KR20220026243A - Flavor and Fragrance composition reproducing rose scent and manufacturing method thereof - Google Patents
Flavor and Fragrance composition reproducing rose scent and manufacturing method thereof Download PDFInfo
- Publication number
- KR20220026243A KR20220026243A KR1020200107037A KR20200107037A KR20220026243A KR 20220026243 A KR20220026243 A KR 20220026243A KR 1020200107037 A KR1020200107037 A KR 1020200107037A KR 20200107037 A KR20200107037 A KR 20200107037A KR 20220026243 A KR20220026243 A KR 20220026243A
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- South Korea
- Prior art keywords
- acetate
- weight
- parts
- scent
- composition
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- 239000000203 mixture Substances 0.000 title claims abstract description 114
- 241000220317 Rosa Species 0.000 title claims abstract description 49
- 239000003205 fragrance Substances 0.000 title claims description 86
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 239000000796 flavoring agent Substances 0.000 title description 7
- 235000019634 flavors Nutrition 0.000 title description 7
- 239000002304 perfume Substances 0.000 claims abstract description 67
- 241000109329 Rosa xanthina Species 0.000 claims abstract description 39
- 235000004789 Rosa xanthina Nutrition 0.000 claims abstract description 39
- 235000016623 Fragaria vesca Nutrition 0.000 claims abstract description 32
- 235000011363 Fragaria x ananassa Nutrition 0.000 claims abstract description 32
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims description 60
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims description 48
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims description 36
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 claims description 30
- HIGQPQRQIQDZMP-DHZHZOJOSA-N Neryl acetate Natural products CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 claims description 28
- HIGQPQRQIQDZMP-UHFFFAOYSA-N geranil acetate Natural products CC(C)=CCCC(C)=CCOC(C)=O HIGQPQRQIQDZMP-UHFFFAOYSA-N 0.000 claims description 28
- MDHYEMXUFSJLGV-UHFFFAOYSA-N phenethyl acetate Chemical compound CC(=O)OCCC1=CC=CC=C1 MDHYEMXUFSJLGV-UHFFFAOYSA-N 0.000 claims description 28
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims description 26
- AOGQPLXWSUTHQB-UHFFFAOYSA-N hexyl acetate Chemical compound CCCCCCOC(C)=O AOGQPLXWSUTHQB-UHFFFAOYSA-N 0.000 claims description 26
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 claims description 24
- JOZKFWLRHCDGJA-UHFFFAOYSA-N citronellol acetate Chemical compound CC(=O)OCCC(C)CCC=C(C)C JOZKFWLRHCDGJA-UHFFFAOYSA-N 0.000 claims description 24
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 24
- NPNUFJAVOOONJE-ZIAGYGMSSA-N β-(E)-Caryophyllene Chemical compound C1CC(C)=CCCC(=C)[C@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-ZIAGYGMSSA-N 0.000 claims description 24
- 239000005792 Geraniol Substances 0.000 claims description 18
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 claims description 18
- 235000000484 citronellol Nutrition 0.000 claims description 18
- 229940113087 geraniol Drugs 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 16
- QUMXDOLUJCHOAY-UHFFFAOYSA-N alpha-methylbenzyl acetate Natural products CC(=O)OC(C)C1=CC=CC=C1 QUMXDOLUJCHOAY-UHFFFAOYSA-N 0.000 claims description 15
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims description 14
- 239000002537 cosmetic Substances 0.000 claims description 14
- NHCQMVNKPJAQJZ-UHFFFAOYSA-N geranyl n-butyrate Natural products CCCCOCC=C(C)CCC=C(C)C NHCQMVNKPJAQJZ-UHFFFAOYSA-N 0.000 claims description 13
- 229940067107 phenylethyl alcohol Drugs 0.000 claims description 13
- NPFVOOAXDOBMCE-UHFFFAOYSA-N trans-3-hexenyl acetate Natural products CCC=CCCOC(C)=O NPFVOOAXDOBMCE-UHFFFAOYSA-N 0.000 claims description 13
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims description 12
- 229940098795 (3z)- 3-hexenyl acetate Drugs 0.000 claims description 12
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 claims description 12
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims description 12
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 claims description 12
- IYYUJCKJSSPXQQ-UHFFFAOYSA-N 2-pyridin-4-yl-1,3-thiazolidin-3-ium-4-carboxylate Chemical compound N1C(C(=O)O)CSC1C1=CC=NC=C1 IYYUJCKJSSPXQQ-UHFFFAOYSA-N 0.000 claims description 12
- NVEQFIOZRFFVFW-UHFFFAOYSA-N 9-epi-beta-caryophyllene oxide Natural products C=C1CCC2OC2(C)CCC2C(C)(C)CC21 NVEQFIOZRFFVFW-UHFFFAOYSA-N 0.000 claims description 12
- JOZKFWLRHCDGJA-LLVKDONJSA-N Citronellyl acetate Natural products CC(=O)OCC[C@H](C)CCC=C(C)C JOZKFWLRHCDGJA-LLVKDONJSA-N 0.000 claims description 12
- 241000134874 Geraniales Species 0.000 claims description 12
- GLZPCOQZEFWAFX-JXMROGBWSA-N Nerol Natural products CC(C)=CCC\C(C)=C\CO GLZPCOQZEFWAFX-JXMROGBWSA-N 0.000 claims description 12
- FAMPSKZZVDUYOS-UHFFFAOYSA-N alpha-Caryophyllene Natural products CC1=CCC(C)(C)C=CCC(C)=CCC1 FAMPSKZZVDUYOS-UHFFFAOYSA-N 0.000 claims description 12
- 235000019445 benzyl alcohol Nutrition 0.000 claims description 12
- NPNUFJAVOOONJE-UHFFFAOYSA-N beta-cariophyllene Natural products C1CC(C)=CCCC(=C)C2CC(C)(C)C21 NPNUFJAVOOONJE-UHFFFAOYSA-N 0.000 claims description 12
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 claims description 12
- 229940117948 caryophyllene Drugs 0.000 claims description 12
- NPNUFJAVOOONJE-UONOGXRCSA-N caryophyllene Natural products C1CC(C)=CCCC(=C)[C@@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-UONOGXRCSA-N 0.000 claims description 12
- NPFVOOAXDOBMCE-PLNGDYQASA-N cis-3-Hexenyl acetate Natural products CC\C=C/CCOC(C)=O NPFVOOAXDOBMCE-PLNGDYQASA-N 0.000 claims description 12
- RRGOKSYVAZDNKR-ARJAWSKDSA-M cis-3-hexenylacetate Chemical compound CC\C=C/CCCC([O-])=O RRGOKSYVAZDNKR-ARJAWSKDSA-M 0.000 claims description 12
- WTEVQBCEXWBHNA-YFHOEESVSA-N citral B Natural products CC(C)=CCC\C(C)=C/C=O WTEVQBCEXWBHNA-YFHOEESVSA-N 0.000 claims description 12
- UFLHIIWVXFIJGU-UHFFFAOYSA-N hex-3-en-1-ol Natural products CCC=CCCO UFLHIIWVXFIJGU-UHFFFAOYSA-N 0.000 claims description 12
- 229930007744 linalool Natural products 0.000 claims description 12
- HIGQPQRQIQDZMP-FLIBITNWSA-N neryl acetate Chemical compound CC(C)=CCC\C(C)=C/COC(C)=O HIGQPQRQIQDZMP-FLIBITNWSA-N 0.000 claims description 12
- ZSBOMYJPSRFZAL-JLHYYAGUSA-N [(2e)-3,7-dimethylocta-2,6-dienyl] butanoate Chemical compound CCCC(=O)OC\C=C(/C)CCC=C(C)C ZSBOMYJPSRFZAL-JLHYYAGUSA-N 0.000 claims description 10
- 229940007550 benzyl acetate Drugs 0.000 claims description 9
- OJISWRZIEWCUBN-UHFFFAOYSA-N geranylnerol Natural products CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CCO OJISWRZIEWCUBN-UHFFFAOYSA-N 0.000 claims description 8
- 239000004480 active ingredient Substances 0.000 claims description 7
- ZKWFMIAGZQACFE-UHFFFAOYSA-N geranylcitronellol Natural products OCCC(C)CCC=C(C)CCC=C(C)CCC=C(C)C ZKWFMIAGZQACFE-UHFFFAOYSA-N 0.000 claims description 6
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 5
- XWRJRXQNOHXIOX-UHFFFAOYSA-N geranylgeraniol Natural products CC(C)=CCCC(C)=CCOCC=C(C)CCC=C(C)C XWRJRXQNOHXIOX-UHFFFAOYSA-N 0.000 claims description 4
- FERIUCNNQQJTOY-UHFFFAOYSA-M Butyrate Chemical compound CCCC([O-])=O FERIUCNNQQJTOY-UHFFFAOYSA-M 0.000 claims description 3
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Natural products CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims description 3
