CN109846734A - A kind of scent perfume and preparation method thereof - Google Patents
A kind of scent perfume and preparation method thereof Download PDFInfo
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- CN109846734A CN109846734A CN201811585740.0A CN201811585740A CN109846734A CN 109846734 A CN109846734 A CN 109846734A CN 201811585740 A CN201811585740 A CN 201811585740A CN 109846734 A CN109846734 A CN 109846734A
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Abstract
The present invention relates to a kind of scent perfume and preparation method thereof, the scent perfume carries out appropriate weight proportion using 45 kinds of raw materials such as dipropylene glycol, dihydrojasmonate, natural Italian lemon oil, bergamio, lilial, natural patchouli oil, hydroxycitronellal, dihydromyrcenol, natural Brazilian orange oil, linalool and isomethylionones, and the scent perfume with pure and fresh citrus regulating the qi flowing in the channels taste is finally prepared.The preceding taste of perfume of the present invention is the fragrant and sweet fragrance of mixing of lemon bitter orange and mandarin orange, and middle taste is pepper sweet basil, Pogostemon cablin and the thymic mixed flavor of white, and after 18-20h, taste is the mixed flavor of vetiver and santal after perfume.Perfume of the present invention gives off a strong fragrance persistently, and compatibility is rationally scientific, each component interaction, and collaboration plays the role of extending fragrance remaining time, and fragrance makes one salubrious comfortable, spiritual happiness, and has no toxic side effect.
Description
Technical field
The invention belongs to all natural perfume technical fields, and in particular to a kind of scent perfume and preparation method thereof.
Background technique
The English " Perfume " of perfume is derived from Latin " Parfumare ", means " penetrating smog ".Early in Christian era
First 1500, Cleopatra gram Lou Bate drew seven generation just to have begun and is had a bath with the perfume of 15 kinds of different odors.Second of generation
After boundary's Great War, fragrance supply country and the connection of perfume producing country are interrupted, and people start to go into overdrive to develop new raw material, at this time perfume
Also it is not common daily necessities, is the present of special occasions giff-gaff.Into in the 1980s, perfume is become by personal belongings suddenly
It is no longer the luxury goods in pure meaning at the necessity for decorateeing the shop front, and more like a kind of life style with master's label,
Perfume designer exhausts one's ability to manufacture perfume products that are noveler, more having great master's characteristic.In the 1990s, perfume day by day at
Ripe, various styles emerge one after another, and people no longer go overboard for brand, and what is more valued is the displaying of individual culture, are that perfume is most numerous
Flourish 10 years.
The fragrance that perfume has fragrance strong, main function is to be sprayed on the positions such as the hem, handkerchief and hairline, is distributed pleasant
Fragrance, be important one of cosmetics.The fragrance of perfume can reach catchy by people's smell or taste perception,
Material and culture, the purpose of life of spiritual happiness and abundant beautification people.Perfume is the product that fragrance is dissolved in ethyl alcohol, sometimes root
According to needs, the additives such as micro pigment, antioxidant, fungicide, glycerol, surfactant can also be added.Pass through blending
Art (i.e. the technology of preparing essence and art), makes different types of perfume, can be divided into floral type perfume and unreal according to fragrance
Think type perfume two major classes.
Summary of the invention
In order to solve the above problems existing in the present technology, the present invention provides a kind of perfume of scent, fragrance
Strong lasting, preceding taste gives the fragrant and sweet fragrance of mixing of lemon bitter orange and mandarin orange, and middle taste gives pepper sweet basil, Pogostemon cablin
With the thymic mixed flavor of white, after 18-20h, taste is the fragrance of vetiver and santal after perfume.Plant of the present invention
Object fragrance perfume has the effect of capable of making one salubrious comfortable, spiritual happiness loosens.
