CN104130863B - A kind of agate card extract and preparation method thereof and the application in cigarette - Google Patents
A kind of agate card extract and preparation method thereof and the application in cigarette Download PDFInfo
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- CN104130863B CN104130863B CN201410336561.9A CN201410336561A CN104130863B CN 104130863 B CN104130863 B CN 104130863B CN 201410336561 A CN201410336561 A CN 201410336561A CN 104130863 B CN104130863 B CN 104130863B
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Abstract
The present invention relates to a kind of agate card extract and preparation method thereof and the application in cigarette, belong to tobacco aromatics technical field.Agate card extract of the present invention obtains by the following method: pulverize after being dried by agate card rhizome, sieve; The maca powder end obtained after taking sieve, adds solvent, soaks, water-bath refluxing extraction, filtration, concentrated i.e. get Ma Ka extract.The application of agate card extract of the present invention in cigarette: agate card extract in cigarette shreds, thin slice or offal weight 0.1 ~ 10 ‰ ratio, be dissolved in the solution of certain density ethanol or certain density ethanol and propane diols, and be sprayed on cigarette shreds, thin slice or offal equably, and roll into cigarette, the cigarette adding agate card extract have sweet soft, improve the effects such as comfortableness, sweet sense be more natural.
Description
Technical field
The invention belongs to tobacco aromatics technical field, be specifically related to a kind of agate card extract and preparation method thereof and the application in cigarette.
Background technology
Agate card (Maca) is the annual or 2 years raw herbaceous plant of Cruciferae (Cruciferae) separate row Vegetable spp (Lepidium), originate in the mountain area, Andean of Peru height above sea level 3500 ~ 4500m, it is the cultivated plant that height above sea level is the highest, conventional food and the herbal medicine of American Indian, there is special health-care efficacy, energy, antifatigue can be strengthened, improve fertility, improvement function, regulate endocrine, treatment rheumatism, anaemia, depression etc., therefore, FAO (Food and Agriculture Organization of the United Nation) (FAO) also advocates extensively this high nutrition crop of plantation.Modern medicine study proves: agate card is rich in Kohlenhydrate, protein, unrighted acid and mineral matter element, main chemical is agate card alkene (Maceaene), macamides (Macamide), Glucosinolates (Glucosinolates) etc., agate card alkene, macamides are considered in agate extract can direct effect people pituitary gland, activate and each organ of restoring human original physiological function, promote and regulate hormonal secreting function, being a lot present in alcohol extract.All kinds of health products being main material production with agate card are promoted rapidly on the state market such as American-European, Japanese, obtain the favor of more and more consumer, agate card is used in health food by domestic appearance, as the preparation method of a CN102524465A maca health-care Puer tea cream, CN103756831A agate card purple sweet potato liquor, and the application in cigarette has no report.
Summary of the invention
The object of this invention is to provide a kind of agate card extract, another object of the present invention is to provide a kind of preparation method of agate card extract, and another object of the present invention is to provide the application of a kind of agate card extract in cigarette.
Technical scheme of the present invention is:
A preparation method for agate card extract, comprises the following steps:
(1) pulverize after agate card rhizome being dried, sieve, dry, be cooled to room temperature;
(2) take maca powder end, solubilizer soaks, water-bath refluxing extraction;
(3) by filtrate in 50-60 DEG C of reduced pressure concentration, i.e. get Ma Ka extract.
Preferably, dry 3 hours are spent after No. 3 sieves in 60 DEG C of thermostatic drying chambers in described step (1).
Preferably, in step (2), solvent is the ethanolic solution of 50 ~ 95%, and solid-liquid ratio is 1:6.
Preferably, in step (2), soak time is 6 ~ 12h.
Preferably, in step (2), bath temperature is 60 ~ 100 DEG C, and return time is 3-6h.
Preferably, the half being equivalent to material quality is evaporated in step (3).
A kind of agate card extract, is prepared from by above-mentioned method.
The application of agate card extract of the present invention in cigarette, agate card extract adds in cigarette shreds in reinforced mode.
Preferably, agate card extract is dissolved in the solution of certain density ethanol or certain density ethanol and propane diols, is sprayed at equably on cigarette shreds, thin slice or offal.
