KR100567584B1 - Perfume using essential oil of tymus quinquecostatus var.japonica hara and manufacturing process of the same - Google Patents
Perfume using essential oil of tymus quinquecostatus var.japonica hara and manufacturing process of the same Download PDFInfo
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Abstract
본 발명은 섬백리향 식물정유를 이용한 향수 및 그 제조방법에 관한 것으로, 인체에 유용한 약리기능을 가지며, 좋은 향기를 발산시키는 성분이 함유된 섬백리향의 꽃, 잎 및 줄기로부터 천연의 식물정유(精油:Essential oil)를 추출하여 정제한 다음 정제된 식물정유를 주요 성분으로 하는 향수를 제조함으로써 그 활용도를 진작시킬 수 있도록 하고, 섬백리향의 재배를 활성화시켜 농가소득의 증대 및 지방자치단체의 재정자립에 기여할 수 있도록 한 것이다.The present invention relates to a perfume using a thyme plant essential oil and a method for producing the same, natural plant essential oils from the flowers, leaves and stems of the island thyme containing a component that has a useful pharmacological function and emits a good fragrance to the human body (精油) Extract and refine essential oils to produce perfumes based on refined plant essential oils to enhance their utilization, and to promote cultivation of island thyme, to increase farm incomes and to help local governments regain their financial independence. To contribute.
본 발명에 따른 섬백리향 식물정유를 이용한 향수는 순수 증류수 80∼81.7중량%에 섬백리향 식물정유 1∼3중량%, 에틸알코올 10∼15중량%, 계면활성제 3∼6중량%, 보습제 4∼5중량%, 색소 0.0001중량% 및 방부제 0.1∼0.3중량%를 첨가하고, 40∼45℃에서 균일하게 교반·혼합한 다음 냉암소에서 55∼65일 동안 숙성시킨 후 침전물을 여과시켜 얻어진다.Perfume using the thyme plant essential oil according to the present invention is 1 to 3% by weight of thyme plant essential oil, 10 to 15% by weight ethyl alcohol, 3 to 6% by weight surfactant, 4 to 5 in pure distilled water 80-81.7% by weight By weight, 0.0001% by weight of pigment and 0.1-0.3% by weight of preservative are added, uniformly stirred and mixed at 40-45 ° C., and aged in a cool dark for 55-65 days, followed by filtration of the precipitate.
본 발명을 적용하면, 섬백리향으로부터 추출된 천연의 식물정유성분(티몰)이 향기성분으로 첨가됨에 따라 섬백리향 고유의 향을 발산시키는 향수를 얻을 수 있는바, 이와 같이 제조된 향수는 천연상태로부터 추출된 식물정유를 이용하고 유기용매인 디에틸에테르를 완전히 제거한 다음 다양한 화합물을 첨가 및 혼합하기 때문에 인체에 무해하여 안심하고 사용할 수 있다.Applying the present invention, as the natural plant essential oil (Timole) extracted from the island thyme is added as a scent component can be obtained a perfume that emits the unique aroma of island thyme, fragrance thus prepared is from a natural state Since the extracted plant essential oil is used and the organic solvent diethyl ether is completely removed, and then various compounds are added and mixed, it can be used safely because it is harmless to the human body.
또한, 천연기념물인 섬백리향의 재배가 활성화되는 것은 물론, 부가가치의 향상에 따라 섬백리향 재배농가의 소득이 증대될 수 있으며, 특산품으로 개발되는 경우 관광객 유치 및 지방자치단체의 안정적인 재정확보를 꾀할 수 있다는 부수적인 효과가 있다. In addition, the cultivation of island thyme, a natural monument, can be activated, and the income of island thyme growers can be increased according to the improvement of added value, and when it is developed as a special product, it can attract tourists and secure financial stability of local governments. It has a side effect.
