CN105105319A - Preparation method of maca extracts and application of maca extracts in cigarettes - Google Patents
Preparation method of maca extracts and application of maca extracts in cigarettes Download PDFInfo
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- CN105105319A CN105105319A CN201510404576.9A CN201510404576A CN105105319A CN 105105319 A CN105105319 A CN 105105319A CN 201510404576 A CN201510404576 A CN 201510404576A CN 105105319 A CN105105319 A CN 105105319A
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- agate card
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Abstract
The invention relates to a preparation method, which includes the following steps: 1) crushing maca and obtaining maca particles of 60 to 80 mesh; 2) mixing the maca particles with a solvent, performing heating reflux extraction for 2-4h, and then performing filtering to obtain a first filter residue and a first filtrate; 3) mixing the first filter residue with a solvent and performing heating reflux extraction for 1 to 3 hours, and then performing filtering to obtain a first filter residue and a second filtrate; and 4) mixing the first filtrate and the second filtrate, removing the solvent by distilling, and obtaining brownish-yellow maca extracts. The invention also relates to an application of the maca extracts in cigarettes. The maca extracts can significantly improve the aroma concentration and the volume of the aroma of the smoke of the cigarettes, so that the smoke of the cigarettes has cream sweetness and herb sweetness, the aroma of the cigarettes is enriched, the remaining taste of the smoke of the cigarettes is improved, and the sensory quality of smoking of the cigarettes is improved. As a cigarette additive, the maca extracts have a promising application.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of preparation method and this application of agate card extract in cigarette of agate card extract.
Background technology
Along with the change of people's habits and customs, increasing people pays close attention to health more, and in order to meet these consumer demands, the parent that low-coke tar cigarette just more and more obtains consumer looks at.In Cigarette processing process, mainly through improving air permeance for cigarette paper, adopt the mouth of composite structure rod, the punching technology such as dilution method and reconstituted tobacoo reduces tar content in cigarette smoke, the method for single reduction tar is for tobacco scientific worker not being a difficult thing.Although reducing year by year of cigarette packs mark tar content meets the pursuit of consumer for health, but the quality that the thing followed is cigarette product also changes thereupon, that this perfume of the general tobacco of low-coke tar cigarette is not enough, fragrance weakens the most significantly, cigarette sense organ suction quality declines, and the style and features of cigarette is weakened and even changes.How to improve cigarette flavor concentration, promote perfume quantity, strengthen the rich of flue gas note, become and improved Chinese-style cigarette quality, advance cigarette brand development problem demanding prompt solution.In order to better address these problems, increasing perfume additive technology is applied.
Taking natural plants as the research that object carries out cigarette additive aspect, is always the research emphasis of tobacco business tobacco aromatics exploitation.Agate card (Maca) is the herbaceous plant originating in mountain area, Peru Andean, is also often referred to as agate coffee, and be Cruciferae separate row Vegetable spp plant (LepidiummeyeniiWalpers), its application site is the fleshy root of plant.Agate card has long cultivation and edible history, and at South American region, agate card both also used as conventional medicament as food by locals.Existing research shows, the multiple efficacies such as agate jig has antifatigue, build up health.In recent years, at the ground such as Chinese yunnan, Qinghai a large amount of introducing and planting agate card, the agate card industry taken on a certain scale.
At present, both at home and abroad to the research of agate card mainly to the analysis of its composition, as the research of macamides and Ma Ka alkene, and using the correlative study of agate card as food materials, medicinal material, and there is not been reported for its application study at Field of Tobacco.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of agate card extract, and the present invention also aims to this agate card extract to add in cigarette shreds, to promote cigarette smoke fragrance level, increase cigarette smoke perfume quantity, imparting cigarette smoke cream is fragrant and sweet and medicine is fragrant and sweet, enrich cigarette smoke note, improve cigarette smoke pleasant impression and improve cigarette sense organ suction quality.
The object of the invention is to be achieved by the following technical programs.
First aspect present invention relates to a kind of preparation method of agate card extract, and it comprises the following steps:
(1) maca powder is broken, obtain 60-80 object agate card particle;
(2) above-mentioned agate card particle is mixed with solvent, heating and refluxing extraction 2-4h, filter and obtain the first filter residue and the first filtrate;
(3) above-mentioned first filter residue is mixed with solvent, heating and refluxing extraction 1-3h, filter and obtain the second filter residue and the second filtrate;
(4) merge described first filtrate and described second filtrate, distillation, except desolventizing, obtains the agate card extract of brown color.
Preferably, filter while hot in step (2) and step (3).
In a preferred embodiment of the present invention, described solvent is ethanol.
In a preferred embodiment of the present invention, described ethanol is 75% ethanol water.
In a preferred embodiment of the present invention, the mass ratio of solvent described in step (2) and described agate card particle is (2-10): 1; Described in step (3), the mass ratio of solvent and described first filter residue is (2-5): 1.
