CN104099181A - Method for extracting aromatic oil from Chinese prickly ash shoots - Google Patents
Method for extracting aromatic oil from Chinese prickly ash shoots Download PDFInfo
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- CN104099181A CN104099181A CN201410338720.9A CN201410338720A CN104099181A CN 104099181 A CN104099181 A CN 104099181A CN 201410338720 A CN201410338720 A CN 201410338720A CN 104099181 A CN104099181 A CN 104099181A
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- oil
- prickly ash
- chinese prickly
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Abstract
The invention relates to a method for extracting aromatic oil from Chinese prickly ash shoots. Chinese prickly ash shoots at senescence stage are utilized for extracting multi-purpose vegetable oil. The method comprises seven procedures as follows: purchasing of the Chinese prickly ash shoots, installation of vegetable oil extraction equipment, purchasing of petroleum ether soluble oil, treatment of the Chinese prickly ash shoots, extraction of crude aromatic oil of the Chinese prickly ash shoots, recovery of petroleum ether soluble oil, and chromatography, filtration and package of the crude aromatic oil of the Chinese prickly ash shoots. The aromatic oil of the Chinese prickly ash shoots processed by the vegetable oil extraction equipment not only has aromatic odor, but also contains volatile components and aliphatic acid components with abundant nutrients and can be used as a daily-use chemical product raw material and a functional food raw material, cheap agricultural products are more sufficiently used, and the purpose of increase of enterprise efficiency and farmer incomes can be achieved simultaneously.
Description
Affiliated technical field
The extracting method of Chinese prickly ash bud-leaf perfume oil of the present invention relates to Chemicals manufacture field, relates in particular to the production technique of utilizing Chinese prickly ash bud-leaf processing vegetable oil.
Background technology
Zanthoxylum rutaceae, in China, cultivation history is long, economic worth is very high, Adaptable growth field is extensive, there is easy cultivation, good management, good growth, result early, the feature that income is large, whole nation cultivated area is very large, but time limit in its 10-15 only in best fruiting period, enter after senescence phase thereupon, tree body growing way is growing on and on, with luxuriant foliage and spreading branches in leafy profusion but result declines year by year, the Pricklyash Garden area that enters senescence phase is expanding year by year, because Chinese prickly ash bud-leaf contains abundant aromatic vegetable oil, , in addition tender leaf collection period is long, output is high, production cost is low, made concessions and be widely used by the technology of Chinese prickly ash bud-leaf exploitation pepper bud, I utilize Chinese prickly ash bud composite seasoning sauce and the food of the exploitation of Chinese prickly ash bud-leaf also to obtain application, and give and utilize Chinese prickly ash bud-leaf exploitation perfume oil that raw material sources are provided, also will bring the new way of widening income to green pepper agriculture.
Technical scheme
The object of this invention is: gather Chinese pricklyash bud-leaf senescence phase, utilize vegetables oil extraction equipment to process Chinese prickly ash bud-leaf perfume oil, not only will keep pungent fragrance taste, also will become multiduty industrial chemicals and food raw material, and want promoting enterprise synergy increasing peasant income.
To achieve these goals, the technical solution used in the present invention is: take dried flower green pepper bud-leaf is first ground into fine silt as basis, select respectively again vegetables oil extraction equipment to extract perfume oil, the extracting method of Chinese prickly ash bud-leaf perfume oil is that Chinese prickly ash bud-leaf buying, vegetables oil extraction equipment are installed, the molten oil of sherwood oil is bought, processings of Chinese prickly ash bud-leaf, the extraction of Chinese prickly ash bud-leaf perfume oil crude oil, the molten recovery of oil of sherwood oil, Chinese prickly ash bud-leaf perfume oil are analysed and layer filtered and packaged seven road programs, first utilizes spring Chinese prickly ash bud-leaf to grow to and fall leaves that to purchase dried flower green pepper bud-leaf season standby late autumn; Selection and installation advanced person's vegetables oil extraction equipment again; Before processing, buying the molten oil measure of sherwood oil deposits in secure closed tank standby; Again standby dried flower green pepper bud-leaf being crossed to 30 mesh sieves by mechanical disintegration, to obtain Chinese prickly ash bud-leaf powder standby; Add and man-hour standby Chinese prickly ash bud-leaf powder is added in vegetables oil extraction equipment, after petroleum ether extraction leaches, obtain Chinese prickly ash bud-leaf perfume oil crude oil; And reclaim the molten oil measure of sherwood oil and deposit; Finally get the seasoning of Chinese prickly ash bud-leaf perfume oil crude oil in refrigerating chamber, control temperature between 0--15 ℃, after first quarter moon refrigeration, take out and filter, abandon after depositing cured shape greasy filth and obtain limpid Chinese prickly ash bud-leaf perfume oil.
Through document, record, in Chinese prickly ash bud-leaf perfume oil, be rich in ethereal oil and fatty acid grease, wherein volatile oil main component is the precious compositions such as limonene, Elemenum, myrcene, terpinene, phantol, Geraniol, piperitone, in lipid acid, be also rich in linoleic acid plus linolenic acid, Chinese prickly ash bud-leaf perfume oil not only can be used for the daily chemical product raw materials such as perfumed soap, paste shampoo accordingly, also can be used for processing functional foodstuff; Owing to containing piperitone in Chinese prickly ash bud-leaf perfume oil, can guarantee that shelf life of products reaches more than 5 years.
