CN110251425B - Natural essential oil fragrance perfume and preparation method thereof - Google Patents
Natural essential oil fragrance perfume and preparation method thereof Download PDFInfo
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- CN110251425B CN110251425B CN201910532334.6A CN201910532334A CN110251425B CN 110251425 B CN110251425 B CN 110251425B CN 201910532334 A CN201910532334 A CN 201910532334A CN 110251425 B CN110251425 B CN 110251425B
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/35—Ketones, e.g. benzophenone
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
- A61K8/492—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid having condensed rings, e.g. indol
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
Abstract
The invention relates to a natural essential oil fragrance perfume and a preparation method thereof, wherein the natural essential oil fragrance perfume is prepared by adopting more than sixty raw materials such as salicylic acid-2-ethylhexyl ester, galbanum ester, ambrox and the like in proper weight proportion. The finally prepared natural essential oil fragrance perfume realizes the perfect fusion of the fragrance of natural essential oil and synthetic perfume, has clearer fragrance layering sense, softer fragrance, more harmonious fragrance and more lasting fragrance compared with the existing perfume, and the natural essential oil fragrance perfume has the advantages that the front pitch is the mixed fruit fragrance of citrus and lemon, the middle pitch is the delicate fragrance of lily of the valley and jasmine, and the tail pitch is the mixed sweet soil fragrance of natural ambergris and amber.
Description
Technical Field
The invention belongs to the technical field of essences and spices, and particularly relates to natural essential oil fragrance perfume and a preparation method thereof.
Background
The perfume, as the important cosmetics that women increasingly advocate to use in the modern life, not only can mark the personality, increase confidence and personal glamour, promote the life taste, also convey politeness and connotation, become an important social etiquette of modern society, in addition, the perfume can also play the effect such as relaxing nerve, adjusting mood, pacifying peace of mind.
Patent application No. 201510291567.3 discloses a lily essence for daily use and a preparation method thereof, wherein the raw material components of the lily essence for daily use comprise cis-6-nonenol: 0.05 to 0.15 percent; clamping a dragon: 0.05 to 0.15 percent; ethyl vanillin: 0.1 to 0.3 percent; cyanine aldehyde: 0.1 to 0.3 percent; cyclic galbanum ester: 0.2 to 0.4 percent; and (3) pyrinol ester: 0.2-0.4%, etc. According to the scheme, a large amount of synthetic spices are adopted for proportioning, so that the lily essence with good floral aroma, strong natural aroma and lasting base aroma is obtained. However, due to the natural difference in the flavor and texture between synthetic flavors and natural flavors, the natural flavor obtained by the preparation thereof is still to be improved, and is still deficient in the sense of flavor hierarchy, flavor softness and flavor harmony.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides the natural essential oil fragrance perfume which has stronger natural feeling, clearer fragrance layering feeling, softer fragrance, more harmonious fragrance and more lasting fragrance, and the preparation method thereof.
The technical scheme of the invention is as follows:
the natural essential oil fragrance perfume comprises the following raw material components:
5.68-8.52 parts by weight of 2-ethylhexyl salicylate, 1.2-1.8 parts by weight of galbanum ester, 1.6-2.4 parts by weight of ambrofuran, 2.4-3.6 parts by weight of BHT, 25.68-38.52 parts by weight of ethoxymethoxy cycloundecane, 0.176-0.264 part by weight of borneol, 0.608-0.912 part by weight of Borelabane aldehyde, 0.192-0.288 part by weight of decanal, 0.48-0.72 part by weight of undecanal, 3.2-4.8 parts by weight of Carlon, 0.56-0.84 part by weight of citral, 0.096-0.144 part by weight of citronellyl formate, 1.328-1.992 parts by weight of coumarin, 2.72-4.08 parts by weight of conyzaldehyde, 150.4-225.6 parts by weight of methyl dihydroketonate, 49.6-74.4 parts by weight of dihydromyrcenol, 32-48 parts by weight of dipropylene glycol, 6-48 parts by weight of linalool, 6.32.32 parts by weight of linalool, 26.32 parts by weight of ethyl linalyl acetate, 36 11.448 parts by weight of jasmonate, 3.32 parts by weight of jasmonate, 0.8 parts by weight of bornyl acetate, 28-42 parts of cyclopentadecanolide, 0.544-0.816 part of galaxolide, 0.048-0.072 part of geranyl formate, 0.208-0.312 part of geraniol, 0.8-1.2 parts of geranyl acetate, 3.024-4.536 parts of guaiacyl acetate, 62.88-94.32 parts of cyclopentadecanolide, 0.096-0.144 part of methylhexylagalaldehyde, 7.44-11.16 parts of helional, 0.04-0.06 part of indole, 70.4-105.6 parts of ambroxone, 0.424-0.636 part of isoeugenol, 3.12-4.68 parts of karanal, 0.488-0.732 part of patchouli, 9.76-14.64 parts of linalool, 21.2-31.8 parts of linalyl acetate, 0.252-0.252 part of L-4.68 parts of geranial, 0.252-36 parts of menthone, 3.36-36 parts of geranyl ketone, 3-36 parts of tangeretinone, 3.36-3632 parts of menthone, 3-4.192 parts of tangeretinene, 3 parts of linalool, 73.6 to 110.4 parts of musk T, 0.288 to 0.432 part of neryl acetate, 0.16 to 0.24 part of octanal diethyl acetal, 0.056 to 0.084 part of octyl acetate, 0.064 to 0.096 part of phenethyl alcohol, 2.24 to 3.36 parts of storax acetate, 2.16 to 3.24 parts of Temuchun, 18.48 to 27.72 parts of triethyl citrate, 0.8 to 1.2 parts of synthetic oak moss, 1.48 to 2.22 parts of o-tert-butylcyclohexyl acetate, 0.4 to 0.6 part of ambergris acetal, 0.384 to 0.576 part of methyl damascone, 3.92 to 5.88 parts of ethyl ionone, 0.352 to 0.528 part of ethyl citronellol and 165.536 to 248.304 parts of compound natural essential oil;
the compound natural essential oil is a mixture consisting of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, olive oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of (40-60), (0.8-1.2), (1.6-2.4), (84-126), (0.736-1.104), (1.6-2.4), (16-24) and (4.8-7.2).
