CN111249180B - Refreshing perfume and preparation method thereof - Google Patents

Refreshing perfume and preparation method thereof Download PDF

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CN111249180B
CN111249180B CN201910964627.1A CN201910964627A CN111249180B CN 111249180 B CN111249180 B CN 111249180B CN 201910964627 A CN201910964627 A CN 201910964627A CN 111249180 B CN111249180 B CN 111249180B
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essential oil
parts
rosewood
bergamot
ethanol
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CN111249180A (en
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张妙玲
范文静
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Shenzhen Yuechang Technology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention belongs to the field of perfume preparation, and particularly relates to refreshing perfume and a preparation method thereof. The refreshing perfume is prepared from the raw materials including green lemons, bergamot, rosewood, orange flowers and the like through cold pressing, organic solvent extraction and steam distillation, and the perfume also comprises auxiliary materials including maltol, ethanol, isoamylol and geraniol besides the essential oil prepared from the four raw materials. The prepared essential oil has good refreshing effect, and the preparation method is simple and easy.

Description

Refreshing perfume and preparation method thereof
Technical Field
The invention belongs to the field of perfume preparation, and particularly relates to refreshing perfume and a preparation method thereof.
Background
In short, perfume, essence and spice belong to volatile substances; they have certain fragrance and aroma and can be sensed by the sense of smell or taste of people; the aims of being lovely, delightful and rich in and beautifying the material culture and life of people are required to be achieved.
The perfume is divided into a plurality of types according to different requirements, has different effects, is changed into the same as eating, sleeping, dressing and making up, becomes an essential part of life, work, study, leisure and even love at present, adds the color of people and improves the taste of people.
People are tired when being concentrated on a work for a long time, and are particularly tired and inattentive in spring, autumn and summer. Clerks in offices, for example, always use computers, and are not active, particularly for long-distance bus drivers. However, some people are sensitive to the strong taste of the perfume, and some perfumes with refreshing effect are not suitable for all people.
For example, the Chinese patent application CN 105534751A discloses a refreshing perfume which is prepared from the following raw materials in parts by weight: 8-10 parts of mint essential oil, 8-10 parts of tea essential oil, 4-6 parts of lemon essential oil, 2-5 parts of jasmine essential oil, 2-5 parts of chamomile essential oil, 3-5 parts of lavender essential oil, 5-8 parts of borneol, 0.6-0.8 part of camphor and 80-100 parts of solvent; the solvent consists of 65-75% of ethanol and 25-35% of propylene glycol, is low in cost and has the effect of refreshing. However, the perfume uses materials with relatively irritating taste such as camphor, so that the taste of the perfume is difficult to be accepted by many people.
Chinese patent application CN 107496281 a discloses a refreshing perfume. The refreshing perfume is prepared from the following raw materials in parts by weight: 65-80 parts of ethanol, 20-30 parts of propylene glycol, 10-18 parts of essential oil, 3-10 parts of rosemary, 5-10 parts of lavender, 4-12 parts of mint, 2-7 parts of green tea, 1-5 parts of honeysuckle, 3-9 parts of liquorice, 1-7 parts of clove, 3-9 parts of oregano and 1-5 parts of duckweed.
Meanwhile, most of perfumes in the market at present are prepared by using chemical perfumes, and the chemical perfumes contain aromatic benzene ring compounds, and along with volatilization of alcohol, the chemical perfumes can stimulate human organs, particularly respiratory systems, so that symptoms such as cough, dizziness and vomiting appear in people in the automobile, and the health of the people is harmed. If the composition is used for a long time, the composition can cause slow smell, weak vision and even become a carcinogenic cause.
Furthermore, with efficient raw materials, the degree of extraction of essential oils is strongly related to the manufacturing costs. In the process of preparing the perfume, attention needs to be paid to improving the extraction efficiency of essential oil as much as possible.
Therefore, the problem that the perfume is thick in taste, uncomfortable and high in irritation is solved, the extraction efficiency of the essential oil is improved, and the technical problem which needs to be solved in the current perfume research is urgent.
Disclosure of Invention
In order to overcome the technical problems, the invention provides the refreshing perfume and the preparation method thereof, the refreshing perfume is fresh and natural, has the functions of relieving emotion and refreshing, and the preparation method is simple and easy to implement.
In order to achieve the above purpose, the technical scheme provided by the invention is as follows:
the refreshing perfume comprises the following raw materials: green lemon, bergamot, rosewood and orange flower;
the refreshing perfume comprises the following components: lemon essential oil, bergamot essential oil, rosewood essential oil and orange flower essential oil;
preferably, the refreshing perfume further comprises auxiliary materials, wherein the auxiliary materials are maltol, ethanol, isoamylol and geraniol;
preferably, the refreshing perfume comprises the following components in parts by weight: 5-15 parts of green lemon essential oil, 5-15 parts of bergamot essential oil, 1-15 parts of rosewood essential oil, 1-15 parts of neroli essential oil, 20-50 parts of maltol, 100 parts of ethanol, 160 parts of isoamylol and 10-30 parts of geraniol;
preferably, the refreshing perfume comprises the following components in parts by weight: 5-10 parts of green lemon essential oil, 10-15 parts of bergamot essential oil, 4-10 parts of rosewood essential oil, 5-10 parts of orange flower essential oil, 30-40 parts of maltol, 140 parts of ethanol 120-doped materials, 40-50 parts of isoamylol and 15-20 parts of geraniol;
preferably, the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 10 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 35 parts of maltol, 135 parts of ethanol, 45 parts of isoamylol and 20 parts of geraniol;
preferably, the preparation method of the essential oil comprises the following steps:
(1) respectively cutting green lemon and bergamot into small pieces, squeezing, and filtering to obtain filtrate and residue;
(2) respectively placing the obtained residues in petroleum ether for reflux extraction, and mixing the residues with the filtrate after reduced pressure distillation to obtain a crude extract;
(3) respectively carrying out steam distillation extraction on the crude extracts, and heating and refluxing to obtain the green lemon essential oil and the bergamot essential oil;
(4) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
Preferably, the essential oil is prepared by a method, wherein in the step (1), the squeezing is carried out at 20-40 ℃;
preferably, in the step (2), the amount of the petroleum ether is 3-5 times of the mass of the residue;
preferably, in step (2), the petroleum ether has a boiling range of 30 to 60 ℃;
preferably, in the step (3) or (4), the heating and refluxing are carried out until the essential oil is not increased any more;
another object of the present invention is to provide a method for preparing the refreshing perfume, comprising the steps of:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Preferably, in step (1) or (2), the stirring is performed at 100-500 rpm.
Compared with the prior art, the invention has the technical advantages that:
(1) according to the invention, the green lemon essential oil, the bergamot essential oil, the rosewood essential oil and the orange flower essential oil are used for promoting the hydrogen freshness and nature effects of the perfume together, so that the prepared perfume has the functions of relieving the mood and refreshing;
(2) in the invention, besides the green lemon essential oil and the orange flower essential oil, the bergamot essential oil and the pear flower wood essential oil are also used, so that the comfortable sensation of human smell is improved under the condition of over-rich perfume taste;
(3) according to the invention, the green lemon and the bergamot are respectively subjected to cold pressing extraction, petroleum ether extraction and steam distillation extraction processes, so that essential oil in the green lemon and the bergamot can be fully extracted, and the utilization rate of raw materials is improved;
(4) the perfume prepared by the invention also has good performance of improving human immunity.
Detailed Description
Example 1
The refreshing perfume comprises the following raw materials: green lemon, bergamot, rosewood and orange flower;
the preparation method of the essential oil in the embodiment comprises the following steps:
(1) cutting green lemon and bergamot into small pieces, squeezing at 30 deg.C, and filtering to obtain filtrate and residue;
(2) respectively placing the obtained residues in petroleum ether with the mass 4 times that of the residues for reflux extraction, and mixing the residues with the filtrate after reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, heating and refluxing until essential oil is not increased to obtain fructus Citri Limoniae essential oil and fructus Citri Sarcodactylis essential oil;
(4) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
In the embodiment, the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 10 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 35 parts of maltol, 135 parts of ethanol, 45 parts of isoamylol and 20 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein at 300rpm, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Example 2
The refreshing perfume comprises the following raw materials: green lemon, bergamot, rosewood and orange flower;
the preparation method of the essential oil in the embodiment comprises the following steps:
(1) cutting green lemon and bergamot into small pieces, squeezing at 20 deg.C, and filtering to obtain filtrate and residue;