섬백리향, 식물정유, 향수 Island Thyme, Plant Essential Oil, Fragrance
Description
본 발명은 섬백리향 식물정유를 이용한 향수 및 그 제조방법에 관한 것으로, 보다 상세하게는 인체에 유용한 약리기능을 가지며, 좋은 향기를 발산시키는 성분이 함유된 섬백리향의 꽃, 잎 및 줄기로부터 천연의 식물정유(精油:Essential oil)를 추출하여 정제한 다음 정제된 식물정유를 주요 성분으로 하는 향수를 제조함으로써 그 활용도를 진작시킬 수 있도록 하고, 섬백리향의 재배를 활성화시켜 농가소득의 증대 및 지방자치단체의 재정자립에 기여할 수 있도록 한 섬백리향 식물정유를 이용한 향수 및 그 제조방법에 관한 것이다.The present invention relates to a perfume using an thyme plant essential oil and a method of manufacturing the same, and more particularly, from the flowers, leaves and stems of the island thyme containing a component that has a pharmacological function useful for the human body and emits a good fragrance. After extracting and refining essential oils, they can be used to make perfumes with the main ingredients of refined plant oils to promote their utilization and to increase farm household income and promote local autonomy by activating cultivation of thyme. The present invention relates to a perfume using an island thyme plant essential oil and a method for producing the same, which contribute to the financial independence of the organization.
일반적으로, 경제의 발달과 더불어 생활수준이 향상됨에 따라 외모를 아름답게 가꾸고자 하는 욕구가 증대되고 있으며, 이와 같은 외모를 아름답게 가꿀 수 있는 재료로서 각종 화장품 및 향수 등이 제안되어 시판되고 있다.In general, with the development of the economy, as the standard of living improves, the desire to enhance the appearance beautifully increases, and various cosmetics and perfumes have been proposed and marketed as materials that can beautifully shape the appearance.
한편, 향수는 화장품의 일종으로서 향을 내는 물질들을 적당한 비율로 배합한 후 알코올 등에 용해시켜 제조하고, 신체의 일부분이나 옷에 뿌려 사용하며, 피 부로부터 발산되는 체온 또는 체취와 함께 섞여서 향기를 발산시키는 것이다.On the other hand, perfume is a kind of cosmetics, it is made by mixing fragrance substances in proper ratios and dissolving them in alcohol, etc., spraying them on parts of clothes or clothes, and mixing them with body temperature or body odor emitted from skin to give off fragrance. It is to let.
이와 같이 향수를 신체 또는 의복에 사용하면, 신체로부터 발산되는 나쁜 냄새가 저감 또는 차단되고, 향수로부터 발산되는 좋은 향기에 의하여 타인으로 하여금 호감을 불러일으키기 때문에 남녀를 불문하고 현대인들에게 매우 선호되는 화장품의 일종으로 자리매김하게 되었다.The use of perfume in the body or clothing in this way, the bad smell emitted from the body is reduced or blocked, and the good fragrance emitted from the perfume attracts others, so cosmetics that are highly favored by modern people regardless of gender It became a kind of.
한편, 이와 같은 향수의 주요 성분으로 첨가·혼합되는 향을 내는 물질로는 천연향료와 화학합성 향료가 있는데, 현재 대량으로 생산되는 향수에 첨가되는 향료는 대부분 화학합성 향료가 사용되고 있다.On the other hand, as a main component of the perfume, the fragrance material added and mixed as a natural perfume and chemical synthetic fragrance, the perfume is added to the perfume produced in large quantities, mostly chemical synthetic fragrance is used.
그러나, 이와 같은 인공적으로 합성된 화학합성 향료를 첨가하여 제조되는 향수의 경우 향이 자연스럽지 못하고, 장시간 사용하는 경우 쉽게 싫증나는 것은 물론, 향을 오래지속시키기 위한 다른 화학성분이 함유됨으로 피부에 알러지(Alergy)반응을 일으킨다는 문제가 있으며, 인체에 유용한 약리기능을 기대할 수 없기 때문에 최근에는 식물로부터 추출한 천연의 식물정유를 이용한 향수에 대한 관심이 점차 높아지고 있는 실정이다.However, perfumes prepared by adding such artificially synthesized chemical synthetic fragrances do not have a natural aroma, easily get tired of using it for a long time, and contain other chemical ingredients to keep the fragrance for a long time. There is a problem of causing an Alergy) reaction, and since the pharmacological function useful to the human body cannot be expected, the interest in perfumes using natural plant essential oils extracted from plants has recently increased.
또한, 최근 소비자들은 화장품을 사용하였을 때 피부 및 인체에 대한 일정한 케어효과(Care effect)를 나타내거나 또는 결점을 없앨 수 있도록 하는 기능성의 화장품을 기대하는 경향이 크기 때문에 사용시 일정한 약리효과를 가지면서 좋은 향을 발산시키는 성분이 함유된 식물에 대한 연구가 활발하게 이루어지고 있는 실정이다.In addition, recently, consumers have a tendency to expect functional cosmetics that can exhibit a certain care effect on the skin and the human body or eliminate defects when using cosmetics, and thus have a good pharmacological effect when using the cosmetics. There is an active research on plants containing components that emit scents.
