CN102703215B - Perfume essence and preparation method thereof - Google Patents
Perfume essence and preparation method thereof Download PDFInfo
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- CN102703215B CN102703215B CN201210167645.5A CN201210167645A CN102703215B CN 102703215 B CN102703215 B CN 102703215B CN 201210167645 A CN201210167645 A CN 201210167645A CN 102703215 B CN102703215 B CN 102703215B
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Abstract
The invention discloses a perfume essence and a preparation method thereof and relates to essence. The preparation method comprises the following steps of: sequentially adding methyl dihydrojasmonate, linalool, ebanol, cis-4-(1-methyl ethyl)-cyclohexyl methanol, cyclopentadecanolide, lyral, helional, methyl cedryl ketone, ambrotone, musk ketene, iso-mythyl ionone, ambergris ether, 3-campholeny-2-butanol and okoumal into an agitator kettle; then sequentially adding watermelon ketone, coumarin, ethyl vanillin and synthetic oakmoss into the agitator kettle; and after a solid is dissolved, sequentially adding xintiandi incense, linalool oxide, patchouli oil, bergamot oil and lavender oil into the agitator kettle; and filtering the mixture subjected to purification to obtain the perfume essence.
Description
Technical field
The present invention relates to a kind of essence, especially relate to a kind of perfume fragrance and preparation method thereof.
Background technology
In today that synthetic Chemical Engineering Technology makes rapid progress, the development of synthetic perfume is advanced by leaps and bounds especially, and a lot of new spices provide alternative material for we create the fragrance that nature can't occur.
Chinese patent CN102234577A discloses a kind of compound method of violet perfume hay-scented essence, and it is comprised of different violet phenol, an unusually sweet smell pasture and water phenol, violet absolute, Heliotropium arborescens absolute oil, violet ester, Heliotropium arborescens ester, Tuberose alcohol, isolan flower ester, mango absolute oil, Leaf and twig of Common Jasminorange absolute oil, watermelon ester, Fructus Fici absolute oil, safflower ester, Japanese Honeysuckle ester, chrysanthemum alcohol, Motherwort Herb ester, Rhizoma Alpiniae Officinarum alcohol; Its fragrance is responded as echo to sound, the moment volatilization of each level fragrance, namely open and see that perfume (or spice), fragrance are plentiful, fragrance is attacked people, lasting stability, have again simultaneously the intelligence development of allaying excitement, regulate nerve, clearing away the heart fire and tranquillizing, the effect that produces refreshing effect to the mind, the dense fragrance that gives out can make us again stopping forgetting to return.
Chinese patent CN101864343A discloses a kind of compound method of lily and albizia essence, and it is aromatic by different lily phenol, different silk tree phenol, lily absolute oil, silk tree absolute oil, lily perfume base, silk tree perfume base, lily aldehyde, silk tree aldehyde, root tuber of aromatic turmeric, rhodinol, Rose absolute oil, tea rose absolute oil, silk tree caul-fat, fragrant flower Chinese scholar tree absolute oil, windproof ester, glossy ganoderma ester, Root of Heterophylly Faalsestarwort ester, Radix Glycyrrhizae ester, Unibract Fritillary Bulb alcohol gram form.In proportion front 8 kinds of materials are put into stirrer and stir 40min; then add 11 kinds of spices; add while stirring; requirement keeps adding another kind of spices more than stirrer running 2min after adding a kind of spices again; until all 11 flavor spices are added rear shutdown 20min; starting the stirrer running after standing 20min stirs again; until after the whole dissolvings of all solids; stirring 60min; put into the solid transformation cylinder after pouring out still aging from the softening stirrer of mechanical liquid, take out filtration, clarification, can after 3 days.
Summary of the invention
The object of the present invention is to provide harmonious tempting perfume fragrance of a kind of fragrance and preparation method thereof.
