CN103405359A - Natural chionanthus retusus flower perfume and preparation method thereof - Google Patents

Natural chionanthus retusus flower perfume and preparation method thereof Download PDF

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Publication number
CN103405359A
CN103405359A CN2013102973129A CN201310297312A CN103405359A CN 103405359 A CN103405359 A CN 103405359A CN 2013102973129 A CN2013102973129 A CN 2013102973129A CN 201310297312 A CN201310297312 A CN 201310297312A CN 103405359 A CN103405359 A CN 103405359A
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flower
natural
oil
diffuse coptosapelta
parts
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CN103405359B (en
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尹卫平
刘普
范文瑞
高嘉屿
李欣
牛兰岚
李海迪
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Henan University of Science and Technology
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Henan University of Science and Technology
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Abstract

The invention provides natural chionanthus retusus flower perfume and a preparation method thereof, relating to the perfume. The natural chionanthus retusus flower perfume is composed of following components in parts by volume: 1.4-2.8 parts of chionanthus retusus flower natural essential oil, 0.05-0.12 part of sandalwood essential oil, 0.05-0.13 part of rosemary essential oil, 0.05-0.10 part of tea tree oil, 0.08-0.2 part of geranium essential oil, 0.08-0.17 part of bergamot essential oil, 0.15-0.23 part of sweet orange oil and 96.25-98.14 parts of ethanol with the volume concentration of 95%, wherein all the components are mixed uniformly, and then are aged and filtered to obtain the natural chionanthus retusus flower perfume. The natural chionanthus retusus flower perfume provided by the invention is clear is color and luster, smooth and soft in aroma and reasonable in formula; the dispersion of aromas of all spice components in the perfume is harmonious and stable; a special rich flower aroma of a chionanthus retusus flower is kept; a main aroma of a single flower aroma type perfume is highlighted and the aroma keeping time can be up to 3-5 days.