The technical scheme adopted by the invention is as follows:
A kind of scent perfume, raw material components include:
Dipropylene glycol (DPG) 150-190 parts by weight, natural Italy lemon oil (Gamma-Terpinene) 100-140 weight
Measure part, dihydrojasmonate (Dihydro methyl jasmonate) 100-130 parts by weight, bergamio
(Linalyl acetate) 70-82 parts by weight, natural Brazil orange oil (Limonene) 70-80 parts by weight, lilial
(Lilial) oily (Patchoulic alcohol) 65-75 parts by weight, linalool of 65-75 parts by weight, natural patchouli
(Linalool) 60-70 parts by weight, hydroxycitronellal (Hydroxycitronellal) 40-50 parts by weight, dihydromyrcenol
(Dihydromyrcenol) 40-50 parts by weight, isomethylionone (Iso-methyl ionone) 20-30 parts by weight, not
Sieve send (Floropal [Symrise]) 18-30 parts by weight, triethyl citrate (Triethyl citrate) 15-21 parts by weight,
Ethoxymethyl) epoxide ring hendecane (Boisambrene forte) 10-15 parts by weight, natural vetiver oil (Vetiverol) 8-15
Parts by weight, methylionone (Alpha-methyl ionone) 8-12 parts by weight, Gree gram force dioxolane
(Glycolierral [Givaudan]) 8-12 parts by weight, synthesis oak moss (Veramoss) 4-8 parts by weight, alpha-amyl cinnamic aldehyde
(ACA) 1-2 parts by weight, vertofix coeur (Acetylcedrene80) 2-4 parts by weight, arbricolin (Aldehyde C-18
[Prunolide]) 0.2-0.4 parts by weight, first position terpinol (Alpha-Terpineol) 0.5-1.5 parts by weight, benzyl acetate
(Benzyl acetate) 0.1-0.3 parts by weight, benzyl salicylate (Benzyl salicylate) 0.2-0.8 parts by weight, capraldehyde
(C10) 1.0-2.0 parts by weight, lauric aldehyde (C12) 0.1-0.2 parts by weight, octanal (C8) 0.1-0.2 parts by weight, natural camphor
(Camphor) 0.3-0.7 parts by weight, Leaf Acetate (Cis-3-Hexenyl acetate) 2.0-3.0 parts by weight, citronellal
(Citronella) 0.05-0.15 parts by weight, dimethyl heptanol (dimethyl heptanol [BASF]) 0.05-0.15 weight
Part, ethyl linalool (Ethyl linalool) 0.05-0.15 parts by weight, crocetin ethyl ester (Ethyl safranate)
0.04-0.10 parts by weight, geraniol (Geraniol) 2.0-3.0 parts by weight, Vanillin acetate (Geranyl acetate) 2-3
Parts by weight, first position hexyl cinnamic aldehyde (HCA) 0.2-0.6 parts by weight, hexyl acetate (Hexyl acetate) 0.20-0.24 parts by weight,
L- carvol (Levo-Carvone) 1-2 parts by weight, 10% cinnamic aldehyde (Mandarine Aldehyde) 0.8-1.3 parts by weight, benzene
Ethyl alcohol (Phenylethyl Alcohol) 0.1-0.2 parts by weight, terpinyl acetate (Terpinyl acetate) 0.5-0.9 weight
Measure part, Thymol (Thymol) 0.2-0.6 parts by weight, verdox (Verdox) 0.2-0.6 parts by weight, second
Acid is to t-butyl cyclohexyl methacrylate (Vertenex) 1-2 parts by weight, second position citronellol (β-Citronellol) 0.1-0.2 parts by weight, double
Dealcoholization 8000-9000 parts by weight, pure water 400-600 parts by weight.
The raw material components of the further preferred scent perfume include:
172 parts by weight of dipropylene glycol, 120 parts by weight of natural Italian lemon oil, 116 weight of dihydrojasmonate
Part, 78.6 parts by weight of bergamio, 75 parts by weight of natural Brazilian orange oil, 71.7 parts by weight of lilial, natural patchouli oil
71 parts by weight, 66.4 parts by weight of linalool, 46.6 parts by weight of hydroxycitronellal, 45.2 parts by weight of dihydromyrcenol, different methyl
24 parts by weight of irisone, not sieve send 23.2 parts by weight, 18 parts by weight of triethyl citrate, ethoxymethyl) epoxide ring hendecane
12.8 parts by weight, 11 parts by weight of natural vetiver oil, 10.2 parts by weight of methylionone, 10.3 weight of Gree gram force dioxolane
Part, synthesis 6.22 parts by weight of oak moss, 1.68 parts by weight of alpha-amyl cinnamic aldehyde, 2.8 parts by weight of vertofix coeur, 0.32 weight of arbricolin
Measure part, 1.2 parts by weight of first position terpinol, 0.22 parts by weight of benzyl acetate, 0.5 parts by weight of benzyl salicylate, 1.4 weight of capraldehyde
Part, 0.16 parts by weight of lauric aldehyde, 0.18 parts by weight of octanal, 0.48 parts by weight of natural camphor, 2.5 parts by weight of Leaf Acetate, perfume (or spice)
0.1 parts by weight of thatch aldehyde, 0.1 parts by weight of dimethyl heptanol, 0.1 parts by weight of ethyl linalool, 0.07 parts by weight of crocetin ethyl ester,
2.4 parts by weight of geraniol, 2.4 parts by weight of Vanillin acetate, 0.4 parts by weight of first position hexyl cinnamic aldehyde, 0.22 parts by weight of hexyl acetate,
1.54 parts by weight of L- carvol, 10% cinnamic aldehyde, 1.12 parts by weight, 0.14 parts by weight of benzyl carbinol, 0.74 parts by weight of terpinyl acetate,
0.45 parts by weight of Thymol, 0.46 parts by weight of verdox, 1.34 parts by weight of vertenex,
0.14 parts by weight of second position citronellol, 8500 parts by weight of double dealcoholizations, 500 parts by weight of pure water.