Preferably, agate card extract by weight 0.1 ~ 10 ‰ ratio add in cigarette shreds in reinforced mode.
Beneficial effect of the present invention:
(1) application of the present invention can improve cigarette sucking quality, have sweet soft, improve the effects such as comfortableness, sweet sense be more natural.
(2) agate card extract production process is simple to operate, and its application does not change existing Cigarette processing technique, has actual production meaning and value, and can produce good flavoring and casing effect to cigarette, improve cigarette smoking quality on the whole.
Detailed description of the invention
(1) agate card extract preparation
By dry agate card rhizome, pulverize, cross No. three sieves, in 60 DEG C of thermostatic drying chambers, drying 3 hours, is chilled to room temperature, and precision takes maca powder end 50g, put in round-bottomed flask, be the ethanolic solution that 1:6 adds 50 ~ 95% by solid-liquid ratio, soak 6 ~ 12h, 60-100 DEG C of water-bath backflow 4-6h, filter, collect filtrate, be evaporated to 25g, i.e. get Ma Ka extract.
(2) application in cigarette
Agate card extract in cigarette shreds, thin slice or offal weight 0.1 ~ 10 ‰ ratio, be dissolved in the solution of certain density ethanol or certain density ethanol and propane diols, and be sprayed at equably on cigarette shreds, thin slice or offal, and roll into cigarette.
Technology contents of the present invention and effect is further illustrated below by example.
Embodiment 1
Get dry agate card rhizome, pulverize, cross No. three sieves, drying 3 hours in 60 DEG C of thermostatic drying chambers, be chilled to room temperature, precision takes 50g respectively, put in round-bottomed flask, precision adds 300mL95% ethanol, soaks 8h, 65 DEG C of water-bath backflow 4h, filter, collect filtrate, be evaporated to 25g, i.e. get Ma Ka alcohol extract.
With miniaturised nebuliser, extract is dissolved in certain density ethanolic solution, evenly be sprayed onto hard gold holy formula Ye Zushang with 0.2 ‰ adding proportions, deposit, after 4 hours with band sealing after sprinkling, rolling sample cigarette with making cigarette device, to deposit in climatic chamber 48 hours.
Embodiment 2
Get dry agate card rhizome, pulverize, cross No. three sieves, drying 3 hours in 60 DEG C of thermostatic drying chambers, be chilled to room temperature, precision takes 50g respectively, put in round-bottomed flask, precision adds 300mL80% ethanol respectively, soaks 10h, 75 DEG C of water-bath backflow 5h, filter, collect filtrate, be evaporated to 25g, i.e. get Ma Ka alcohol extract.
With miniaturised nebuliser, extract is dissolved in certain density ethanol and propylene glycol solution, evenly be sprayed onto hard gold holy formula Ye Zushang with 0.5 ‰ adding proportions, deposit, after 4 hours with band sealing after sprinkling, rolling sample cigarette with making cigarette device, to deposit in climatic chamber 48 hours.
Embodiment 3
Get dry agate card rhizome, pulverize, cross No. three sieves, drying 3 hours in 60 DEG C of thermostatic drying chambers, be chilled to room temperature, precision takes 50g respectively, put in round-bottomed flask, precision adds 300mL50% ethanol respectively, soaks 12h, 85 DEG C of water-bath backflow 6h, filter, collect filtrate, be evaporated to 25g, i.e. get Ma Ka alcohol extract.
With miniaturised nebuliser, extract is dissolved in certain density ethanol and propylene glycol solution, evenly be sprayed onto hard gold holy formula Ye Zushang with 0.1 ‰ adding proportions, deposit, after 4 hours with band sealing after sprinkling, rolling sample cigarette with making cigarette device, to deposit in climatic chamber 48 hours.
Claims (2)
1. the application of agate card extract in cigarette, is characterized in that, agate card extract is dissolved in the solution of certain density ethanol or certain density ethanol and propane diols, is sprayed on cigarette shreds, thin slice or offal equably; Described agate card extract is prepared from by the following method:
(1) pulverize after being dried by agate card rhizome, cross No. 3 sieves, in 60 DEG C of thermostatic drying chambers, drying 3 hours, is cooled to room temperature;
(2) take maca powder end, add the alcohol solution dipping of 50 ~ 95%, solid-liquid ratio is 1:6, and soak time is 6 ~ 12h; Water-bath refluxing extraction, bath temperature is 60 ~ 100 DEG C, and return time is 3-6h;
(3) filtrate is evaporated in 50-60 DEG C the half being equivalent to material quality, i.e. get Ma Ka extract.