한편, 이와 같이 좋은 향을 발산시키는 성분이 함유되어 있으면서 인체에 유 용한 약리기능을 갖는 식물의 일종으로서 울릉도의 도동주변 일원에 분포되어 자생하며, 천연기념물로 지정된 섬백리향(학명:Tymus quinquecostatus var.japonica Hara)을 들 수 있다.On the other hand, it is a kind of plant that contains a component that emits good fragrance and has a useful pharmacological function to the human body, and is native to Ulleungdo's Dodong area and is native to the island's thyme (Tymus quinquecostatus var. japonica Hara).
우리나라에서 천연기념물로 지정된 상기 섬백리향은 꿀풀과에 속하는 식물로서, 스쿠텔라레인-헤테로사이드(Scutellarein-heteroside), 루테올린-7-글루코사이드(Luteoline-7-glucoside), 아피게닌(Apigenin)등의 플라본류와 식물정유성분에는 티몰(Tymol), 리날로올(Linalool), 카바크롤(Carvacrol), p-사이멘(p-Cymene), γ-테르피넨(Terpinene), α-테르피네올(Terpineol), 징기베렌(Zingiberene), 보르네올(Borneol) 등이 주성분으로 함유되어 있다.The island thyme, which is designated as a natural monument in Korea, is a plant belonging to the family Lamiaceae, such as Scutellarein-heteroside, Luteoline-7-glucoside, Apigenin, etc. Flavones and plant essential oils include Tymol, Linalool, Carvacrol, p-Cymene, γ-terpinene, and α-terpineol ), Zingiberene and Borneol are the main ingredients.
상기한 섬백리향에는 티몰(Tymol), p-사이멘(p-Cymene), 리날로올(Linalool)등의 성분이 함유되어 있어 섬백리향 특유의 향기가 발산되며, 전초 또는 꽃의 전재는 기관지염, 인후염, 백일해, 상부 호흡기질환에 대한 진정, 진경의 약효가 있으며, 위통이나 류마티스, 치통 등에 효과가 있고, 혈당강하작용, 항산화작용 등의 약리기능이 있는 것으로 알려진다.The island thyme contains components such as Tymol, p-Cymenene, Linalool, etc., and the unique scent of island thyme is emitted. Sore throat, pertussis, upper respiratory disease sedation, jingyeong medicinal effect, and is effective in stomach pain, rheumatism, toothache, etc. It is known to have pharmacological functions such as hypoglycemic action, antioxidant action.
그러나, 이와 같이 섬백리향에는 인체에 유용한 약리작용을 하는 성분과, 좋은 향기를 발산시키는 성분이 함유되어 있는 것으로 알려졌음에도 불구하고, 현재까지 화장품 특히 향수의 원료로서 이용되고 있지 않으며, 다른 분야에서의 활용 또한 미미한 실정이다.However, although it is known that the island thyme contains ingredients that have a useful pharmacological effect on the human body and a component that emits a good scent, it has not been used as a raw material for cosmetics, especially perfumes. The use is also insignificant.
백리향의 활용예로서, 백리향으로부터 얻어진 백리향 추출물과 그 정유성분을 음료의 원료로 이용하는 활용예가 대한민국 공개특허 제2003-6163호에 개시된 다.As an example of the use of thyme, an example of using the thyme extract obtained from the thyme and its essential oil component as a raw material of the beverage is disclosed in Korean Patent Publication No. 2003-6163.
상기 공개특허 제2003-6163호의 발명은 전체 음료조성물 대비, 백리향 추출물이 0.5∼20중량%, 백리향 정유성분이 0.01∼0.5중량%의 범위내에서 첨가되도록 하여 관능미가 우수하고, 기능성이 보강되도록 한 백리향 음료조성물에 관한 것이다.The invention of the Patent Publication No. 2003-6163 is to be added in the range of 0.5 to 20% by weight thyme extract, 0.01 to 0.5% by weight of the thyme essential oil components compared to the total beverage composition, so that the functional beauty is excellent, and the functionality is reinforced It relates to a thyme beverage composition.
