is special, naturally, fragrance coordinates plentiful, the features such as lasting is lasting, therefore find effective flavor component as low coke from natural plants
Oily tobacco aromaticss, it has also become the inexorable trend of cigarette development.
Chinese prickly ash is Rutaceae xanthoxylum, machaka or dungarunga, originates in East Asia and North America, global there are about 250 kinds,
China has nearly 60 kinds, blazons China, each provinces and regions, north and south.Chinese prickly ash has fragrance and spicy characteristic, edible and medicinal, can promote saliva
Liquid secretion, increases appetite, has antiulcer, anti diar rhea, liver protection, cardioprotection, blood pressure lowering, anticoagulation, inhibits pathogenic microorganism, is anti-
The effects of cancer.Domestic and foreign scholars have carried out series of studies to the chemical component of Chinese prickly ash, it is found that it contains volatile oil, alkaloid, Huang
The ingredients such as letones, organic acid.
Since Chinese prickly ash has special strong aroma, adds in cigarette, can assign cigarette special aromatic style.But flower
Green pepper acrid flavour, fiber crops and it is lasting, while abundant cigarette perfume, also will increase stimulation of the cigarette to oral cavity and nasal cavity, destroy the mouth of cigarette
Sense.Notification number is that the Chinese patent of CN102499433B discloses a kind of Chinese prickly ash alcohol extracting thing answering in perfuming cigarette charging
With, by extraction Chinese prickly ash alcohol, so that pepper extract had not only been remained the Main Fragrance in Chinese prickly ash, but also eliminate wood fibre etc.
Impurity, not only method is simple but also can be improved cigarette sucks texture.
Purple perilla alias: osmanthus is weak, common perilla, red Soviet Union etc., is Labiatae annual herb plant, North China, Central China, south China,
There are wild species and cultivar in southwest and Taiwan Province.It breaks with special fragrance, the more shrinkage curlings of blade, the purple green of spray
Middle face has marrow, gas faint scent, taste micro-pungent.
The substances such as volatile oil rich in, glucoside, flavonoids, organic acid, sterols in perilla leaf, by perilla leaf
The extractive of perilla (or perilla herb oil etc.) of preparation be GB-2760 allow using food additives and food, daily use chemicals, tobacco
In one of common fragrance kind.According to " similar to mix " principle, extractive of perilla generally uses water to mention or alcohol extraction process.But
Simple water mentions or alcohol extraction process, can only extract polarity ingredient similar or similar with Extraction solvent, other polarity and extraction are molten
The biggish ingredient of agent difference can not be extracted effectively, cannot achieve effective comprehensive utilization of perilla leaf.
Fragrant also referred to as villus Rabdosia amethystoides is touched, is a kind of potted plant that can distribute fragrance.Because that can be given out after touching
The fragrance of comfortable and gain the name, and because of its thick flavor sweet tea, quite like apple aroma, therefore enjoy " apple is fragrant " good reputation again, Wen Zhiling
People's spirit and QI cleaning；Can clearing away summerheat, mosquito repellent.
Summary of the invention
The purpose of the present invention is to provide a kind of clear spicy tobacco aromaticss, and add as low tar tobacco aromaticss
Agent is added in cigarette, to solve the problem of to lead to fragrance loss due to reducing tar content content in existing cigarette preparation process.
The present invention also provides the preparation method of above-mentioned clear spicy tobacco aromaticss and the clear spicy tobacco aromaticss
Application in cigarette blending.
To achieve the goals above, the invention adopts the following technical scheme:
A kind of clear spicy tobacco aromaticss, are made of the raw material of following mass percent: 20%-30% Chinese prickly ash bud-leaf, 30%-60% are purple
Perilla leaf and 20%-40% touch perfume (or spice).
Preferably, the clear spicy tobacco aromaticss, are made of the raw material of following mass percent: 20% Chinese prickly ash bud-leaf,
40% perilla leaf and 40% touch perfume (or spice).
The preparation method of the clear spicy tobacco aromaticss, comprising the following steps:
(1) it pre-processes: winning fresh Chinese prickly ash bud-leaf, perilla leaf and touch spiceleaf and cleaned with clear water, drain, be put into baking oven, 50-
It is dried under the conditions of 70 DEG C, 60 meshes is crossed after three plant leafs after drying are ground；
(2) distillation extraction:, which taking Chinese prickly ash bud, perilla leaf, and touches face powder end is mixed, and addition weight is powder total weight 10-20
Distilled water again, water-bath 3-5h；Aroma substance is extracted under water bath with ether again, obtains a feed liquid；
(3) concentration purification: anhydrous sodium sulfate being added into the feed liquid that step (2) is obtained by extraction, and dry 6-8 h takes supernatant
Liquid obtains secondary feed liquid；Secondary feed liquid is carried out to rotary evaporation under conditions of water-bath and is concentrated, the substance after concentration is institute
State clear spicy tobacco aromaticss.