- ZVQUYMKKXHCGGQ-UHFFFAOYSA-N CC(=O)OCC1=CC=CC=C1.OC(=O)CCC1=CC=CC=C1 Chemical compound CC(=O)OCC1=CC=CC=C1.OC(=O)CCC1=CC=CC=C1 ZVQUYMKKXHCGGQ-UHFFFAOYSA-N 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- -1 phenyl Phenyl ethyl Chemical group 0.000 claims description 3
- 241000220223 Fragaria Species 0.000 claims 2
- 244000307700 Fragaria vesca Species 0.000 abstract description 27
- 240000000851 Vaccinium corymbosum Species 0.000 abstract description 8
- 235000003095 Vaccinium corymbosum Nutrition 0.000 abstract description 8
- 235000017537 Vaccinium myrtillus Nutrition 0.000 abstract description 8
- 235000021014 blueberries Nutrition 0.000 abstract description 8
- 241000220324 Pyrus Species 0.000 abstract description 7
- 238000009402 cross-breeding Methods 0.000 abstract description 5
- 235000021017 pears Nutrition 0.000 abstract description 5
- 235000019629 palatability Nutrition 0.000 abstract description 2
- 238000011156 evaluation Methods 0.000 description 7
- 239000004615 ingredient Substances 0.000 description 6
- 239000006071 cream Substances 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 5
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 4
- 239000000341 volatile oil Substances 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 241000402754 Erythranthe moschata Species 0.000 description 3
- 240000009088 Fragaria x ananassa Species 0.000 description 3
- 241000208152 Geranium Species 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000004817 gas chromatography Methods 0.000 description 3
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- 239000006210 lotion Substances 0.000 description 3
- 239000002324 mouth wash Substances 0.000 description 3
- 229940051866 mouthwash Drugs 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 238000002470 solid-phase micro-extraction Methods 0.000 description 3
- 241000894007 species Species 0.000 description 3
- 238000001256 steam distillation Methods 0.000 description 3
- 208000035240 Disease Resistance Diseases 0.000 description 2
- 235000014443 Pyrus communis Nutrition 0.000 description 2
- 244000052585 Rosa centifolia Species 0.000 description 2
- 235000016588 Rosa centifolia Nutrition 0.000 description 2
- 210000002421 cell wall Anatomy 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 239000000686 essence Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000005923 long-lasting effect Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 239000008371 vanilla flavor Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 240000007311 Commiphora myrrha Species 0.000 description 1
- 235000006965 Commiphora myrrha Nutrition 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 241000208150 Geraniaceae Species 0.000 description 1
- 235000007265 Myrrhis odorata Nutrition 0.000 description 1
- 241000745768 Pluchea carolinensis Species 0.000 description 1
- 235000011449 Rosa Nutrition 0.000 description 1
- 244000181025 Rosa gallica Species 0.000 description 1
- 235000009499 Vanilla fragrans Nutrition 0.000 description 1
- 244000263375 Vanilla tahitensis Species 0.000 description 1
- 235000012036 Vanilla tahitensis Nutrition 0.000 description 1
- 229940022663 acetate Drugs 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 239000013040 bath agent Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 1
- 239000011280 coal tar Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002781 deodorant agent Substances 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 239000008269 hand cream Substances 0.000 description 1
- OYPXPMBBXCHKGC-UHFFFAOYSA-N hexyl acetate octanoic acid Chemical compound CCCCCCCC(O)=O.CCCCCCOC(C)=O OYPXPMBBXCHKGC-UHFFFAOYSA-N 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 229940041678 oral spray Drugs 0.000 description 1
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- 239000006072 paste Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
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- 239000002994 raw material Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
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- 238000005063 solubilization Methods 0.000 description 1
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- 229940061368 sonata Drugs 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
- C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Epidemiology (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
장미 향취를 재현하는 향료 조성물 및 이의 제조방법에 관한 것으로, 구체적으로는, 숙성된 배의 향과 블루베리향을 가지는 장미 향취를 재현한 향료 조성물에 관한 것이다. 더욱 구체적으로는, 장미의 신선하고 달콤한향의 향기성분인, 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트(Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나노올(Linalool), 카리오필렌(Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol) 및 제라니올(Geraniol)을 포함하는, 장미 향취를 재현한 향료 조성물에 관한 것이다. The present invention relates to a perfume composition reproducing the scent of roses and a method for preparing the same, and more particularly, to a perfume composition reproducing the scent of roses having a scent of aged pears and a scent of blueberries. More specifically, hexyl acetate, cis-3-hexenol, and cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol, benzyl acetate, phenyl ethyl alcohol, phenyl ethyl acetate, linalool, caryophyllene, citro Citronellyl acetate, Neral, Neryl acetate, Geranial, Geranyl acetate, Citronellol, Nerol and Geraniol ( Geraniol), which relates to a perfume composition that reproduces the scent of roses.
장미는 18세기 말에 아시아의 각 원종이 유럽에 도입되고 이들 유럽과 아시아 원종간의 교배가 이루어져 화색이나 화형은 물론 사계성이나 개화성 등 생태적으로 변화가 많은 품종들이 만들어졌다. 1867년 라 프랑스(La France)품종이 개발되기 이전을 고전장미(old rose), 이후를 현대장미(modern rose)라 한다. 장미의 향기는 「꽃 중의 꽃」이라 칭찬받을 만큼 우수한 향기로, 수천년 전부터 각종 형태로 사용되어 왔다. 화장료 조성물 등에 있어서, 천연의 장미(꽃잎)에서 추출한 천연 로즈 정유를 배합하여 사용되어 왔다. 이와 같이 천연 로즈 정유는, 기원전부터 향기를 즐길 목적으로 사용되었고, 이 외에도 약용으로 사용되어 왔다. 천연 로즈 정유는 고대 로사 다마세나(Rosa damascena) 또는 로사 센티폴리아(Rosa centifolia) 등의 꽃잎에서 추출되고 있다. As for the rose, each native species from Asia was introduced to Europe at the end of the 18th century, and crossbreeding between these European and Asian native species produced varieties with many ecological changes such as flower color and flower shape as well as four seasons and flowering. Before the La France variety was developed in 1867, the old rose is called the old rose, and after that, the modern rose. The fragrance of roses has been used in various forms for thousands of years since it is an excellent fragrance that is praised as “the flower of flowers”. In cosmetic compositions, etc., natural rose essential oil extracted from natural roses (petals) has been mixed and used. As such, natural rose essential oil has been used for the purpose of enjoying the fragrance since BC, and has been used for medicinal purposes in addition to this. Natural rose essential oil is extracted from the petals of ancient Rosa damascena or Rosa centifolia .
한편, 장미는 로사 다마세나 또는 로사 센티폴리아 등의 고전장미(old rose)를 베이스로, 그 후, 원종간의 자연교잡과 더불어, 감상용으로 우수한 품종을 만들어 내기 위해 19세기 이후의 활발한 인공교잡에 의해, 품종의 수가 2만 종에 이르도록 폭발적으로 증가하였고 이에 수반하여 장미의 향기에도 변화가 생기고 있다. On the other hand, roses are based on old roses such as Rosa damacena or Rosa centifolia, and then, along with natural crossbreeding between original species, active artificial crossbreeding since the 19th century to create excellent varieties for appreciation. , the number of varieties has increased explosively to 20,000, and the fragrance of roses is also changing.
