CN111249181B - Long-acting slow-release perfume and preparation method thereof - Google Patents
Long-acting slow-release perfume and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the field of perfume preparation, and particularly relates to a long-acting slow-release perfume and a preparation method thereof. The perfume is prepared from bergamot essential oil, geranium essential oil, patchouli essential oil, linalool, amyl acetate, sodium alginate, citric acid, ethanol, glycerol and the like, the preparation method is simple and feasible, the cost is low, and the prepared perfume has good effects of refreshing and relieving pressure, and also has the effects of lasting fragrance and long-acting slow release.
Description
Technical Field
The invention belongs to the field of perfume preparation, and particularly relates to a long-acting slow-release perfume and a preparation method thereof.
Background
The perfume is a mixture of alcohol solution of essence and proper amount of perfume. Has aromatic and rich fragrance, is mainly sprayed on the parts such as lappets, handkerchiefs, hairlines and the like to emit pleasant fragrance, and is one of important cosmetics.
With the gradual improvement of living standard, people have higher and higher demands on living goods, and the perfume is changed from the previous rare article to the common article of the public. The perfume is a cosmetic made of perfume, alcohol and distilled water, and can give off strong, lasting and pleasant fragrance, and improve the aesthetic feeling and attraction of users. However, the perfume sold in the market has not very strong persistence, and the fragrance of the sprayed perfume gradually disappears in a short time.
Most of the existing perfume processes are composed of a balsam material and a solvent, the perfume has a strong taste at the beginning, but the fragrance gradually becomes lighter or even disappears along with the emission of the solvent, and the lasting fragrance of the existing perfume is between 2 and 3 hours. Prolonging the volatilization time of the perfume and keeping the fragrance to be released persistently are the hot spots of the current perfume process research and the demands of the consumers.
Chinese patent application CN 103405357 a discloses a process for preparing a long-acting slow-release perfume, which comprises jasmine essence, violet essence, citric acid, hydroxypropyl methylcellulose, ethanol, polyethylene glycol, tartaric acid, sodium chloride and other components, and has a good fragrance-retaining effect, but the variety of the components affects the original taste and efficacy of the perfume, and is not a good choice.
The Chinese patent application CN 106491398A discloses a slow-release long-acting perfume, which comprises rosemary, sweet osmanthus flower, Jinlu plum, gardenia, evening primrose, clove, roasted ginger, malic acid, nano platinum, slow-release solvent, antioxidant and other components, and has a certain slow-release effect, but the use of the nano platinum greatly increases the manufacturing cost of the perfume and is not beneficial to the use of common consumers.
In the prior art, the long-acting slow-release perfume which does not affect the taste and the efficacy of the perfume, has a good long-acting slow-release effect and reduces the production cost is difficult to find.
Particularly, the problem of fragrance retention of the refreshing and pressure-relieving perfume which is greatly demanded by the current consumers is not successfully solved.
Disclosure of Invention
In order to overcome the technical problems, the invention provides the long-acting slow-release perfume which has better refreshing and pressure relieving effects, and meanwhile, the perfume has lasting fragrance and is simple to prepare.
In order to achieve the above purpose, the technical scheme provided by the invention is as follows:
the long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
preferably, the long-acting slow-release perfume comprises the following components: bergamot essential oil, geranium essential oil, and patchouli essential oil;
preferably, the long-acting slow-release perfume further comprises the following auxiliary materials: linalool, amyl acetate, sodium alginate, citric acid, ethanol and glycerol;
preferably, the long-acting slow-release perfume comprises the following components in parts by weight: 0.1-3 parts of bergamot essential oil, 0.1-3 parts of geranium essential oil, 0.1-6 parts of patchouli essential oil, 1-10 parts of linalool, 10-25 parts of amyl acetate, 1-3 parts of sodium alginate, 1-10 parts of citric acid, 80-140 parts of ethanol and 10-30 parts of glycerol;
preferably, the long-acting slow-release perfume comprises the following components in parts by weight: 0.5-1 part of bergamot essential oil, 0.5-1 part of geranium essential oil, 0.5-2 parts of patchouli essential oil, 2-5 parts of linalool, 15-20 parts of amyl acetate, 1.5-2 parts of sodium alginate, 2-5 parts of citric acid, 120 parts of 100 parts of ethanol and 15-25 parts of glycerol;
preferably, the mass ratio of the bergamot essential oil to the geranium essential oil to the patchouli essential oil is 1:1: 1-2;
preferably, the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 15 parts of amyl acetate, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
preferably, the preparation method of the essential oil comprises the following steps:
(1) pulverizing fructus Citri Sarcodactylis and herba Agastaches respectively, adding ethanol and palmitic acid, extracting with supercritical carbon dioxide fluid, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil respectively;
(2) putting geranium into petroleum ether for reflux extraction, and obtaining a crude extract after reduced pressure distillation;
(3) and (3) carrying out steam distillation extraction on the crude extract, and adding reflux to obtain the geranium essential oil.
