CN101878953B - Aromatic additive for citron natural tobaccos and preparation method thereof - Google Patents
Aromatic additive for citron natural tobaccos and preparation method thereof Download PDFInfo
- Publication number
- CN101878953B CN101878953B CN2010102342378A CN201010234237A CN101878953B CN 101878953 B CN101878953 B CN 101878953B CN 2010102342378 A CN2010102342378 A CN 2010102342378A CN 201010234237 A CN201010234237 A CN 201010234237A CN 101878953 B CN101878953 B CN 101878953B
- Authority
- CN
- China
- Prior art keywords
- citron
- additive
- natural
- aromatic additive
- propane diols
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 77
- 239000000654 additive Substances 0.000 title claims abstract description 58
- 230000000996 additive effect Effects 0.000 title claims abstract description 58
- 240000004307 Citrus medica Species 0.000 title claims abstract description 52
- 125000003118 aryl group Chemical group 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 241000208125 Nicotiana Species 0.000 claims abstract description 76
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 51
- 239000012046 mixed solvent Substances 0.000 claims abstract description 21
- 239000000284 extract Substances 0.000 claims abstract description 17
- 238000010992 reflux Methods 0.000 claims abstract description 12
- 239000002904 solvent Substances 0.000 claims abstract description 6
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 31
- 239000012141 concentrate Substances 0.000 claims description 11
- 238000000605 extraction Methods 0.000 claims description 5
- 238000005304 joining Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 11
- 241000220317 Rosa Species 0.000 abstract description 10
- 230000000391 smoking effect Effects 0.000 abstract description 7
- 239000000779 smoke Substances 0.000 abstract description 4
- 241000196324 Embryophyta Species 0.000 abstract description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract 3
- 230000028327 secretion Effects 0.000 abstract 1
- 239000002304 perfume Substances 0.000 description 32
- 235000019504 cigarettes Nutrition 0.000 description 17
- 239000000178 monomer Substances 0.000 description 14
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 10
- 239000003546 flue gas Substances 0.000 description 10
- 239000003205 fragrance Substances 0.000 description 8
- 238000009835 boiling Methods 0.000 description 7
- 241001038563 Pseudostellaria Species 0.000 description 6
- 235000011449 Rosa Nutrition 0.000 description 6
- 238000001914 filtration Methods 0.000 description 6
- 238000006062 fragmentation reaction Methods 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 206010025482 malaise Diseases 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 208000024891 symptom Diseases 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 241000207199 Citrus Species 0.000 description 1
- 241001549247 Citrus wilsonii Species 0.000 description 1
- 229920000832 Cutin Polymers 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 241000160563 Dumetella carolinensis Species 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 241001579180 Matthiola longipetala Species 0.000 description 1
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 240000008530 Rosa canina Species 0.000 description 1
- 235000000539 Rosa canina Nutrition 0.000 description 1
- 240000006066 Rosa rugosa Species 0.000 description 1
- 235000000659 Rosa rugosa Nutrition 0.000 description 1
- 235000004789 Rosa xanthina Nutrition 0.000 description 1
- 241000109329 Rosa xanthina Species 0.000 description 1
- 241001093501 Rutaceae Species 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000005456 alcohol based solvent Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000021028 berry Nutrition 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000000039 congener Substances 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 230000004345 fruit ripening Effects 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Abstract
The invention relates to an aromatic additive for tobaccos, in particular to an aromatic additive for citron natural tobaccos and a preparation method thereof, and the spicy additive can increase the quality of aroma, soften the smoke and improve the residual smell and the throat comfort. 70 to 95 percent of alcohol solvent is used for respectively extracting citrons, rose hips and heterophylly falsestarwort root by reflux, extracts are respectively collected, and after being mixed, the three types of extracts are added into the mixed solvent of ethanol and propylene glycol, so that the aromatic additive is obtained. The aromatic additive, the natural aromatic plants of which are reasonably prepared, extracted, concentrated and then added into sampled cut tobacco, can remarkably increase the quality of aroma, soften the smoke and improve the residual smell and the throat comfort, and can promote the salivary secretion of the cavity to alleviate the ailment of the throat and achieve the effect of reducing the harm of smoking.
Description
Technical field
The present invention relates to a kind of tobacco aromatics using additive, specifically a kind ofly can improve fragrance matter, soft fine and smooth flue gas improves pleasant impression, improves aromatic additive for citron natural tobaccos of throat's comfortableness and preparation method thereof.