Described perfume fragrance raw material by mass percentage is composed as follows:
Ageratum oil (Patchouli oil) 4% ~ 5%, Oils, bergamot peel (Bergamot oil) 5% ~ 7%; Oleum lavandula angustifolia (Lavender oil) 2% ~ 4%; Methyl dihydrojasmonate (Hedione) 7% ~ 8%; Phantol (Linalool) 5% ~ 7%; Ebony alcohol (Ebanol) 3% ~ 5%; Convallarol in May (Mayol) 3% ~ 4%; Linalool oxide (linalool oxide) 0.4% ~ 0.6%; Cyclopentadecylene lactone (Habanolide) 2% ~ 4%; LYRAL (Lyral) 1% ~ 3%; Helional (Helional) 3% ~ 6%; Vertofix coeur (Vertofix Coeur) 3% ~ 5%; Watermelon ketone (Oceanone) 0.5% ~ 1%; Ambrotone (Iso E Super) 8% ~ 12%; Moschus ketenes (Muscenone) 0.6% ~ 1%; Isoraldeine (Isoraldeine) 5% ~ 7%; Tonka bean camphor (Coumarin) 1% ~ 2%, vanirone (Ethyl vanillin) 0.1% ~ 0.3%, imperial saliva ether (Ambrox DL) 1% ~ 2%, 3-borneol alkenyl-2-butanols (Sandalore) 1% ~ 2%; Ancient alkane difficult to understand (Okumal) 0.1% ~ 0.3%; Synthetic oak moss (Evernil) 1.5% ~ 2.5%; New world perfume base 25% ~ 31%.
Described methyl dihydrojasmonate (Hedione) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 24851-98-7; Described ebony alcohol (Ebanol) can be available from the commodity of Switzerland Qi Huadun company, CAS numbering: 67801-20-1; Described convallarol in May (Mayol) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 13828-37-0; Described Kazakhstan bar lactone (Habanolide) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 34902-57-3; Described LYRAL (Lyral) can be available from the commodity of U.S. international fragrance company, CAS numbering: 51414-04-4; 51414-25-6; Described helional (Helional) can be available from the commodity of U.S. international fragrance company, CAS numbering: 1205-17-0; Described vertofix coeur (Vertofix Coeur) can be available from the commodity of U.S. international fragrance company, CAS numbering: 32388-55-9; Described watermelon ketone (Oceanone) can be available from the commodity of U.S. Europe Lao Fulin company, CAS numbering: 28940-11-6; Described ambrotone (Iso E Super) can be available from the commodity of U.S. international fragrance company, CAS numbering: 54464-57-2; Described Moschus ketenes (Muscenone) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 82356-51-2; Described isoraldeine (Isoraldeine) can be available from the commodity of Switzerland Qi Huadun company, CAS numbering: 1335-46-2,127-42-4,127-43-5,127-51-5,7779-30-8; Described imperial saliva ether (Ambrox DL) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 0003738-00-9; Described 3-borneol alkenyl-2-butanols (Sandalore) can be available from the commodity of Switzerland Qi Huadun company, CAS numbering: 65113-99-7; The ancient alkane of described Austria (Okumal) can be available from the commodity of Switzerland Qi Huadun company, CAS numbering: 131812-67-4,131812-51-6,131812-52-7; Described synthetic oak moss (Evernil) can be available from the commodity of French Roure company, CAS numbering: 4707-47-5.
Described new world perfume base is prepared by following methods:
with following raw material: second position firpene (β-Pinene), rose oxide (Rose oxide), imperial court's ketone (Dynascone 10), leaf-alcohol (Cis-3-Hexenol), cover special green (Montaverdi), ligustral (Triplal), evertal (Cyclovertal), all roads ketone (Veloutone), fourth position damascone (δ-Damascone), oxa-sulfo-pentamethylene (Oxane), first position Terpineol 350 (α-Terpineol), geraniol (Citronellol), vernol (Nerol), Geraniol (Geraniol), voitol (maltol), pepper ether (Rhubofix), methyl dihydrojasmonate (Hedione), triethyl citrate (TEC), synthetic oak moss (Evernil), to Butylated Hydroxytoluene (BHT), oranger terpene (Orange oil Terpnene) and dipropylene glycol (DPG) ratio mixing in order add agitator kettle successively, filter after purifying, namely get the new world perfume base.