본 발명자는 인체에 유용한 약리기능을 가지며, 좋은 향기를 발산시키는 성분이 함유된 섬백리향으로부터 식물정유를 추출하여 향수를 제조함으로써 그 활용도를 한층 더 진작시킬 수 있도록 하고, 섬백리향의 재배를 활성화시켜 농가소득의 증대 및 지방자치단체의 재정확보에 기여할 수 있도록 하기 위하여 본 발명을 제안하였다.The present inventors have a pharmacological function useful to the human body, extract the plant essential oil from the island thyme containing a component that emits a good fragrance to make the perfume to further increase its utilization, and to activate the cultivation of island thyme The present invention has been proposed in order to contribute to the increase of farm household income and the financial security of local governments.
본 발명의 목적은 인체에 유용한 약리기능을 가지며, 좋은 향기를 발산시키는 성분이 함유된 섬백리향의 꽃, 잎 및 줄기로부터 천연의 식물정유(精油:Essential oil)를 추출하여 정제한 다음 정제된 식물정유를 주요 성분으로 하는 향수를 제조함으로써 그 활용도를 진작시킬 수 있도록 하고, 섬백리향의 재배를 활성화시켜 농가소득의 증대 및 지방자치단체의 재정자립에 기여할 수 있도록 한 새로운 섬백리향 식물정유를 이용한 향수를 제공하는 것이다. An object of the present invention has a pharmacological function useful to the human body, natural plant essential oils extracted from the flowers, leaves and stems of the island thyme containing ingredients that give off a good scent and then purified plant Perfume using the new thyme plant essential oil, which makes it possible to increase its utilization by making perfumes containing essential oils, and to contribute to the increase of farm household income and the financial independence of local governments by activating the cultivation of island thyme. To provide.
본 발명의 다른 목적은 섬백리향의 꽃과 잎사귀 및 줄기로부터 천연의 식물정유(精油:Essential oil)를 추출 및 정제한 후 정제된 식물정유를 주요 성분으로 하는 향수를 제조함으로써 그 활용도를 진작시킬 수 있도록 하고, 섬백리향의 재배 를 활성화시켜 농가소득의 증대 및 지방자치단체의 재정자립에 기여할 수 있도록 한 새로운 섬백리향 식물정유를 이용한 향수의 제조방법을 제공하는 것이다. It is another object of the present invention to extract and refine natural plant essential oils from the flowers, leaves and stems of the island thyme, and to promote their utilization by preparing perfumes based on purified plant essential oils. It is to provide a new manufacturing method of perfume using the island thyme plant essential oil that can contribute to the increase of farm household income and the local government's financial independence by activating the cultivation of island thyme.
상기한 목적을 달성하기 위하여, 본 발명에 따른 섬백리향 식물정유를 이용한 향수는 순수 증류수 80∼81.7중량%에 에틸알코올 10∼15중량%, 섬백리향 식물정유 1∼3중량%, 계면활성제 3∼6중량%, 보습제 4∼5중량%, 색소 0.0001중량% 및 방부제 0.1∼0.3중량%가 함유된 특징을 갖는다.In order to achieve the above object, the fragrance using the island thyme plant essential oil according to the present invention is 10 to 15% by weight of ethyl alcohol, 1 to 3% by weight of thyme plant essential oil, 3 to 3% surfactant in pure distilled water 6% by weight, 4-5% by weight of moisturizer, 0.0001% by weight of pigment and 0.1-0.3% by weight of preservative.