장미 향기를 재현하기 위해 한국 등록특허 제10-1470062호에서 로즈 향기를 가지는 향료 조성물을 제공하지만, 이와 달리, 본 발명은 장미 품종 중 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하고자 하는 것이다.In order to reproduce the fragrance of roses, Korean Patent Registration No. 10-1470062 provides a fragrance composition having a rose fragrance, but in contrast to this, the present invention crosses Candlelight and Strawberry Hill among rose varieties. It is intended to reproduce the scent of the obtained rose.
본 발명자들은 장미 품종 중 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하고자 하였다. The present inventors tried to reproduce the scent of a rose obtained by crossing Candlelight and Strawberry Hill among rose varieties.
본 발명의 목적은 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물로서, 상기 향료 조성물은 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트(Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌 (Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol) 및 제라니올(Geraniol)을 포함하는, 장미 향취를 재현하는 향료 조성물을 제공하는 것이다.It is an object of the present invention to provide a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill, wherein the perfume composition comprises hexyl acetate, cis-3-hexenol ( c-3-Hexenol), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol, benzyl acetate, phenyl ethyl alcohol, phenyl ethyl acetate ( Phenyl ethyl acetate), Linalool, Caryophyllene, Citronellyl acetate, Neral, Neryl acetate, Geranial, Geranyl acetate ( Geranyl acetate), citronellol (Citronellol), including nerol (Nerol) and geraniol (Geraniol), to provide a perfume composition for reproducing the scent of roses.
본 발명의 다른 목적은 상기 향료 조성물을 포함하는 화장료 조성물을 제공하는 것이다.Another object of the present invention is to provide a cosmetic composition comprising the perfume composition.
본 발명의 다른 목적은 상기 향료 조성물을 포함하는 방향제 조성물을 제공하는 것이다.Another object of the present invention is to provide a perfume composition comprising the perfume composition.
본 발명의 다른 목적은 상기 향료 조성물을 포함하는 피부 외용제 조성물을 제공하는 것이다. Another object of the present invention is to provide a composition for external application to the skin comprising the perfume composition.
본 발명의 다른 목적은 상기 향료 조성물을 제조하는 방법을 제공하는 것이다. Another object of the present invention is to provide a method for preparing the perfume composition.
그러나, 본 발명이 해결하고자 하는 과제는 이상에서 언급한 과제로 제한되지 않으며, 언급되지 않은 또 다른 과제들은 아래의 기재로부터 해당 기술분야의 통상의 지식을 가진 자에게 명확하게 이해될 수 있을 것이다.However, the problems to be solved by the present invention are not limited to the problems mentioned above, and other problems not mentioned will be clearly understood by those of ordinary skill in the art from the following description.
본 발명의 향료 조성물에 의하면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 천연 장미의 향, 특히 숙성된 배의 향과 블루베리향을 재현할 수 있다. 또한, 본 발명의 향료 조성물에 의하면, 향의 강도와 선호도가 높으며, 향이 오래 지속되는 효과를 나타내므로 향료 조성물, 화장료 조성물, 방향제 조성물 및 피부 외용제 조성물로 유용하게 사용할 수 있다.According to the perfume composition of the present invention, it is possible to reproduce the scent of natural roses obtained by crossing Candlelight and Strawberry Hill, in particular, the scent of aged pears and blueberry scent. In addition, according to the perfume composition of the present invention, the strength and preference of the fragrance is high, and since the fragrance exhibits a long-lasting effect, it can be usefully used as a fragrance composition, a cosmetic composition, a fragrance composition, and a composition for external application to the skin.
본 발명의 효과는 상기한 효과로 한정되는 것은 아니며, 본 발명의 상세한 설명 또는 청구범위에 기재된 발명의 구성으로부터 추론 가능한 모든 효과를 포함하는 것으로 이해되어야 한다.It should be understood that the effects of the present invention are not limited to the above-described effects, and include all effects that can be inferred from the configuration of the invention described in the detailed description or claims of the present invention.
도 1은 캔들라이트(Candlelight)를 모본으로 하고 스트로베리 힐(Strawberry Hill)을 부본으로 교배하여 얻은 장미의 특성을 나타낸다.
도 2는 본 발명의 일 실시예에 따라 향료 조성물을 제조하고 향료 조성물을 포함하는 화장료 조성물, 방향제 조성물, 피부 외용제 조성물을 제조하는 단계를 나타낸다.
도 3은 본 발명의 일 실시예에 따라 재현된 향의 종류와 강도를 나타낸다.1 shows the characteristics of a rose obtained by crossing Candlelight as a model and Strawberry Hill as a parent.
2 shows the steps of preparing a perfume composition according to an embodiment of the present invention, and preparing a cosmetic composition, a perfume composition, and a composition for external application for skin including the perfume composition.
3 shows the type and intensity of incense reproduced according to an embodiment of the present invention.
이하에서, 첨부된 도면을 참조하여 실시예들을 상세하게 설명한다. 그러나, 실시예들에는 다양한 변경이 가해질 수 있어서 특허출원의 권리 범위가 이러한 실시예들에 의해 제한되거나 한정되는 것은 아니다. 실시예들에 대한 모든 변경, 균등물 내지 대체물이 권리 범위에 포함되는 것으로 이해되어야 한다.Hereinafter, embodiments will be described in detail with reference to the accompanying drawings. However, since various changes may be made to the embodiments, the scope of the patent application is not limited or limited by these embodiments. It should be understood that all modifications, equivalents and substitutes for the embodiments are included in the scope of the rights.
실시예에서 사용한 용어는 단지 설명을 목적으로 사용된 것으로, 권리 범위를 한정하려는 의도로 해석되어서는 안된다. 단수의 표현은 문맥상 명백하게 다르게 뜻하지 않는 한, 복수의 표현을 포함한다. 본 명세서에서, "포함하다" 또는 "가지다" 등의 용어는 명세서 상에 기재된 특징, 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것이 존재함을 지정하려는 것이지, 하나 또는 그 이상의 다른 특징들이나 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것들의 존재 또는 부가 가능성을 미리 배제하지 않는 것으로 이해되어야 한다.The terms used in the examples are used for description purposes only, and should not be construed as limiting the scope of rights. The singular expression includes the plural expression unless the context clearly dictates otherwise. In this specification, terms such as "comprise" or "have" are intended to designate that a feature, number, step, operation, component, part, or a combination thereof described in the specification exists, but one or more other features It should be understood that this does not preclude the existence or addition of numbers, steps, operations, components, parts, or combinations thereof.
다르게 정의되지 않는 한, 기술적이거나 과학적인 용어를 포함해서 여기서 사용되는 모든 용어들은 실시예가 속하는 기술 분야에서 통상의 지식을 가진 자에 의해 일반적으로 이해되는 것과 동일한 의미를 가지고 있다. 일반적으로 사용되는 사전에 정의되어 있는 것과 같은 용어들은 관련 기술의 문맥 상 가지는 의미와 일치하는 의미를 가지는 것으로 해석되어야 하며, 본 출원에서 명백하게 정의하지 않는 한, 이상적이거나 과도하게 형식적인 의미로 해석되지 않는다.Unless defined otherwise, all terms used herein, including technical or scientific terms, have the same meaning as commonly understood by one of ordinary skill in the art to which the embodiment belongs. Terms such as those defined in commonly used dictionaries should be interpreted as having a meaning consistent with the meaning in the context of the related art, and should not be interpreted in an ideal or excessively formal meaning unless explicitly defined in the present application. does not
또한, 첨부 도면을 참조하여 설명함에 있어, 도면 부호에 관계없이 동일한 구성 요소는 동일한 참조부호를 부여하고 이에 대한 중복되는 설명은 생략하기로 한다. 실시예를 설명함에 있어서 관련된 공지 기술에 대한 구체적인 설명이 실시예의 요지를 불필요하게 흐릴 수 있다고 판단되는 경우 그 상세한 설명을 생략한다.In addition, in the description with reference to the accompanying drawings, the same components are given the same reference numerals regardless of the reference numerals, and the overlapping description thereof will be omitted. In describing the embodiment, if it is determined that a detailed description of a related known technology may unnecessarily obscure the gist of the embodiment, the detailed description thereof will be omitted.