Technical background
Because Smoking is harmful to your health, smoking has become serious social concern day by day, and the production of safe cigarette has become the problem that cigarette industry extremely is concerned about.Its main method is exactly the T/N content that reduces in the flue gas, yet this tends to cause smoke deficiency and fragrance to alleviate.Therefore; Under the prerequisite of lowering harm and decreasing coking; How to remedy the loss of fragrance and the task of raising smoke perfume quality; And, become an urgent demand that current cigarette factory industry essence spice for cigarette is researched and proposed, and promoting the raising and the development of development of cigarette odor additive and flavouring essence for tobacco meat flavor formulating technology thus about the flavoring and casing problem of inferior tobacco leaf, expanded cut tobacco, tobacco leaf substitute etc.Global tobacco business is all attached great importance to the development and utilization of essence spice for cigarette, and is used as oneself wuwa to the technology that can produce high-quality essence and flavoring agent, to seek in intense market competition, occupying catbird seat.Assorted gas in the flue gas and flue gas all have much relations with the sucking quality of cigarette to the stimulation of cavity, throat; How effectively to reduce assorted gas in the flue gas, reduce flue gas to the stimulation of throat, reduce flue gas dry sensation, improve the cigarette comfort level; Reduce the harm that smoking brings the smoker, be the technical problem that the tobacco scientific workers need to be resolved hurrily always.
Summary of the invention
The technical problem that the present invention will solve is exactly to the deficiency of existing tobacco with the spices existence, provides a kind of and can improve fragrance matter, and soft fine and smooth flue gas improves pleasant impression, improves perfume additive for natural tobacco of throat's comfortableness and preparation method thereof.
The present invention solves the problems of the technologies described above with following technical scheme: it is that citron, fructus rosae, radix pseudostellariae are carried out refluxing extraction with 70%～95% spirit solvent respectively; Collect extract respectively; With joining in the mixed solvent of ethanol and propane diols after three kinds of extracts mixing, promptly obtain aromatic additive for citron natural tobaccos.
Citron wherein: fructus rosae: the weight ratio of radix pseudostellariae is 2: 1: 1.The percentage by weight of propane diols is 0-30% in the mixed solvent of ethanol and propane diols.
Preparation method of the present invention carries out refluxing extraction with 70%～95% spirit solvent respectively with citron, fructus rosae, radix pseudostellariae; Collect extract respectively; With joining in the mixed solvent of ethanol and propane diols after three kinds of extracts mixing, promptly obtain aromatic additive for citron natural tobaccos.Citron wherein: fructus rosae: the weight ratio of radix pseudostellariae is 2: 1: 1; After collecting extract, respectively three kinds of extracts are concentrated into the concentrate that relative density is 1.03-1.3, mix then; The percentage by weight of propane diols is 0-30% in the mixed solvent of ethanol and propane diols.Add propane diols and can protect fragrance not volatilize, and can make spices have good outward appearance with ethanol.
The effect of perfume additive for natural tobacco of the present invention is:
(1) citron: have another name called citron, be the Rutaceae citrus plant.Citron is the general designation of plant citron and medicinal material citron.The plant citron is evergreen dungarunga of Rutaceae or shrub plant, is born in the many wet environments of high temperature of 350 meters to 1750 meters of height above sea level.In the broad-leaf forest in Xishuangbanna, Yunnan, the citron that is in the semi-wild state is arranged.The Chinese medicine citron is plant citron and the fragrant circle of congener (formal name used at school: ripening fruits Citrus wilsonii Tanaka).Main product in Zhejiang, ground such as Jiangsu, Guangdong, Guangxi.Gather during fruit maturation autumn.Take advantage of fresh slices, remove seed and flesh, dry or low temperature drying.Have regulating the flow of QI to ease the stomach, the effect of phlegm falls in dissipate-swelling.
(2) fructus rosae: scarlet fructus rosae is also referred to as cynarrhodion, is to grow the meat berry form by holder after the rose blossom fall, belongs to a kind of pseudocarp (capsule), and oval profile is petite begs for happiness.Though many kinds of roses all can bear fruit, (Rosa rugosa) produced edible fructus rosae is main with rose (Rosa canina) and wrinkle leaf rose.Be rich in vitamin C and E in the fructus rosae, can improve body immunity, and can promote the absorption of calcium, iron.That these article have is anti-oxidant, delay senility, prevent melanin to form, and promotes calcium, iron to absorb reinforced immunological function and the effect that stimulates circulation.