상기한 다른 목적을 달성하기 위하여, 본 발명에 따른 섬백리향 식물정유를 이용한 향수의 제조방법은 섬백리향 식물정유 1∼3중량%를 10∼15중량%의 에틸알코올에 첨가하여 용해시키는 단계와; 상기 섬백리향 식물정유가 용해된 에틸알코올에 3∼6중량%의 계면활성제를 첨가·혼합하는 단계와; 상기 식물정유, 에틸알코올 및 계면활성제의 혼합용액을 80∼81.7중량%의 순수 증류수에 첨가하여 혼합하는 단계와; 상기 순수 증류수에 0.0001중량%의 색소와, 4∼5중량%의 보습제 및 0.1∼0.3중량%의 방부제를 순차적으로 첨가·혼합하는 단계와; 상기 식물정유, 에틸알코올, 계면활성제, 순수 증류수, 색소, 보습제 및 방부제의 혼합용액을 40∼45℃의 온도로 가온하면서 균일하게 교반하여 혼합하는 단계와; 상기 혼합용액을 냉암소에서 55일∼65일 동안 보관하면서 숙성시키는 단계와; 숙성된 혼합용액을 여과하여 침전물을 걸러내는 단계를 포함한다. In order to achieve the above another object, a method for producing a perfume using the thyme plant essential oil according to the present invention comprises the steps of dissolving 1 to 3% by weight of thyme plant essential oil to 10 to 15% by weight of ethyl alcohol; Adding and mixing 3 to 6% by weight of surfactant to ethyl alcohol in which the island thyme plant essential oil is dissolved; Adding the mixed solution of the plant essential oil, ethyl alcohol and the surfactant to 80-81.7% by weight of pure distilled water and mixing the mixture; Sequentially adding and mixing 0.0001% by weight of pigment, 4-5% by weight of moisturizer and 0.1-0.3% by weight of preservative in distilled water; Mixing the plant essential oil, ethyl alcohol, a surfactant, pure distilled water, a dye, a humectant, and a mixed solution of a preservative at a temperature of 40 to 45 ° C. with uniform stirring and mixing; Aging the mixed solution while stored for 55 to 65 days in a cool dark place; Filtering the aged mixed solution to filter out the precipitate.
이하, 본 발명의 바람직한 실시예를 보다 상세하게 설명한다.Hereinafter, preferred embodiments of the present invention will be described in more detail.
본 발명에 따른 섬백리향 식물정유를 이용한 향수는 80∼81.7중량%의 순수 증류수에 1∼3중량%의 섬백리향 식물정유와, 10∼15중량%의 에틸알코올과, 3∼6중량%의 계면활성제와, 4∼5중량%의 보습제가 첨가되며, 미량(0.0001중량%)의 색소 및 0.1∼0.3중량%의 방부제가 첨가·혼합된다.Perfume using the thyme plant essential oil according to the present invention is 1 to 3% by weight of thyme plant essential oil in 80 to 87.1% by weight pure distilled water, 10 to 15% by weight of ethyl alcohol, 3 to 6% by weight of the interface An active agent and 4-5 weight% of humectants are added, and a trace amount (0.0001 weight%) of pigment | dye and 0.1-0.3 weight% of preservatives are added and mixed.
본 발명에서 상기 계면활성제로는 소르비탄 지방산 에스테르(Sorbitan fatty acid ester)의 다가알코올형 비이온계면활성제에 에틸렌 옥사이드(Ethylene Oxide)를 부가시킨 수용성의 에테르형 비이온계면활성제인 TW-80이 사용되며, 색소로는 수용성 색소인 블우안 401이 적용된다.In the present invention, as the surfactant, TW-80, a water-soluble ether type nonionic surfactant obtained by adding ethylene oxide (Ethylene Oxide) to a polyalcohol-type nonionic surfactant of sorbitan fatty acid ester, is used. As the dye, the bloan 401 which is a water-soluble dye is applied.
또, 보습제로는 히솔이 적용되며, 함유된 유기물의 부패를 방지하기 위하여 메틸파라벤(Methylparaben)이 방부제로 적용된다.In addition, a hysol is applied as a moisturizing agent, and methylparaben is applied as a preservative to prevent the decay of organic substances contained therein.
한편, 본 발명에 따른 섬백리향 식물정유를 이용한 향수의 제조방법은 다음과 같다.On the other hand, the production method of the perfume using the island thyme plant essential oil according to the present invention is as follows.
먼저, 섬백리향 식물로부터 추출하여 정제한 섬백리향 식물정유 1∼3중량%를 10∼15중량%의 에틸알코올에 첨가하여 용해시킨다. First, 1-3 wt% of the purified thyme plant essential oil extracted from the thyme plant is added to 10-15 wt% of ethyl alcohol and dissolved.
그런 다음, 상기 섬백리향 식물정유가 용해된 에틸알코올에 3∼6중량%의 계면활성제를 첨가하여 혼합한 후 상기 식물정유, 에틸알코올 및 계면활성제의 혼합용액을 80∼81.7중량%의 순수 증류에 첨가하여 혼합한다. Then, 3-6% by weight of the surfactant is added to the ethyl alcohol in which the island thyme plant essential oil is dissolved, followed by mixing. The mixed solution of the plant essential oil, ethyl alcohol and the surfactant is subjected to 80 to 87.1% by weight of pure distillation. Add and mix.