Preferably, in the step (1), the extraction temperature is 37-38 ℃, the extraction pressure is 8-10MPa, the flow rate is 8-12kg/h, and the extraction time is 1-2 h;
preferably, the ethanol and the palmitic acid are essential oil extraction promoters, and the addition amount of the ethanol is 10-30% of the mass of the bergamot or the pogostemon cablin respectively; the addition amount of the palmitic acid is 1-5% of the mass of the bergamot or the patchouli respectively;
preferably, in the step (2), the amount of the petroleum ether is 3-5 times of the mass of the geranium; the boiling range of the petroleum ether is 30-60 ℃;
preferably, in the step (3), the heating and refluxing are carried out until the essential oil is not increased any more;
the invention also aims to provide a preparation method of the long-acting slow-release perfume, which comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution, adding bergamot essential oil, patchouli essential oil and geranium essential oil, and stirring to obtain the long-acting slow-release perfume.
Preferably, in step (1) or (2), the stirring is carried out under the conditions of 300-500 rpm;
preferably, step (3) is carried out at 15-30 ℃;
preferably, in the step (3), the stirring is performed under the conditions of 100-200 rpm;
preferably, the step (3) further comprises performing ultrasound under the conditions of 80-100HZ, 200-500W.
Compared with the prior art, the invention has the technical advantages that:
(1) the essential oil of bergamot, patchouli and geranium is used together, so that the health care tea has good functions of refreshing and relieving pressure;
(2) the linalool and the amyl acetate used in the perfume have good synergistic effect, and can better promote the refreshing effect of the perfume and relieve the mood;
(3) according to the perfume, the volatilization of perfume essential oil can be effectively controlled by the sodium alginate, the citric acid, the ethanol and the glycerol, so that the perfume has a long-acting slow-release effect;
(4) in the invention, ethanol and palmitic acid are used as extraction promoters in the process of extracting the bergamot essential oil and the pogostemon cablin essential oil, so that the essential oil in the bergamot and the pogostemon cablin can be effectively extracted, the utilization rate of raw materials is effectively improved, and the production cost of the perfume is reduced.
Detailed Description
Example 1
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 15 parts of amyl acetate, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol and 2% palmitic acid, extracting with supercritical carbon dioxide fluid at 37 deg.C under 9MPa and flow rate of 10kg/h for 1.5h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 4 times of that of the geranium for reflux extraction, and obtaining a crude extract after reduced pressure distillation; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Example 2
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.1 part of bergamot essential oil, 0.1 part of geranium essential oil, 0.1 part of patchouli essential oil, 1 part of linalool, 10 parts of amyl acetate, 1 part of sodium alginate, 1 part of citric acid, 80 parts of ethanol and 10 parts of glycerol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 10% ethanol and 1% palmitic acid, extracting with supercritical carbon dioxide fluid at 37 deg.C under 8MPa and flow rate of 8kg/h for 1h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 3 times, performing reflux extraction, and performing reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 300rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 300rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 15 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 100rpm, and performing ultrasonic treatment at 80HZ and 200W to obtain the long-acting slow-release perfume.
Example 3
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 3 parts of bergamot essential oil, 3 parts of geranium essential oil, 6 parts of patchouli essential oil, 10 parts of linalool, 25 parts of amyl acetate, 3 parts of sodium alginate, 10 parts of citric acid, 140 parts of ethanol and 30 parts of glycerol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 30% ethanol and 5% palmitic acid, extracting with supercritical carbon dioxide fluid at 38 deg.C under 10MPa and flow rate of 12kg/h for 2 hr, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass 5 times of that of the geranium for reflux extraction, and obtaining a crude extract after reduced pressure distillation; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 500rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 500rpm to form an ethanol solution;
(3) mixing glycerol solution and ethanol solution at 30 deg.C, adding bergamot essential oil, herba Pogostemonis essential oil, and flos Pelargonii Hortori essential oil, stirring at 200rpm, and performing ultrasonic treatment at 100Hz and 500W to obtain the long-acting slow-release perfume.