Described new world perfume base consisting of by mass percentage: (β-Pinene) 14% ~ 16% for second position firpene; Rose oxide 0.1% ~ 0.2%; Imperial court's ketone (Dynascone 10) 0.4% ~ 0.6%; Leaf-alcohol (Cis-3-Hexenol) 0.01% ~ 0.05%; Cover special green (Montaverdi) 0.01% ~ 0.05%; Ligustral (Triplal) 1% ~ 1.5%; Evertal (Cyclovertal) 0.01% ~ 0.05%; All roads ketone (Veloutone) 1% ~ 2%; (δ-Damascone) 0.02% ~ 0.05% for fourth position damascone; Oxa-sulfo-pentamethylene (Oxane) 0.4% ~ 0.6%; First position Terpineol 350 0.03% ~ 0.05%; Geraniol 3% ~ 4%; Vernol 0.01% ~ 0.05%; Geraniol 0.01% ~ 0.05%; Voitol 0.2% ~ 0.4%; Pepper ether (Rhubofix) 1% ~ 2%; Methyl dihydrojasmonate (Hedione) 12% ~ 13%; Triethyl citrate 13% ~ 15%; Synthetic oak moss (Evernil) 0.04% ~ 0.06%; To Butylated Hydroxytoluene (also claiming antioxidant BHT .) 0.5% ~ 1%; Oranger terpene (Orange oil Terpnene) 6% ~ 10%; Dipropylene glycol (DPG) 40% ~ 45%.
Described imperial court ketone (Dynascone 10) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 56973-85-4; Described illiteracy special green (Montaverdi) can be available from the commodity of U.S. state international fragrance company, CAS numbering: 188570-78-7; Described ligustral (Triplal) can be available from the commodity of U.S. state international fragrance company, CAS numbering: 68039-49-6,7939-60-2,68737-61-1; Described evertal (Cyclovertal) can be available from the commodity of U.S. state international fragrance company, CAS numbering: 27939-60-2; Described all roads ketone (Veloutone) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 0065443-14-3; Described fourth position damascone (δ-Damascone) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 0057378-68-4; Described oxa-sulfo-pentamethylene (Oxane) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 0059323-76-1; Described pepper ether (Rhubofix) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 0041816-03-9; Described methyl dihydrojasmonate (Hedione) can be available from the commodity of Switzerland Firmenich ﹠ Cie, CAS numbering: 24851-98-7; Described synthetic oak moss (Evernil) can be available from the commodity of French Roure company, CAS numbering: 4707-47-5).
The preparation method of described perfume fragrance is as follows:
With methyl dihydrojasmonate, phantol, ebony alcohol, May convallarol, cyclopentadecylene lactone, LYRAL, helional, vertofix coeur, ambrotone, Moschus ketenes, isoraldeine, imperial saliva ether, 3-borneol alkenyl-2-butanols, ancient alkane difficult to understand add successively agitator kettle, turn on agitator; Again watermelon ketone, tonka bean camphor, vanirone and synthetic oak moss are added agitator kettle successively, after dissolution of solid, new world perfume base, linalool oxide, ageratum oil, Oils, bergamot peel and Oleum lavandula angustifolia are added agitator kettle successively, filter after purifying, namely get perfume fragrance.The time of described purifying can be 24h, and the filter screen of described filtration can be more than 120 orders.
The prepared related perfume material of perfume fragrance product can be daily according to the world spices institute (being called for short RIFM), international daily spices and essence association (being called for short IFRA), U.S. essential oil association (being called for short EOA), Council of Europe's (being called for short CEorCOE) is thought: it is generally acknowledged safety (being called for short GRAS).
Embodiment
Embodiment 1
With natural or natural equivalent spices: ageratum oil (Patchouli oil) 4% ~ 4.5%, Oils, bergamot peel (Bergamot oil) 5% ~ 7%; Oleum lavandula angustifolia (Lavender oil) 5% ~ 7%; Methyl dihydrojasmonate (Hedione Switzerland Firmenich ﹠ Cie trade name, CAS numbering: 24851-98-7) 7% ~ 8%; Phantol (Linalool) 5% ~ 7%; Linalool oxide (linalool oxide) 0.4% ~ 0.6%; Tonka bean camphor (Coumarin) 1% ~ 2%, imperial saliva ether (Ambrox DL Switzerland Firmenich ﹠ Cie trade name, CAS numbering: 0003738-00-9) 1% ~ 2%; Solvent: dipropylene glycol 65% ~ 75%.