또한, 실시 예의 구성 요소를 설명하는 데 있어서, 제1, 제2, A, B, (a), (b) 등의 용어를 사용할 수 있다. 이러한 용어는 그 구성 요소를 다른 구성 요소와 구별하기 위한 것일 뿐, 그 용어에 의해 해당 구성 요소의 본질이나 차례 또는 순서 등이 한정되지 않는다.In addition, in describing the components of the embodiment, terms such as first, second, A, B, (a), (b), etc. may be used. These terms are only for distinguishing the elements from other elements, and the essence, order, or order of the elements are not limited by the terms.
어느 하나의 실시 예에 포함된 구성요소와, 공통적인 기능을 포함하는 구성요소는, 다른 실시 예에서 동일한 명칭을 사용하여 설명하기로 한다. 반대되는 기재가 없는 이상, 어느 하나의 실시 예에 기재한 설명은 다른 실시 예에도 적용될 수 있으며, 중복되는 범위에서 구체적인 설명은 생략하기로 한다.Components included in one embodiment and components having a common function will be described using the same names in other embodiments. Unless otherwise stated, descriptions described in one embodiment may be applied to other embodiments as well, and detailed descriptions within the overlapping range will be omitted.
본 발명의 일 실시예에 따르면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물로서, 상기 향료 조성물은 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트(Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌 (Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol) 및 제라니올(Geraniol)을 포함하는, 장미 향취를 재현하는 향료 조성물이 제공된다.According to one embodiment of the present invention, there is provided a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill, wherein the perfume composition includes hexyl acetate, cis-3 -Hexenol (c-3-Hexenol), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol (Benzyl alcohol), benzyl acetate (Benzyl acetate), phenyl ethyl alcohol (Phenyl ethyl alcohol), Phenyl ethyl acetate, Linalool, Caryophyllene, Citronellyl acetate, Neral, Neryl acetate, Geranial, There is provided a perfume composition for reproducing the scent of roses, including geranyl acetate, citronellol, nerol, and geraniol.
본 발명의 일 실시예에 따르면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물에 있어서, 상기 향료 조성물 총 중량부에 대하여, 헥실 아세테이트(Hexyl acetate) 20 ~ 30 중량부, 시스-3-헥센올(c-3-Hexenol) 1 ~ 10 중량부, 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate) 1 ~ 10 중량부, 벤질알코올(Benzyl alcohol) 1~ 10 중량부, 벤질아세테이트(Benzyl acetate) 0.01 ~ 1 중량부, 페닐에틸알코올(Phenyl ethyl alcohol) 10 ~ 20 중량부, 페닐에틸아세테이트(Phenyl ethyl acetate) 1 ~ 10 중량부, 리나로올(Linalool) 1 ~ 5 중량부, 카리오필렌(Caryophyllene) 1 ~ 5 중량부, 시트로넬릴아세테이트(Citronellyl acetate) 1 ~ 5 중량부, 네랄(Neral) 0.01 ~ 1 중량부, 네릴 아세테이트(Neryl acetate) 0.01 ~ 1 중량부, 제라니알(Geranial) 0.01 ~ 1 중량부, 제라닐 아세테이트(Geranyl acetate) 10 ~ 20 중량부, 시트로넬롤(Citronellol) 0.01 ~ 1 중량부, 네롤(Nerol) 1 ~ 10 중량부 및 제라니올(Geraniol) 10 ~ 20 중량부를 포함하는, 장미 향취를 재현하는 향료 조성물이 제공된다.According to one embodiment of the present invention, in a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill, based on the total weight of the perfume composition, hexyl acetate (Hexyl acetate) 20-30 parts by weight, cis-3-hexenol (c-3-Hexenol) 1-10 parts by weight, cis-3-hexenyl acetate (c-3-Hexenyl acetate) 1-10 parts by weight, benzyl alcohol (Benzyl alcohol) 1 to 10 parts by weight, Benzyl acetate 0.01 to 1 parts by weight, Phenyl ethyl alcohol 10 to 20 parts by weight,
본 발명의 일 실시예에 따르면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물에 있어서, 제라닐 부티레이트(Geranyl butyrate) 또는 시트로넬롤 부티레이트(Citronellyl butyrate) 중 어느 하나를 더 포함하는, 장미 향취를 재현하는 향료 조성물이 제공된다.According to an embodiment of the present invention, in a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill, geranyl butyrate or citronellol butyrate ( Citronellyl butyrate) further comprising any one of, is provided a perfume composition that reproduces the scent of roses.
본 발명의 일 실시예에 따르면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물에 있어서, 상기 향료 조성물 총 중량부에 대하여, 제라닐 부티레이트(Geranyl butyrate) 0.01 ~ 1 중량부 또는 시트로넬롤 부티레이트(Citronellyl butyrate) 0.01 ~ 1 중량부를 더 포함하는, 장미 향취를 재현하는 향료 조성물이 제공된다.According to an embodiment of the present invention, in a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill, geranyl butyrate ( Geranyl butyrate) 0.01 to 1 parts by weight or citronellyl butyrate (Citronellyl butyrate) 0.01 to 1 parts by weight, further comprising a perfume composition that reproduces the scent of roses is provided.
본 발명의 일 실시예에 따르면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물을 유효성분으로 포함하는, 화장료 조성물이 제공된다. According to one embodiment of the present invention, there is provided a cosmetic composition comprising, as an active ingredient, a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill.
본 발명의 일 실시예에 따르면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물을 유효성분으로 포함하는, 방향제 조성물이 제공된다.According to one embodiment of the present invention, there is provided a perfume composition comprising, as an active ingredient, a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill.
본 발명의 일 실시예에 따르면, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물을 유효성분으로 포함하는, 피부 외용제 조성물이 제공된다.According to one embodiment of the present invention, there is provided a composition for external application to the skin comprising, as an active ingredient, a perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill.
본 발명의 다른 일 실시예에 따르면, 캔들라이트와 스트로베리 힐을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물의 제조방법으로, 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트 (Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌(Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol), 제라니올(Geraniol), 제라닐 부티레이트(Geranyl butyrate) 및 시트로넬롤 부티레이트(Citronellyl butyrate)을 혼합하는 단계; 및 상기 혼합물을 여과하는 단계를 포함하는, 장미 향취를 재현하는 향료 조성물의 제조방법이 제공된다.According to another embodiment of the present invention, there is provided a method for preparing a perfume composition that reproduces the scent of a rose obtained by crossing candlelight and strawberry hill, hexyl acetate, cis-3-hexenol (c-3). -Hexenol), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol, benzyl acetate, phenyl ethyl alcohol, phenyl ethyl acetate ), Linalool, Caryophyllene, Citronellyl acetate, Neral, Neryl acetate, Geranial, Geranyl acetate , mixing citronellol (Citronellol), nerol (Nerol), geraniol (Geraniol), geranyl butyrate and citronellyl butyrate; And there is provided a method for producing a perfume composition for reproducing the scent of roses, comprising the step of filtering the mixture.
본 발명에 따른 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미의 향취를 재현하는 향료 조성물은, 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트(Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌 (Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol) 및 제라니올(Geraniol)을 포함할 수 있다.A perfume composition for reproducing the scent of a rose obtained by crossing Candlelight and Strawberry Hill according to the present invention is hexyl acetate, cis-3-hexenol (c-3-Hexenol) ), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol, benzyl acetate, phenyl ethyl alcohol, phenyl ethyl acetate, Linalool, Caryophyllene, Citronellyl acetate, Neral, Neryl acetate, Geranial, Geranyl acetate, sheet ronellol (Citronellol), nerol (Nerol) and geraniol (Geraniol) may be included.
본 발명에 있어서, "향취"는 오취의 하나로서, 향기로우면서 약간 고소한 냄새로 코로 들어가는 냄새를 말한다.In the present invention, "fragrance" refers to a smell that enters the nose with a fragrant and slightly fragrant smell as one of the five odors.
상기 향기성분은 수증기 증류법, 용매추출법, SPME(solid phase micro extraction)등을 이용하여 분석할 수 있다.The fragrance component may be analyzed using steam distillation, solvent extraction, solid phase micro extraction (SPME), or the like.