Preferably, the natural essential oil fragrance perfume comprises the following raw material components: 6.39-7.81 parts by weight of 2-ethylhexyl salicylate, 1.35-1.65 parts by weight of galbanum ester, 1.8-2.2 parts by weight of ambrofuran, 2.7-3.3 parts by weight of BHT, 28.89-35.31 parts by weight of ethoxymethoxy cycloundecane, 0.198-0.242 parts by weight of borneol, 0.684-0.836 parts by weight of Borela aldehyde, 0.216-0.264 parts by weight of decanal, 0.54-0.66 parts by weight of undecanal, 3.6-4.4 parts by weight of Carlon, 0.63-0.77 parts by weight of citral, 0.108-0.132 parts by weight of citronellyl formate, 1.494-1.826 parts by weight of coumarin, 3.06-3.74 parts by weight of Lageraldehyde, 169.2-206.8 parts by weight of methyl dihydroketonate, 55.8-68.2 parts by weight of dihydromyrcenol, 36-44 parts by weight of dipropylene glycol, 36.24-19.24 parts by weight of linalyl acetate, 36 10.494 parts by weight of ethyl linalyl acetate, 36 10.494 parts by weight of jasmonate, 31.5 to 38.5 weight portions of cyclopentadecanolide, 0.612 to 0.748 weight portion of galaxolide, 0.054 to 0.066 weight portion of geranyl formate, 0.234 to 0.286 weight portion of geraniol, 0.9 to 1.1 weight portion of geranyl acetate, 3.402 to 4.158 weight portions of guaiacyl acetate, 70.74 to 86.46 weight portions of cyclopentadecanolide, 0.108 to 0.132 weight portion of methylhexylagalaldehyde, 8.37 to 10.23 weight portions of helional, 0.045 to 0.055 weight portion of indole, 79.2 to 96.8 weight portions of ambroxone, 0.477 to 0.583 weight portion of isoeugenol, 3.51 to 4.29 weight portions of karanal, 0.671 to 0.671 weight portion of linalool, 10.98 to 13.42 weight portions of linalool, 23.85 to 29.85 weight portions of linalyl acetate, 0.231 to 4.18 weight portions of geranial, 0.549 to 36 weight portions of menthenone, 0.189 to 36 weight portions of menthone, 0.549 to 36 weight portions of menthone, 3 weight portions of menthone, 82.8-101.2 parts of musk T, 0.324-0.396 part of neryl acetate, 0.18-0.22 part of octanal diethyl acetal, 0.063-0.077 part of octyl acetate, 0.072-0.088 part of phenethyl alcohol, 2.52-3.08 parts of storax acetate, 2.43-2.97 parts of Temuchun, 20.79-25.41 parts of triethyl citrate, 0.9-1.1 part of synthetic oak moss, 1.665-2.035 parts of o-tert-butylcyclohexyl acetate, 0.45-0.55 part of ambrox acetal, 0.432-0.528 part of methyl damascenone, 4.41-5.39 parts of ethyl ionone, 0.396-0.484 part of ethyl citronellol and 186.228-227.612 parts of compound natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, olive oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of (45-55): (0.9-1.1): 1.8-2.2): 94.5-115.5): 0.828-1.012): 1.8-2.2): 18-22): 5.4-6.6.
Preferably, the natural essential oil fragrance perfume comprises the following raw material components: 7.1 parts by weight of 2-ethylhexyl salicylate, 1.5 parts by weight of galbanum ester, 2 parts by weight of ambrofuran, 3 parts by weight of BHT, 32.1 parts by weight of ethoxymethoxycycloundecane, 0.22 parts by weight of borneol, 0.76 parts by weight of boehalol, 0.24 parts by weight of decanal, 0.6 parts by weight of undecanal, 4 parts by weight of caron, 0.7 parts by weight of citral, 0.12 parts by weight of citronellyl formate, 1.66 parts by weight of coumarin, 3.4 parts by weight of cyclamen aldehyde, 188 parts by weight of methyl dihydrojasmonate, 62 parts by weight of dihydromyrcenol, 40 parts by weight of dipropylene glycol, 22 parts by weight of ethyl linalool, 9.54 parts by weight of ethyl linalyl acetate, 35 parts by weight of cyclopentadecanolide, 0.68 parts by weight of galaxolide, 0.06 parts by weight of geranyl formate, 0.26 parts by weight of geraniol, 1 part by weight of geranyl acetate, 3.78 parts by weight of guaiacyl acetate, 6.78 parts by weight of pentadecanoic lactone, 12.12 parts by weight of methyl cinnamaldehyde, 9.3 parts of helional, 0.05 part of indole, 88 parts of ambergris ketone, 0.53 part of isoeugenol, 3.9 parts of caraway aldehyde, 0.61 part of patchouli, 12.2 parts of linalool, 26.5 parts of linalyl acetate, 0.2 part of L-menthone, 0.21 part of tangerine aldehyde, 17.88 parts of grapefruit methane, 5.24 parts of musk ketene, 92 parts of musk T, 0.36 part of neryl acetate, 0.2 part of octanal diethyl acetal, 0.07 part of octyl acetate, 0.08 part of phenethyl alcohol, 2.8 parts of styryl acetate, 2.7 parts of terpineol, 23.1 parts of triethyl citrate, 1 part of synthetic oak moss, 1.85 parts of o-tert-butylcyclohexyl acetate, 0.5 part of ambroxol, 0.48 part of alpha-damascone, 4.9 parts of ethyl ionone, 0.44 part of ethyl citronellol and 206.92 parts of composite natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 50:1:2:105:0.92:2:20:20: 6.