Description

A kind of natural Diffuse Coptosapelta fragrance of a flower water and preparation method thereof
Technical field
The present invention relates to a kind of perfume, be specially a kind of natural Diffuse Coptosapelta fragrance of a flower water and preparation method thereof.
Background technology
Chionanthus retusa Lindl et Paxt is Oleaceae Diffuse Coptosapelta platymiscium, defoliation small arbor or shrub, and Chinese Second Class Key Protected Plant, be the good species of viewing and admiring.In time early summer, full tree is spent a thousand li drifting fragrance in vain, as covers frost lid snow, luicd and elegant pleasant, suitable planting in the building surrounding, or by Zhong Chi side, park and trade.The Diffuse Coptosapelta tender leaf can be made beverage for Folium Camelliae sinensis, and the fruit rich in oil can extract oil, and for industrial, timber is hard heavy careful, but manufacturing appliance.The bud of chionanthus retusa Lindl et Paxt, leaf also have medical value.Diffuse Coptosapelta is multiplex in folk medicine aspect medicinal, and the effect of relieving heat and thirst is arranged, the tender leaf of Diffuse Coptosapelta and flower among the people make tea to drink also can be used for preventing and treating chronic hepatopathy.Therefore the cultivated plant Diffuse Coptosapelta, have exploitation in China and be worth.
The volatile oil fragrance of extraction from Diffuse Coptosapelta is spent is pure, for the typical fragrance of a flower, contain after measured tens kinds of fragrance components, mainly contain benzyl alcohol, phenethanol, p-methoxybenzene ethanol, p-hydroxyphenylethanol, ethyl anisate, trans-(+)-nerolidol, hexyl-benzoate, (E)-2-hexyl-benzoate, myristic aldehyde, farnesol, benzyl benzoate, linalool oxide, eugenol, p-methoxybenzene ethanol, trans-jasmone, a large amount of natural perfume material compositions such as dehydrogenation ionol, not only can be used as essence but also can be used as the natural perfume material application, especially can be used in the preparation of specific single floral type perfume.Current single floral type perfume is mostly the fragrance of a flower perfume such as common Flos Rosae Rugosae, jasmine, there is not yet so far report and take the Diffuse Coptosapelta flower as the natural single floral type perfume of main note.
Summary of the invention
Purpose of the present invention just is to provide a kind ofly take the Diffuse Coptosapelta fragrance of a flower and is main note, be equipped with natural single floral type Diffuse Coptosapelta fragrance of a flower water of other auxiliary spice and preparation method thereof, prepared perfume fragrance exquisiteness is soft, each spice fragrance distribute harmony, stable, and can give prominence to the main note gas of Diffuse Coptosapelta flower, the fragrant time of guarantor is longer.
To achieve these goals, technical scheme of the present invention is: a kind of natural Diffuse Coptosapelta fragrance of a flower water, by volume the umber meter its consist of: 1.4 ~ 2.8 parts of Diffuse Coptosapelta flower natural essential oils, 0.05 ~ 0.12 part of Lignum Santali Albi quintessence oil, 0.05 ~ 0.13 part of rosemary ethereal oil, 0.05 ~ 0.10 part of tea tree oil, 0.08 ~ 0.2 part of Flos Pelargonii quintessence oil, 0.08 ~ 0.17 part of Bergamot, 0.15 ~ 0.23 part of oleum Citri sinensis and volumetric concentration are 96.25 ~ 98.14 parts of 95% ethanol.
As preferably, 2.5 parts of Diffuse Coptosapelta flower natural essential oils, 0.08 part of Lignum Santali Albi quintessence oil, 0.08 part of rosemary ethereal oil, 0.08 part of tea tree oil, 0.15 part of Flos Pelargonii quintessence oil, 0.14 part of Bergamot, 0.21 part of oleum Citri sinensis and volumetric concentration are 96.76 parts of 95% ethanol.
The preparation method of described natural Diffuse Coptosapelta fragrance of a flower water is:
(1), the preparation of natural Diffuse Coptosapelta flower essential oil: spend nature to dry in the shade, pulverize and be placed in distil container Diffuse Coptosapelta, adopt steam distillation distillation 6 ~ 7 hours, the gained distillate namely obtains natural Diffuse Coptosapelta flower essential oil through extraction, after filtering;
(2), the modulation of perfume: umber by volume, get 1.4 ~ 2.8 parts of Diffuse Coptosapelta flower natural essential oils, 0.05 ~ 0.13 part of rosemary ethereal oil, 0.08 ~ 0.2 part of Flos Pelargonii quintessence oil, 0.15 ~ 0.23 part of 0.08 ~ 0.17 part of Bergamot and oleum Citri sinensis, by above-mentioned spice mix homogeneously and kept in Dark Place 3 ~ 5 days, and then add 0.05 ~ 0.12 part of Lignum Santali Albi quintessence oil, 0.05 ~ 0.10 part of tea tree oil and volumetric concentration are 96.25 ~ 98.14 parts of 95% ethanol, after mix homogeneously, obtain mixed liquor, above-mentioned mixed liquor was placed 40 ~ 60 days under 0 ~ 5 ℃, then remove by filter precipitate, gained filtrate is natural Diffuse Coptosapelta fragrance of a flower water.