(2) respectively placing the obtained residues in petroleum ether with the mass 3 times that of the residues for reflux extraction, and mixing the residues with the filtrate after reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, heating and refluxing until essential oil is not increased to obtain fructus Citri Limoniae essential oil and fructus Citri Sarcodactylis essential oil;
(4) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
In the embodiment, the refreshing perfume comprises the following components in parts by weight: 5 parts of green lemon essential oil, 15 parts of bergamot essential oil, 1 part of rosewood essential oil, 15 parts of orange flower essential oil, 50 parts of maltol, 160 parts of ethanol, 60 parts of isoamylol and 30 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein under the condition of 100rpm, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Example 3
The refreshing perfume comprises the following raw materials: green lemon, bergamot, rosewood and orange flower;
the preparation method of the essential oil in the embodiment comprises the following steps:
(1) cutting green lemon and bergamot into small pieces, squeezing at 40 deg.C, and filtering to obtain filtrate and residue;
(2) respectively placing the obtained residues into petroleum ether with the mass 5 times that of the residues for reflux extraction, and mixing the residues with the filtrate after reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, heating and refluxing until essential oil is not increased to obtain fructus Citri Limoniae essential oil and fructus Citri Sarcodactylis essential oil;
(4) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
In the embodiment, the refreshing perfume comprises the following components in parts by weight: 15 parts of green lemon essential oil, 5 parts of bergamot essential oil, 15 parts of rosewood essential oil, 1 part of neroli essential oil, 20 parts of maltol, 100 parts of ethanol, 20 parts of isoamylol and 30 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein at 500rpm, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Example 4
The refreshing perfume comprises the following raw materials: green lemon, bergamot, rosewood and orange flower;
the preparation method of the essential oil in the embodiment comprises the following steps:
(1) cutting green lemon and bergamot into small pieces, squeezing at 20 deg.C, and filtering to obtain filtrate and residue;
(2) respectively placing the obtained residues into petroleum ether with the mass 5 times that of the residues for reflux extraction, and mixing the residues with the filtrate after reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, heating and refluxing until essential oil is not increased to obtain fructus Citri Limoniae essential oil and fructus Citri Sarcodactylis essential oil;
(4) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
In the embodiment, the refreshing perfume comprises the following components in parts by weight: 5 parts of green lemon essential oil, 10 parts of bergamot essential oil, 10 parts of rosewood essential oil, 5 parts of orange flower essential oil, 40 parts of maltol, 140 parts of ethanol, 40 parts of isoamylol and 20 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein under the condition of 100rpm, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Example 5
The refreshing perfume comprises the following raw materials: green lemon, bergamot, rosewood and orange flower;
the preparation method of the essential oil in the embodiment comprises the following steps:
(1) cutting green lemon and bergamot into small pieces, squeezing at 20 deg.C, and filtering to obtain filtrate and residue;
(2) respectively placing the obtained residues in petroleum ether with the mass 3 times that of the residues for reflux extraction, and mixing the residues with the filtrate after reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, heating and refluxing until essential oil is not increased to obtain fructus Citri Limoniae essential oil and fructus Citri Sarcodactylis essential oil;
(4) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
In the embodiment, the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 15 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 30 parts of maltol, 120 parts of ethanol, 50 parts of isoamylol and 15 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein under the condition of 200rpm, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Comparative example 1
Compared to example 1, it does not contain maltol.
The raw materials of the refreshing perfume in the embodiment are the same as those of the embodiment 1;
the preparation method of the essential oil in the embodiment is the same as that of the embodiment 1;
in the embodiment, the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 10 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 135 parts of ethanol, 45 parts of isoamylol and 20 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) dissolving geraniol in ethanol, dissolving rosewood essential oil and neroli essential oil in the geraniol, and stirring at 300rpm to obtain an ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Comparative example 2
In comparison with example 1, geraniol was not contained.
The raw materials of the refreshing perfume in the embodiment are the same as those of the embodiment 1;