Preferably, the cedar wood oil, the clove leaf oil and the elemi oil are respectively prepared by the following methods:
(1) removing impurities from the raw materials, drying at low temperature, and crushing to obtain raw material powder;
(2) and adding an extraction solvent into the raw material powder, soaking, performing subcritical fluid countercurrent extraction, and removing the extraction solvent by reduced pressure evaporation after the subcritical fluid countercurrent extraction is completed to obtain the powder.
Preferably, in the step (1), the low-temperature drying is performed for 4 to 8 hours under the conditions that the vacuum degree is 0.1 to 0.2MPa and the temperature is 25 to 30 ℃.
Preferably, in step (1), the pulverization is carried out to a particle size of less than 40 mesh.
Preferably, in the step (2), the extraction solvent is any one of propane and butane; the weight ratio of the raw material powder to the extraction solvent is 1:2-1: 3; the soaking time is 2-6h, the extraction temperature for performing subcritical fluid countercurrent extraction is 35-45 ℃, the extraction pressure is 0.1-0.4 MPa, the extraction time is 50-70min, and the extraction is performed for 3-4 times; the pressure for the reduced pressure evaporation is-0.4 to-0.25 MPa, and the temperature for the reduced pressure evaporation is 45-50 ℃.
A method for preparing the natural essential oil fragrance perfume comprises the following specific steps:
respectively weighing the raw material components, stirring to uniformly mix, aging, and filtering to obtain the natural essential oil fragrance perfume.
Preferably, the stirring speed is 40-100r/min, and the stirring time is 10-30 min.
Preferably, the aging temperature is 15-25 ℃, the aging time is 3-5 months, and the filtering temperature is below 10 ℃.
The invention has the beneficial effects that:
the natural essential oil fragrance perfume is prepared by adopting more than sixty raw materials such as salicylic acid-2-ethylhexyl ester, galbanum ester, ambergris furan and the like and carrying out proper weight proportion, the perfect fusion of the fragrance of natural essential oil and synthetic perfume is realized, compared with the existing perfume, the fragrance natural feeling is stronger, the layering sense is clearer, the fragrance is softer, the fragrance is more harmonious, and the fragrance is more lasting.
Detailed Description
The present invention is further illustrated by the following specific examples.
In the following examples, 1 part by weight represents 1 g.
Example 1
The embodiment provides a natural essential oil fragrance perfume, which comprises the following raw material components:
5.68 parts by weight of 2-ethylhexyl salicylate, 1.2 parts by weight of galbanum ester, 1.6 parts by weight of ambrofuran, 2.4 parts by weight of BHT, 25.68 parts by weight of ethoxymethoxycycloundecane, 0.176 part by weight of borneol, 0.608 part by weight of Boraginal, 0.192 part by weight of decanal, 0.48 part by weight of undecanal, 3.2 parts by weight of Carlon, 0.56 part by weight of citral, 0.096 part by weight of citronellyl formate, 1.328 parts by weight of coumarin, 2.72 parts by weight of Lagota aldehyde, 150.4 parts by weight of methyl dihydrojasmonate, 49.6 parts by weight of dihydromyrcenol, 32 parts by weight of dipropylene glycol, 17.6 parts by weight of ethyl linalool, 7.632 parts by weight of ethyl linalyl acetate, 28 parts by weight of cyclopentadecanolide, 0.544 parts by weight of geranyl formate, 0.048 parts by weight of geranyl formate, 0.208 parts by weight of geranyl acetate, 3588 parts by weight of guaiacyl acetate, 0.096 parts by weight of cyclohexyl cinnamaldehyde, 0.096 parts by weight of cinnamic aldehyde, 0.8 parts by weight of geranyl formate, 0.8 parts of geranyl acetate, 7.44 parts of helional, 0.04 part of indole, 70.4 parts of ambergris ketone, 0.424 part of isoeugenol, 3.12 parts of caraway aldehyde, 0.488 part of green flower fen, 9.76 parts of linalool, 21.2 parts of linalyl acetate, 0.16 part of L-menthone, 0.168 part of tangerine aldehyde, 14.304 parts of grapefruit methane, 4.192 parts of musk ketene, 73.6 parts of musk T, 0.288 part of neryl acetate, 0.16 part of octanal diethyl acetal, 0.056 part of octyl acetate, 0.064 part of phenethyl alcohol, 2.24 parts of styryl acetate, 2.16 parts of terpineol, 18.48 parts of triethyl citrate, 0.8 part of synthetic oak moss, 1.48 parts of o-tert-butyl cyclohexyl acetate, 0.4 part of ambroxol, 0.384 part of alpha-damascone, 3.92 parts of beta-ionone, 0.352 part of beta-citronellol and 165.536 parts of composite natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 40:0.8:1.6:84:0.736:1.6:16:16: 4.8;
the cedar oil, clove leaf oil and elemi oil are respectively prepared by the following method:
(1) removing impurities from the raw materials, drying at 30 deg.C and vacuum degree of 0.1MPa for 4 hr, and pulverizing to obtain 60 mesh raw material powder;
(2) adding 2 times of propane by mass into the raw material powder, soaking for 2h, performing subcritical fluid countercurrent extraction at 35 ℃, under 0.4MPa for 50min, extracting for 3 times, and evaporating under reduced pressure at-0.4 MPa and 45 ℃ to remove extracted propane to obtain cedar oil, clove leaf oil or elemi oil.