Beneficial effect: natural Diffuse Coptosapelta fragrance of a flower water colour of the present invention pool is limpid, and the fragrance exquisiteness is soft, and formula rationally, in perfume, each fragrance component fragrance distributes harmony, stable, retained Diffuse Coptosapelta and spent distinctive foundation for heavy florals breath, given prominence to the main note flavor of single floral type perfume, fragrance remaining time can reach 3 ~ 5 days.In perfume of the present invention, select the spice oleum Citri sinensis as head perfume (or spice), add have happiness, that Bergamot nice and cool, aromatic odour is used for modifying head is fragrant.Natural Diffuse Coptosapelta flower essential oil is as body note, and comes to be in harmonious proportion body note with Flos Pelargonii and Herba Rosmarini Officinalis, and to give prominence to the main note flavor of Diffuse Coptosapelta flower, Herba Rosmarini Officinalis also plays the antiseptical function simultaneously.The Lignum Santali Albi that bottom note selects the Radix Aucklandiae to adjust, not only retained the strong of the Diffuse Coptosapelta fragrance of a flower but also increased wooden pure and fresh, form a kind of fresh scent of uniqueness, and together with tea tree oil, play the effect of slow-release fragrance, to coordinate the volatility of each spice, make each spice fragrance emission become slowly, harmonious stable, make simultaneously perfume fragrance more lasting, extend fragrance remaining time.
In addition, in the modulation process of perfume of the present invention, first several spice is mixed and preserves, add again bottom note spice and ethanol fully to be in harmonious proportion, then carry out ageing, this can make the fragrant and body note of the head of perfume become and be connected and coordinate in the distributing of fragrance, and it is more fine and smooth soft that the fragrance of perfume becomes, and fragrance emissions is more stable, lastingly.
The specific embodiment
A kind of natural Diffuse Coptosapelta fragrance of a flower water, by volume the umber meter its consist of: 1.4 ~ 2.8 parts of Diffuse Coptosapelta flower natural essential oils, 0.05 ~ 0.12 part of Lignum Santali Albi quintessence oil, 0.05 ~ 0.13 part of rosemary ethereal oil, 0.05 ~ 0.10 part of tea tree oil, 0.08 ~ 0.2 part of Flos Pelargonii quintessence oil, 0.08 ~ 0.17 part of Bergamot, 0.15 ~ 0.23 part of oleum Citri sinensis and volumetric concentration are 96.25 ~ 98.14 parts of 95% ethanol.
The preparation method of described natural Diffuse Coptosapelta fragrance of a flower water is:
(1), the preparation of natural Diffuse Coptosapelta flower essential oil: spend nature to dry in the shade, pulverize and be placed in distil container Diffuse Coptosapelta, adopt steam distillation distillation 6 ~ 7 hours, the gained distillate namely obtains natural Diffuse Coptosapelta flower essential oil through extraction, after filtering;
(2), the modulation of perfume: umber by volume, get 1.4 ~ 2.8 parts of Diffuse Coptosapelta flower natural essential oils, 0.05 ~ 0.13 part of rosemary ethereal oil, 0.08 ~ 0.2 part of Flos Pelargonii quintessence oil, 0.15 ~ 0.23 part of 0.08 ~ 0.17 part of Bergamot and oleum Citri sinensis, by above-mentioned spice mix homogeneously and kept in Dark Place 3 ~ 5 days, and then add 0.05 ~ 0.12 part of Lignum Santali Albi quintessence oil, 0.05 ~ 0.10 part of tea tree oil and volumetric concentration are 96.25 ~ 98.14 parts of 95% ethanol, after mix homogeneously, obtain mixed liquor, above-mentioned mixed liquor was placed 40 ~ 60 days under 0 ~ 5 ℃, then remove by filter precipitate, gained filtrate is natural Diffuse Coptosapelta fragrance of a flower water.
Embodiment 1
A kind of natural Diffuse Coptosapelta fragrance of a flower water, by volume the umber meter its consist of: 1.4 parts of Diffuse Coptosapelta flower natural essential oils, 0.05 part of Lignum Santali Albi quintessence oil, 0.05 part of rosemary ethereal oil, 0.05 part of tea tree oil, 0.08 part of Flos Pelargonii quintessence oil, 0.08 part of Bergamot, 0.15 part of oleum Citri sinensis and volumetric concentration are 98.14 parts of 95% ethanol.
Embodiment 2
A kind of natural Diffuse Coptosapelta fragrance of a flower water, by volume the umber meter its consist of: 2.5 parts of Diffuse Coptosapelta flower natural essential oils, 0.08 part of Lignum Santali Albi quintessence oil, 0.08 part of rosemary ethereal oil, 0.08 part of tea tree oil, 0.15 part of Flos Pelargonii quintessence oil, 0.14 part of Bergamot, 0.21 part of oleum Citri sinensis and volumetric concentration are 96.76 parts of 95% ethanol.
Embodiment 3
A kind of natural Diffuse Coptosapelta fragrance of a flower water, by volume the umber meter its consist of: 2.8 parts of Diffuse Coptosapelta flower natural essential oils, 0.12 part of Lignum Santali Albi quintessence oil, 0.13 part of rosemary ethereal oil, 0.1 part of tea tree oil, 0.2 part of Flos Pelargonii quintessence oil, 0.17 part of Bergamot, 0.23 part of oleum Citri sinensis and volumetric concentration are 96.25 parts of 95% ethanol.
Embodiment 4
A kind of natural Diffuse Coptosapelta fragrance of a flower water, by volume the umber meter its consist of: 2.0 parts of Diffuse Coptosapelta flower natural essential oils, 0.1 part of Lignum Santali Albi quintessence oil, 0.1 part of rosemary ethereal oil, 0.1 part of tea tree oil, 0.2 part of Flos Pelargonii quintessence oil, 0.17 part of Bergamot, 0.23 part of oleum Citri sinensis and volumetric concentration are 97.1 parts of 95% ethanol.