(3) radix pseudostellariae: have another name called caryophyllaceous ginseng, mainly originate in build, ground such as Guizhou, Anhui, elongated anti-capitate of root or elongated strip shaped, crooked slightly.Long 3～10cm, diameter 0.2～0.6cm.There is the stem trace on the top, and surperficial yellow-white is more smooth, and little have a vertical wrinkle, and recess has mark of fibrous root.Matter is hard and crisp, and section is smooth, yellowish white, cutin appearance (scalding); Or off-white color, mealiness (sun-dried article).Gas is little, and it is little sweet to distinguish the flavor of.Radix pseudostellariae contains radix pseudostellariae polysaccharide, several amino acids and trace element, ability tonifying Qi benefit spleen, nourishing Yin and promoting production of body fluid.
The invention has the beneficial effects as follows a natural perfume plant through reasonable compatibility, extract concentrated back and add in the sample pipe tobacco, can obviously improve fragrance matter; Soft fine and smooth flue gas improves pleasant impression, comfortable taste; Can promote that cavity salivates, alleviate throat's malaise symptoms, reach the effect that alleviates harmfulness of smoking.This perfume additive for natural tobacco is based on local resource, and preparation technology is simple, cost is low, has good market prospects.
The specific embodiment
Below in conjunction with embodiment the present invention is elaborated:
The present invention adopts following method to prepare perfume additive for natural tobacco of the present invention:
A, preparation perfume additive for natural tobacco monomer: with above-mentioned raw materials pulverize be with a certain size after; Place boiling flask to add 70%～95% spirit solvent respectively and carry out the water-bath heating and refluxing extraction twice; The time that citron, fructus rosae, radix pseudostellariae extract was respectively 1～3 hour; Decompression afterwards concentrates, and collects the concentrate of citron, fructus rosae, radix pseudostellariae, obtains the raw material monomer of natural tobacco additive;
The allotment of b, perfume additive for natural tobacco: with the concentrate of the citron that extracts, fructus rosae, radix pseudostellariae, be dissolved in the mixed solvent of ethanol and propane diols and allocate, obtain natural tobacco additive.Wherein the percentage by weight of propane diols is 0-30% in the mixed solvent of ethanol and propane diols.
The perfume additive for natural tobacco that makes is used for the production of cigarette, cigarette, pipe tobacco, stem or reconstituted tobacoo by 0.05%～0.5% of pipe tobacco weight.
Embodiment 1
(1) preparation natural tobacco additive monomer: after getting 200 gram citrons, 100 gram fructus rosaes, 100 gram radix pseudostellariaes difference fragmentations; Citron is placed boiling flask; Add 8 times of 75% alcohol reflux and extracted fructus rosae 3 hours, radix pseudostellariae 2 hours 1 hour; It is 1.05 that extracting liquid filtering is concentrated into relative density, collects the concentrate of citron, fructus rosae, radix pseudostellariae respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, be dissolved in 1 kilogram the mixed solvent of ethanol and propane diols and allocate, obtain perfume additive for natural tobacco.Wherein the percentage by weight of propane diols is 15% in the mixed solvent of ethanol and propane diols.
With 0.05% the ratio of the perfume additive for natural tobacco that makes in pipe tobacco weight, be sprayed at according to conventional perfuming process program and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 24 hours.Sensory evaluating smoking result shows: fragrance passes through to be sent out, and comparatively coordinates with simple and elegant odor type cigarette, can obviously improve fragrance matter, and soft fine and smooth flue gas improves pleasant impression, and comfortable taste can promote that cavity salivates, and alleviates throat's malaise symptoms, reaches the effect that alleviates harmfulness of smoking.
Embodiment 2
(1) preparation natural tobacco additive monomer: after getting 100 gram citrons, 200 gram fructus rosaes, 100 gram radix pseudostellariaes difference fragmentations; Fructus rosae is placed boiling flask; Add 8 times of 75% alcohol reflux and extracted citron 2 hours, radix pseudostellariae 3 hours 1 hour; Extracting liquid filtering contract to relative density be 1.3, collect the concentrate of citron, fructus rosae, radix pseudostellariae respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, be dissolved in 1.5 kilograms the mixed solvent of ethanol and propane diols and allocate, obtain perfume additive for natural tobacco.Wherein the percentage by weight of propane diols is 20% in the mixed solvent of ethanol and propane diols.