Further, natural patchouli is cleaned, after water is impregnated, drained, successively carries out cryo-conservation, crushing, low
Temperature is dried, be placed in dehydrated alcohol and impregnate, and extracted in Pogostemon cablin using supercritical carbon dioxide extraction method
Oil obtains natural patchouli oil.
Further, natural cus-cus is cleaned, water impregnate, drain after, successively carry out cryo-conservation, crushing, low temperature
Be dried, be placed in dehydrated alcohol and impregnate, and extract the oil in cus-cus using supercritical carbon dioxide extraction method, obtain
To natural vetiver oil.
Further, the water impregnates to impregnate 8~10h in 15 DEG C~20 DEG C of water；The cryo-conservation is in liquid
4~6min is saved in nitrogen；It is described to crush to be crushed to 130 mesh~150 mesh.
Further, the temperature of the low temperature drying is 40 DEG C~50 DEG C；After water content reaches 8%~10%, in nothing
4~5h is impregnated in water-ethanol, the addition quality of dehydrated alcohol is 0.8~1.2 times of Pogostemon cablin or cus-cus quality.
Further, the extracting pressure of the supercritical carbon dioxide extraction method is 23~35Mpa, extraction temperature 35
DEG C~45 DEG C, extraction time is 50~90min, and carbon dioxide flow is 15~18L/h.
A method of the scent perfume is prepared, is included the following steps:
(1) each raw material component is weighed according to the weight, is successively mixed, stirred, be aged and is cooled down, obtain the perfume (or spice)
Water stoste；
(2) the perfume stoste is filtered and is mixed colours, obtain the scent perfume.
Further, in step (1), the mixing speed is 20-30r/min, and the mixing time is 15-30min.
Further, in step (1), the Aging Temperature is 10-20 DEG C, and the digestion time is 6-12 months；It is described
Cooling temperature be subzero 6 DEG C-it is 4 DEG C subzero.
Further, in step (2), the filtration temperature is 0-3 DEG C；It is food grade oil-based liquid that the toning, which uses,
Pigment.