Specifically, every 50g Chinese prickly ash bud in step (2), perilla leaf and touching 30-50 mL second being added in fragrant mixed-powder
Ether is extracted；
Specifically, every 50g Chinese prickly ash bud in step (3), perilla leaf and touching the defective material that fragrant mixed-powder obtains after extracting
10-30 g anhydrous sodium sulfate is added in liquid.
Preferably, bath temperature described in step (2) is 55-65 DEG C.
Preferably, bath temperature described in step (3) is 35-50 DEG C.
Application of the clear spicy tobacco aromaticss in cigarette blending, in application, in cigarette preparation process, it will be clear pungent
Odor type tobacco aromaticss, which are dissolved in organic solvent, obtains blending solution, and blending solution is uniformly sprayed on pipe tobacco, makes clear Xin Xiang
The additive amount of type tobacco aromaticss accounts for the 0.01 ~ 0.1% of pipe tobacco weight.
Specifically, the organic solvent is the ethyl alcohol of volume fraction 90-95%.
The beneficial effects of the present invention are:
1, gained fragrance contains the distinctive pungent fragrant characteristic flavor compounds of Chinese prickly ash bud, and with purple perilla and touches fragrant faint scent sense, fragrant
Taste is pure and mild full, and holding fragrance can be good.
2, gained fragrance can enrich cigarette smoke on perfuming cigarette, play effective flavouring to cigarette products and make
With the extract can also assign cigarette unique note, prominent cigarette characteristic, whole to promote cigarette interior quality.
3, low in cost, simple process is safe and healthy, and raw material and processing technology are widely used in field of food, no
There are poisonous substance residue problems.
4, the present invention be clear spicy tobacco aromaticss extract open a new application field, increase Chinese prickly ash bud,
The purple perilla effect and effect new with perfume is touched.For the extract as tobacco aromaticss, effect is obvious, to the cigarette with distinctive style
Product has good application prospect, is suitable for cigarette industry metaplasia and produces.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail, and embodiments of the present invention are not limited thereto.
The equipment used when rotary evaporation in following embodiments is LC-RE-52A type Rotary Evaporators.Using length in following implementation
Degree is the Chinese prickly ash bud-leaf of 1-2cm.
Embodiment 1
A kind of clear spicy tobacco aromaticss, are made of raw material from the following weight: 10 g of Chinese prickly ash bud, 20 g of purple perilla, touching perfume 20
g.The preparation method of the composite natral plant extracting solution the following steps are included:
(1) it pre-processes: winning fresh Chinese prickly ash bud-leaf, perilla leaf and touch spiceleaf and cleaned with clear water, drain, be put into baking oven, 60
It is dried under the conditions of DEG C, 60 meshes is crossed after three plant leafs after drying are ground；
(2) distillation extraction: taking Chinese prickly ash bud, perilla leaf, touch the mixing of face powder end, take Chinese prickly ash bud, purple perilla and touch fragrant mixed-powder,
1000 mL distilled water are added, 55 DEG C of heating 4h of water-bath extract aroma substance under 60 DEG C of water baths with 30 mL ether solvents,
Obtain a feed liquid；
(3) concentration purification: 15 g anhydrous sodium sulfates being added into the feed liquid that step (2) is obtained by extraction, and dry 6 h take
Clear liquid obtains secondary feed liquid；By secondary feed liquid under the conditions of bath temperature is 45 DEG C, rotary evaporation, the substance after concentration are carried out
As extract A.
Embodiment 2
A kind of clear spicy tobacco aromaticss, are made of raw material from the following weight: 12.5 g of Chinese prickly ash bud, 25 g of purple perilla, touching perfume (or spice)
12.5 g.The preparation methods of the clear spicy tobacco aromaticss the following steps are included:
(1) pre-treatment step is same as Example 1；
(2) distillation extraction: taking Chinese prickly ash bud, purple perilla and touches fragrant mixed-powder, and 1000 mL distilled water, 65 DEG C of water-bath heating are added
3.5 hours, aroma substance is extracted under 60 DEG C of environment of water-bath with 40 mL ether solvents, obtains a feed liquid；
(3) concentration purification: 20 g anhydrous sodium sulfates being added into the feed liquid that step (2) is obtained by extraction, and dry 7 h take
Clear liquid obtains secondary feed liquid；By secondary feed liquid under the conditions of bath temperature is 48 DEG C, rotary evaporation, the substance after concentration are carried out
As extract B.