수증기 증류법(steam distillation)은 가장 기본적이고 과거로부터 널리 사용되어 오는 에센셜 오일의 추출법으로 뜨거운 물이나 수증기를 이용하여 식물의 세포벽을 깨고 오일을 추출하는 방법을 말한다. 일정 온도 이상이 되면 식물의 세포벽이 깨어져 향기 물질이 증발되는데, 이 증발된 향기물질을 다시 냉각시키면 액체 상태의 오일을 얻을 수 있다. 수증기 증류법은 고온에서 일부 열에 불안정한 성분이 파괴된다는 단점이 있으나 대량으로 오일을 얻어 낼 수 있어 많이 사용되고 있다.Steam distillation is the most basic and widely used essential oil extraction method from the past. It refers to a method of extracting oil by breaking the cell wall of a plant using hot water or steam. When the temperature is higher than a certain temperature, the cell wall of the plant is broken and the fragrance material is evaporated. If the evaporated fragrance material is cooled again, liquid oil can be obtained. The steam distillation method has the disadvantage that some heat-unstable components are destroyed at high temperatures, but it is widely used because it can obtain a large amount of oil.
용매 추출법(solvent extraction)은 헥산(hexane)과 같은 휘발성 유기용매에 식물의 꽃을 일정시간 냉암소에서 침적시킨 후 향기성분을 녹여내는 방법으로, 자스민, 장미 오일 같은 오일의 함량이 매우 적은 식물에서 향을 효율적으로 추출가능하나, 공정이 복잡하고 시간이 많이 소요되며 비용이 많이 드는 단점이 있다.Solvent extraction is a method of immersing plant flowers in a volatile organic solvent such as hexane for a certain period of time in a cool and dark place and then dissolving the fragrance. The fragrance can be efficiently extracted, but the process is complex, time-consuming, and expensive.
SPME법은 GC(Gas chromatography)용 실린지에 내재된 흡착제에 향기성분을 직접 흡착, 농축, 추출하는 방법이다. 유기용매를 사용하지 않고 적은 양의 시료로 간단하게 전처리 할 수 있으며, 휘발성이 약한 향기성분의 분석이 가능하여 점차 활용빈도가 높아지고 있다.The SPME method is a method of directly adsorbing, concentrating, and extracting fragrance components to the adsorbent contained in a syringe for GC (gas chromatography). It can be simply pre-treated with a small amount of sample without using an organic solvent, and it is possible to analyze fragrance components with weak volatility, so the frequency of use is gradually increasing.
본 발명의 “장미 향취”는 캔들라이트(Candlelight)를 모본으로 하고 스트로베리 힐(Strawberry Hill)을 부본으로 교배하여 얻은 장미의 향취일 수 있다. 상기 “장미 향취”는 캔들라이트와 스트로베리 힐을 교배하여 얻은 장미의 향취로서, 구미를 당기는 달콤한 장미향과 신선하고 달콤한 향들이 어우러져 감출 수 없는 화려함을 지닌 플로럴향을 포함하고, 숙성된 배의 향과 블루베리의 향의 달콤함이 코 끝을 간지럽히고, 장미와 제라늄의 향이 더해져 잔잔한 삶의 소나타를 연주해주는 향일 수 있다. The "scent of roses" of the present invention may be the scent of roses obtained by crossing Candlelight as a model and Strawberry Hill as a parent. The “scent of rose” above is the scent of roses obtained by crossing Candlelight and Strawberry Hill, and includes a floral scent that cannot be hidden by a combination of sweet rose scent that attracts taste and fresh and sweet scent, It may be a fragrance that tickles the tip of the nose with the sweetness of the fragrance and blueberry, and plays the sonata of a calm life with the fragrance of roses and geraniums.
상기 캔들라이트는 장미 품종 중 하나로 꽃의 색이 다양하고 은은한 향기를 내며 26 내지 40개의 초대형의 노란색 꽃잎을 피운다. 가지마다 신초에서 계속적으로 꽃이 피는 습성이 있다. The candlelight is one of the rose varieties, and the flowers have various colors and have a delicate fragrance, and 26 to 40 extra-large yellow petals bloom. Each branch has a habit of continuously blooming from a new shoot.
상기 스트로베리 힐은 장미 품종 중 하나로 연속개화성이 좋으며 꽃이 크고 가지가 잘 생기는 특징이 있다. 향기가 강하고 그 중에서 몰약향이 강한 특성이 있다. The Strawberry Hill is one of the rose varieties and has good continuous flowering and large flowers and good branching. It has a strong scent, and among them, there is a strong myrrh scent.
도 1을 참조하면, 교배된 장미의 특성 중 꽃크기, 연속개화성, 꽃잎수, 수세, 향기, 내한성, 다화성 및 내병성을 수치화하여 매우 약함(1), 약함(2), 중간(3), 강함(4), 매우 강함(5)로 표시하였다. 상기 캔들라이트와 스트로베리 힐을 교배하여 얻은 장미는 강한 달콤한 향을 지닌 정원장미로서 향기가 강하고, 꽃잎 수가 매우 많고 향과 연속개화성 및 내병성이 강한 특성이 있다. 캔들라이트와 스트로베리 힐을 교배하여 얻는 장미의 향은 달콤한 향기를 풍기며 춤을 추고 있는 신부의 드레스를 연상하게 하는 향이다.Referring to FIG. 1, among the characteristics of crossed roses, flower size, continuous flowering, number of petals, number, fragrance, cold resistance, multiplicity, and disease resistance are quantified to be very weak (1), weak (2), medium (3), Strong (4) and very strong (5) were indicated. The rose obtained by crossing the Candlelight and Strawberry Hill is a garden rose with a strong sweet fragrance. It has a strong fragrance, a very large number of petals, and a strong fragrance, continuous flowering and disease resistance. The scent of roses obtained by crossing Candlelight and Strawberry Hill is a scent reminiscent of a dancing bride's dress with a sweet fragrance.
상기 캔들라이트와 스트로베리 힐을 교배하여 얻은 장미는 숙성된 배의 향과 블루베리향 등을 가지는 특성이 있다. 상기 캔들라이트와 상기 스트로베리 힐을 교배하여 얻은 장미는 장미(rose)향, 제라늄(geranium)향, 머스크(musk)향, 엠버(amber)향, 바닐라(vanilla)향을 더 가질 수 있다. The rose obtained by crossing the Candlelight and Strawberry Hill has the characteristic of having the aroma of matured pears and the aroma of blueberries. The rose obtained by crossing the candlelight and the strawberry hill may further have a rose scent, a geranium scent, a musk scent, an amber scent, and a vanilla scent.
상기 캔들라이트와 스트로베리 힐을 교배하여 얻은 장미 향취를 재현한 향료 조성물은 탑 노트(top note)로 배의향과 블루베리향을 가지고, 미들 노트(middle note)로 장미향, 제라늄향을 가지며, 베이스 노트(base note)로 머스크향, 엠버향, 바닐라향을 가질 수 있다. 캔들라이트와 스트로베리 힐을 교배하여 얻은 장미 향취를 재현하는 것이라면, 상기 향에 한정되지 않는다.The perfume composition reproducing the scent of roses obtained by crossing the candlelight and strawberry hill has a pear scent and blueberry scent as a top note, and a rose scent and a geranium scent as a middle note, and a base As a base note, you can have musk, amber, and vanilla flavors. As long as it reproduces the scent of roses obtained by crossing Candlelight and Strawberry Hill, the present invention is not limited to the above scent.
