CN104327952A - Pelargonium odoratissimum essential oil and extraction method and application of essential oil - Google Patents
Pelargonium odoratissimum essential oil and extraction method and application of essential oil Download PDFInfo
- Publication number
- CN104327952A CN104327952A CN201410581466.5A CN201410581466A CN104327952A CN 104327952 A CN104327952 A CN 104327952A CN 201410581466 A CN201410581466 A CN 201410581466A CN 104327952 A CN104327952 A CN 104327952A
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- China
- Prior art keywords
- essential oil
- volatile oil
- pelargonium odoratissimum
- odoratissimum
- pelargonium
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses Pelargonium odoratissimum essential oil and an extraction method and application of the essential oil. The extraction method comprises the steps of placing Pelargonium odoratissimum into a volatile oil extractor, adding water for soaking, carrying out steam distillation extraction, and separating after condensation to obtain the transparent yellow oily Pelargonium odoratissimum essential oil. Fresh Pelargonium odoratissimum is used as a raw material for extracting essential oil, the fragrance ingredients and the active substances of the Pelargonium odoratissimum are kept to the maximum extent, the operation procedure is simple, the requirement for production equipment is low, the cost is low, any organic reagent is not adopted and the Pelargonium odoratissimum essential oil is environment-friendly. The Pelargonium odoratissimum essential oil has fragrant flavor and lasting fragrance, has the bacteriostatic action, and can be used for blending cosmetics, washing products and medicinal essences.
Description
Technical field
The present invention relates to plants essential oil, specifically belong to one and touch volatile oil and extracting method thereof and application.
Background technology
Touching perfume (or spice) (Plectranthus tomentosa), Labiatae Rabdosia, is perennial shrub shape herbaceous plant, blade is strange fragrant tempting, have and produce refreshing effect to the mind, clearing away summer heat, walk quickly and keep away the effects such as mosquito, can make tea, stew, eat raw, there is certain pharmaceutical use.
Rabdosia plant contains abundant diterpene-kind compound, there is antisepsis and anti-inflammation and the multiple physiologically active such as antitumor, therefore the research of Rabdosia plant is focused mostly on the extraction and isolation in total diterpene or single diterpene compound, very few to the report such as extraction, analysis of its essential oil.
Essential oil is from the root of plant, stem, leaf, flower or fruit, by the general name with the oily mater of characteristic perfume that some row purification extracting process obtain, have inhibiting bacteria and diminishing inflammation, anti-oxidant, purify air, the effect such as endocrine regulation, can be used for the production of perfume, makeup, healthcare products, foodstuff additive and sanitas etc.
Xiong Wei in 2011 etc. adopt head space bagging method to carry out analyzing and testing with gas chromatograph-mass spectrometer (GC-MS) to the fragrance body that touches collected under thermal desorption system condition, and the employing such as Kong Weiwei in 2013 solid-phase microextraction-Gas chromatographyMass spectrometry crashes and touches fragrant different sites volatile component and analyze.Analytical results shows to touch in spiceleaf containing volatile compositions of various active such as limonene, α-pinene, terpinolene, Bornyl acetates.Two authors just analyze volatile component, do not obtain essential oil product.The composition of plants essential oil and its extracting method have much relations, but touch the extracting method of volatile oil and application has no report.
Summary of the invention
The object of the invention is to isolate and touch fragrant plants essential oil, a kind of extracting method touching volatile oil is provided.This extracting method is not with an organic solvent, equipment is simple, practical, can extract on a large scale and touch volatile oil.
A kind of extracting method touching volatile oil provided by the invention, comprise the steps: to get and freshly touch perfume (or spice), be placed in volatile oil extractor, add distilled water according to solid-liquid ratio 1:10-20, soak 1-3 hour, occasional agitation or concussion in immersion process, carry out wet distillation after immersion, extracts after 3-6 hour and terminate distillation, collect essential oil, through anhydrous sodium sulfate drying, the yellow transparent shape obtaining strong smell touches volatile oil, in-4 DEG C of preservations after sealing.