With 0.1% the ratio of the perfume additive for natural tobacco that makes in pipe tobacco weight, be sprayed at according to conventional perfuming process program and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 24 hours.Effect is with embodiment 1
Embodiment 3
(1) preparation natural tobacco additive monomer: after getting 100 gram citrons, 200 gram radix pseudostellariaes, 100 gram Hangzhoupro fructus rosaes difference fragmentations; Radix pseudostellariae is placed boiling flask; Add 8 times of 75% alcohol reflux and extracted citron 1 hour, fructus rosae 3 hours 1 hour; It is 1.3 that extracting liquid filtering is concentrated into relative density, collects the concentrate of citron, fructus rosae, radix pseudostellariae respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, be dissolved in 5 kilograms the mixed solvent of ethanol and propane diols and allocate, obtain perfume additive for natural tobacco.Wherein the percentage by weight of propane diols is 10% in the mixed solvent of ethanol and propane diols.
With 0.15% the ratio of the perfume additive for natural tobacco that makes in pipe tobacco weight, be sprayed at according to conventional perfuming process program and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 24 hours.Effect is with embodiment 1
Embodiment 4
(1) preparation natural tobacco additive monomer: after getting 150 gram citrons, 150 gram fructus rosaes, 100 gram radix pseudostellariaes difference fragmentations; Citron is placed boiling flask; Add 8 times of 75% alcohol reflux and extracted fructus rosae 3 hours, radix pseudostellariae 1 hour 2 hours; It is 1.1 that extracting liquid filtering is concentrated into relative density, collects the concentrate of citron, fructus rosae, radix pseudostellariae respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, be dissolved in 10 kilograms the mixed solvent of ethanol and propane diols and allocate, obtain perfume additive for natural tobacco.Wherein the percentage by weight of propane diols is 25% in the mixed solvent of ethanol and propane diols.
With 0.25% the ratio of the perfume additive for natural tobacco that makes in pipe tobacco weight, be sprayed at according to conventional perfuming process program and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 24 hours.Effect is with embodiment 1
Embodiment 5
(1) preparation natural tobacco additive monomer: after getting 100 gram citrons, 150 gram fructus rosaes, 100 gram radix pseudostellariaes difference fragmentations; Citron is placed boiling flask; Add 8 times of 75% alcohol reflux and extracted fructus rosae 2 hours, radix pseudostellariae 1 hour 2 hours; It is 1.2 that extracting liquid filtering is concentrated into relative density, collects the concentrate of citron, fructus rosae, radix pseudostellariae respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, be dissolved in 15 kilograms the mixed solvent of ethanol and propane diols and allocate, obtain perfume additive for natural tobacco.Wherein the percentage by weight of propane diols is 30% in the mixed solvent of ethanol and propane diols.
With 0.3% the ratio of the perfume additive for natural tobacco that makes in pipe tobacco weight, be sprayed at according to conventional perfuming process program and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 24 hours.Effect is with embodiment 1
Embodiment 6
(1) preparation natural tobacco additive monomer: after getting 150 gram citrons, 100 gram fructus rosaes, 150 gram radix pseudostellariaes difference fragmentations; Citron is placed boiling flask; Add 8 times of 75% alcohol reflux and extracted fructus rosae 2 hours, radix pseudostellariae 2 hours 3 hours; It is 1.12 that extracting liquid filtering is concentrated into relative density, collects the concentrate of citron, fructus rosae, radix pseudostellariae respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, be dissolved in 15 kilograms of alcohol solvents and allocate, obtain perfume additive for natural tobacco.
With 0.5% the ratio of the perfume additive for natural tobacco that makes in pipe tobacco weight, be sprayed at according to conventional perfuming process program and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 24 hours.Effect is with embodiment 1
Claims (5)
1. aromatic additive for citron natural tobaccos; It is that citron, fructus rosae, radix pseudostellariae are carried out refluxing extraction with 70%～95% spirit solvent respectively; Collect extract respectively; With joining in the mixed solvent of ethanol and propane diols after three kinds of extracts mixing, promptly obtain aromatic additive for citron natural tobaccos, wherein citron: fructus rosae: the weight ratio of radix pseudostellariae is 2: 1: 1.
2. a kind of aromatic additive for citron natural tobaccos according to claim 1, wherein the percentage by weight of propane diols is 0-30% in the mixed solvent of ethanol and propane diols.
3. the preparation method of an aromatic additive for citron natural tobaccos; It is that citron, fructus rosae, radix pseudostellariae are carried out refluxing extraction with 70%～95% spirit solvent respectively; Collect extract respectively; With joining in the mixed solvent of ethanol and propane diols after three kinds of extracts mixing, promptly obtain aromatic additive for citron natural tobaccos, wherein citron: fructus rosae: the weight ratio of radix pseudostellariae is 2: 1: 1.