Further, a method for preparing the natural essential oil fragrance perfume is provided, which comprises the following steps:
respectively weighing the raw material components, stirring for 30min at 40r/min to uniformly mix, then aging for 5 months at 15 ℃, and filtering at 5 ℃ to obtain the natural essential oil fragrance perfume.
Example 2
The embodiment provides a natural essential oil fragrance perfume, which comprises the following raw material components:
8.52 parts by weight of 2-ethylhexyl salicylate, 1.8 parts by weight of galbanum ester, 2.4 parts by weight of ambrofuran, 3.6 parts by weight of BHT, 38.52 parts by weight of ethoxymethoxycycloundecane, 0.264 parts by weight of borneol, 0.912 parts by weight of Boraginal, 0.288 parts by weight of decanal, 0.72 parts by weight of undecanal, 4.8 parts by weight of Carlon, 0.84 parts by weight of citral, 0.144 parts by weight of citronellyl formate, 1.992 parts by weight of coumarin, 4.08 parts by weight of Lagill aldehyde, 225.6 parts by weight of methyl dihydrojasmonate, 74.4 parts by weight of dihydromyrcenol, 48 parts by weight of dipropylene glycol, 26.4 parts by weight of ethyl linalool, 11.448 parts by weight of ethyl linalyl acetate, 42 parts by weight of cyclopentadecanolide, 0.816 parts by weight of muskines, 0.072 formate, 0.312 parts by weight of geraniol, 1.2 parts by weight of geranyl acetate, 4.32 parts by weight of guaiacyl acetate, 0.144 parts by weight of deca-cyclohexyl carbamate, 144 parts by weight of cinnamic aldehyde, 11.16 parts of helional, 0.06 part of indole, 105.6 parts of ambergris ketone, 0.636 part of isoeugenol, 4.68 parts of caraway aldehyde, 0.732 part of patchouli, 14.64 parts of linalool, 31.8 parts of linalyl acetate, 0.24 part of L-menthone, 0.252 part of tangerine aldehyde, 21.456 parts of grapefruit methane, 6.288 parts of musk ketene, 110.4 parts of musk T, 0.432 part of neryl acetate, 0.24 part by weight of octanal diacetal, 0.084 part by weight of octyl acetate, 0.096 part by weight of phenethyl alcohol, 3.36 parts by weight of styryl acetate, 3.24 parts by weight of Temukurol, 27.72 parts by weight of triethyl citrate, 1.2 parts by weight of synthetic oak moss, 2.22 parts by weight of o-tert-butylcyclohexyl acetate, 0.6 part by weight of ambroxol acetal, 0.576 part by weight of alpha-damascone, 5.88 parts by weight of beta-ionone, 0.528 part by weight of beta-citronellol and 248.304 parts by weight of composite natural essential oil;
the compound natural essential oil is a mixture consisting of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 60:1.2:2.4:126:1.104:2.4:24:24: 7.2;
the cedar oil, clove leaf oil and elemi oil are respectively prepared by the following method:
(1) removing impurities from the raw materials, drying at 25 deg.C and vacuum degree of 0.2MPa for 8 hr, and pulverizing to obtain 60 mesh raw material powder;
(2) adding 3 times of propane by mass into the raw material powder, soaking for 6h, performing subcritical fluid countercurrent extraction for 4 times at the extraction temperature of 45 ℃, the extraction pressure of 0.1MPa and the extraction time of 70min, and removing the extracted propane by reduced pressure evaporation at 50 ℃ under the pressure of-0.25 MPa to obtain the cedar oil, clove leaf oil or elemi oil.
Further, a method for preparing the natural essential oil fragrance perfume is provided, which comprises the following steps:
respectively weighing the raw material components, stirring for 10min at 100r/min to uniformly mix, then aging for 3 months at 25 ℃, and filtering at 5 ℃ to obtain the natural essential oil fragrance perfume.