The invention has the benefit that
Scent perfume of the present invention, by using dihydrojasmonate, natural Italian lemon oil, second
Sour virtue camphor tree ester, lilial, dipropylene glycol, natural patchouli oil, hydroxycitronellal, dihydromyrcenol, natural Brazil's orange oil,
45 kinds of raw materials such as linalool and isomethylionone carry out appropriate weight proportion, are finally prepared with pure and fresh citrus regulating the qi flowing in the channels
The scent perfume of taste.The preceding taste of perfume of the present invention is the fragrant and sweet fragrance of mixing of lemon bitter orange and mandarin orange, middle taste
For pepper sweet basil, Pogostemon cablin and the thymic mixed flavor of white, after 18-20h, taste is vetiver and santal after perfume
Mixed flavor.Perfume of the present invention gives off a strong fragrance persistently, and compatibility is rationally scientific, and each component interaction, collaboration, which plays, prolongs
The effect of long fragrance remaining time, fragrance makes one salubrious comfortable, spiritual happiness, and has no toxic side effect.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
Embodiment 1
The present embodiment provides a kind of scent perfume, raw material components include:
Dipropylene glycol 150-190g, natural Italian lemon oil 100-140g, dihydrojasmonate 100-130g, second
Sour virtue camphor tree ester 70-82g, natural Brazilian orange oil 70-80g, lilial 65-75g, natural patchouli oil 65-75g, linalool 60-
70g, hydroxycitronellal 40-50g, dihydromyrcenol 40-50g, isomethylionone 20-30g, not sieve sends 18-30g, lemon
Lemon triethylenetetraminehexaacetic acid ester 15-21g, ethoxymethyl) epoxide ring hendecane 10-15g, natural vetiver oil 8-15g, methylionone 8-
12g, Gree gram force dioxolane 8-12g, synthesis oak moss 4-8g, alpha-amyl cinnamic aldehyde 1-2g, vertofix coeur 2-4g, arbricolin
0.2-0.4g, first position terpinol 0.5-1.5g, benzyl acetate 0.1-0.3g, benzyl salicylate 0.2-0.8g, capraldehyde 1.0-2.0g,
Lauric aldehyde 0.1-0.2g, octanal 0.1-0.2g, natural camphor 0.3-0.7g, Leaf Acetate 2.0-3.0g, citronellal 0.05-
0.15g, dimethyl heptanol 0.05-0.15g, ethyl linalool 0.05-0.15g, crocetin ethyl ester 0.04-0.10g, geraniol
2.0-3.0g, Vanillin acetate 2-3g, first position hexyl cinnamic aldehyde 0.2-0.6g, hexyl acetate 0.20-0.24g, L- carvol 1-2g,
10% cinnamic aldehyde 0.8-1.3g, benzyl carbinol 0.1-0.2g, terpinyl acetate 0.5-0.9g, Thymol 0.2-0.6g, acetic acid uncle neighbour
It is butylcyclohexyl ester 0.2-0.6g, vertenex 1-2g, second position citronellol 0.1-0.2g, double dealcoholization 8000g, pure
Water purification 400g.
Further, the present embodiment provides the preparation method of the scent perfume, include the following steps:
(1) Pogostemon cablin and cus-cus are cleaned respectively, impregnates 8h in 15 DEG C of water, drain, 4min is saved in liquid nitrogen
After be crushed to 130 mesh, then carry out low temperature drying temperature be 40 DEG C, after water content reaches 8%, impregnated in dehydrated alcohol
4h, the addition quality of dehydrated alcohol are 0.8 times of Pogostemon cablin or cus-cus quality, are extracted using supercritical carbon dioxide extraction method
Oil in Pogostemon cablin and cus-cus, extracting pressure 23Mpa, extraction temperature are 35 DEG C, extraction time 50min, carbon dioxide stream
Amount is 15L/h, and final extract obtains natural patchouli oil and natural vetiver oil；
(2) it weighs each raw material component according to the weight to be mixed, 20r/min stirs 15min, is aged 6 at 10 DEG C
Month, it is then cooled down at subzero 6 DEG C, obtains the perfume stoste；
(3) the perfume stoste is filtered at 0 DEG C, is then mixed colours, is obtained with food grade oiliness liquid pigment
To the scent perfume.
Embodiment 2
The present embodiment provides a kind of scent perfume, raw material components include:
Dipropylene glycol 150-190g, natural Italian lemon oil 100-140g, dihydrojasmonate 100-130g, second
Sour virtue camphor tree ester 70-82g, natural Brazilian orange oil 70-80g, lilial 65-75g, natural patchouli oil 65-75g, linalool 60-
70g, hydroxycitronellal 40-50g, dihydromyrcenol 40-50g, isomethylionone 20-30g, not sieve sends 18-30g, lemon
Lemon triethylenetetraminehexaacetic acid ester 15-21g, ethoxymethyl) epoxide ring hendecane 10-15g, natural vetiver oil 8-15g, methylionone 8-
12g, Gree gram force dioxolane 8-12g, synthesis oak moss 4-8g, alpha-amyl cinnamic aldehyde 1-2g, vertofix coeur 2-4g, arbricolin
0.2-0.4g, first position terpinol 0.5-1.5g, benzyl acetate 0.1-0.3g, benzyl salicylate 0.2-0.8g, capraldehyde 1.0-2.0g,
Lauric aldehyde 0.1-0.2g, octanal 0.1-0.2g, natural camphor 0.3-0.7g, Leaf Acetate 2.0-3.0g, citronellal 0.05-
0.15g, dimethyl heptanol 0.05-0.15g, ethyl linalool 0.05-0.15g, crocetin ethyl ester 0.04-0.10g, geraniol
2.0-3.0g, Vanillin acetate 2-3g, first position hexyl cinnamic aldehyde 0.2-0.6g, hexyl acetate 0.20-0.24g, L- carvol 1-2g,
10% cinnamic aldehyde 0.8-1.3g, benzyl carbinol 0.1-0.2g, terpinyl acetate 0.5-0.9g, Thymol 0.2-0.6g, acetic acid uncle neighbour
It is butylcyclohexyl ester 0.2-0.6g, vertenex 1-2g, second position citronellol 0.1-0.2g, double dealcoholization 9000g, pure
Water purification 600g.