그런 다음, 상기 순수 증류수 혼합액에 0.0001중량%의 색소와, 4∼5중량%의 보습제 및 0.1∼0.3중량%의 방부제를 순차적으로 첨가하여 혼합한 다음, 그 혼합용액을 40∼45℃의 온도로 가온하면서 교반·혼합한다. Then, 0.0001% by weight of pigment, 4-5% by weight of moisturizer and 0.1-0.3% by weight of preservative were added sequentially to the pure distilled water mixture and mixed, and then the mixed solution was brought to a temperature of 40-45 ° C. Stir and mix while warming.
상기 40∼45℃의 온도로 가온하면서 혼합한 혼합용액은 냉암소에서 55일∼60 일간 보관하여 숙성키고, 숙성기간이 종료되면 숙성된 혼합용액을 여과하여 침전물을 걸러내면 본 발명에 따른 섬백리향 식물정유를 이용한 향수가 얻어진다.The mixed solution mixed with warming at the temperature of 40 ~ 45 ℃ is stored in a cool dark place for 55 to 60 days to aging, and when the aging period is over, the aged mixed solution is filtered to filter out the precipitate, according to the present invention A perfume using plant essential oils is obtained.
한편, 향수제조시 주요 향기성분중 하나인 티몰(Thymol:2-isopropyl-5-methylphenol, 화학식:C10H14O)은 인공적으로 유기합성시켜 제조한 것은 법적으로 향수제조에 이용할 수 없다. Meanwhile, thymol (Thymol: 2-isopropyl-5-methylphenol, Chemical Formula: C 10 H 14 O), one of the main fragrance components in the manufacture of perfume, may not be legally used for preparing perfumes.
따라서, 향수제조시 티몰을 향기성분으로 적용하고자 하는 경우에는 사향초유나 꿀풀과 식물로부터 추출한 천연의 티몰을 이용하는데, 본 발명에서는 섬백리향 식물로부터 다음과 같이 추출하여 얻는다.Therefore, in the case of perfume production, if you want to apply thymol as a fragrance component, natural thymol extracted from musk colostrum or nectar and plants, in the present invention is obtained by extracting from the island thyme plant as follows.
먼저, 자연상태에서 자란 섬백리향의 꽃, 잎 및 줄기를 잘게 절단한 다음 즉시 수증기 증류장치에 넣는다.First, the flowers, leaves and stems of the island-grown thyme grown in nature are chopped and immediately placed in a steam distillation apparatus.
섬백리향으로부터 식물정유를 추출하기 위한 수증기 증류장치에서는 그 가동시간을 40분으로 제한하여 실시한다. 수증기 증류추출 방식으로 얻어진 식물정유에 포함된 수분을 제거하기 위하여 일정 양의 무수황산마그네슘을 식물정유에 혼합하여 24시간동안 냉장고에 밀봉하여 보관한다.In a steam distillation apparatus for extracting plant essential oils from island thyme, the operation time is limited to 40 minutes. In order to remove the water contained in the plant essential oil obtained by the steam distillation extraction method, a certain amount of anhydrous magnesium sulfate is mixed with the plant essential oil and kept sealed in a refrigerator for 24 hours.
24시간이 경과되면 식물정유를 여과지로 거른 다음 감압 농축기를 이용하여 수분을 완전히 제거하여 순수한 식물정유를 얻는다.After 24 hours, the plant essential oil is filtered through a filter paper, and the water is completely removed using a vacuum concentrator to obtain pure plant essential oil.
이와 같이 얻어진 식물정유 성분을 소정의 비율로 에틸알코올에 첨가하여 용해시키고, 계면활성제, 순수 증류수, 색소, 보습성분, 방부제를 정해진 비율로 혼합하여 완전히 밀봉한 다음, 55∼65일동안 냉암소(냉장고)에서 숙성시킨 후 여과하 면 섬백리향의 고유한 향을 느낄 수 있는 섬백리향 식물정유를 이용한 향수가 완성된다.The plant essential oil component thus obtained is added to ethyl alcohol at a predetermined ratio to dissolve it, and the surfactant, pure distilled water, pigment, moisturizing component, and preservative are mixed at a predetermined ratio and completely sealed, and then cooled in a dark place (55-65 days) After aging in the refrigerator), the perfume is completed using an island thyme plant essential oil that can feel the unique aroma of island thyme.