2. the application of agate card extract according to claim 1 in cigarette, is characterized in that, agate card extract by weight 0.1 ~ 10 ‰ ratio add in cigarette shreds in reinforced mode.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410336561.9A CN104130863B (en) | 2014-07-15 | 2014-07-15 | A kind of agate card extract and preparation method thereof and the application in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410336561.9A CN104130863B (en) | 2014-07-15 | 2014-07-15 | A kind of agate card extract and preparation method thereof and the application in cigarette |
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| Publication Number | Publication Date |
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| CN104130863A CN104130863A (en) | 2014-11-05 |
| CN104130863B true CN104130863B (en) | 2016-03-02 |
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| CN201410336561.9A Active CN104130863B (en) | 2014-07-15 | 2014-07-15 | A kind of agate card extract and preparation method thereof and the application in cigarette |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105105319A (en) * | 2015-07-10 | 2015-12-02 | 云南中烟工业有限责任公司 | Preparation method of maca extracts and application of maca extracts in cigarettes |
| CN106562469A (en) * | 2015-10-07 | 2017-04-19 | 惠州市吉瑞科技有限公司 | Electronic cigarette tobacco liquid |
| CN105231482B (en) * | 2015-10-20 | 2021-06-22 | 贵州中烟工业有限责任公司 | Gum base type smoke-free tobacco product with anti-fatigue effect and preparation method thereof |
| CN105230940B (en) * | 2015-10-20 | 2021-06-22 | 贵州中烟工业有限责任公司 | Functional hard candy and preparation method thereof |
| CN106947598A (en) * | 2017-04-27 | 2017-07-14 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl agate card essence and its application in cigarette |
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| CN1473594A (en) * | 2003-07-01 | 2004-02-11 | 华中科技大学 | Extract of Maka root |
| CN102526161A (en) * | 2012-02-10 | 2012-07-04 | 中国科学院过程工程研究所 | Preparation method for high-activity lepidium meyenii extract |
| CN102836196A (en) * | 2012-09-29 | 2012-12-26 | 楚雄州百草岭药业发展有限公司 | Maca extract and preparation method thereof |
| CN103040896A (en) * | 2013-01-06 | 2013-04-17 | 云南圣草峰生物科技有限公司 | Preparation method of maca extractive |
| CN103319360A (en) * | 2013-06-21 | 2013-09-25 | 劲牌有限公司 | Process for extracting macamides from maca |
| CN103750319A (en) * | 2014-01-21 | 2014-04-30 | 西藏月王生物技术有限公司 | Instant maca preparation and preparation method thereof |
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2014
- 2014-07-15 CN CN201410336561.9A patent/CN104130863B/en active Active
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|---|---|---|---|---|
| CN1473594A (en) * | 2003-07-01 | 2004-02-11 | 华中科技大学 | Extract of Maka root |
| CN102526161A (en) * | 2012-02-10 | 2012-07-04 | 中国科学院过程工程研究所 | Preparation method for high-activity lepidium meyenii extract |
| CN102836196A (en) * | 2012-09-29 | 2012-12-26 | 楚雄州百草岭药业发展有限公司 | Maca extract and preparation method thereof |
| CN103040896A (en) * | 2013-01-06 | 2013-04-17 | 云南圣草峰生物科技有限公司 | Preparation method of maca extractive |
| CN103319360A (en) * | 2013-06-21 | 2013-09-25 | 劲牌有限公司 | Process for extracting macamides from maca |
| CN103750319A (en) * | 2014-01-21 | 2014-04-30 | 西藏月王生物技术有限公司 | Instant maca preparation and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| 《Tobacco with rose essence includes citronellol, geraniol, rose essential oil, ethyl acetate, isoamyl isovalerate, acetic acid, eugenol, maltol, ethyl vanillin, menthol, tobacco extract, furfural, fennel oil, alcohol and propylene glycol》;《德温特数据库》;《德温特数据库》;20130116;摘要部分 * |
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| CN104130863A (en) | 2014-11-05 |
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