Further, the present embodiment provides the preparation method of the scent perfume, include the following steps:
(1) Pogostemon cablin and cus-cus are cleaned respectively, impregnates 10h in 20 DEG C of water, drain, 6min is saved in liquid nitrogen
After be crushed to 150 mesh, then carry out low temperature drying temperature be 50 DEG C, after water content reaches 10%, soaked in dehydrated alcohol
5h is steeped, the addition quality of dehydrated alcohol is 1.2 times of Pogostemon cablin or cus-cus quality, is mentioned using supercritical carbon dioxide extraction method
The oil in Pogostemon cablin and cus-cus, extracting pressure 35Mpa are taken, extraction temperature is 45 DEG C, extraction time 90min, carbon dioxide
Flow is 18L/h, and final extract obtains natural patchouli oil and natural vetiver oil；
(2) it weighs each raw material component according to the weight to be mixed, 30r/min stirs 30min, is aged 12 at 20 DEG C
Month, it is then cooled down at subzero 4 DEG C, obtains the perfume stoste；
(3) the perfume stoste is filtered at 3 DEG C, is then mixed colours, is obtained with food grade oiliness liquid pigment
To the scent perfume.
Embodiment 3
The present embodiment provides a kind of scent perfume, raw material components include:
Dipropylene glycol 172g, natural Italian lemon oil 120g, dihydrojasmonate 116g, bergamio
78.6g, natural Brazilian orange oil 75g, lilial 71.7g, natural patchouli oil 71g, linalool 66.4g, hydroxycitronellal
46.6g, dihydromyrcenol 45.2g, isomethylionone 24g, not sieve sends 23.2g, triethyl citrate 18g, ethyoxyl
Methoxy basic ring hendecane 12.8g, it natural vetiver oil 11g, methylionone 10.2g, Gree gram force dioxolane 10.3g, closes
At oak moss 6.22g, alpha-amyl cinnamic aldehyde 1.68g, vertofix coeur 2.8g, arbricolin 0.32g, first position terpinol 1.2g, acetic acid
Benzyl ester 0.22g, benzyl salicylate 0.5g, capraldehyde 1.4g, lauric aldehyde 0.16g, octanal 0.18g, natural camphor 0.48g, acetic acid leaf
Alcohol ester 2.5g, citronellal 0.1g, dimethyl heptanol 0.1g, ethyl linalool 0.1g, crocetin ethyl ester 0.07g, geraniol
2.4g, Vanillin acetate 2.4g, first position hexyl cinnamic aldehyde 0.4g, hexyl acetate 0.22g, L- carvol 1.54g, 10% cinnamic aldehyde
1.12g, benzyl carbinol 0.14g, terpinyl acetate 0.74g, Thymol 0.45g, verdox 0.46g, acetic acid
To t-butyl cyclohexyl methacrylate 1.34g, second position citronellol 0.14g, double dealcoholization 8500g, pure water 500g.
Further, the present embodiment provides the preparation method of the scent perfume, include the following steps:
(1) Pogostemon cablin and cus-cus are cleaned respectively, impregnates 9h in 18 DEG C of water, drain, 5min is saved in liquid nitrogen
After be crushed to 140 mesh, then carry out low temperature drying temperature be 45 DEG C, after water content reaches 9%, impregnated in dehydrated alcohol
4.5h, the addition quality of dehydrated alcohol are 1 times of Pogostemon cablin or cus-cus quality, are extracted using supercritical carbon dioxide extraction method
Oil in Pogostemon cablin and cus-cus, extracting pressure 30Mpa, extraction temperature are 40 DEG C, extraction time 70min, carbon dioxide stream
Amount is 17L/h, and final extract obtains natural patchouli oil and natural vetiver oil；
(2) it weighs each raw material component according to the weight to be mixed, 25r/min stirs 23min, is aged 8 at 15 DEG C
Month, it is then cooled down at subzero 5 DEG C, obtains the perfume stoste；
(3) the perfume stoste is filtered at 1 DEG C, is then mixed colours, is obtained with food grade oiliness liquid pigment
To the scent perfume.