실시예Example
섬백리향 식물정유 추출 Island Thyme Plant Essential Oil Extraction
아랫쪽으로부터 열을 가할 수 있도록 준비되고, 중간에 U자형 유리관이 연결된 두개의 둥근 플라스크로 이루어지는 수증기 증류장치를 준비한 다음, 한쪽의 둥근 플라스크에 증류수 800㎖를 넣고 여기에 잘게 절단된 섬백리향의 식물조직(꽃, 잎, 줄기)을 넣어 100℃의 온도에서 끓였다.Prepare a steam distillation apparatus consisting of two round flasks prepared in order to apply heat from the bottom and connected with a U-shaped glass tube in the middle, and then put 800 ml of distilled water in one round flask and finely chopped island thyme plant tissue. (Flowers, leaves, stems) were put and boiled at a temperature of 100 ° C.
다른쪽 둥근 플라스크에는 디에틸에테르(Diethyl ether) 80㎖를 넣은 후 온도를 40℃로 유지시켰다. In another round flask, 80 ml of diethyl ether was added and the temperature was maintained at 40 ° C.
이 상태에서 약 40∼50분 정도가 경과된 후 수증기 증류장치 중간의 U자형 유리관에 향기성분인 식물정유 성분이 모아졌다.After about 40 to 50 minutes had elapsed in this state, the plant essential oil component as an aromatic component was collected in a U-shaped glass tube in the middle of the steam distillation apparatus.
이들 식물정유 성분을 비이커에 담아 무수황산마그네슘 50g을 혼합한 다음 24시간동안 냉장고에 밀봉하여 보관하였다. These plant essential oils were placed in a beaker, mixed with 50 g of anhydrous magnesium sulfate, and then sealed and stored in a refrigerator for 24 hours.
24시간 후에 식물정유를 여과지로 거르고 감압농축기를 이용하여 수분을 완전히 제거시켜 생체 무게의 2.3% 정도되는 엷은 노란색과 연두색을 띠는 순수한 섬백리향 식물정유를 얻었다.After 24 hours, the plant essential oil was filtered through a filter paper, and the water was completely removed using a vacuum concentrator to obtain a pure yellow thyme plant oil having a pale yellow color and a light green color, which is about 2.3% of the body weight.
식물정유를 이용한 향수제조Production of perfume using plant essential oils
위와 같은 추출방식에 의하여 얻어진 섬백리향 식물정유를 이용하여 다음과 같이 향수를 제조하였다.Using the thyme plant essential oil obtained by the above extraction method to prepare a perfume as follows.
섬백리향 식물정유가 함유된 향수 100㎖를 제조하는 것을 기준으로 하여, 식물정유 1중량%를 에틸알코올 10중량%에 넣어 용해시키고, 여기에 계면활성제인 TW-80 3중량%를 첨가·혼합하였다.Based on preparing 100 ml of perfume containing island thyme plant essential oil, 1% by weight of plant essential oil was dissolved in 10% by weight of ethyl alcohol, and 3% by weight of surfactant TW-80 was added and mixed. .
그런 다음 상기 혼합액을 순수 증류수 81중량%에 넣어 혼합한 다음 색소로서 블루안401 0.0001중량%, 보습제로서 히솔 4중량%, 방부제로서 메틸파라벤 0.1중량%를 첨가하고, 40∼45℃의 온도로 가온하면서 교반하여 균일하게 혼합하였다.Then, the mixed solution was added to 81% by weight of pure distilled water, and mixed. Then, 0.0001% by weight of Bluean 401 as a pigment, 4% by weight of hysol as a moisturizer, and 0.1% by weight of methylparaben as a preservative were added and warmed to a temperature of 40 to 45 ° C. While stirring, the mixture was uniformly mixed.
상기 혼합용액을 냉장고에 60일 보관하여 숙성시키고, 숙성된 혼합용액을 여과지로 걸러 본 발명에 따른 섬백리향 식물정유를 이용한 향수를 제조하였다.The mixed solution was stored in a refrigerator for 60 days to mature, and the aged mixed solution was filtered through a filter paper to prepare a perfume using an island thyme plant essential oil according to the present invention.