Example 4
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.5 part of bergamot essential oil, 0.5 part of geranium essential oil, 0.5 part of patchouli essential oil, 2 parts of linalool, 15 parts of amyl acetate, 2 parts of sodium alginate, 5 parts of citric acid, 100 parts of ethanol and 15 parts of glycerol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol and 3% palmitic acid, extracting with supercritical carbon dioxide fluid at 38 deg.C under 10MPa and flow rate of 9kg/h for 1h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 3 times, performing reflux extraction, and performing reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing glycerol solution and ethanol solution at 20 deg.C, adding bergamot essential oil, herba Pogostemonis essential oil, and flos Pelargonii Hortori essential oil, stirring at 200rpm, and performing ultrasonic treatment at 100Hz and 500W to obtain the long-acting slow-release perfume.
Example 5
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 1 part of bergamot essential oil, 1 part of geranium essential oil, 2 parts of patchouli essential oil, 5 parts of linalool, 20 parts of amyl acetate, 1.5 parts of sodium alginate, 2 parts of citric acid, 120 parts of ethanol and 25 parts of glycerol;
the mass ratio of the bergamot essential oil to the geranium essential oil to the patchouli essential oil is 1:1: 1-2;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 15% ethanol and 1-5% palmitic acid, extracting with supercritical carbon dioxide fluid at 38 deg.C under 10MPa and flow rate of 12kg/h for 2 hr, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 3 times, performing reflux extraction, and performing reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 300rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 300rpm to form an ethanol solution;
mixing the glycerol solution and the ethanol solution at 15 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 100rpm, and performing ultrasonic treatment at 80HZ and 250W to obtain the long-acting slow-release perfume.
Comparative example 1
Compared with example 1, amyl acetate was not included.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
the essential oil was prepared as in example 1.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool and citric acid in ethanol, and stirring at 400rpm to form ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Comparative example 2
In comparison with example 1, linalool was not included.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 15 parts of amyl acetate, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
the preparation method of the essential oil is the same as that of the example 1;
the preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving amyl acetate and citric acid in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Comparative example 3
Compared with example 1, no palmitic acid was added during extraction of the essential oil.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the components of the long-acting slow-release perfume are the same as those in the embodiment 1;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol, extracting with supercritical carbon dioxide fluid at 37 deg.C under 9MPa and flow rate of 10kg/h for 1.5h, and separating to obtain essential oil of fructus Citri Sarcodactylis and herba Agastaches;
(2) - (3) same as in example 1.
The preparation method of the long-acting slow-release perfume is the same as that of the example 1.
Comparative example 4
The essential oil extraction process was different compared to example 1.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the components of the long-acting slow-release perfume are the same as those in the embodiment 1;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol and 2% palmitic acid, extracting with supercritical carbon dioxide fluid at 37 deg.C under 9MPa and flow rate of 10kg/h for 1.5h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 4 times, performing reflux extraction, and performing reduced pressure distillation to obtain geranium essential oil; the boiling range of the petroleum ether is 30-60 ℃;
the preparation method of the long-acting slow-release perfume is the same as that of the example 1.
Comparative example 5
Compared to example 1, no citric acid was included.
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 15 parts of amyl acetate, 1.5 parts of sodium alginate and 120 parts of ethanol;
the essential oil was prepared as in example 1.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool and amyl acetate in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Examples of effects
(I) testing the effect of the long-acting sustained release:
the absorbent tissue paper was soaked in the perfume of the groups of examples 1, 3, 5 and comparative examples 1 to 4 for 6 hours, and naturally dried in the shade in a closed space at a constant temperature of 30 ℃ to obtain a fragrant sheet. The obtained incense tablet is placed in a place with good indoor air fluidity, and tested by smelling at 15 days, 30 days, and 45 days for whether it has fragrance (+ +: normal fragrance; + light fragrance; -: no fragrance). The results are shown in the following table:
| test group | 15 days | 30 days | 45 days |
| Example 1 | ++ | + | + |
| Example 2 | ++ | + | + |
| Example 3 | ++ | + | + |
| Comparative example 1 | + | + | - |
| Comparative example 2 | ++ | - | - |
| Comparative example 3 | + | - | - |
| Comparative example 4 | + | - | - |
| Comparative example 5 | + | - |
Therefore, the perfume prepared by the invention has a long-acting slow-release effect.
