CN104928040A - Preparation method and application of eucalyptus oil - Google Patents
Preparation method and application of eucalyptus oil Download PDFInfo
- Publication number
- CN104928040A CN104928040A CN201510341382.9A CN201510341382A CN104928040A CN 104928040 A CN104928040 A CN 104928040A CN 201510341382 A CN201510341382 A CN 201510341382A CN 104928040 A CN104928040 A CN 104928040A
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- CN
- China
- Prior art keywords
- eucalyptus oil
- eucalyptus
- cigarette
- preparation
- entrainment agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000010642 eucalyptus oil Substances 0.000 title claims abstract description 38
- 229940044949 eucalyptus oil Drugs 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 238000000605 extraction Methods 0.000 claims abstract description 22
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 16
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 7
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 7
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract description 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 19
- 239000002994 raw material Substances 0.000 claims description 7
- 239000000796 flavoring agent Substances 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical group CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 235000012054 meals Nutrition 0.000 claims description 5
- 238000005057 refrigeration Methods 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 4
- 235000013355 food flavoring agent Nutrition 0.000 claims description 2
- 239000004744 fabric Substances 0.000 claims 2
- 230000000694 effects Effects 0.000 abstract description 7
- 244000166124 Eucalyptus globulus Species 0.000 abstract description 5
- 239000003205 fragrance Substances 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 230000007794 irritation Effects 0.000 abstract 1
- 239000000779 smoke Substances 0.000 abstract 1
- 230000000391 smoking effect Effects 0.000 abstract 1
- 238000000194 supercritical-fluid extraction Methods 0.000 abstract 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 239000000294 eucalyptus globulus labille leaf/twig oil Substances 0.000 description 3
- 206010022000 influenza Diseases 0.000 description 3
- 241000219926 Myrtaceae Species 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 230000000975 bioactive effect Effects 0.000 description 2
- 229960005233 cineole Drugs 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- 241001083082 Angophora Species 0.000 description 1
- 208000004429 Bacillary Dysentery Diseases 0.000 description 1
- 208000032841 Bulimia Diseases 0.000 description 1
- 206010006550 Bulimia nervosa Diseases 0.000 description 1
- 241000006100 Corymbia <angiosperm> Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 208000004232 Enteritis Diseases 0.000 description 1
- 206010017915 Gastroenteritis shigella Diseases 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 244000062730 Melissa officinalis Species 0.000 description 1
- 235000010654 Melissa officinalis Nutrition 0.000 description 1
- 208000018569 Respiratory Tract disease Diseases 0.000 description 1
- 208000005392 Spasm Diseases 0.000 description 1
- 230000000202 analgesic effect Effects 0.000 description 1
- 230000001355 anti-mycobacterial effect Effects 0.000 description 1
- 230000003260 anti-sepsis Effects 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 239000002781 deodorant agent Substances 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 230000000249 desinfective effect Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000077 insect repellent Substances 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 201000005113 shigellosis Diseases 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 201000008827 tuberculosis Diseases 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
Abstract
The invention provides a preparation method and application of eucalyptus oil. According to the method, eucalyptus leaves are subjected to carbon dioxide supercritical extraction so that the eucalyptus oil can be obtained, and the eucalyptus oil is added into a cigarette. The eucalyptus oil extraction method is simple in technology and easy and convenient to operate, solution mediums can be cyclically utilized, safety and environmental protection are achieved, extraction efficiency is high, production cost is low, the fragrance of the prepared eucalyptus oil is natural and rich, and the eucalyptus oil can well coordinate with tobacco scents. When the eucalyptus oil is added into the cigarette, the aroma amount of the cigarette can be increased, the smoking aroma quality can be improved, irritation is reduced, and the effect of softening smoke is achieved.
Description
Technical field
The present invention relates to a kind of preparation method and application of eucalyptus oil, is a kind of preparation method being used as the eucalyptus oil of essence spice for cigarette specifically.
Technical background
Eucalyptus is the general designation that the eucalyptus of Myrtaceae (Myrtaceae) belongs to (Eucalyptus), cup fruit tree belongs to (Angophora) and umbrella room eucalyptus genus (Corymbia) these three genus all categories plant, is the fast-growing deciduous species that tropical and subtropical region is important.
Eucalyptus oil is the volatile oil by the emiocytosis of leaf oil droplet, is one of important outlet spices of China.On international perfume oil market, eucalyptus oil occupies very important status, is at present in the world from all kinds of natural essential oils that leaf class is extracted, the one that quantity is maximum.Eucalyptus oil not only has the smell of fragrance, an or class bioactive ingredients, has the effect of antibacterial, anti-inflammatory, anticorrosion and desinsection mosquito repellent.Eucalyptus oil, due to its special aromatic odour and good sterilization, disinfecting power, is widely used in food, household chemicals and medical aspect.