Example 3
The embodiment provides a natural essential oil fragrance perfume, which comprises the following raw material components:
6.39 parts by weight of 2-ethylhexyl salicylate, 1.35 parts by weight of galbanum ester, 1.8 parts by weight of ambrofuran, 2.7 parts by weight of BHT, 28.89 parts by weight of ethoxymethoxycycloundecane, 0.198 parts by weight of borneol, 0.684 parts by weight of Boraginal, 0.216 parts by weight of decanal, 0.54 parts by weight of undecanal, 3.6 parts by weight of Carlon, 0.63 parts by weight of citral, 0.108 parts by weight of citronellyl formate, 1.494 parts by weight of coumarin, 3.06 parts by weight of Lagota aldehyde, 169.2 parts by weight of methyl dihydrojasmonate, 55.8 parts by weight of dihydromyrcenol, 36 parts by weight of dipropylene glycol, 19.8 parts by weight of ethyl linalool, 8.586 parts by weight of ethyl linalyl acetate, 31.5 parts by weight of cyclopentadecanolide, 0.612 parts by weight of Cola muskines, 0.054 parts by weight of geranyl formate, 0.234 parts by weight of geraniol, 0.9 parts by weight of geranyl acetate, 108.74 parts by weight of guaiacyl acetate, 52.52 parts by weight of cyclohexyl cinnamaldehyde, 0.52 parts by weight of cinnamyl acetate, 0.52 parts by weight of cinnamyl acetate, 0.7 parts of cinnamyl acetate, 0.8 parts by weight of cinnamyl acetate, 0.8 parts by weight of cinnamyl acetate, 0.8 parts of cinnamyl acetate and 3 parts by weight of cinnamyl acetate, 8.37 parts of helional, 0.045 part of indole, 79.2 parts of ambergris ketone, 0.477 part of isoeugenol, 3.51 parts of caraway aldehyde, 0.549 parts of patchouli, 10.98 parts of linalool, 23.85 parts of linalyl acetate, 0.18 part of L-menthone, 0.189 parts of tangerine aldehyde, 16.092 parts of grapefruit methane, 4.716 parts of musk ketene, 82.8 parts of musk T, 0.324 parts of neryl acetate, 0.18 part of octanal diethyl acetal, 0.063 part of octyl acetate, 0.072 part of phenethyl alcohol, 2.52 parts of styryl acetate, 2.43 parts of terpineol, 20.79 parts of triethyl citrate, 0.9 part of synthetic oak moss, 1.665 parts of o-tert-butyl cyclohexyl acetate, 0.45 part of ambroxol acetal, 0.432 part of alpha-damascone, 4.41 parts of beta-ionone, 0.396 part of beta-citronellol and 186.228 parts of composite natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 45:0.9:1.8:94.5:0.828:1.8:18:18: 5.4;
the cedar oil, clove leaf oil and elemi oil are respectively prepared by the following method:
(1) removing impurities from the raw materials, drying at 30 deg.C and vacuum degree of 0.15MPa for 6 hr, and pulverizing to obtain 80 mesh raw material powder;
(2) adding 2.6 times of propane into the raw material powder, soaking for 3.5h, performing subcritical fluid countercurrent extraction at 40 deg.C under 0.3MPa for 60min for 3 times, and evaporating under-0.3 MPa and 50 deg.C under reduced pressure to remove propane to obtain cedar oil, clove leaf oil or elemi oil.
Further, a method for preparing the natural essential oil fragrance perfume is provided, which comprises the following steps:
respectively weighing the raw material components, stirring for 20min at the speed of 60r/min to uniformly mix, then aging for 4 months at the temperature of 20 ℃, and filtering at the temperature of 5 ℃ to obtain the natural essential oil fragrance perfume.
Example 4
The embodiment provides a natural essential oil fragrance perfume, which comprises the following raw material components:
7.81 parts by weight of 2-ethylhexyl salicylate, 1.65 parts by weight of galbanum ester, 2.2 parts by weight of ambrofuran, 3.3 parts by weight of BHT, 35.31 parts by weight of ethoxymethoxycycloundecane, 0.242 parts by weight of borneol, 0.836 parts by weight of Boraginal, 0.264 parts by weight of decanal, 0.66 parts by weight of undecanal, 4.4 parts by weight of Carlon, 0.77 parts by weight of citral, 0.132 parts by weight of citronellyl formate, 1.826 parts by weight of coumarin, 3.74 parts by weight of Lagota aldehyde, 206.8 parts by weight of methyl dihydrojasmonate, 68.2 parts by weight of dihydromyrcenol, 44 parts by weight of dipropylene glycol, 24.2 parts by weight of ethyl linalool, 10.494 parts by weight of ethyl linalyl acetate, 38.5 parts by weight of cyclopentadecanolide, 0.748 parts by weight of Columbo de, 0.066 parts by weight of geraniol, 0.286 parts by weight of geraniol, 1.1.1 part by weight of geranyl acetate, 86.46.158 parts by weight of guaiacyl acetate, 35.158 parts by weight of cyclohexyl cinnamaldehyde, 132 parts by weight of cinnamyl acetate, 0.158 parts of cinnamyl acetate, 10.23 parts of helional, 0.055 part of indole, 96.8 parts of ambergris ketone, 0.583 parts of isoeugenol, 4.29 parts of caraway aldehyde, 0.671 part of patchouli, 13.42 parts of linalool, 29.15 parts of linalyl acetate, 0.22 part of L-menthone, 0.231 part of tangerine aldehyde, 19.668 parts of grapefruit methane, 5.764 parts of musk ketene, 101.2 parts of musk T, 0.396 part of neryl acetate, 0.22 part of octanal diethyl acetal, 0.077 part of octyl acetate, 0.088 part of phenethyl alcohol, 3.08 parts of styryl acetate, 2.97 parts of Temuchu, 25.41 parts of triethyl citrate, 1.1 parts of synthetic oak moss, 2.035 parts of o-tert-butylcyclohexyl acetate, 0.55 part of ambroxol, 0.528 part of alpha damascone, 5.39 parts of beta ionone, 0.484 parts of beta citronellol and 227.612 parts of composite natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 55:1.1:2.2:115.5:1.012:2.2:22:22: 6.6;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 45:0.9:1.8:94.5:0.828:1.8:18:18: 5.4;
the cedar oil, clove leaf oil and elemi oil are respectively prepared by the following method:
(1) removing impurities from the raw materials, drying at 30 deg.C and vacuum degree of 0.2MPa for 5 hr, and pulverizing to obtain 80 mesh raw material powder;
(2) adding 3 times of propane by mass into the raw material powder, soaking for 5h, performing subcritical fluid countercurrent extraction at 42 ℃ under 0.2MPa for 60min, performing the extraction for 3 times, and evaporating under reduced pressure at-0.3 MPa and 45 ℃ to remove the extracted propane to obtain the cedar oil, clove leaf oil or elemi oil.