본 발명에 따른 향료 조성물은, 상기 향료 조성물 총 중량부에 대하여, 헥실 아세테이트(Hexyl acetate) 20 ~ 30 중량부, 시스-3-헥센올(c-3-Hexenol) 1 ~ 10 중량부, 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate) 1 ~ 10 중량부, 벤질알코올(Benzyl alcohol) 1~ 10 중량부, 벤질아세테이트(Benzyl acetate) 0.01 ~ 1 중량부, 페닐에틸알코올(Phenyl ethyl alcohol) 10 ~ 20 중량부, 페닐에틸아세테이트(Phenyl ethyl acetate) 1 ~ 10 중량부, 리나로올(Linalool) 1 ~ 5 중량부, 카리오필렌(Caryophyllene) 1 ~ 5 중량부, 시트로넬릴아세테이트(Citronellyl acetate) 1 ~ 5 중량부, 네랄(Neral) 0.01 ~ 1 중량부, 네릴 아세테이트(Neryl acetate) 0.01 ~ 1 중량부, 제라니알(Geranial) 0.01 ~ 1 중량부, 제라닐 아세테이트(Geranyl acetate) 10 ~ 20 중량부, 시트로넬롤(Citronellol) 0.01 ~ 1 중량부, 네롤(Nerol) 1 ~ 10 중량부 및 제라니올(Geraniol) 10 ~ 20 중량부를 포함할 수 있다.The perfume composition according to the present invention, based on the total weight of the perfume composition, 20 to 30 parts by weight of hexyl acetate, 1 to 10 parts by weight of cis-3-hexenol (c-3-Hexenol), cis- 3-Hexenyl acetate (c-3-Hexenyl acetate) 1 to 10 parts by weight,
본 발명에 따른 향료 조성물은, 제라닐 부티레이트(Geranyl butyrate) 또는 시트로넬롤 부티레이트(Citronellyl butyrate) 중 어느 하나를 더 포함할 수 있다.The perfume composition according to the present invention may further include any one of geranyl butyrate and citronellyl butyrate.
본 발명에 따른 향료 조성물은, 상기 향료 조성물 총 중량부에 대하여, 제라닐 부티레이트(Geranyl butyrate) 0.01 ~ 1 중량부 또는 시트로넬롤 부티레이트(Citronellyl butyrate) 0.01 ~ 1 중량부를 더 포함할 수 있다.The perfume composition according to the present invention may further include 0.01 to 1 part by weight of geranyl butyrate or 0.01 to 1 part by weight of citronellyl butyrate, based on the total weight of the perfume composition.
본 발명에 따른 향료 조성물의 성분 중에서, 헥실 아세테이트, 제라닐아세테이트 또는 페닐에틸아세테이트는, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 천연 장미의 향을 재현하기 위한 필수 성분이다. 상기 헥실 아세테이트, 제라닐아세테이트, 페닐에틸아세테이트를 상기 범위를 벗어난 범위로 사용할 경우, 교배하여 얻은 장미의 향취와의 유사성이 낮아지고, 향취의 기호성도 낮아지므로 바람직하지 않다. 그 외의 성분들은 상기 범위 내에서 사용하는 것이 바람직하지만, 교배하여 얻은 장미 향취 재현에 크게 영향을 미치지 않기 때문에, 상기 향취를 재현하는데 영향을 미치지 않는 한, 상기 범위를 벗어나는 양으로도 함유될 수 있다.Among the ingredients of the perfume composition according to the present invention, hexyl acetate, geranyl acetate or phenylethyl acetate is an essential ingredient for reproducing the scent of a natural rose obtained by crossing Candlelight and Strawberry Hill. . When the hexyl acetate, geranyl acetate, and phenylethyl acetate are used outside the above range, the similarity with the scent of a rose obtained by crossing is lowered, and the palatability of the scent is also lowered, so it is not preferable. Other ingredients are preferably used within the above range, but since they do not significantly affect the reproduction of the scent of roses obtained by crossing, they may be contained in amounts outside the above range as long as they do not affect reproduction of the scent. .
본 발명에 따른 향료 조성물을 유효성분으로 포함하는, 화장료 조성물, 방향제 조성물, 피부 외용제 조성물이 제공된다.There is provided a cosmetic composition, a fragrance composition, and a composition for external application to the skin, comprising the fragrance composition according to the present invention as an active ingredient.
본 발명에 있어서, "향료"는 화장품, 식료품 등의 생활용품에 향기를 가하기 위해 첨가하는 향기가 강한 유기물질로서, 상온에서 휘발성이 우수하다. 향료는 장미·레몬 등에서 얻는 천연향료, 천연향료·콜타르 등의 원료로부터 분리·정제한 단리향료, 화학반응을 거쳐 합성시킨 합성향료 등으로 크게 구분할 수 있다. 단리향료와 합성향료를 합하여 인조향료라고도 한다. 용도별로는 화장품 향료와 식품 향료로 크게 구분할 수 있는데, 화장품향료는 단지 향기 부여를 목적으로 하지만 식품향료는 냄새에 맛을 가미한 플레이버(flavor)를 주체로 한다. In the present invention, "fragrance" is an organic material with strong fragrance added to add fragrance to household products such as cosmetics and food, and has excellent volatility at room temperature. Fragrances can be broadly classified into natural fragrances obtained from roses and lemons, isolated fragrances separated and refined from raw materials such as natural fragrances and coal tar, and synthetic fragrances synthesized through chemical reaction. It is also called artificial fragrance by combining isolated fragrances and synthetic fragrances. By use, they can be broadly divided into cosmetic fragrances and food fragrances. Cosmetic fragrances are only used to impart a fragrance, whereas food fragrances mainly use flavors that add flavor to odors.
본 발명의 향료 조성물은 장미의 향취를 재현하는 향료 조성물로서, 향의 강도와 선호도가 높으며, 향이 오래 지속되는 효과를 나타내므로 향료 조성물, 화장료 조성물, 방향제 조성물 및 피부 외용제 조성물로 유용하게 사용할 수 있다.The fragrance composition of the present invention is a fragrance composition that reproduces the fragrance of a rose, has high fragrance strength and preference, and exhibits a long-lasting effect, so it can be usefully used as a fragrance composition, a cosmetic composition, a fragrance composition, and a composition for external application to the skin .
본 발명의 향료 조성물은 화장료 조성물, 방향제 조성물, 피부 외용제 조성물 등에 발향을 위하여 적용할 수 있다. The perfume composition of the present invention can be applied to a cosmetic composition, a perfume composition, a composition for external application for skin, and the like for scent diffusion.
본 발명의 향료 조성물은 스킨, 로션, 에센스, 화장수, 젤, 영양크림, 마사지 크림, 핸드 크림, 풋 크림, 파운데이션, 메이크업 베이스, 헤어크림, 헤어토닉, 헤어컨디셔너, 헤어트리트먼트, 헤어스타일링젤, 입욕제, 액체세안제, 비누 또는 샴푸 등의 화장료 조성물로 제공될 수 있으며, 향료 조성물이 적용될 수 있는 물품이라면, 상기에 한정되지 않는다.The perfume composition of the present invention includes skin, lotion, essence, lotion, gel, nourishing cream, massage cream, hand cream, foot cream, foundation, makeup base, hair cream, hair tonic, hair conditioner, hair treatment, hair styling gel, It may be provided as a cosmetic composition such as a bath agent, liquid cleanser, soap or shampoo, and is not limited thereto, as long as it is an article to which the perfume composition can be applied.
본 발명의 향료 조성물은 향수, 방향제, 소취제, 디퓨저 또는 아로마캔들 등의 방향제 조성물로 제공될 수 있다.The perfume composition of the present invention may be provided as a perfume composition such as a perfume, a perfume, a deodorant, a diffuser or an aroma candle.
본 발명의 향료 조성물은 연고, 로션, 가용화상, 현탁액, 에멀젼, 크림, 젤, 스프레이, 파프제, 경고제, 패치제 또는 물파스 등의 피부 외용제 조성물로 제공될 수 있다.The perfume composition of the present invention may be provided as a composition for external application to the skin, such as ointment, lotion, solubilization, suspension, emulsion, cream, gel, spray, patch, warning agent, patch, or water paste.