What the present invention obtained touches volatile oil for yellow, and with enhanced aroma taste, and lasting is lasting, also has bacteriostatic action widely.It can be used as essence for allocating makeup, washing product use, and is used as medicinal essence etc.
The present invention has following remarkable advantage:
(1) touch fragrant for raw material with fresh, avoid and deposit process mesometamorphism or dehydration loses the problems such as fragrance, remain to large extent and touch aroma component in perfume (or spice) and other active substance.
(2) touch fragrant blade when being subject to touching and stimulating, intracellular moisture is had an effect, and pulvinus turgescence changes, and pore is expanded.Therefore, first will touch fragrant immersion before it is distilled, and frequently stir concussion in immersion process, be conducive to the dispersal events of fragrance material, and then reduce the required energy consumption of heating.
In a word, present invention process is simple, easy, and cost is low, pollution-free; What the present invention obtained touches volatile oil for yellow, and with enhanced aroma taste, and lasting is lasting, also has bacteriostatic action widely, can be used as essence.
Embodiment
Embodiment 1
Touch volatile oil preparation:
Get and freshly touch perfume (or spice), be placed in volatile oil extractor, add distilled water according to solid-liquid ratio 1:15, soak 2 hours, be interrupted concussion in immersion process, after immersion, carry out wet distillation, extracts after 6 hours and terminate to distill.Collect essential oil, through anhydrous sodium sulfate drying, the yellow transparent shape obtaining strong smell touches volatile oil, in-4 DEG C of preservations after sealing.
Embodiment 2
Touch volatile oil bacteriostatic experiment:
Adopt disc diffusion method, for examination bacterial classification be: subtilis (Bacillus subtilis), streptococcus aureus (Staphylococcus aureus), intestinal bacteria (Escherichia coli), yeast saccharomyces cerevisiae (Saccharomyces cerevisiae), Penicllium chrysogenum (Penicillium Chrysogenum) and aspergillus niger (Aspergillus niger).Concrete grammar step is as follows:
1) preparation is dull and stereotyped: bacterium LB substratum, i.e. Tryptones (Tryptone) 10g/L, yeast extract (Yeast extract) 5g/L, sodium-chlor (NaCl) 10g/L and agar (Agar) 15g/L.Fungus culture PDA substratum, i.e. potato 200g/L (boil filtration, get filtrate), glucose 15g//L, agar (Agar) 20g/L.After medium sterilization, cultivate 24h for necessary 37 DEG C, asepsis growth can use.Below all aseptic technique is needed.
2) be coated with bacteria suspension: with the well-grown bacterial classification test tube slant of aseptic water washing, and gently scrape bacterium colony with transfering loop, mixing, prepares bacteria suspension.Draw 0.2mL bacteria suspension spread plate, often kind of bacterium arranges three and repeats dull and stereotyped.
3) filter paper dosing: the filter paper (diameter 9mm) after sterilizing is affixed on dull and stereotyped corresponding position, carries out mark.Essential oil DMSO (dimethyl sulfoxide (DMSO)) dilutes different multiples, take DMSO as contrast.Draw the essential oil after 20 μ L DMSO and dilution respectively, point sample is on filter paper.
4) cultivate: flat board is inverted and cultivates.Bacterium cultivates 24h in 37 DEG C, and fungi is cultivated after 72h in 26 DEG C, observes the size that has that it's too late of inhibition zone around filter paper disk respectively.The results are shown in Table 1.
Table 1 touches bacteriostatic activity (antibacterial circle diameter) measurement result of volatile oil
mm
As shown in Table 1, touching volatile oil has stronger bacteriostatic activity to for the 3 kinds of fungies tried and 3 bacterium kinds, all has restraining effect to gram-positive microorganism and negative bacterium.Show, touch volatile oil and there is bacteriostatic action widely.
It is aromatic that gained of the present invention touches volatile oil smell, and lasting is lasting, has bacteriostatic activity, can be used for allotment makeup, washing product essence and medicinal essence etc.
