CN110251425A - A kind of natural essential oil fragrance perfume and preparation method thereof - Google Patents
A kind of natural essential oil fragrance perfume and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to a kind of natural essential oil fragrance perfume and preparation method thereof, the natural essential oil fragrance perfume is by using more than 60 raw materials such as Neo Heliopan OS, the fluffy ester of lattice, imperial saliva furans and carries out suitable weight proportion.The natural essential oil fragrance perfume being finally prepared, realize being perfectly combined for natural essential oil and synthetic perfume fragrance, more existing perfume fragrance stereovision is apparent, fragrance is softer, fragrance is more coordinated, lasting is more longlasting, citrus is adjusted to before natural essential oil fragrance perfume of the present invention, the mixing fruity of lemon, in be adjusted to the lily of the valley, the quiet and beautiful fragrance of a flower of jasmine, tail is adjusted to natural ambergris and the mixing sweetness soil property of amber is fragrant, the alcohol-free sharp aroma of the present invention, it is non-stimulated to skin, quality is reliable and stable, preparation method is simple, user experience with higher and marketing application value.
Description
Technical field
The invention belongs to flavors and fragrances technical fields, and in particular to a kind of natural essential oil fragrance perfume and preparation method thereof.
Background technique
Perfume increasingly praises highly the important cosmetics used as Contemporary Female, can not only indicate individual character, increases self-confident
The heart and charisma promote life grade, also convey courtesy and intension, become the important social gift of one kind of modern society
Instrument, in addition, perfume can also play calm nerves, adjust mood, smooth the effects of soul.
Number of patent application 201510291567.3 discloses a kind of daily use chemicals lily essence and preparation method thereof, the daily use chemicals
Raw material components with lily essence include cis- 6- nonenol: 0.05-0.15%；Card dragon: 0.05-0.15%；Ethyl vanillin:
0.1-0.3%；Cyanine aldehyde: 0.1-0.3%；The fluffy ester of ring lattice: 0.2-0.4%；Pears alcohol ester: 0.2-0.4% etc..The program is by adopting
It is matched with a large amount of synthetic perfume, it is good to have obtained a kind of fragrance of a flower sense, and natural sense is strong, the fragrance lasting lily essence of basic note.
But the natural differences due to synthetic perfume and natural perfume material in fragrance texture, the natural sense being prepared still need to be mentioned
Height, and be also lacking in terms of fragrance stereovision, fragrance mildness and fragrance harmony.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the present invention provides one kind and naturally feels stronger, fragrance stereovision
Natural essential oil fragrance perfume apparent, fragrance is softer, fragrance is more coordinated, lasting is more longlasting, and preparation method is provided.
The technical solution of the present invention is as follows:
A kind of natural essential oil fragrance perfume, raw material components include:
The fluffy ester 1.2-1.8 parts by weight of Neo Heliopan OS 5.68-8.52 parts by weight, lattice, imperial saliva furans 1.6-
2.4 parts by weight, BHT2.4-3.6 parts by weight, ethoxymethyl) epoxide ring hendecane 25.68-38.52 parts by weight, borneol 0.176-
The clean flood aldehyde 0.608-0.912 parts by weight of 0.264 parts by weight, wave, capraldehyde 0.192-0.288 parts by weight, hendecanal 0.48-0.72 weight
Measure part, card dragon 3.2-4.8 parts by weight, citral 0.56-0.84 parts by weight, citronellyl formate 0.096-0.144 parts by weight, tonka-bean
Plain 1.328-1.992 parts by weight, cyclamen aldehyde 2.72-4.08 parts by weight, dihydrojasmonate 150.4-225.6 weight
Part, dihydromyrcenol 49.6-74.4 parts by weight, dipropylene glycol 32-48 parts by weight, ethyl linalool 17.6-26.4 parts by weight,
Ethyl linalyl acetate 7.632-11.448 parts by weight, pentadacanolide 28-42 parts by weight, Jiale muskiness 0.544-0.816 weight
Measure part, geranyl formate 0.048-0.072 parts by weight, geraniol 0.208-0.312 parts by weight, geranyl acetate 0.8-1.2 weight
Measure part, acid guaiacyl ester 3.024-4.536 parts by weight, cyclopentadecylene lactone 62.88-94.32 parts by weight, first position hexyl cinnamic aldehyde
0.096-0.144 parts by weight, helional 7.44-11.16 parts by weight, indoles 0.04-0.06 parts by weight, ambrotone 70.4-
105.6 parts by weight, karanal 3.12-4.68 parts by weight, green spend fragrant 0.488- at isoeugenol 0.424-0.636 parts by weight
0.732 parts by weight, linalool 9.76-14.64 parts by weight, bergamio 21.2-31.8 parts by weight, L- menthones 0.16-
0.24 parts by weight, red tangerine aldehyde 0.168-0.252 parts by weight, grapefruit methane 14.304-21.456 parts by weight, Moschus ketenes 4.192-
6.288 parts by weight, astrotone 73.6-110.4 parts by weight, neryl acetate 0.288-0.432 parts by weight, octyl aldehyde diethyl acetal
0.16-0.24 parts by weight, octyl acetate 0.056-0.084 parts by weight, benzyl carbinol 0.064-0.096 parts by weight, acetic acid storax
Ester 2.24-3.36 parts by weight, timberol 2.16-3.24 parts by weight, triethyl citrate 18.48-27.72 parts by weight, synthesis
Oak moss 0.8-1.2 parts by weight, o-tert-butyl cyclohexyl-acetic acid ester 1.48-2.22 parts by weight, dragon saliva acetal 0.4-0.6 parts by weight,
First position damascone 0.384-0.576 parts by weight, B position violet ketone 3.92-5.88 parts by weight, second position citronellol 0.352-0.528
Parts by weight, composite natral essential oil 165.536-248.304 parts by weight；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
Oil, patchouli oil, vetiver oil are by weight (40-60): (0.8-1.2): (1.6-2.4): and (84-126): (0.736-1.104):
(1.6-2.4): (16-24): (16-24): the mixture of (4.8-7.2) composition.