Experimental example
The fragrance remaining time of scent perfume described in embodiment 1-3 is tested
1, test material: scent perfume, commercially available perfume described in embodiment 1-3.
2, subjects: subject 80, men and women is fifty-fifty, and the age 20-50 years old, physical condition was good.
3, test method: subject is divided into four groups immediately, every group of 20 people, respectively example 1 group, 2 groups of embodiment, reality
3 groups of example and commercially available perfume group are applied, allows subject to use embodiment 1, embodiment 2, embodiment 3 and commercially available perfume respectively, tests it
Fragrance remaining time.The test of every kind of perfume three times, take three times average value be used as final testing result, adjacent evaluation and test time interval one twice
It.
4, test result: fragrance remaining time record is shown in Table 1
1 test result of table
It can be seen from the above result that perfume fragrance remaining time prepared by the present invention is more lasting, explanation compared with commercially available perfume group
Scent perfume compatibility of the present invention is rationally scientific, and each component interaction, collaboration plays the work for extending fragrance remaining time
With.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of scent perfume, which is characterized in that raw material components include:
Dipropylene glycol 150-190 parts by weight, natural Italy lemon oil 100-140 parts by weight, dihydrojasmonate 100-
130 parts by weight, bergamio 70-82 parts by weight, natural Brazil's orange oil 70-80 parts by weight, lilial 65-75 parts by weight,
Natural patchouli oil 65-75 parts by weight, linalool 60-70 parts by weight, hydroxycitronellal 40-50 parts by weight, dihydromyrcenol
40-50 parts by weight, isomethylionone 20-30 parts by weight, not sieve sends 18-30 parts by weight, triethyl citrate 15-21 weight
Part, ethoxymethyl) epoxide ring hendecane 10-15 parts by weight, natural vetiver oil 8-15 parts by weight, methylionone 8-12 weight
Part, Gree gram force dioxolane 8-12 parts by weight, synthesis oak moss 4-8 parts by weight, alpha-amyl cinnamic aldehyde 1-2 parts by weight, methyl cypress
The wooden ketone 2-4 parts by weight, arbricolin 0.2-0.4 parts by weight, first position terpinol 0.5-1.5 parts by weight, benzyl acetate 0.1-0.3 weight
Part, benzyl salicylate 0.2-0.8 parts by weight, capraldehyde 1.0-2.0 parts by weight, lauric aldehyde 0.1-0.2 parts by weight, octanal 0.1-0.2
Parts by weight, natural camphor 0.3-0.7 parts by weight, Leaf Acetate 2.0-3.0 parts by weight, citronellal 0.05-0.15 parts by weight, two
Isoocanol 0.05-0.15 parts by weight, ethyl linalool 0.05-0.15 parts by weight, crocetin ethyl ester 0.04-0.10 weight
Part, geraniol 2.0-3.0 parts by weight, Vanillin acetate 2-3 parts by weight, first position hexyl cinnamic aldehyde 0.2-0.6 parts by weight, hexyl acetate
0.20-0.24 parts by weight, L- carvol 1-2 parts by weight, 10% cinnamic aldehyde 0.8-1.3 parts by weight, benzyl carbinol 0.1-0.2 parts by weight,
Terpinyl acetate 0.5-0.9 parts by weight, Thymol 0.2-0.6 parts by weight, verdox 0.2-0.6 weight
Part, vertenex 1-2 parts by weight, second position citronellol 0.1-0.2 parts by weight, double dealcoholization 8000-9000 weight
Part, pure water 400-600 parts by weight.