Further, a method for preparing the natural essential oil fragrance perfume is provided, which comprises the following steps:
respectively weighing the raw material components, stirring at 50r/min for 25min to mix uniformly, then aging at 20 ℃ for 4 months, and filtering at 5 ℃ to obtain the natural essential oil fragrance perfume.
Example 5
The embodiment provides a natural essential oil fragrance perfume, which comprises the following raw material components:
7.1 parts by weight of 2-ethylhexyl salicylate, 1.5 parts by weight of galbanum ester, 2 parts by weight of ambrofuran, 3 parts by weight of BHT, 32.1 parts by weight of ethoxymethoxycycloundecane, 0.22 parts by weight of borneol, 0.76 parts by weight of boehalol, 0.24 parts by weight of decanal, 0.6 parts by weight of undecanal, 4 parts by weight of caron, 0.7 parts by weight of citral, 0.12 parts by weight of citronellyl formate, 1.66 parts by weight of coumarin, 3.4 parts by weight of cyclamen aldehyde, 188 parts by weight of methyl dihydrojasmonate, 62 parts by weight of dihydromyrcenol, 40 parts by weight of dipropylene glycol, 22 parts by weight of ethyl linalool, 9.54 parts by weight of ethyl linalyl acetate, 35 parts by weight of cyclopentadecanolide, 0.68 parts by weight of galaxolide, 0.06 parts by weight of geranyl formate, 0.26 parts by weight of geraniol, 1 part by weight of geranyl acetate, 3.78 parts by weight of guaiacyl acetate, 6.78 parts by weight of pentadecanoic lactone, 12.12 parts by weight of methyl cinnamaldehyde, 9.3 parts of helional, 0.05 part of indole, 88 parts of ambergris ketone, 0.53 part of isoeugenol, 3.9 parts of caraway aldehyde, 0.61 part of patchouli, 12.2 parts of linalool, 26.5 parts of linalyl acetate, 0.2 part of L-menthone, 0.21 part of tangerine aldehyde, 17.88 parts of grapefruit methane, 5.24 parts of musk ketene, 92 parts of musk T, 0.36 part of neryl acetate, 0.2 part of octanal diethyl acetal, 0.07 part of octyl acetate, 0.08 part of phenethyl alcohol, 2.8 parts of styryl acetate, 2.7 parts of terpineol, 23.1 parts of triethyl citrate, 1 part of synthetic oak moss, 1.85 parts of o-tert-butylcyclohexyl acetate, 0.5 part of ambroxol, 0.48 part of alpha-damascone, 4.9 parts of ethyl ionone, 0.44 part of ethyl citronellol and 206.92 parts of composite natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 50:1:2:105:0.92:2:20:20: 6;
the cedar oil, clove leaf oil and elemi oil are respectively prepared by the following method:
(1) removing impurities from the raw materials, drying at 25 deg.C and vacuum degree of 0.2MPa for 7 hr, and pulverizing to obtain 60 mesh raw material powder;
(2) adding 3 times of propane by mass into the raw material powder, soaking for 3h, performing subcritical fluid countercurrent extraction at 38 ℃, under 0.2MPa for 50min, extracting for 3 times, and evaporating under reduced pressure at-0.3 MPa and 50 ℃ to remove extracted propane to obtain cedar oil, clove leaf oil or elemi oil.
Further, a method for preparing the natural essential oil fragrance perfume is provided, which comprises the following steps:
respectively weighing the raw material components, stirring for 20min at 40r/min to uniformly mix, then aging for 4 months at 20 ℃, and filtering at 5 ℃ to obtain the natural essential oil fragrance perfume.
Examples of the experiments
1. Test sample
Sample 1: example 1 the sample prepared
Sample 2: example 2 sample prepared
Sample 3: example 3 sample prepared
Sample 4: example 4 sample prepared
Sample 5: example 5 preparation of the resulting sample
Sample 6: the sample obtained was prepared as in example one of patent application No. 201510291567.3
2. Test method
100 μ l of each of the above test samples was placed on a glass slide, the glass slide was placed on a 32 ℃ hot plate to simulate skin temperature, 20 persons, half of men and women, who had an evaluation experience of fragrance were selected, and the evaluation and scoring were performed for 30min, 2h, 4h, 8h, and 10h, respectively, to test the gradation of fragrance (full score of 25), the harmony of fragrance (full score of 25), and the change of fragrance intensity with time (full score of 50), and the test was repeated 5 times for each sample, and the average value was taken as the final test result.