the preparation method of the essential oil in the embodiment is the same as that of the embodiment 1;
in the embodiment, the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 10 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 35 parts of maltol, 135 parts of ethanol and 45 parts of isoamylol;
the preparation method of the refreshing perfume comprises the following steps:
(1) dissolving maltol in ethanol, dissolving rosewood essential oil and neroli essential oil in the ethanol, and stirring at 300rpm to obtain an ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Comparative example 3
Compared with example 1, the essential oil preparation process is different.
The raw materials of the refreshing perfume in the embodiment are the same as those of the embodiment 1;
the preparation method of the essential oil in the embodiment comprises the following steps:
(1) cutting green lemon and bergamot into small pieces, squeezing at 30 deg.C, and filtering to obtain filtrate and residue;
(2) extracting the filtrate by steam distillation, heating and refluxing until essential oil is not increased to obtain fructus Citri Limoniae essential oil and fructus Citri Sarcodactylis essential oil;
(3) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
In the embodiment, the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 10 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 35 parts of maltol, 135 parts of ethanol, 45 parts of isoamylol and 20 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein at 300rpm, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Comparative example 4
Compared with example 1, the essential oil preparation process is different.
The refreshing perfume comprises the following raw materials: green lemon, bergamot, rosewood and orange flower;
the preparation method of the essential oil in the embodiment comprises the following steps:
(1) respectively cutting the green lemon and the bergamot into small pieces, respectively placing the small pieces in petroleum ether with the mass of 4 times of the weight of the small pieces for reflux extraction, and obtaining a crude extract after reduced pressure distillation; the boiling range of the petroleum ether is 30-60 ℃;
(2) extracting the crude extract by steam distillation, heating and refluxing until essential oil is not increased to obtain fructus Citri Limoniae essential oil and fructus Citri Sarcodactylis essential oil;
(3) cutting rosewood and orange flower, respectively extracting by steam distillation, and heating and refluxing to obtain rosewood essential oil and orange flower essential oil.
In the embodiment, the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 10 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 35 parts of maltol, 135 parts of ethanol, 45 parts of isoamylol and 20 parts of geraniol;
the preparation method of the refreshing perfume comprises the following steps:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein at 300rpm, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
Examples of effects
The experimental method comprises the following steps: wistar rats 90, weighing 180 + -20 g, were randomly divided into 8 groups of 10 rats each, which were blank control group, model group, examples 1, 3, 5 groups, comparative examples 1-4 groups, the rats in the model group, examples 1, 3, 5 groups, comparative examples 1-4 groups were injected with diphenhydramine 0.2mg/kg subcutaneously, and after injection, the rats in the examples 1, 3, 5 groups, comparative examples 1-4 groups were coated with 0.1mg/kg of perfume prepared in the corresponding examples or comparative examples at their ears, and the timing was started, and the sleep time and duration of the rats were observed, and the results are shown in Table 1.
TABLE 1
Test group Sleep latency/min Sleep duration/min
Blank control group 37.12±13.56a 23.77±9.82e
Model set 11.67±5.98b 46.21±12.34f
Example 1 29.81±8.07c 25.65±9.67g
Example 3 27.62±6.25c 26.11±7.32g
Example 5 28.29±9.36c 25.98±4.98g
Comparative example 1 18.12±4.65d 36.46±10.23h
Comparative example 2 15.63±8.21d 39.12±6.41h
Comparative example 3 19.71±6.99d 31.54±8.63h
Comparative example 4 21.39±10.33d 33.75±12.64h
Remarking: the different letters in the same column have significant difference, and P is less than 0.05;
as can be seen from the table, compared with the blank control group, the sleep condition of the model group is obviously changed and has significant difference, which indicates that the low mental activity of the rat is caused after the diphenhydramine injection; compared with the model group, the example group significantly reduced the sleep time of rats, thus demonstrating that the perfume prepared by the invention has the effect of refreshing mind; meanwhile, the components of the perfume and the preparation method of the essential oil have great influence on the refreshing effect of the perfume.
The above detailed description is specific to one possible embodiment of the present invention, and the embodiment is not intended to limit the scope of the present invention, and all equivalent implementations or modifications without departing from the scope of the present invention should be included in the technical scope of the present invention.