Embodiment 2
For the perfume fragrance that makes preparation reaches fragrant with oranges and tangerines, the fragrance of a flower, santal, the ocean novel aroma mixes the sense of modernness that has that gives out, and can utilize complete synthesis spices, and the partial solvent dipropylene glycol has been replaced to following spices:
Ebony alcohol (Ebanol Switzerland Qi Huadun company trade name, CAS numbering: 67801-20-1) 3% ~ 5%; May convallarol (Mayol Switzerland Firmenich ﹠ Cie trade name, CAS numbering: 13828-37-0) 3% ~ 4%; Cyclopentadecylene lactone (Habanolide Switzerland Firmenich ﹠ Cie trade name, CAS numbering: 34902-57-3) 2% ~ 4%; LYRAL (Lyral U.S. international fragrance company trade name, CAS numbering: 51414-04-4; 51414-25-6) 1% ~ 3%; Helional (Helional U.S. international fragrance company trade name, CAS numbering: 1205-17-0) 3% ~ 6%; Vertofix coeur (Vertofix Coeur U.S. international fragrance company trade name, CAS numbering: 32388-55-9) 3% ~ 5%; Watermelon ketone (Oceanone U.S. Europe Lao Fulin company trade name, CAS numbering: 28940-11-6) 0.5% ~ 1%; Ambrotone (Iso E Super U.S. international fragrance company trade name, CAS numbering: 54464-57-2) 8% ~ 12%; Moschus ketenes (Muscenone Switzerland Firmenich ﹠ Cie trade name, CAS numbering: 82356-51-2) 0.6% ~ 1%; Isoraldeine (trade name of Isoraldeine Switzerland Qi Huadun company, CAS numbering: 1335-46-2,127-42-4,127-43-5,127-51-5,7779-30-8) 5% ~ 7%; Vanirone (Ethyl vanillin) 0.1% ~ 0.3%, 3-borneol alkenyl-2-butanols (Sandalore Switzerland Qi Huadun company trade name, CAS numbering: 65113-99-7) 1% ~ 2%; Ancient alkane difficult to understand (Okumal Switzerland Qi Huadun company trade name, CAS numbering: 131812-67-4,131812-51-6,131812-52-7) 0.1% ~ 0.3%; Synthetic oak moss (Evernil France Roure company trade name, CAS numbering: 4707-47-5) 1.5% ~ 2.5%; Solvent: dipropylene glycol 25% ~ 30%.
Embodiment 3
Similar to Example 2, its difference is the dipropylene glycol in embodiment 2 is replaced to the new world perfume base, and consumption is 25%～31%., wherein make this formula that the crucial touch effect be arranged adding of watermelon ketone.Whole formula fragrance has embodied bustling city modern sense and natural style perfect adaptation.
Prepared product after testing, each analysis project is with to detect index as follows:
Main application: configuration perfume.
Fragrance: Ribes nigrum L., oranges and tangerines, clear (green grass or young crops) perfume (or spice), the fragrance of a flower, the wingceltis Moschus, the ocean is fragrant.
Color and luster: yellow to golden transparent liquid.
Relative density/d
4 25: 0.9670 ± 0.010.
Refractive power/n
D 20: 1.4800 ± 0.010.
Heavy metal content/(in Pb) :≤10mg/kg.
Arsenic content/(in As) :≤5mg/kg.
Quality guaranteed period: shady and cool, dry, ventilate and preserved 1 year under the condition of Kaifeng.
Above said content is the basic explanation under conceiving for the present invention only, and according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Claims (4)
1. perfume fragrance is characterized in that raw material by mass percentage is composed as follows:
Ageratum oil 4%～5%, Oils, bergamot peel 5%～7%; Oleum lavandula angustifolia 2%～4%; Methyl dihydrojasmonate 7%～8%; Phantol 5%～7%; Ebony alcohol 3%～5%; May, convallarol 3%～4%; Linalool oxide 0.4%～0.6%; Cyclopentadecylene lactone 2%～4%; LYRAL 1%～3%; Helional 3%～6%; Vertofix coeur 3%～5%; Watermelon ketone 0.5%～1%; Ambrotone 8%～12%; Moschus ketenes 0.6%～1%; Isoraldeine 5%～7%; Coumarin 1 %～2%, vanirone 0.1%～0.3%, imperial saliva ether 1%～2%, 3-borneol alkenyl-2-butanols 1%～2%; Ancient alkane 0.1%～0.3% difficult to understand; Synthetic oak moss 1.5%～2.5%; New world perfume base 25%～31%;
Described new world perfume base is to add successively in order agitator kettle to mix by mass percentage following raw material, filters gained after purifying: second position firpene 14%～16%; Rose oxide 0.1%～0.2%; Imperial court's ketone 0.4%～0.6%; Leaf-alcohol 0.01%～0.05%; Cover special green 0.01%～0.05%; Ligustral 1%～1.5%; Evertal 0.01%～0.05%; All roads ketone 1%～2%; Fourth position damascone 0.02%～0.05%; Oxa-sulfo-pentamethylene 0.4%～0.6%; First position Terpineol 350 0.03%～0.05%; Geraniol 3%～4%; Vernol 0.01%～0.05%; Geraniol 0.01%～0.05%; Voitol 0.2%～0.4%; Pepper ether 1%～2%; Methyl dihydrojasmonate 12%～13%; Triethyl citrate 13%～15%; Synthetic oak moss 0.04%～0.06%; To Butylated Hydroxytoluene 0.5%～1%; Oranger terpene 6%～10%; Dipropylene glycol 40%～45%.