The invention has the beneficial effects as follows: gather purchase Chinese pricklyash bud-leaf senescence phase, utilize vegetables oil extraction equipment to process Chinese prickly ash bud-leaf perfume oil, not only there is aromatic odour, the volatile component and the fatty acid component that also contain abundant nutrition, can become daily chemical product raw material and machining functions food raw material, more take full advantage of cheap agricultural prods, and can realize the target of enterprise's synergy increasing peasant income simultaneously.
Embodiment
1, Chinese prickly ash bud-leaf buying: first utilize spring Chinese prickly ash bud-leaf to grow to and fall leaves that to purchase dried flower green pepper bud-leaf season standby late autumn, also can purchase autumn and winter Chinese pricklyash fallen leaves standby.
2, vegetables oil extraction equipment is installed: selection and installation advanced person's vegetables oil extraction equipment, supporting good warming-up device, starting material conveying belt, molten oil adds and recovery channel and Chinese prickly ash bud-leaf crude oil transport pipe.
3, the molten oil of sherwood oil is bought: before processing, buy the molten oil of sherwood oil and deposit in secure closed tank standbyly, it is 60-90 ℃ of product that sherwood oil is selected volatilization temperature.
4, Chinese prickly ash bud-leaf is processed: standby dried flower green pepper bud-leaf is crossed to 30 mesh sieves by mechanical disintegration, and to obtain Chinese prickly ash bud-leaf powder standby.
5, Chinese prickly ash bud-leaf perfume oil crude oil extracts: add and man-hour standby Chinese prickly ash bud-leaf powder is added in vegetables oil extraction equipment through conveying belt, obtain Chinese prickly ash bud-leaf perfume oil crude oil after petroleum ether extraction leaches.
6, the molten recovery of oil of sherwood oil: store after reclaiming the molten oil of sherwood oil.
7, Chinese prickly ash bud-leaf perfume oil is analysed layer and is filtered and packaged: finally get the seasoning of Chinese prickly ash bud-leaf perfume oil crude oil in refrigerating chamber, control temperature between 0--15 ℃, after first quarter moon refrigeration, take out and filter, abandon after depositing cured shape greasy filth and obtain limpid Chinese prickly ash bud-leaf perfume oil.
Claims (1)
1. the extracting method of a Chinese prickly ash bud-leaf perfume oil, it is characterized in that: the extracting method of Chinese prickly ash bud-leaf perfume oil is that Chinese prickly ash bud-leaf buying, vegetables oil extraction equipment are installed, the molten oil of sherwood oil is bought, processings of Chinese prickly ash bud-leaf, the extraction of Chinese prickly ash bud-leaf perfume oil crude oil, the molten recovery of oil of sherwood oil, Chinese prickly ash bud-leaf perfume oil are analysed and layer filtered and packaged seven road programs, first utilize spring Chinese prickly ash bud-leaf to grow to and fall leaves that to purchase dried flower green pepper bud-leaf season standby late autumn; Selection and installation advanced person's vegetables oil extraction equipment again; Before processing, buying the molten oil measure of sherwood oil deposits in secure closed tank standby; Again standby dried flower green pepper bud-leaf being crossed to 30 mesh sieves by mechanical disintegration, to obtain Chinese prickly ash bud-leaf powder standby; Add and man-hour standby Chinese prickly ash bud-leaf powder is added in vegetables oil extraction equipment, after petroleum ether extraction leaches, obtain Chinese prickly ash bud-leaf perfume oil crude oil; And reclaim the molten oil measure of sherwood oil and deposit; Finally get the seasoning of Chinese prickly ash bud-leaf perfume oil crude oil in refrigerating chamber, control temperature between 0--15 ℃, after first quarter moon refrigeration, take out and filter, abandon after depositing cured shape greasy filth and obtain limpid Chinese prickly ash bud-leaf perfume oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410338720.9A CN104099181A (en) | 2014-07-08 | 2014-07-08 | Method for extracting aromatic oil from Chinese prickly ash shoots |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410338720.9A CN104099181A (en) | 2014-07-08 | 2014-07-08 | Method for extracting aromatic oil from Chinese prickly ash shoots |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104099181A true CN104099181A (en) | 2014-10-15 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410338720.9A Pending CN104099181A (en) | 2014-07-08 | 2014-07-08 | Method for extracting aromatic oil from Chinese prickly ash shoots |
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| CN (1) | CN104099181A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104479874A (en) * | 2014-10-25 | 2015-04-01 | 韩城市秦龙花椒科技有限责任公司 | Extraction equipment and extraction method of zanthoxylum bungeanum leaf aromatic oil |
| CN110358630A (en) * | 2019-06-25 | 2019-10-22 | 河南中烟工业有限责任公司 | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette |
-
2014
- 2014-07-08 CN CN201410338720.9A patent/CN104099181A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104479874A (en) * | 2014-10-25 | 2015-04-01 | 韩城市秦龙花椒科技有限责任公司 | Extraction equipment and extraction method of zanthoxylum bungeanum leaf aromatic oil |
| CN110358630A (en) * | 2019-06-25 | 2019-10-22 | 河南中烟工业有限责任公司 | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette |
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| C06 | Publication | ||
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Application publication date: 20141015 |
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| WD01 | Invention patent application deemed withdrawn after publication |