Second aspect present invention relates to a kind of to the method for cigarette flavouring, be mixed with agate card extract solution after agate card extract diluent preparation method described according to a first aspect of the present invention prepared dissolves, by the 0.010%-0.025% of tobacco quality, above-mentioned agate card extract solution added on pipe tobacco by spray pattern.Described agate card extract does not need to change cigarette original processing technology when can be applicable to production of cigarettes and apply, such as, can directly be added in cigarette shreds in flavoring and casing operation by described agate card extract solution.
In a preferred embodiment of the present invention, described diluent is ethanol, propane diols or glycerine.Such as, 75% ethanol water or 95% ethanol water can be adopted as diluent.
In a preferred embodiment of the present invention, the mass concentration of described agate card extract solution is 1 ~ 2.5%.
Third aspect present invention relates to the agate card extract preparation method described in first aspect present invention prepared and is used for promoting cigarette smoke fragrance level, increases cigarette smoke perfume quantity, gives the purposes that cigarette smoke cream is fragrant and sweet and medicine is fragrant and sweet, enrich cigarette smoke note, improve cigarette smoke pleasant impression or raising cigarette sense organ suction quality.
Relative to prior art, the present invention achieves following beneficial effect:
1, the preparation method of agate card extract of the present invention is simple and practical, and operation is succinct easily to be implemented.
2, the agate card extract that prepared by the present invention can be used as novel high-grade tobacco aromatics, for cigarette flavouring upgrading successful, significantly can promote cigarette smoke fragrance level, increase cigarette smoke perfume quantity, imparting cigarette smoke cream is fragrant and sweet and medicine is fragrant and sweet, enrich cigarette smoke note, improve cigarette smoke pleasant impression and improve cigarette sense organ suction quality, have broad application prospects as cigarette additive.But agate card itself British plain spirits, its extract but can be the upgrading of cigarette flavouring as tobacco aromatics, and this exceeds those skilled in the art and expect.
Detailed description of the invention
With specific embodiment, the present invention is described in detail below, but embodiment is not limited to the technical solution.
Embodiment 1
A preparation method for agate card extract, it comprises the following steps:
(1) maca powder is broken, obtain 60-80 object agate card particle;
(2) accurately take above-mentioned agate card particle 500g, in agate card particle, add 75% ethanol of its weight 5 times amount, heating and refluxing extraction 3h, filter while hot and obtain the first filter residue and the first filtrate;
(3) in above-mentioned first filter residue, add 75% ethanol of its weight 3 times amount, heating and refluxing extraction 2h, filter while hot and obtain the second filter residue and the second filtrate;
(4) merge described first filtrate and described second filtrate, distillation removing ethanol, obtains the agate card extract of 95g brown color.
The agate card extract prepared by above step is used for Yuxi cigarette tobacco leaf formulation, first the agate card extract solution that mass concentration is 1% is mixed with after being dissolved with 95% ethanol water by described agate card extract, in 0.010%, 0.020%, 0.025% ratio of tobacco quality, above-mentioned agate card extract solution is added on pipe tobacco by spray pattern respectively, under constant temperature (22 ± 1 DEG C) constant humidity (60 ± 2%) condition, balance 48h, rolls into Cigarette A, B and C respectively.
The Cigarette rolled into Yuxi cigarette tobacco leaf formulation is for blank, and the Cigarette that with the addition of agate card extract and the Cigarette not adding agate card extract are carried out organoleptic quality comparative evaluation by the specialty personnel that smoke panel test, and acquired results is as shown in table 1:
Table 1: the Cigarette that with the addition of agate card extract with contrast cigarette smoking result
Organoleptic quality evaluations is carried out to the cigarette and blank cigarette that with the addition of agate card extract, result shows, agate card extract prepared by the present invention is for cigarette flavouring upgrading successful, significantly can promote cigarette flavor concentration, increase perfume quantity, imparting cigarette cream is fragrant and sweet and medicine is fragrant and sweet, enrich note, improve pleasant impression, improve cigarette sense organ suction quality, have broad application prospects as cigarette additive.
Above content is the detailed description made the present invention in conjunction with detailed description of the invention.For those skilled in the art, the obvious distortion made without departing from the inventive concept of the premise, all should be considered as protection scope of the present invention.
Claims (9)
1. a preparation method for agate card extract, is characterized in that, it comprises the following steps:
(1) maca powder is broken, obtain 60-80 object agate card particle;
(2) above-mentioned agate card particle is mixed with solvent, heating and refluxing extraction 2-4h, filter and obtain the first filter residue and the first filtrate;
(3) above-mentioned first filter residue is mixed with solvent, heating and refluxing extraction 1-3h, filter and obtain the second filter residue and the second filtrate;
(4) merge described first filtrate and described second filtrate, distillation, except desolventizing, obtains the agate card extract of brown color.