Claims (4)
1. one kind is touched the extracting method of volatile oil, it is characterized in that, comprise the steps: to get and freshly touch perfume (or spice), be placed in volatile oil extractor, distilled water is added according to solid-liquid ratio 1:10-20, soak 1-3 hour, occasional agitation or concussion in immersion process, carry out wet distillation 3-6 hour after immersion, collect essential oil, through anhydrous sodium sulfate drying, obtain yellow transparent shape and touch volatile oil, in-4 DEG C of preservations after sealing.
2. the volatile oil that touches that extracting method obtains as claimed in claim 1 is allocating the application in makeup as essence.
3. as claimed in claim 1 extracting method obtain touch volatile oil as the application of essence in articles for washing.
4. as claimed in claim 1 extracting method obtain touch volatile oil as medicinal essence.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410581466.5A CN104327952A (en) | 2014-10-27 | 2014-10-27 | Pelargonium odoratissimum essential oil and extraction method and application of essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410581466.5A CN104327952A (en) | 2014-10-27 | 2014-10-27 | Pelargonium odoratissimum essential oil and extraction method and application of essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104327952A true CN104327952A (en) | 2015-02-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410581466.5A Pending CN104327952A (en) | 2014-10-27 | 2014-10-27 | Pelargonium odoratissimum essential oil and extraction method and application of essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104327952A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106010793A (en) * | 2016-07-14 | 2016-10-12 | 杭州易则通工业设计有限公司 | Multi-functional hydrolat device |
| CN110051613A (en) * | 2019-05-24 | 2019-07-26 | 贵州花锦谷生物科技有限公司 | A kind of preparation method of ferment surfactant |
| CN110358630A (en) * | 2019-06-25 | 2019-10-22 | 河南中烟工业有限责任公司 | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette |
| CN112022750A (en) * | 2020-09-29 | 2020-12-04 | 青岛科技大学 | Compound essential oil, preparation method thereof and application of compound essential oil in anti-allergy acne-removing cosmetics |
| CN112336769A (en) * | 2020-11-18 | 2021-02-09 | 青岛科技大学 | Natural plant fresh leaf extract composition and preparation for promoting wound healing and preparation method thereof |
| CN113373010A (en) * | 2021-07-19 | 2021-09-10 | 安顺学院 | Natural plant sterilization handmade soap and preparation method thereof |
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| CN101716209A (en) * | 2009-12-02 | 2010-06-02 | 中国科学院西北高原生物研究所 | Artemisia dalai-lamae Krasch. essential oil and preparation method and application thereof |
| CN102258751A (en) * | 2011-07-21 | 2011-11-30 | 泰一和浦（北京）中医药研究院有限公司 | Traditional Chinese medicine composition mint for treating melancholia, dispelling melancholy and relieving depression |
| CN102952642A (en) * | 2012-10-24 | 2013-03-06 | 内蒙古农业大学 | Steam distillation method for extracting cornutcd pugionium fruit essential oil |
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| CN101584721A (en) * | 2009-07-06 | 2009-11-25 | 江苏泰灵生物科技有限公司 | Chinese traditional medicine antibiotic hemostatic plaster |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106010793A (en) * | 2016-07-14 | 2016-10-12 | 杭州易则通工业设计有限公司 | Multi-functional hydrolat device |
| CN110051613A (en) * | 2019-05-24 | 2019-07-26 | 贵州花锦谷生物科技有限公司 | A kind of preparation method of ferment surfactant |
| CN110358630A (en) * | 2019-06-25 | 2019-10-22 | 河南中烟工业有限责任公司 | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette |
| CN112022750A (en) * | 2020-09-29 | 2020-12-04 | 青岛科技大学 | Compound essential oil, preparation method thereof and application of compound essential oil in anti-allergy acne-removing cosmetics |
| CN112336769A (en) * | 2020-11-18 | 2021-02-09 | 青岛科技大学 | Natural plant fresh leaf extract composition and preparation for promoting wound healing and preparation method thereof |
| CN113373010A (en) * | 2021-07-19 | 2021-09-10 | 安顺学院 | Natural plant sterilization handmade soap and preparation method thereof |
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Application publication date: 20150204 |
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