Embodiment 3
A kind of clear spicy tobacco aromaticss, are made of raw material from the following weight: 15 g of Chinese prickly ash bud, 20 g of purple perilla, touching perfume 15
g.The preparation methods of the clear spicy tobacco aromaticss the following steps are included:
(1) pre-treatment step is same as Example 1；
(2) distillation extraction: taking Chinese prickly ash bud, purple perilla and touches fragrant mixed-powder, and 1000 mL distilled water, 60 DEG C of water-bath heating 5 are added
Hour, aroma substance is extracted under 60 DEG C of environment of water-bath with 40 mL ether solvents, obtains a feed liquid；
(3) concentration purification: about 30 g anhydrous sodium sulfates being added into the feed liquid that step (2) is obtained by extraction, and dry 7.5 h,
Supernatant is taken, secondary feed liquid is obtained；By secondary feed liquid in the case where bath temperature is 47 DEG C of the following conditions, rotary evaporation, concentration are carried out
Substance afterwards is extract C.
Comparative example 1
The Chinese prickly ash bud powder that 50 g are pretreated is taken, 1000 mL distilled water are added, 55 DEG C of water-bath are heated 4 hours, with 30 mL second
Ether solvents extract aroma substance under 60 DEG C of water baths, obtain a feed liquid.About 15 are added into a feed liquid extracted
G anhydrous sodium sulfate, dry 6 h, takes supernatant, obtains secondary feed liquid；By secondary feed liquid under the conditions of bath temperature is 45 DEG C, into
Row rotary evaporation, the substance after concentration are extract D.
Comparative example 2
The purple perilla powder that 50 g are pretreated is taken, 1000 mL distilled water are added, 55 DEG C of water-bath are heated 4 hours, with 30 mL ether
Solvent extracts aroma substance under 60 DEG C of water baths, obtains a feed liquid.About 15 g are added into a feed liquid extracted
Anhydrous sodium sulfate, dry 6 h, takes supernatant, obtains secondary feed liquid；By secondary feed liquid under the conditions of bath temperature is 45 DEG C, into
Row rotary evaporation, the substance after concentration are extract E.
Comparative example 3
Taking 50 g pretreated touching, face powder is last, and 1000 mL distilled water of addition, 55 DEG C of water-bath are heated 4 hours, with 30 mL second
Ether solvents extract aroma substance under 60 DEG C of water baths, obtain a feed liquid.About 15 are added into a feed liquid extracted
G anhydrous sodium sulfate, dry 6 h, takes supernatant, obtains secondary feed liquid；By secondary feed liquid under the conditions of bath temperature is 45 DEG C, into
Row rotary evaporation, the substance after concentration are extract F.
Test example 1
By the extract of obtained clear the spicy tobacco aromaticss extract and comparative example 1-3 of embodiment 1-3, it is dissolved in volume point
Blending solution is obtained in the ethyl alcohol of number 95%, and blending solution is uniformly sprayed on pipe tobacco, and the additive amount of extract is made to account for pipe tobacco
The 0.05% of weight, according to Conventional feed introduction process, equilibrium water conten to 14%, in the case where other consistent, pipe tobacco is passed through
Cigarette machine rolls into test sample cigarette, and the expert that smokes panel test carries out sensory quality assessment to flavoring cigarette.The cigarette of extract will not added
As a result the cigarette that silk rolls into see the table below 1 as control.
Influence of 1 extract of table to Sensory Quality of Cigarette.
The result shows that the cigarette of purple perilla and Chinese prickly ash bud extract is used alone, Xin Xiang is prominent, but pleasant impression comfort is poor, thorn
It is obvious to swash property.The cigarette for touching fragrant extract is used alone, slightly, pleasant impression is refrigerant for faint scent, and mouthfeel is moistened only, and irritation is smaller.Add
Adding Chinese prickly ash bud, purple perilla and the cigarette for touching fragrant three kinds of substance extracts, full aroma is abundant, and harmony is good, and it is clear pungent fragrant prominent, it is remaining
Taste makes moderate progress.