4. the preparation method of a kind of aromatic additive for citron natural tobaccos according to claim 3, wherein collect extract after, respectively three kinds of extracts are concentrated into the concentrate that relative density is 1.03-1.3, mix then.
5. the preparation method of a kind of aromatic additive for citron natural tobaccos according to claim 3, wherein the percentage by weight of propane diols is 0-30% in the mixed solvent of ethanol and propane diols.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102342378A CN101878953B (en) | 2010-07-22 | 2010-07-22 | Aromatic additive for citron natural tobaccos and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102342378A CN101878953B (en) | 2010-07-22 | 2010-07-22 | Aromatic additive for citron natural tobaccos and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101878953A CN101878953A (en) | 2010-11-10 |
| CN101878953B true CN101878953B (en) | 2012-10-31 |
Family
ID=43051205
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010102342378A Expired - Fee Related CN101878953B (en) | 2010-07-22 | 2010-07-22 | Aromatic additive for citron natural tobaccos and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101878953B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102771888A (en) * | 2011-05-13 | 2012-11-14 | 湖北中烟工业有限责任公司 | Perfume additive for natural uncaria cigarettes and preparation method thereof |
| CN102499433B (en) * | 2011-10-19 | 2014-06-04 | 江苏中烟工业有限责任公司 | Application of suberenol extract in cigarette flavoring additive |
| CN105950296A (en) * | 2014-09-10 | 2016-09-21 | 邹玉华 | Preparing method for black tea spice |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1259321A (en) * | 1999-12-14 | 2000-07-12 | 张建祥 | Health care cigarette |
| CN101053447A (en) * | 2006-04-14 | 2007-10-17 | 钱玉章 | Liquid compound for eliminating smoke harm and preparing method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11209274A (en) * | 1998-01-22 | 1999-08-03 | Bae O-Sung | Smoking material for treating disease |
-
2010
- 2010-07-22 CN CN2010102342378A patent/CN101878953B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1259321A (en) * | 1999-12-14 | 2000-07-12 | 张建祥 | Health care cigarette |
| CN101053447A (en) * | 2006-04-14 | 2007-10-17 | 钱玉章 | Liquid compound for eliminating smoke harm and preparing method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101878953A (en) | 2010-11-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106387990B (en) | High-nicotine tobacco extract and its application | |
| CN103989245B (en) | The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity | |
| CN104489911A (en) | Tobacco juice of electronic cigarette | |
| CN101962598B (en) | Essence composition for tobacco and preparation method thereof | |
| CN103113989B (en) | Tobacco essence capable of improving cigarette taste and aroma | |
| CN102304423B (en) | Fragrance-enhancing tobacco essence | |
| CN102204715B (en) | Formula of hawthorn-extract-containing tobacco casing flavor | |
| CN104544549A (en) | Electronic cigarette smoke solution prepared through green tea leaf extract | |
| CN104544545A (en) | Electronic cigarette smoke solution with blood pressure decreasing function | |
| CN102090712B (en) | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes | |
| CN104489908A (en) | Tobacco juice of electronic cigarette | |
| CN104544543A (en) | Electronic cigarette smoke solution prepared through black tea leaf extract | |
| CN104544552A (en) | Electronic cigarette smoke solution prepared through oolong leaf extract | |
| CN103919274A (en) | Electronic cigarette atomized liquid | |
| CN103054173A (en) | Electronic cigarette liquid prepared from discarded tobacco | |
| CN102517151B (en) | Fructus evodiae, bergamot or symplocos sumuntia essential oil, as well as preparation method and application thereof in cigarettes | |
| CN102031194A (en) | Ginkgo leaf volatile oil extraction method and method for flavoring cigarettes by utilizing volatile oil | |
| CN101843364B (en) | Spice additive for natural cigarettes and preparation method thereof | |
| CN104544544A (en) | Electronic cigarette smoke solution prepared through white tea leaf extract | |
| CN104544546A (en) | Electronic cigarette smoke solution with appetite improving and digestion prompting functions | |
| CN101878953B (en) | Aromatic additive for citron natural tobaccos and preparation method thereof | |
| CN103330282B (en) | The application of oil ben in cigarette and the cigarette containing oil ben | |
| CN102771888A (en) | Perfume additive for natural uncaria cigarettes and preparation method thereof | |
| CN104543195A (en) | Preparation method of pueraria shoot tip tea and products of pueraria shoot tip tea | |
| CN104664588B (en) | Nebulized liquid containing ginseng |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121031 Termination date: 20140722 |
|
| EXPY | Termination of patent right or utility model |