3. The test results are shown in Table 1
TABLE 1 results of scoring by sample evaluation
The result shows that compared with the sample 6, the samples 1-5 have clearer aroma layering, more coordinated overall aroma and more lasting aroma, and the natural essential oil aroma perfume disclosed by the invention has the advantages that through reasonable compatibility, all components play a synergistic effect, so that the overall aroma quality of the perfume is improved, and the user experience is higher.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention, and all the changes or substitutions should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (10)
1. The natural essential oil fragrance perfume is characterized by comprising the following raw material components:
5.68-8.52 parts by weight of 2-ethylhexyl salicylate, 1.2-1.8 parts by weight of galbanum ester, 1.6-2.4 parts by weight of ambrofuran, 2.4-3.6 parts by weight of BHT, 25.68-38.52 parts by weight of ethoxymethoxy cycloundecane, 0.176-0.264 part by weight of borneol, 0.608-0.912 part by weight of Borelabane aldehyde, 0.192-0.288 part by weight of decanal, 0.48-0.72 part by weight of undecanal, 3.2-4.8 parts by weight of Carlon, 0.56-0.84 part by weight of citral, 0.096-0.144 part by weight of citronellyl formate, 1.328-1.992 parts by weight of coumarin, 2.72-4.08 parts by weight of conyzaldehyde, 150.4-225.6 parts by weight of methyl dihydroketonate, 49.6-74.4 parts by weight of dihydromyrcenol, 32-48 parts by weight of dipropylene glycol, 6-48 parts by weight of linalool, 6.32.32 parts by weight of linalool, 26.32 parts by weight of ethyl linalyl acetate, 36 11.448 parts by weight of jasmonate, 3.32 parts by weight of jasmonate, 0.8 parts by weight of bornyl acetate, 28-42 parts of cyclopentadecanolide, 0.544-0.816 part of galaxolide, 0.048-0.072 part of geranyl formate, 0.208-0.312 part of geraniol, 0.8-1.2 parts of geranyl acetate, 3.024-4.536 parts of guaiacyl acetate, 62.88-94.32 parts of cyclopentadecanolide, 0.096-0.144 part of methylhexylagalaldehyde, 7.44-11.16 parts of helional, 0.04-0.06 part of indole, 70.4-105.6 parts of ambroxone, 0.424-0.636 part of isoeugenol, 3.12-4.68 parts of karanal, 0.488-0.732 part of patchouli, 9.76-14.64 parts of linalool, 21.2-31.8 parts of linalyl acetate, 0.252-0.252 part of L-4.68 parts of geranial, 0.252-36 parts of menthone, 3.36-36 parts of geranyl ketone, 3-36 parts of tangeretinone, 3.36-3632 parts of menthone, 3-4.192 parts of tangeretinene, 3 parts of linalool, 73.6 to 110.4 parts of musk T, 0.288 to 0.432 part of neryl acetate, 0.16 to 0.24 part of octanal diethyl acetal, 0.056 to 0.084 part of octyl acetate, 0.064 to 0.096 part of phenethyl alcohol, 2.24 to 3.36 parts of storax acetate, 2.16 to 3.24 parts of Temuchun, 18.48 to 27.72 parts of triethyl citrate, 0.8 to 1.2 parts of synthetic oak moss, 1.48 to 2.22 parts of o-tert-butylcyclohexyl acetate, 0.4 to 0.6 part of ambergris acetal, 0.384 to 0.576 part of methyl damascone, 3.92 to 5.88 parts of ethyl ionone, 0.352 to 0.528 part of ethyl citronellol and 165.536 to 248.304 parts of compound natural essential oil;
the compound natural essential oil is a mixture consisting of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, olive oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of (40-60), (0.8-1.2), (1.6-2.4), (84-126), (0.736-1.104), (1.6-2.4), (16-24) and (4.8-7.2).
2. The natural essential oil fragrance perfume of claim 1, wherein the raw material components comprise: 6.39-7.81 parts by weight of 2-ethylhexyl salicylate, 1.35-1.65 parts by weight of galbanum ester, 1.8-2.2 parts by weight of ambrofuran, 2.7-3.3 parts by weight of BHT, 28.89-35.31 parts by weight of ethoxymethoxy cycloundecane, 0.198-0.242 parts by weight of borneol, 0.684-0.836 parts by weight of Borela aldehyde, 0.216-0.264 parts by weight of decanal, 0.54-0.66 parts by weight of undecanal, 3.6-4.4 parts by weight of Carlon, 0.63-0.77 parts by weight of citral, 0.108-0.132 parts by weight of citronellyl formate, 1.494-1.826 parts by weight of coumarin, 3.06-3.74 parts by weight of Lageraldehyde, 169.2-206.8 parts by weight of methyl dihydroketonate, 55.8-68.2 parts by weight of dihydromyrcenol, 36-44 parts by weight of dipropylene glycol, 36.24-19.24 parts by weight of linalyl acetate, 36 10.494 parts by weight of ethyl linalyl acetate, 36 10.494 parts by weight of jasmonate, 31.5 to 38.5 weight portions of cyclopentadecanolide, 0.612 to 0.748 weight portion of galaxolide, 0.054 to 0.066 weight portion of geranyl formate, 0.234 to 0.286 weight portion of geraniol, 0.9 to 1.1 weight portion of geranyl acetate, 3.402 to 4.158 weight portions of guaiacyl acetate, 70.74 to 86.46 weight portions of cyclopentadecanolide, 0.108 to 0.132 weight portion of methylhexylagalaldehyde, 8.37 to 10.23 weight portions of helional, 0.045 to 0.055 weight portion of indole, 79.2 to 96.8 weight portions of ambroxone, 0.477 to 0.583 weight portion of isoeugenol, 3.51 to 4.29 weight portions of karanal, 0.671 to 0.671 weight portion of linalool, 10.98 to 13.42 weight portions of linalool, 23.85 to 29.85 weight portions of linalyl acetate, 0.231 to 4.18 weight portions of geranial, 0.549 to 36 weight portions of menthenone, 0.189 to 36 weight portions of menthone, 0.549 to 36 weight portions of menthone, 3 weight portions of menthone, 82.8-101.2 parts of musk T, 0.324-0.396 part of neryl acetate, 0.18-0.22 part of octanal diethyl acetal, 0.063-0.077 part of octyl acetate, 0.072-0.088 part of phenethyl alcohol, 2.52-3.08 parts of storax acetate, 2.43-2.97 parts of Temuchun, 20.79-25.41 parts of triethyl citrate, 0.9-1.1 part of synthetic oak moss, 1.665-2.035 parts of o-tert-butylcyclohexyl acetate, 0.45-0.55 part of ambrox acetal, 0.432-0.528 part of methyl damascenone, 4.41-5.39 parts of ethyl ionone, 0.396-0.484 part of ethyl citronellol and 186.228-227.612 parts of compound natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, olive oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of (45-55): (0.9-1.1): 1.8-2.2): 94.5-115.5): 0.828-1.012): 1.8-2.2): 18-22): 5.4-6.6.