2. preparation method according to claim 1, is characterized in that, described solvent is ethanol.
3. preparation method according to claim 2, is characterized in that, described ethanol is 75% ethanol water.
4. preparation method according to claim 1, is characterized in that, the mass ratio of solvent described in step (2) and described agate card particle is (2-10): 1; Described in step (3), the mass ratio of solvent and described first filter residue is (2-5): 1.
5. give the method for cigarette flavouring for one kind, it is characterized in that, agate card extract diluent preparation method according to any one of claim 1-4 prepared is mixed with agate card extract solution after dissolving, and is added on pipe tobacco by above-mentioned agate card extract solution by the 0.010%-0.025% of tobacco quality by spray pattern.
6. method according to claim 5, is characterized in that, described diluent is ethanol, propane diols or glycerine.
7. method according to claim 6, is characterized in that, described ethanol is 75% ethanol water or 95% ethanol water.
8. method according to claim 5, is characterized in that, the mass concentration of described agate card extract solution is 1 ~ 2.5%.
9. agate card extract prepared by the preparation method according to any one of claim 1-4 is for promoting cigarette smoke fragrance level, increasing cigarette smoke perfume quantity, giving the purposes that cigarette smoke cream is fragrant and sweet and medicine is fragrant and sweet, enrich cigarette smoke note, improve cigarette smoke pleasant impression or raising cigarette sense organ suction quality.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510404576.9A CN105105319A (en) | 2015-07-10 | 2015-07-10 | Preparation method of maca extracts and application of maca extracts in cigarettes |
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| CN201510404576.9A CN105105319A (en) | 2015-07-10 | 2015-07-10 | Preparation method of maca extracts and application of maca extracts in cigarettes |
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| CN105105319A true CN105105319A (en) | 2015-12-02 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106666736A (en) * | 2016-07-11 | 2017-05-17 | 周晗生 | Extraction method for maca extract |
| CN106947598A (en) * | 2017-04-27 | 2017-07-14 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl agate card essence and its application in cigarette |
| CN109105947A (en) * | 2018-07-05 | 2019-01-01 | 湖北中烟工业有限责任公司 | A kind of multistage solvent extraction preparation method and applications of cocoa extract |
| CN112064406A (en) * | 2020-09-07 | 2020-12-11 | 云南中烟工业有限责任公司 | Special aroma forming paper prepared from jatropha roots of Dai nationality traditional edible spice plants of Xishuangbanna, method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090065013A1 (en) * | 2006-04-28 | 2009-03-12 | Swedish Match North Europe Ab | moist snuff non-tobacco composition and a method for producing thereof |
| US20120031415A1 (en) * | 2008-11-05 | 2012-02-09 | Swedish Match North Europe Ab | Non-tobacco moist snuff composition and a method for its manufacture |
| CN104116132A (en) * | 2014-07-15 | 2014-10-29 | 江西中烟工业有限责任公司 | Maca enzymatic hydrolysis extract, preparing method thereof and application to cigarettes |
| CN104130863A (en) * | 2014-07-15 | 2014-11-05 | 江西中烟工业有限责任公司 | Maca extract as well as preparation method thereof and application thereof to cigarettes |
-
2015
- 2015-07-10 CN CN201510404576.9A patent/CN105105319A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090065013A1 (en) * | 2006-04-28 | 2009-03-12 | Swedish Match North Europe Ab | moist snuff non-tobacco composition and a method for producing thereof |
| US20120031415A1 (en) * | 2008-11-05 | 2012-02-09 | Swedish Match North Europe Ab | Non-tobacco moist snuff composition and a method for its manufacture |
| CN104116132A (en) * | 2014-07-15 | 2014-10-29 | 江西中烟工业有限责任公司 | Maca enzymatic hydrolysis extract, preparing method thereof and application to cigarettes |
| CN104130863A (en) * | 2014-07-15 | 2014-11-05 | 江西中烟工业有限责任公司 | Maca extract as well as preparation method thereof and application thereof to cigarettes |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106666736A (en) * | 2016-07-11 | 2017-05-17 | 周晗生 | Extraction method for maca extract |
| CN106947598A (en) * | 2017-04-27 | 2017-07-14 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl agate card essence and its application in cigarette |
| CN109105947A (en) * | 2018-07-05 | 2019-01-01 | 湖北中烟工业有限责任公司 | A kind of multistage solvent extraction preparation method and applications of cocoa extract |
| CN112064406A (en) * | 2020-09-07 | 2020-12-11 | 云南中烟工业有限责任公司 | Special aroma forming paper prepared from jatropha roots of Dai nationality traditional edible spice plants of Xishuangbanna, method and application thereof |
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Application publication date: 20151202 |