Folium eucalypti is commonly used for herbal medicine among the people.If Eucalyptus Globulus oil is a kind of conventional medicine, there is anti-inflammatory analgesic action, can anti-mycobacterium tuberculosis.Eucalyptus Globulus oil can also be inhaled people's agent as gas and be used for the treatment of respiratory tract disease, influenza, alleviates headache gentle solution spasm.Eucalyptus Globulus oil also can be used as sanitas and sterilant, is usually used in rheocamphoradin, menthocamphorate, essential balm, bactericidal deodorant.
1,8-eucalyptol in eucalyptus oil can treat influenza, flu, bacillary dysentery, enteritis and various infection, can be used as anti-sepsis and the deodorizing component of cleaning agent for mouth cavity in stomatology.1,8-eucalyptol also has the function of depress appetite, by liquid medicine agent and the solid tablet of its preparation, to treatment bulimia with in order to fat-reducing, has good effect.
Because eucalyptus oil has good aromatic odour and bioactive functions thereof, so the eucalyptus oil potential middle paper novel fragrance that is a kind of tool.The announcement and the carbon dioxide upercritical fluid extraction method of eucalyptus oil and the application of eucalyptus oil in essence spice for cigarette field also do not appear in the newspapers.
Summary of the invention
The object of the invention is the blank according to prior art, a kind of cigarette eucalyptus oil and preparation method thereof is provided.Technical scheme of the present invention is by following realization:
(1) folium eucalypti of drying is pulverized, after crossing 80 ~ 160 eye mesh screens, get meal as in raw material powder loading extraction kettle for subsequent use;
(2) the entrainment agent dehydrated alcohol of raw material powder quality 10% ~ 40% is loaded in entrainment agent tank;
(3) start carbon dioxide refrigerating system, the recycle system, control extraction kettle pressure 20 ~ 40MPa, temperature 30 ~ 50 DEG C, separating still pressure 2 ~ 7MPa, temperature 15 ~ 50 DEG C;
(4) extraction time continues 2 ~ 5 hours, obtains eucalyptus oil.
Using eucalyptus oil as in the tobacco leaf that essence and flavoring agent adds, make cigarette finished product.
Eucalyptus oil extracting method of the present invention, technique is simple, easy and simple to handle, solvent reusable edible, safety and environmental protection, and extraction efficiency is high, and production cost is low, and the eucalyptus oil fragrance prepared is naturally abundant, has better Harmony with this perfume (or spice) of tobacco.Add in cigarette, cigarette flavor amount can be increased, improve aroma quality, reduce and stimulate, the effect of soft flue gas.
Embodiment
Embodiment 1:
The folium eucalypti of drying is pulverized, crosses 120 eye mesh screens, take a certain amount of folium eucalypti meal and pour charging basket into, then charging basket is loaded in extraction kettle, the dehydrated alcohol of account for raw materials quality 15% is loaded in entrainment agent tank as entrainment agent.Start carbon dioxide refrigeration, the recycle system, control extraction kettle pressure 25MPa, temperature 35 DEG C, separating still pressure 3MPa, temperature 18 DEG C.When the pressure and temperature set all reaches test requirements document, start entrainment agent pump, inject entrainment agent, and start timing, extraction time continues 2.5 hours.After extraction terminates, obtain eucalyptus oil from separating still drain hole, extracting yield is 5.6%.The eucalyptus oil of acquisition is added in cigarette, cigarette flavor amount can be increased, improve aroma quality, reduce and stimulate, the effect of soft flue gas.
Embodiment 2:
The folium eucalypti of drying is pulverized, crosses 160 eye mesh screens, take a certain amount of folium eucalypti meal and pour charging basket into, then charging basket is loaded in extraction kettle, the dehydrated alcohol of account for raw materials quality 20% is loaded in entrainment agent tank as entrainment agent.Start carbon dioxide refrigeration, the recycle system, control extraction kettle pressure 30MPa, temperature 40 DEG C, separating still pressure 4MPa, temperature 30 DEG C.When the pressure and temperature set all reaches test requirements document, start entrainment agent pump, inject entrainment agent, and start timing, extraction time continues 3 hours.After extraction terminates, obtain eucalyptus oil from a point separating still drain hole, yield is 5.55%.The eucalyptus oil of acquisition is added in cigarette, cigarette flavor amount can be increased, improve aroma quality, reduce and stimulate, the effect of soft flue gas.