본 발명의 향료 조성물은 가글액, 치약, 치실, 구강 스프레이, 구강 세정제, 구강청결용 물휴지 등의 구강용 조성물로 제공될 수 있다. 이때 상기 조성물들은 물성 개선을 위하여 통상적으로 허용 가능한 색소, 살균제, 방부제, 산화 방지제, 보습제, 점증제 등을 추가로 포함할 수 있다. 또한 구강용 조성물로 제공 시 일부 향기성분 및 추가 성분에 대하여 구강용으로 허용된 성분으로 대체 가능하다.The perfume composition of the present invention may be provided as a composition for oral use, such as mouthwash, toothpaste, dental floss, oral spray, mouthwash, and mouthwash. In this case, the compositions may further include a commonly acceptable colorant, bactericide, preservative, antioxidant, humectant, thickener, and the like to improve physical properties. In addition, when provided as a composition for oral use, it is possible to replace some fragrance ingredients and additional ingredients with ingredients permitted for oral use.
본 발명에 따른 향료 조성물 제조방법은, 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트 (Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌(Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol), 제라니올(Geraniol), 제라닐 부티레이트(Geranyl butyrate) 및 시트로넬롤 부티레이트(Citronellyl butyrate)을 혼합하는 단계; 및 상기 혼합물을 여과하는 단계를 포함할 수 있다.The perfume composition preparation method according to the present invention includes hexyl acetate, cis-3-hexenol (c-3-Hexenol), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol ( Benzyl alcohol), Benzyl acetate, Phenyl ethyl alcohol, Phenyl ethyl acetate, Linalool, Caryophyllene, Citronellyl acetate , Neral, Neryl acetate, Geranial, Geranyl acetate, Citronellol, Nerol, Geraniol, Geranyl Butyrate (Geranyl butyrate) and citronellol butyrate (Citronellyl butyrate) mixing; and filtering the mixture.
도 2를 참조하면, 본 발명의 일 실시예에 따라 향료 조성물을 제조하고 향료 조성물을 포함하는 화장료 조성물, 방향제 조성물 및 피부 외용제 조성물을 제조하는 단계를 나타낸다. Referring to FIG. 2 , it shows the steps of preparing a fragrance composition according to an embodiment of the present invention, and preparing a cosmetic composition, a fragrance composition, and a composition for external application for skin including the fragrance composition.
도 3을 참조하면, 본 발명의 일 실시예에 따라 제조된 향료 조성물은 탑 노트(top note)로 배의향과 블루베리향을 가지고, 미들 노트(middle note)로 장미향, 제라늄향을 가지며, 베이스 노트(base note)로 머스크향, 엠버향, 바닐라향을 가질 수 있다. 다만, 상기 향에 제한되지 않는다. 다만, 본 발명의 일 실시예에 따라 제조된 향료 조성물의 향은 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미 향취를 재현하는 것이라면 상기 향에 한정되지 않는다.Referring to FIG. 3 , the perfume composition prepared according to an embodiment of the present invention has pear flavor and blueberry flavor as top notes, rose scent and geranium flavor as middle notes, and base As a base note, you can have musk, amber, and vanilla flavors. However, it is not limited to the above fragrance. However, the fragrance of the fragrance composition prepared according to an embodiment of the present invention is not limited to the fragrance as long as it reproduces the fragrance of a rose obtained by crossing Candlelight and Strawberry Hill.
캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미Rose obtained by crossing Candlelight and Strawberry Hill 향기성분 분석Fragrance component analysis
캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 장미 중에서 향기가 강한 장미를 골라 향기성분을 포집하였다. Among the roses obtained by crossing Candlelight and Strawberry Hill, roses with strong fragrance were selected and the fragrance components were collected.
향기성분 포집을 위하여 다이나믹 헤드스페이스(dynamic headspace)법을 사용하였다. 기구를 이용하여, 교배하여 얻은 장미를 감싼 상태에서 기체와 펌프를 이용하여 임의로 헤드스페이스를 동적으로 만들어준 후 TENAX 충진관으로 700㎖/min의 속도로 30분간 유체가 흐르도록 하여 향기성분을 흡착 포집하였다. 포집된 향기성분의 분리와 동정을 위해 가스크로마토그래피 질량분석기(gas chromatography mass spectrometry)를 [표 1]과 같은 조건으로 수행하였다.A dynamic headspace method was used to capture fragrance components. Using a device, in the state that the rose obtained by crossbreeding is wrapped, the headspace is created dynamically using gas and a pump, and then the fluid flows through the TENAX filling tube at 700ml/min for 30 minutes to adsorb the fragrance component. captured. Gas chromatography mass spectrometry was performed under the conditions shown in [Table 1] for separation and identification of the captured fragrance components.
[표 1] GC 분석 시 기기설정[Table 1] Instrument settings for GC analysis
분석된 장미의 향기성분은 하기 [표 2]와 같다. The fragrance components of the analyzed rose are shown in [Table 2] below.
[표 2][Table 2]
상기 [표 2]의 R.T.는 향료 조성물의 각 성분의 피크가 확인되는 시간(분)이고 각 성분은 확인되는 시간(분) 순서대로 기재되었다. 상기 [표 2]의 AREA는 각 성분이 발견된 영역의 합을 나타낸다. 지정된 R.T.에서 AREA 수치가 크면 검출양이 많은 성분이고, 지정된 R.T.에서 AREA 수치가 작으면 검출양이 적은 성분이다. PCT total은 AREA의 총합을 상대값으로 나타낸 것이다. AREA의 수치와 향의 강도가 반드시 비례하는 것은 아니다.R.T. of [Table 2] is the time (minutes) at which the peak of each component of the perfume composition is confirmed, and each component is described in the order of the time (minutes) at which it is confirmed. AREA in [Table 2] represents the sum of the areas in which each component was found. If the AREA value is large at the designated R.T., it is a component with a large detectable amount, and if the AREA value is low at the designated R.T. PCT total is the relative value of the total of AREA. The level of AREA is not necessarily proportional to the intensity of the fragrance.
장미 향기성분은 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트 (c-3-Hexenyl acetate), 벤질알코올 (Benzyl alcohol), 벤질아세테이트(Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌 (Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알 (Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol) 및 제라니올(Geraniol)인 것을 확인했다.The rose fragrance component is hexyl acetate, cis-3-hexenol (c-3-Hexenol), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol (Benzyl alcohol), benzyl acetate (Benzyl acetate), Phenyl ethyl alcohol, Phenyl ethyl acetate, Linalool, Caryophyllene, Citronellyl acetate, Neral, Neryl acetate, geranial, geranyl acetate, citronellol, nerol and geraniol were confirmed.
<실험예 1: 항료 조성물의 제조><Experimental Example 1: Preparation of Fragrance Composition>
향취의 관능평가를 통하여 비교하기 위해 [표 3]에서와 같이 다양한 조합으로 향료 조성물을 제조하였다.In order to compare through the sensory evaluation of the scent, perfume compositions were prepared in various combinations as shown in [Table 3].
[표 3][Table 3]
실시예 1에 따른 향료 조성물은, 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 천연 장미의 향취를 가장 유사하게 재현할 수 있고, 특히 숙성된 배의 향과 블루베리향을 재현할 수 있다.The fragrance composition according to Example 1 can most similarly reproduce the fragrance of a natural rose obtained by crossing Candlelight and Strawberry Hill, and in particular, the fragrance of aged pears and blueberry. can be reproduced.
<실험예 2: 향료 조성물과 교배 장미 향취 비교><Experimental Example 2: Comparison of fragrance composition and scent of hybrid roses>
본 발명에서 분석된 장미 향기성분을 포함하는 향료 조성물과 천연 캔들라이트(Candlelight)와 스트로베리 힐(Strawberry Hill)을 교배하여 얻은 천연 장미의 향취와 비교(관능평가)하였다. The fragrance composition containing the rose fragrance component analyzed in the present invention was compared (sensory evaluation) with the fragrance of a natural rose obtained by crossing natural Candlelight and Strawberry Hill.
관능평가는 20-50세 일반 남녀 12명을 대상으로 하였으며, 교배된 천연 장미 향수(비교예)와 실시예 1 및 2에 대하여 향취 유사성과 향료 선호도를 5단계로 나누고 점수를 표시하여 [표 4]와 같이 제시하였다. 유사성 과 향료 선호도 평가 결과는 [표 5]와 같다.The sensory evaluation was conducted for 12 general men and women aged 20-50 years, and for the crossbreed natural rose perfume (comparative example) and Examples 1 and 2, the fragrance similarity and fragrance preference were divided into 5 stages and the scores were displayed [Table 4] ] as shown. [Table 5] shows the similarity and flavor preference evaluation results.