2. scent perfume according to claim 1, which is characterized in that raw material components include:
172 parts by weight of dipropylene glycol, 120 parts by weight of natural Italian lemon oil, 116 parts by weight of dihydrojasmonate, second
Sour 78.6 parts by weight of virtue camphor tree ester, 75 parts by weight of natural Brazilian orange oil, 71.7 parts by weight of lilial, oily 71 weight of natural patchouli
Part, 66.4 parts by weight of linalool, 46.6 parts by weight of hydroxycitronellal, 45.2 parts by weight of dihydromyrcenol, different methyl violet
24 parts by weight of ketone, not sieve send 23.2 parts by weight, 18 parts by weight of triethyl citrate, 12.8 weight of ethoxymethyl) epoxide ring hendecane
Part, 11 parts by weight of natural vetiver oil, 10.2 parts by weight of methylionone, 10.3 parts by weight of Gree gram force dioxolane, synthesis
6.22 parts by weight of oak moss, 1.68 parts by weight of alpha-amyl cinnamic aldehyde, 2.8 parts by weight of vertofix coeur, 0.32 parts by weight of arbricolin, first
Position 1.2 parts by weight of terpinol, 0.22 parts by weight of benzyl acetate, 0.5 parts by weight of benzyl salicylate, 1.4 parts by weight of capraldehyde, lauric aldehyde
0.16 parts by weight, 0.18 parts by weight of octanal, 0.48 parts by weight of natural camphor, 2.5 parts by weight of Leaf Acetate, 0.1 weight of citronellal
Measure part, 0.1 parts by weight of dimethyl heptanol, 0.1 parts by weight of ethyl linalool, 0.07 parts by weight of crocetin ethyl ester, geraniol 2.4
Parts by weight, 2.4 parts by weight of Vanillin acetate, 0.4 parts by weight of first position hexyl cinnamic aldehyde, 0.22 parts by weight of hexyl acetate, L- carvol
1.54 parts by weight, 10% cinnamic aldehyde, 1.12 parts by weight, 0.14 parts by weight of benzyl carbinol, 0.74 parts by weight of terpinyl acetate, Thymol
0.45 parts by weight, 0.46 parts by weight of verdox, 1.34 parts by weight of vertenex, second position lemongrass
0.14 parts by weight of alcohol, 8500 parts by weight of double dealcoholizations, 500 parts by weight of pure water.
3. -2 described in any item scent perfume according to claim 1, which is characterized in that the natural patchouli oil uses
Following technique is prepared:
Natural patchouli is cleaned, water impregnate, drain after, successively carry out cryo-conservation, crushing, low temperature drying processing, it
It is placed in dehydrated alcohol and impregnates, and extract the oil in Pogostemon cablin using supercritical carbon dioxide extraction method, obtain natural wide
Palchouli oil；
The natural vetiver oil is prepared using following technique:
Natural cus-cus is cleaned, water impregnate, drain after, successively carry out cryo-conservation, crushing, low temperature drying processing, later
It is placed in dehydrated alcohol and impregnates, and extract the oil in cus-cus using supercritical carbon dioxide extraction method, obtain natural vetiver oil.
4. scent perfume according to claim 3, which is characterized in that the water impregnates in 15 DEG C~20 DEG C of water
8~10h of middle immersion；The cryo-conservation is that 4~6min is saved in liquid nitrogen；It is described to crush to be crushed to 130 mesh~150 mesh.
5. scent perfume according to claim 3, which is characterized in that the temperature of the low temperature drying is 40 DEG C~50
℃；After water content reaches 8%~10%, in dehydrated alcohol impregnate 4~5h, the addition quality of dehydrated alcohol be Pogostemon cablin or
0.8~1.2 times of cus-cus quality.
6. scent perfume according to claim 3, which is characterized in that the supercritical carbon dioxide extraction method
Extracting pressure is 23~35Mpa, and extraction temperature is 35 DEG C~45 DEG C, and extraction time is 50~90min, carbon dioxide flow 15
~18L/h.
7. the preparation method of any one of the claim 1-6 scent perfume, which comprises the following steps:
(1) each raw material component is weighed according to the weight, is successively mixed, stirred, be aged and is cooled down, it is former to obtain the perfume
Liquid；
(2) the perfume stoste is filtered and is mixed colours, obtain the scent perfume.
8. the preparation method of scent perfume according to claim 7, which is characterized in that in step (1), the stirring speed
Degree is 20-30r/min, and the mixing time is 15-30min.
9. the preparation method of scent perfume according to claim 7, which is characterized in that in step (1), the ageing temperature
Degree is 10-20 DEG C, and the digestion time is 6-12 months；The cooling temperature be subzero 6 DEG C-it is 4 DEG C subzero.
10. the preparation method of scent perfume according to claim 7, which is characterized in that in step (2), the filtering
Temperature is 0-3 DEG C；It is food grade oiliness liquid pigment that the toning, which uses,.
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