Embodiment 3:
The folium eucalypti of drying is pulverized, crosses 80 eye mesh screens, take a certain amount of folium eucalypti meal and pour charging basket into, then charging basket is loaded in extraction kettle, the dehydrated alcohol of account for raw materials quality 30% is loaded in entrainment agent tank as entrainment agent.Start carbon dioxide refrigeration, the recycle system, control extraction kettle pressure 35MPa, temperature 45 C, separating still pressure 5MPa, temperature 35 DEG C.When the pressure and temperature set all reaches test requirements document, start entrainment agent pump, inject entrainment agent, and start timing, extraction time continues 4.5 hours.After extraction terminates, obtain eucalyptus oil from separating still drain hole, yield is 5.58%.The eucalyptus oil of acquisition is added in cigarette, cigarette flavor amount can be increased, improve aroma quality, reduce and stimulate, the effect of soft flue gas.
The above, be only the specific embodiment of the present invention, it should be pointed out that any those of ordinary skill in the art are in the technical scope disclosed by the present invention, the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.
Claims (5)
1. an eucalyptus oil preparation method, is characterized in that: comprise the following steps,
(1) folium eucalypti of drying is pulverized, after crossing screen cloth, get meal as in raw material powder loading extraction kettle for subsequent use;
(2) entrainment agent of raw material powder quality 10% ~ 40% is loaded in entrainment agent tank;
(3) start refrigeration system, the recycle system, control extraction kettle pressure 20 ~ 40MPa, temperature 30 ~ 50 DEG C, separating still pressure 2 ~ 7MPa, temperature 15 ~ 50 DEG C;
(4) extraction time continues 2 ~ 5 hours, obtains eucalyptus oil.
2. a kind of eucalyptus oil preparation method according to claim 1, is characterized in that: in described step (1), screen cloth is 80 ~ 160 eye mesh screens.
3. a kind of eucalyptus oil preparation method according to claim 1, is characterized in that: in described step (2), entrainment agent is dehydrated alcohol.
4. a kind of eucalyptus oil preparation method according to claim 1, is characterized in that: described step (3) refrigeration system is carbon dioxide refrigerating system.
5. an application for the eucalyptus oil made according to claim 1, is characterized in that: using eucalyptus oil as in the tobacco leaf that essence and flavoring agent adds, make cigarette finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510341382.9A CN104928040A (en) | 2015-06-18 | 2015-06-18 | Preparation method and application of eucalyptus oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510341382.9A CN104928040A (en) | 2015-06-18 | 2015-06-18 | Preparation method and application of eucalyptus oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104928040A true CN104928040A (en) | 2015-09-23 |
Family
ID=54115470
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510341382.9A Pending CN104928040A (en) | 2015-06-18 | 2015-06-18 | Preparation method and application of eucalyptus oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104928040A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111704960A (en) * | 2020-06-24 | 2020-09-25 | 江西思派思香料化工有限公司 | Extraction process of high-purity eucalyptus oil |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101731744A (en) * | 2008-11-10 | 2010-06-16 | 湖北中烟工业有限责任公司 | Mixed cigarette essence and preparation method thereof |
| CN102028306A (en) * | 2010-12-07 | 2011-04-27 | 张志军 | Throat nourishing health-care type electronic cigarette liquid |
-
2015
- 2015-06-18 CN CN201510341382.9A patent/CN104928040A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101731744A (en) * | 2008-11-10 | 2010-06-16 | 湖北中烟工业有限责任公司 | Mixed cigarette essence and preparation method thereof |
| CN102028306A (en) * | 2010-12-07 | 2011-04-27 | 张志军 | Throat nourishing health-care type electronic cigarette liquid |
Non-Patent Citations (6)
| Title |
|---|
| 吴青业 等: ""两种方法提取桉树叶挥发油成分的比较研究"", 《中药材》 * |
| 周燕园 等: ""细叶桉叶超临界CO2萃取挥发油的GC-MS分析"", 《中国药房》 * |
| 周莉君 等: ""响应面分析法优化超临界CO2萃取巨尾桉挥发油的工艺研究"", 《四川大学学报（自然科学版）》 * |
| 赵余庆: "《中药及天然产物提取制备关键技术》", 31 January 2012, 中国医药科技出版社 * |
| 陈丽君: ""采用GC-MS/O分析精油和烟草中致香物质"", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 * |
| 陈秋波 等: ""刚果12号桉叶片化感物质的初步分离分析"", 《热带作物学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111704960A (en) * | 2020-06-24 | 2020-09-25 | 江西思派思香料化工有限公司 | Extraction process of high-purity eucalyptus oil |
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|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150923 |
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| RJ01 | Rejection of invention patent application after publication |