Claims (3)

1. natural Diffuse Coptosapelta fragrance of a flower water is characterized in that: by volume the umber meter its consist of: 1.4 ~ 2.8 parts of Diffuse Coptosapelta flower natural essential oils, 0.05 ~ 0.12 part of Lignum Santali Albi quintessence oil, 0.05 ~ 0.13 part of rosemary ethereal oil, 0.05 ~ 0.10 part of tea tree oil, 0.08 ~ 0.2 part of Flos Pelargonii quintessence oil, 0.08 ~ 0.17 part of Bergamot, 0.15 ~ 0.23 part of oleum Citri sinensis and volumetric concentration are 96.25 ~ 98.14 parts of 95% ethanol.
2. a kind of natural Diffuse Coptosapelta fragrance of a flower water as claimed in claim 1 is characterized in that: by volume the umber meter its consist of: 2.5 parts of Diffuse Coptosapelta flower natural essential oils, 0.08 part of Lignum Santali Albi quintessence oil, 0.08 part of rosemary ethereal oil, 0.08 part of tea tree oil, 0.15 part of Flos Pelargonii quintessence oil, 0.14 part of Bergamot, 0.21 part of oleum Citri sinensis and volumetric concentration are 96.76 parts of 95% ethanol.
3. the preparation method of a kind of natural Diffuse Coptosapelta fragrance of a flower water as claimed in claim 1, it is characterized in that: its preparation process is:
(1), the preparation of natural Diffuse Coptosapelta flower essential oil: spend nature to dry in the shade, pulverize and be placed in distil container Diffuse Coptosapelta, adopt steam distillation distillation 6 ~ 7 hours, the gained distillate namely obtains natural Diffuse Coptosapelta flower essential oil through extraction, after filtering;
(2), the modulation of perfume: umber by volume, get 1.4 ~ 2.8 parts of Diffuse Coptosapelta flower natural essential oils, 0.05 ~ 0.13 part of rosemary ethereal oil, 0.08 ~ 0.2 part of Flos Pelargonii quintessence oil, 0.15 ~ 0.23 part of 0.08 ~ 0.17 part of Bergamot and oleum Citri sinensis, by above-mentioned spice mix homogeneously and kept in Dark Place 3 ~ 5 days, and then add 0.05 ~ 0.12 part of Lignum Santali Albi quintessence oil, 0.05 ~ 0.10 part of tea tree oil and volumetric concentration are 96.25 ~ 98.14 parts of 95% ethanol, after mix homogeneously, obtain mixed liquor, above-mentioned mixed liquor was placed 40 ~ 60 days under 0 ~ 5 ℃, then remove by filter precipitate, gained filtrate is natural Diffuse Coptosapelta fragrance of a flower water.
CN201310297312.9A 2013-07-16 2013-07-16 Natural chionanthus retusus flower perfume and preparation method thereof Active CN103405359B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104274369A (en) * 2014-09-28 2015-01-14 青岛康合伟业商贸有限公司 Mixed flower type perfume
CN108117768A (en) * 2017-12-12 2018-06-05 湖北中烟工业有限责任公司 A kind of essence package body nano catalytic material and its preparation method and application
CN109248112A (en) * 2018-11-07 2019-01-22 长沙浩然医疗科技有限公司 A kind of lasting refreshing perfume and preparation method thereof
CN109288732A (en) * 2018-11-26 2019-02-01 金玛瑙香水(明光)有限公司 A kind of natural Yilan perfume
CN115322831A (en) * 2022-08-15 2022-11-11 泉州威士登香精香料有限公司 Mint essence with lasting cool feeling release function and preparation method thereof

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CN1969809A (en) * 2006-10-19 2007-05-30 上海邦成芝麻研究所 Massage oil containing sesame and preparation process thereof

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CN1969809A (en) * 2006-10-19 2007-05-30 上海邦成芝麻研究所 Massage oil containing sesame and preparation process thereof

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胡畔: ""民间药用植物流苏花化学成分分离鉴定"", 《中国优秀硕士学位论文全文数据库医药卫生科技辑(月刊 )》 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104274369A (en) * 2014-09-28 2015-01-14 青岛康合伟业商贸有限公司 Mixed flower type perfume
CN108117768A (en) * 2017-12-12 2018-06-05 湖北中烟工业有限责任公司 A kind of essence package body nano catalytic material and its preparation method and application
CN108117768B (en) * 2017-12-12 2020-04-24 湖北中烟工业有限责任公司 Nano catalytic material for essence package and preparation method and application thereof
CN109248112A (en) * 2018-11-07 2019-01-22 长沙浩然医疗科技有限公司 A kind of lasting refreshing perfume and preparation method thereof
CN109288732A (en) * 2018-11-26 2019-02-01 金玛瑙香水(明光)有限公司 A kind of natural Yilan perfume
CN115322831A (en) * 2022-08-15 2022-11-11 泉州威士登香精香料有限公司 Mint essence with lasting cool feeling release function and preparation method thereof

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