[표 4] 관능평가 질문지[Table 4] Sensory evaluation questionnaire
[표 5] 유사성 및 선호도 평가 결과[Table 5] Similarity and preference evaluation results
상기 [표 5]에서 알 수 있듯이 일반인을 대상으로 한 관능평가에서 실시예 1이 천연 교배 장미의 향취와 가장 유사한 것으로 나타났으며 선호도도 실시예1이 높았다.As can be seen from [Table 5], in the sensory evaluation for the general public, Example 1 was found to be the most similar to the smell of natural crossed roses, and the preference of Example 1 was high.
이상과 같이 실시예들이 비록 한정된 도면에 의해 설명되었으나, 해당 기술분야에서 통상의 지식을 가진 자라면 상기를 기초로 다양한 기술적 수정 및 변형을 적용할 수 있다. 예를 들어, 설명된 기술들이 설명된 방법과 다른 순서로 수행되거나, 및/또는 설명된 구성요소들이 설명된 방법과 다른 형태로 결합 또는 조합되거나, 다른 구성요소 또는 균등물에 의하여 대치되거나 치환되더라도 적절한 결과가 달성될 수 있다.As described above, although the embodiments have been described with reference to the limited drawings, those skilled in the art may apply various technical modifications and variations based on the above. For example, even if the described techniques are performed in an order different from the described method, and/or the described components are combined or combined in a different form from the described method, or replaced or substituted by other components or equivalents Appropriate results can be achieved.
그러므로, 다른 구현들, 다른 실시예들 및 특허청구범위와 균등한 것들도 후술하는 청구범위의 범위에 속한다.Therefore, other implementations, other embodiments, and equivalents to the claims are also within the scope of the following claims.
Claims (8)
상기 향료 조성물은 헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트(Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌 (Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol) 및 제라니올(Geraniol)을 포함하는, 장미 향취를 재현하는 향료 조성물.
A perfume composition that reproduces the scent of a rose obtained by crossing Candlelight and Strawberry Hill,
The fragrance composition is hexyl acetate, cis-3-hexenol (c-3-Hexenol), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol (Benzyl alcohol), benzyl acetate (Benzyl acetate), Phenyl ethyl alcohol, Phenyl ethyl acetate, Linalool, Caryophyllene, Citronellyl acetate, Neral, Fragrances that reproduce the scent of roses, including neryl acetate, geranial, geranyl acetate, citronellol, nerol and geraniol composition.
상기 향료 조성물 총 중량부에 대하여, 헥실 아세테이트(Hexyl acetate) 20 ~ 30 중량부, 시스-3-헥센올(c-3-Hexenol) 1 ~ 10 중량부, 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate) 1 ~ 10 중량부, 벤질알코올(Benzyl alcohol) 1~ 10 중량부, 벤질아세테이트(Benzyl acetate) 0.01 ~ 1 중량부, 페닐에틸알코올(Phenyl ethyl alcohol) 10 ~ 20 중량부, 페닐에틸아세테이트(Phenyl ethyl acetate) 1 ~ 10 중량부, 리나로올(Linalool) 1 ~ 5 중량부, 카리오필렌(Caryophyllene) 1 ~ 5 중량부, 시트로넬릴아세테이트(Citronellyl acetate) 1 ~ 5 중량부, 네랄(Neral) 0.01 ~ 1 중량부, 네릴 아세테이트(Neryl acetate) 0.01 ~ 1 중량부, 제라니알(Geranial) 0.01 ~ 1 중량부, 제라닐 아세테이트(Geranyl acetate) 10 ~ 20 중량부, 시트로넬롤(Citronellol) 0.01 ~ 1 중량부, 네롤(Nerol) 1 ~ 10 중량부 및 제라니올(Geraniol) 10 ~ 20 중량부를 포함하는, 장미 향취를 재현하는 향료 조성물.
The method of claim 1,
Based on the total weight of the perfume composition, 20 to 30 parts by weight of hexyl acetate, 1 to 10 parts by weight of cis-3-hexenol (c-3-Hexenol), cis-3-hexenyl acetate (c- 3-Hexenyl acetate) 1 to 10 parts by weight, Benzyl alcohol 1 to 10 parts by weight, Benzyl acetate 0.01 to 1 parts by weight, Phenyl ethyl alcohol 10 to 20 parts by weight, phenyl Phenyl ethyl acetate 1 to 10 parts by weight, Linalool 1 to 5 parts by weight, Caryophyllene 1 to 5 parts by weight, Citronellyl acetate 1 to 5 parts by weight, Neral 0.01 to 1 parts by weight, Neryl acetate 0.01 to 1 parts by weight, Geranial 0.01 to 1 parts by weight, Geranyl acetate 10 to 20 parts by weight, citronellol (Citronellol) 0.01 to 1 parts by weight, nerol (Nerol) 1 to 10 parts by weight and geraniol (Geraniol) 10 to 20 parts by weight, comprising a perfume composition that reproduces the scent of roses.
제라닐 부티레이트(Geranyl butyrate) 또는 시트로넬롤 부티레이트(Citronellyl butyrate) 중 어느 하나를 더 포함하는, 장미 향취를 재현하는 향료 조성물.
The method of claim 1,
Geranyl butyrate (Geranyl butyrate) or citronellyl butyrate (Citronellyl butyrate) further comprising any one of, a perfume composition for reproducing the scent of roses.
상기 향료 조성물 총 중량부에 대하여, 제라닐 부티레이트(Geranyl butyrate) 0.01 ~ 1 중량부 또는 시트로넬롤 부티레이트(Citronellyl butyrate) 0.01 ~ 1 중량부를 더 포함하는, 장미 향취를 재현하는 향료 조성물.
4. The method of claim 3,
Based on the total weight of the perfume composition, geranyl butyrate (Geranyl butyrate) 0.01 to 1 part by weight or citronellyl butyrate (Citronellyl butyrate) 0.01 to 1 part by weight, further comprising a perfume composition to reproduce the scent of roses.
A cosmetic composition comprising the perfume composition of any one of claims 1 to 4 as an active ingredient.
A fragrance composition comprising the fragrance composition of any one of claims 1 to 4 as an active ingredient.
[Claim 5] A composition for external application to the skin comprising the fragrance composition of any one of claims 1 to 4 as an active ingredient.
헥실 아세테이트(Hexyl acetate), 시스-3-헥센올(c-3-Hexenol), 시스-3-헥세닐 아세테이트(c-3-Hexenyl acetate), 벤질알코올(Benzyl alcohol), 벤질아세테이트 (Benzyl acetate), 페닐에틸알코올(Phenyl ethyl alcohol), 페닐에틸아세테이트(Phenyl ethyl acetate), 리나로올(Linalool), 카리오필렌(Caryophyllene), 시트로넬릴아세테이트(Citronellyl acetate), 네랄(Neral), 네릴 아세테이트(Neryl acetate), 제라니알(Geranial), 제라닐 아세테이트(Geranyl acetate), 시트로넬롤(Citronellol), 네롤(Nerol), 제라니올(Geraniol), 제라닐 부티레이트(Geranyl butyrate) 및 시트로넬롤 부티레이트(Citronellyl butyrate)을 혼합하는 단계; 및
상기 혼합물을 여과하는 단계
를 포함하는, 장미 향취를 재현하는 향료 조성물의 제조방법.
A method for producing a perfume composition that reproduces the scent of roses obtained by crossing Candlelight and Strawberry Hill,
Hexyl acetate, cis-3-hexenol (c-3-Hexenol), cis-3-hexenyl acetate (c-3-Hexenyl acetate), benzyl alcohol, benzyl acetate , Phenyl ethyl alcohol, Phenyl ethyl acetate, Linalool, Caryophyllene, Citronellyl acetate, Neral, Neryl acetate), geranial, geranyl acetate, citronellol, nerol, geraniol, geranyl butyrate, and citronellol butyrate ( Citronellyl butyrate); and
filtering the mixture
A method for producing a perfume composition that reproduces the scent of roses, comprising a.
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