Claims (4)

1. The refreshing perfume is characterized by comprising the following components in parts by weight: 5-15 parts of green lemon essential oil, 5-15 parts of bergamot essential oil, 1-15 parts of rosewood essential oil, 1-15 parts of neroli essential oil, 20-50 parts of maltol, 100 parts of ethanol, 160 parts of isoamylol and 10-30 parts of geraniol; the preparation method of the essential oil comprises the following steps:
(1) respectively cutting green lemon and bergamot into small pieces, squeezing, and filtering to obtain filtrate and residue;
(2) respectively placing the obtained residues in petroleum ether for reflux extraction, and mixing the residues with the filtrate after reduced pressure distillation to obtain a crude extract;
(3) respectively carrying out steam distillation extraction on the crude extracts, and heating and refluxing to obtain the green lemon essential oil and the bergamot essential oil;
(4) cutting rosewood and orange flower, respectively performing steam distillation extraction, heating and refluxing to obtain rosewood essential oil and orange flower essential oil;
in the step (1) of the preparation method of the essential oil, the squeezing is carried out at 20-40 ℃;
in the step (2) of the preparation method of the essential oil, the using amount of the petroleum ether is 3-5 times of the mass of the residue; the boiling range of the petroleum ether is 30-60 ℃.
2. The refreshing perfume according to claim 1, wherein the refreshing perfume comprises the following components in parts by weight: 5-10 parts of green lemon essential oil, 10-15 parts of bergamot essential oil, 4-10 parts of rosewood essential oil, 5-10 parts of orange flower essential oil, 30-40 parts of maltol, 140 parts of ethanol 120-doped materials, 40-50 parts of isoamylol and 15-20 parts of geraniol.
3. The refreshing perfume according to claim 1, wherein the refreshing perfume comprises the following components in parts by weight: 10 parts of green lemon essential oil, 10 parts of bergamot essential oil, 4 parts of rosewood essential oil, 10 parts of orange flower essential oil, 35 parts of maltol, 135 parts of ethanol, 45 parts of isoamylol and 20 parts of geraniol.
4. A process for the preparation of a refreshing perfume according to any of claims 1 to 3, comprising the steps of:
(1) mixing maltol and geraniol, dissolving in ethanol, dissolving rosewood essential oil and orange flower essential oil therein, and stirring to obtain ethanol solution;
(2) dissolving the green lemon essential oil and the bergamot essential oil in isoamyl alcohol, stirring to obtain an isoamyl alcohol solution, and mixing the ethanol solution and the isoamyl alcohol solution to obtain the refreshing perfume.
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CN112391233A (en) * 2020-11-10 2021-02-23 上海应用技术大学 Citron-lemon essence and preparation method thereof
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005187394A (en) * 2003-12-25 2005-07-14 Kanebo Ltd Composition containing essence of chinese crude medicine, and preparation containing the same
CN102232918A (en) * 2011-04-22 2011-11-09 珠海尚尔生物科技有限公司 Antibiotic perfume

Family Cites Families (5)

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Publication number Priority date Publication date Assignee Title
CN1075729A (en) * 1992-09-11 1993-09-01 李有刚 From orange peel, extract the method for natural yellow pigment, tangerine oil and pectin simultaneously
CN103361179A (en) * 2012-04-11 2013-10-23 孙莹 Extraction method of lemongrass essential oil
CN105878078A (en) * 2014-09-24 2016-08-24 王萍 Refreshing perfume formula
CN106691893A (en) * 2015-11-12 2017-05-24 浙江美之源化妆品有限公司 Plant perfume
CN109199948A (en) * 2017-07-06 2019-01-15 吴澄彬 A kind of calmness refreshing perfume

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005187394A (en) * 2003-12-25 2005-07-14 Kanebo Ltd Composition containing essence of chinese crude medicine, and preparation containing the same
CN102232918A (en) * 2011-04-22 2011-11-09 珠海尚尔生物科技有限公司 Antibiotic perfume

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