2. the preparation method of a kind of perfume fragrance as claimed in claim 1 is characterized in that its concrete steps are as follows:
With methyl dihydrojasmonate, phantol, ebony alcohol, May convallarol, cyclopentadecylene lactone, LYRAL, helional, vertofix coeur, ambrotone, Moschus ketenes, isoraldeine, imperial saliva ether, 3-borneol alkenyl-2-butanols, ancient alkane difficult to understand add successively agitator kettle, turn on agitator; Again watermelon ketone, tonka bean camphor, vanirone and synthetic oak moss are added agitator kettle successively, after dissolution of solid, new world perfume base, linalool oxide, ageratum oil, Oils, bergamot peel and Oleum lavandula angustifolia are added agitator kettle successively, filter after purifying, namely get perfume fragrance.
3. the preparation method of a kind of perfume fragrance as claimed in claim 2, the time that it is characterized in that described purifying is 24h.
4. the preparation method of a kind of perfume fragrance as claimed in claim 2, is characterized in that the filter screen of described filtration is more than 120 orders.
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| CN103215130A (en) * | 2013-03-14 | 2013-07-24 | 天津市双马香精香料新技术有限公司 | Perfume essence with karanal added |
| CN105255589A (en) * | 2014-06-12 | 2016-01-20 | 天津市双马香精香料新技术有限公司 | Detergent essence added with peonile |
| CN106109262B (en) * | 2016-07-06 | 2018-10-12 | 上海应用技术学院 | A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance type perfume and preparation method thereof |
| CN106109263B (en) * | 2016-07-06 | 2018-11-13 | 上海应用技术学院 | A kind of Longaacting fragrance-aretaining east floral type perfume and preparation method thereof |
| CN107937132A (en) * | 2017-11-17 | 2018-04-20 | 恩格乐香精香料（上海）有限公司 | A kind of daily use chemicals lemon extract and preparation method |
| CN109846734A (en) * | 2018-12-24 | 2019-06-07 | 广州市荣申贸易有限公司 | A kind of scent perfume and preparation method thereof |
| CN109549166B (en) * | 2018-12-26 | 2022-04-05 | 浙江绿晶生物科技股份有限公司 | Ginger essence |
| CN110152046A (en) * | 2019-05-05 | 2019-08-23 | 上海应用技术大学 | A kind of fragrant atmosphere essence and preparation method thereof with effects of tranquilizing and allaying excitement ingredient |
| CN110129134A (en) * | 2019-05-06 | 2019-08-16 | 上海应用技术大学 | A kind of fragrant atmosphere essence and preparation method thereof with bacteriostasis efficacy ingredient |
| CN113150864B (en) * | 2021-03-02 | 2021-11-02 | 广州芬豪香精有限公司 | Natural and fresh flower and fruit flavor essence and preparation method and application thereof |
| CN112980576B (en) * | 2021-03-02 | 2022-05-10 | 广州芬豪香精有限公司 | Floral-scented fruit-flavored essence and preparation method and application thereof |
| CN113980739A (en) * | 2021-11-26 | 2022-01-28 | 厦门琥珀日化科技股份有限公司 | Flower fragrance essence with fresh flower style aromatic charm and preparation method thereof |
| CN114259592B (en) * | 2021-12-16 | 2023-05-26 | 厦门琥珀日化科技股份有限公司 | High Wen Tanxiang resistant essence and preparation method and application thereof |
| CN115192510B (en) * | 2022-07-29 | 2023-12-05 | 麦吉丽生物科技有限公司 | Fragrance composition and preparation method and application thereof |
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| JP2008255060A (en) * | 2007-04-05 | 2008-10-23 | Hakugen:Kk | Bath agent and method for bathing by using the same |
| CN100556465C (en) * | 2007-04-25 | 2009-11-04 | 上海应用技术学院 | Air freshener composition |
| CN101982539B (en) * | 2010-11-15 | 2012-05-23 | 广州百花香料股份有限公司 | Bamboo juice essence |
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