Test example 2
A, B and C tri- clear spicy tobacco aromaticss extracts obtained above are detected, analyze main chemical compositions content, as a result
It see the table below 2.
The clear pungent fragrant extract main chemical compositions comparision contents (%) of 2 different ratio of table.
Perillaldehyde has pungent fragrant fragrance；Limonene has unique fragrant；Linalool has the wooden green gas of dense leukorrhagia with greenish discharge sweet tea
Breath, like rose wood fragrance, soft aroma and, lightly float hair；Ocimenum has hay-scented, the fragrance of a flower and with neroli oil breath, and fragrance is clear
New hair thoroughly；Laurene is present in Chinese prickly ash bud, there is light balsamic odour；Bergamio has the fragrance of a flower and fruity；Perilla alcohol
With hay-scented, slightly radix aucklandiae and the fragrance of a flower；Citral has citrus scented.The result shows that Chinese prickly ash bud-leaf, perilla leaf and touching spiceleaf
Proportion it is different, the content of contained aroma substance is also different.
Test example 3
It takes 50 g Chinese prickly ash buds, purple perilla and to touch fragrant mixed-powder (10 g of Chinese prickly ash bud, 20 g of purple perilla, touching 20 g of perfume) preparation clear pungent
Fragrant extract, specific implementation step is same as Example 1, and extractant is only changed to ethyl alcohol, and concentrate obtained is to extract
The content of object G, Detection and Extraction object A and extract G aroma substance (perillaldehyde, limonene, ocimenum, linalool and laurene),
And two extracts are dissolved in the ethyl alcohol of volume fraction 95% and obtain blending solution, and blending solution is uniformly sprayed at pipe tobacco
On, so that the additive amount of extract is accounted for the 0.05% of pipe tobacco weight, according to Conventional feed introduction process, equilibrium water conten to 14%, at it
In the case that it is consistent, pipe tobacco rolls into test sample cigarette through cigarette machine, and the expert that smokes panel test carries out sense organ to flavoring cigarette
As a result quality evaluation see the table below 3.
The different extractants of table 3 extract influence of the clear spice substance to Sensory Quality of Cigarette.
It is obtained the result shows that the extract key odorant content of material obtained using ether solvent is more than using alcohol solvent
Aroma substance, it is clear pungent fragrant prominent in conjunction with sensory evaluating smoking as a result, showing that the cigarette smoke fragrance for adding extract A is full abundant,
It is obvious to increase characteristic fragrance effects.
Test example 4
Extract A is dissolved in the ethyl alcohol of volume fraction 95% and obtains blending solution by the extract A that embodiment 1 is obtained, and will
Blending solution is uniformly sprayed on pipe tobacco, and the additive amount of extract is made to account for 0.02%, 0.04%, 0.06% and of pipe tobacco weight
0.08%, according to Conventional feed introduction process, equilibrium water conten to 14%, in the case where other consistent, pipe tobacco is through cigarette machine
Test sample cigarette is rolled into, the expert that smokes panel test carries out sensory quality assessment to flavoring cigarette, as a result see the table below 4.
Wherein, sense organ total score (T)=(A+B) × 2.0+(C+D) × 1.5+E+F+G+H.
Influence of the clear pungent fragrant extract Different adding amount of table 4 to Sensory Quality of Cigarette.
The result shows that from aroma quality (A), perfume quantity (B), concentration (C), soft and fine degree (D), pleasant impression (E), miscellaneous gas (G), stimulation
Property (H), the aspect marking of strength (F) 8, aesthetic quality is preferable when addition 0.04% and 0.06%, and score is respectively 68.25 Hes
68.75, generally speaking, aesthetic quality is best when adding 0.06%.
In conclusion the present invention, as a kind of natural plant extracts with clear spicy, being used in can in perfuming cigarette
Significantly to increase the clear pungent fragrant feature of cigarette, it is worth the application in the production of cigarette novelty.
Above-described embodiment be embodiment of the present invention for example, embodiments of the present invention not by above-described embodiment
Limitation, it is other any without departing from made changes, modifications, substitutions, combinations, simplifications under spirit of the invention and principle,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (10)
1. a kind of clear spicy tobacco aromaticss, which is characterized in that be made of the raw material of following mass percent: 20%-30% Chinese prickly ash
Bud-leaf, 30%-60% perilla leaf and 20%-40% touch perfume (or spice).