(II) emotional response animal model test:
100 Wister rats with the weight of 180-. The behavior of the rats in the angry model group is divided into fighting times, threatening times, climbing times, winning interest times and failure times, three persons observe and record the video and then score, and the average value of the score is taken; the results are shown in Table 1.
TABLE 1 Total behavioral score in rats
| Test group | Total score of behavior |
| Control group | 75.36±8.32a |
| Example 1 | 43.21±5.89b |
| Example 3 | 45.23±7.44b |
| Example 5 | 43.87±10.21b |
| Comparative example 1 | 64.45±9.46c |
| Comparative example 2 | 68.23±13.62c |
| Comparative example 3 | 62.56±9.58c |
| Comparative example 4 | 52.32±6.45d |
| Comparative example 5 | 56.67±11.23d |
Remarking: the significant difference p < 0.05 is found between different letters in the same list.
Therefore, the perfume provided by the invention has a certain mood relieving effect, and the perfume composition and the extraction method of the essential oil have great influence on the perfume.
The above detailed description is specific to one possible embodiment of the present invention, and the embodiment is not intended to limit the scope of the present invention, and all equivalent implementations or modifications without departing from the scope of the present invention should be included in the technical scope of the present invention.
Claims (3)
1. The long-acting slow-release perfume is characterized by comprising the following components in parts by weight: 0.1-3 parts of bergamot essential oil, 0.1-3 parts of geranium essential oil, 0.1-6 parts of patchouli essential oil, 1-10 parts of linalool, 10-25 parts of amyl acetate, 1-3 parts of sodium alginate, 1-10 parts of citric acid, 80-140 parts of ethanol and 10-30 parts of glycerol;
the preparation method of the essential oil comprises the following steps:
(1) pulverizing fructus Citri Sarcodactylis and herba Agastaches respectively, adding ethanol and palmitic acid, extracting with supercritical carbon dioxide fluid, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil respectively;
(2) putting geranium into petroleum ether for reflux extraction, and obtaining a crude extract after reduced pressure distillation;
(3) distilling the crude extract with water vapor, and refluxing to obtain flos Pelargonii Hortori essential oil;
wherein in the step (1), the extraction temperature is 37-38 ℃, the extraction pressure is 8-10MPa, the flow rate is 8-12kg/h, and the extraction time is 1-2 h;
in the step (1), the ethanol and the palmitic acid are used as the essential oil extraction promoters, and the addition amount of the ethanol is 10-30% of the mass of the bergamot or the patchouli respectively; the addition amount of the palmitic acid is 1-5% of the mass of the bergamot or the patchouli respectively;
in the step (2), the using amount of the petroleum ether is 3-5 times of the mass of the geranium; the boiling range of the petroleum ether is 30-60 ℃.
2. The long-acting slow-release perfume as claimed in claim 1, wherein the mass ratio of the bergamot essential oil to the geranium essential oil to the patchouli essential oil is 1:1: 1-2.
3. A process for the preparation of a long-acting slow-release perfume according to any of claims 1-2 comprising the steps of:
(1) dissolving sodium alginate in glycerol, and stirring to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution, adding bergamot essential oil, patchouli essential oil and geranium essential oil, and stirring to obtain the long-acting slow-release perfume.
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| CN101385475A (en) * | 2007-12-27 | 2009-03-18 | 广东省中药研究所 | Slow-release natural insecticide |
| CN103040649A (en) * | 2012-12-20 | 2013-04-17 | 浦江欧妮雅化妆品有限公司 | Patchouli perfume |
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| CN103040649A (en) * | 2012-12-20 | 2013-04-17 | 浦江欧妮雅化妆品有限公司 | Patchouli perfume |
| CN105106068A (en) * | 2015-09-11 | 2015-12-02 | 金玛瑙香水（明光）有限公司 | Nerve soothing perfume |
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