이와 같이 하여 제조된 본 발명의 섬백리향 식물정유를 이용한 향수에서는 섬백리향 고유의 향이 발산되는 것은 물론, 화학합성 향료가 첨가되는 다른 향수에 비하여 사용시 피부 알러지반응 등이 발생되지 않았다. In the perfume using the thyme plant vegetable oil of the present invention prepared as described above, not only the scent of the thyme is released, but also a skin allergy reaction does not occur when used compared to other perfumes to which chemical synthetic fragrance is added.
본 발명을 적용하면, 섬백리향으로부터 추출된 천연의 식물정유성분(티몰)이 향기성분으로 첨가됨에 따라 섬백리향 고유의 향을 발산시키는 향수를 얻을 수 있는바, 이와 같이 제조된 향수는 천연상태로부터 추출된 식물정유를 이용하고 유기용매인 디에틸에테르를 완전히 제거한 다음 다양한 화합물을 첨가 및 혼합하기 때문에 인체에 무해하여 안심하고 사용할 수 있다.Applying the present invention, as the natural plant essential oil (Timole) extracted from the island thyme is added as a scent component can be obtained a perfume that emits the unique aroma of island thyme, fragrance thus prepared is from a natural state Since the extracted plant essential oil is used and the organic solvent diethyl ether is completely removed, and then various compounds are added and mixed, it can be used safely because it is harmless to the human body.
또한, 천연기념물인 섬백리향의 재배가 활성화되는 것은 물론, 부가가치의 향상에 따라 섬백리향 재배농가의 소득이 증대될 수 있으며, 특산품으로 개발되는 경우 관광객 유치 및 지방자치단체의 안정적인 재정확보를 꾀할 수 있다는 부수적 인 효과가 있다. In addition, the cultivation of island thyme, a natural monument, can be activated, and the income of island thyme growers can be increased according to the improvement of added value, and when it is developed as a special product, it can attract tourists and secure financial stability of local governments. It has a side effect.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101072040B1 (en) | 2008-10-20 | 2011-10-10 | (주)아모레퍼시픽 | Perfume composition for expressing the fragrance of Thymus quinquecostatus var. japonica Hara |
| KR20220144197A (en) * | 2021-04-19 | 2022-10-26 | 주식회사 제이에이치 코리아 | Perfume composition using mixed essential oils, Perfume using the same and Preparing method thereof |
| KR102571344B1 (en) | 2023-06-05 | 2023-08-29 | 경상북도(농업기술원 봉화약용작물연구소장) | Perfume composition comprising essential oil of Thymus quinquecostatus var. japonica Hara and aromatic plant and manufacturing method thereof |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20160079608A (en) | 2014-12-26 | 2016-07-06 | 재단법인 홍천메디칼허브연구소 | Composition for anti-inflammation containing an extract of Thymus quinquecostatusvar.japnica Hara |
| KR102075362B1 (en) * | 2017-11-21 | 2020-02-10 | 코스맥스 주식회사 | Apparatus for filtering a perfume and Apparatus for manufacturing a perfume including the same |
| KR102562816B1 (en) * | 2023-03-31 | 2023-08-03 | (주)메르라보 | Perfume composition with excellent durability and manufacturing method thereof |
| KR102562820B1 (en) * | 2023-03-31 | 2023-08-03 | (주)메르라보 | Perfume composition with air purifying effect and manufacturing method thereof |
-
2004
- 2004-03-05 KR KR1020040014875A patent/KR100567584B1/en active IP Right Grant
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101072040B1 (en) | 2008-10-20 | 2011-10-10 | (주)아모레퍼시픽 | Perfume composition for expressing the fragrance of Thymus quinquecostatus var. japonica Hara |
| KR20220144197A (en) * | 2021-04-19 | 2022-10-26 | 주식회사 제이에이치 코리아 | Perfume composition using mixed essential oils, Perfume using the same and Preparing method thereof |
| KR102592814B1 (en) * | 2021-04-19 | 2023-10-24 | 주식회사 제이에이치 코리아 | Perfume composition using mixed essential oils, Perfume using the same and Preparing method thereof |
| KR102571344B1 (en) | 2023-06-05 | 2023-08-29 | 경상북도(농업기술원 봉화약용작물연구소장) | Perfume composition comprising essential oil of Thymus quinquecostatus var. japonica Hara and aromatic plant and manufacturing method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20050089452A (en) | 2005-09-08 |
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