3. The natural essential oil fragrance perfume of claim 1, wherein the raw material components comprise: 7.1 parts by weight of 2-ethylhexyl salicylate, 1.5 parts by weight of galbanum ester, 2 parts by weight of ambrofuran, 3 parts by weight of BHT, 32.1 parts by weight of ethoxymethoxycycloundecane, 0.22 parts by weight of borneol, 0.76 parts by weight of boehalol, 0.24 parts by weight of decanal, 0.6 parts by weight of undecanal, 4 parts by weight of caron, 0.7 parts by weight of citral, 0.12 parts by weight of citronellyl formate, 1.66 parts by weight of coumarin, 3.4 parts by weight of cyclamen aldehyde, 188 parts by weight of methyl dihydrojasmonate, 62 parts by weight of dihydromyrcenol, 40 parts by weight of dipropylene glycol, 22 parts by weight of ethyl linalool, 9.54 parts by weight of ethyl linalyl acetate, 35 parts by weight of cyclopentadecanolide, 0.68 parts by weight of galaxolide, 0.06 parts by weight of geranyl formate, 0.26 parts by weight of geraniol, 1 part by weight of geranyl acetate, 3.78 parts by weight of guaiacyl acetate, 6.78 parts by weight of pentadecanoic lactone, 12.12 parts by weight of methyl cinnamaldehyde, 9.3 parts of helional, 0.05 part of indole, 88 parts of ambergris ketone, 0.53 part of isoeugenol, 3.9 parts of caraway aldehyde, 0.61 part of patchouli, 12.2 parts of linalool, 26.5 parts of linalyl acetate, 0.2 part of L-menthone, 0.21 part of tangerine aldehyde, 17.88 parts of grapefruit methane, 5.24 parts of musk ketene, 92 parts of musk T, 0.36 part of neryl acetate, 0.2 part of octanal diethyl acetal, 0.07 part of octyl acetate, 0.08 part of phenethyl alcohol, 2.8 parts of styryl acetate, 2.7 parts of terpineol, 23.1 parts of triethyl citrate, 1 part of synthetic oak moss, 1.85 parts of o-tert-butylcyclohexyl acetate, 0.5 part of ambroxol, 0.48 part of alpha-damascone, 4.9 parts of ethyl ionone, 0.44 part of ethyl citronellol and 206.92 parts of composite natural essential oil;
the compound natural essential oil is a mixture of cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange oil, patchouli oil and vetiver oil according to the weight ratio of 50:1:2:105:0.92:2:20:20: 6.
4. The natural essential oil fragrance perfume of claim 1, wherein the cedar wood oil, clove leaf oil and elemi oil are prepared by the following method respectively:
(1) removing impurities from the raw materials, drying at low temperature, and crushing to obtain raw material powder;
(2) and adding an extraction solvent into the raw material powder, soaking, performing subcritical fluid countercurrent extraction, and removing the extraction solvent by reduced pressure evaporation after the subcritical fluid countercurrent extraction is completed to obtain the powder.
5. The natural essential oil fragrance perfume of claim 4, wherein in the step (1), the low-temperature drying is performed for 4 to 8 hours under the conditions of a vacuum degree of 0.1 to 0.2MPa and a temperature of 25 to 30 ℃.
6. The natural essential oil fragrance perfume of claim 4, wherein in step (1), the pulverization is to a particle size of less than 40 mesh.
7. The natural essential oil fragrance perfume of claim 4, wherein in the step (2), the extraction solvent is any one of propane and butane; the weight ratio of the raw material powder to the extraction solvent is 1:2-1: 3; the soaking time is 2-6h, the extraction temperature for performing subcritical fluid countercurrent extraction is 35-45 ℃, the extraction pressure is 0.1-0.4 MPa, the extraction time is 50-70min, and the extraction is performed for 3-4 times; the pressure for the reduced pressure evaporation is-0.4 to-0.25 MPa, and the temperature for the reduced pressure evaporation is 45 to 50 ℃.
8. A process for the preparation of a natural essential oil fragrance perfume according to any one of claims 1 to 7, comprising the specific steps of:
respectively weighing the raw material components, stirring to uniformly mix, aging, and filtering to obtain the natural essential oil fragrance perfume.
9. The method according to claim 8, wherein the stirring speed is 40-100r/min and the stirring time is 10-30 min.
10. The method according to claim 8, wherein the aging temperature is 15-25 ℃, the aging time is 3-5 months, and the filtration temperature is 10 ℃ or less.
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