2. clear spicy tobacco aromaticss as described in claim 1, which is characterized in that by the raw material group of following mass percent
At: 20% Chinese prickly ash bud-leaf, 40% perilla leaf and 40% touch perfume (or spice).
3. the preparation method of any clear spicy tobacco aromaticss of claim 1-2, which comprises the following steps:
(1) spiceleaf cleaning is pre-processed: winning fresh Chinese prickly ash bud-leaf, perilla leaf and touch, dries, grinds under the conditions of 50-70 DEG C
After be sieved；
(2) distillation extraction:, which taking Chinese prickly ash bud, perilla leaf, and touches face powder end is mixed, and addition weight is powder total weight 10-20
Distilled water again, water-bath 3-5h；Aroma substance is extracted under water bath with ether again, obtains a feed liquid；
(3) concentration purification: anhydrous sodium sulfate being added into the feed liquid that step (2) is obtained by extraction, and dry 6-8 h takes supernatant
Liquid obtains secondary feed liquid；Secondary feed liquid is carried out to rotary evaporation under conditions of water-bath and is concentrated, the substance after concentration is institute
State clear spicy tobacco aromaticss.
4. preparation method as claimed in claim 3, which is characterized in that every 50g Chinese prickly ash bud, perilla leaf and touched in step (2)
30-50 mL ether is added in fragrant mixed-powder to be extracted.
5. preparation method as claimed in claim 3, which is characterized in that every 50g Chinese prickly ash bud, perilla leaf and touched in step (3)
10-30 g anhydrous sodium sulfate is added in the feed liquid that fragrant mixed-powder obtains after extracting.
6. preparation method as claimed in claim 3, which is characterized in that bath temperature described in step (2) is 55-65 DEG C.
7. preparation method as claimed in claim 3, which is characterized in that bath temperature described in step (3) is 35-50 DEG C.
8. application of any clear spicy tobacco aromaticss of claim 1-2 in cigarette blending.
9. application as claimed in claim 8, which is characterized in that in application, using clear spicy cigarette in cigarette preparation process
Fragrance, which is dissolved in organic solvent, obtains blending solution, and blending solution is uniformly sprayed on pipe tobacco, keeps clear spicy cigarette fragrant
The additive amount of material accounts for the 0.01 ~ 0.1% of pipe tobacco weight.
10. application as claimed in claim 9, which is characterized in that the organic solvent is the ethyl alcohol of volume fraction 90-95%.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114468345A (en) * | 2021-12-28 | 2022-05-13 | 四川三联新材料有限公司 | Electronic cigarette liquid with pepper flavor and preparation method thereof |
| CN116369581A (en) * | 2023-03-30 | 2023-07-04 | 江苏中烟工业有限责任公司 | Incense base module for showing sweet and spicy fragrance of fruits and application of incense base module in cigarettes with different circumferences |
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| CN104099181A (en) * | 2014-07-08 | 2014-10-15 | 韩城市秦龙花椒科技有限责任公司 | Method for extracting aromatic oil from Chinese prickly ash shoots |
| CN104327952A (en) * | 2014-10-27 | 2015-02-04 | 山西大学 | Pelargonium odoratissimum essential oil and extraction method and application of essential oil |
| CN104479874A (en) * | 2014-10-25 | 2015-04-01 | 韩城市秦龙花椒科技有限责任公司 | Extraction equipment and extraction method of zanthoxylum bungeanum leaf aromatic oil |
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| CN101602982A (en) * | 2008-06-11 | 2009-12-16 | 湖北中烟工业有限责任公司 | The step-by-step extracting method of purple perilla and extract obtained application in cigarette |
| CN104099181A (en) * | 2014-07-08 | 2014-10-15 | 韩城市秦龙花椒科技有限责任公司 | Method for extracting aromatic oil from Chinese prickly ash shoots |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114468345A (en) * | 2021-12-28 | 2022-05-13 | 四川三联新材料有限公司 | Electronic cigarette liquid with pepper flavor and preparation method thereof |
| CN114468345B (en) * | 2021-12-28 | 2022-11-15 | 四川三联新材料有限公司 | Electronic cigarette liquid with pepper flavor and preparation method thereof |
| CN116369581A (en) * | 2023-03-30 | 2023-07-04 | 江苏中烟工业有限责任公司 | Incense base module for showing sweet and spicy fragrance of fruits and application of incense base module in cigarettes with different circumferences |
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| CN110358630B (en) | 2022-09-20 |
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