Preferably, the raw material components of the natural essential oil fragrance perfume include: Neo Heliopan OS 6.39-
The fluffy ester 1.35-1.65 parts by weight of 7.81 parts by weight, lattice, dragon saliva furans 1.8-2.2 parts by weight, BHT2.7-3.3 parts by weight, ethoxy
The clean flood aldehyde 0.684-0.836 weight of ylmethoxy ring hendecane 28.89-35.31 parts by weight, borneol 0.198-0.242 parts by weight, wave
Measure part, capraldehyde 0.216-0.264 parts by weight, hendecanal 0.54-0.66 parts by weight, card dragon 3.6-4.4 parts by weight, citral
0.63-0.77 parts by weight, citronellyl formate 0.108-0.132 parts by weight, coumarin 1 .494-1.826 parts by weight, cyclamen aldehyde
3.06-3.74 parts by weight, dihydrojasmonate 169.2-206.8 parts by weight, dihydromyrcenol 55.8-68.2 weight
Part, dipropylene glycol 36-44 parts by weight, ethyl linalool 19.8-24.2 parts by weight, ethyl linalyl acetate 8.586-10.494 weight
Measure part, pentadacanolide 31.5-38.5 parts by weight, Jiale muskiness 0.612-0.748 parts by weight, geranyl formate 0.054-
0.066 parts by weight, geraniol 0.234-0.286 parts by weight, geranyl acetate 0.9-1.1 parts by weight, acid guaiacyl ester
3.402-4.158 parts by weight, cyclopentadecylene lactone 70.74-86.46 parts by weight, first position hexyl cinnamic aldehyde 0.108-0.132 weight
It is part, helional 8.37-10.23 parts by weight, indoles 0.045-0.055 parts by weight, ambrotone 79.2-96.8 parts by weight, different
Eugenol 0.477-0.583 parts by weight, green spend fragrant 0.549-0.671 parts by weight, fragrant camphor tree at karanal 3.51-4.29 parts by weight
Alcohol 10.98-13.42 parts by weight, bergamio 23.85-29.15 parts by weight, L- menthones 0.18-0.22 parts by weight, red tangerine
Aldehyde 0.189-0.231 parts by weight, grapefruit methane 16.092-19.668 parts by weight, Moschus ketenes 4.716-5.764 parts by weight, musk deer
Fragrant T 82.8-101.2 parts by weight, neryl acetate 0.324-0.396 parts by weight, octyl aldehyde diethyl acetal 0.18-0.22 parts by weight,
Octyl acetate 0.063-0.077 parts by weight, benzyl carbinol 0.072-0.088 parts by weight, methyl phenyl carbinyl acetate 2.52-3.08 weight
Part, timberol 2.43-2.97 parts by weight, triethyl citrate 20.79-25.41 parts by weight, synthesis oak moss 0.9-1.1 weight
Part, o-tert-butyl cyclohexyl-acetic acid ester 1.665-2.035 parts by weight, dragon saliva acetal 0.45-0.55 parts by weight, first position damascone
0.432-0.528 parts by weight, second position citronellol 0.396-0.484 parts by weight, are answered at B position violet ketone 4.41-5.39 parts by weight
Close natural essential oil 186.228-227.612 parts by weight；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
Oil, patchouli oil, vetiver oil are by weight (45-55): (0.9-1.1): (1.8-2.2): (94.5-115.5): (0.828-
1.012): (1.8-2.2): (18-22): (18-22): the mixture of (5.4-6.6) composition.
Preferably, the raw material components of the natural essential oil fragrance perfume include: 7.1 weight of Neo Heliopan OS
Part, fluffy 1.5 parts by weight of ester of lattice, imperial 2 parts by weight of saliva furans, BHT3 parts by weight, 32.1 parts by weight of ethoxymethyl) epoxide ring hendecane,
Clean big vast 0.76 parts by weight of aldehyde of 0.22 parts by weight of borneol, wave, 0.24 parts by weight of capraldehyde, 0.6 parts by weight of the hendecanal, block imperial 4 parts by weight,
0.7 parts by weight of citral, 0.12 parts by weight of citronellyl formate, coumarin 1 .66 parts by weight, 3.4 parts by weight of cyclamen aldehyde, dihydro
188 parts by weight of methyl jasmonate, 62 parts by weight of dihydromyrcenol, 40 parts by weight of dipropylene glycol, 22 weight of ethyl linalool
Part, 9.54 parts by weight of ethyl linalyl acetate, 35 parts by weight of pentadacanolide, 0.68 parts by weight of Jiale muskiness, geranyl formate
0.06 parts by weight, 0.26 parts by weight of geraniol, 1 parts by weight of geranyl acetate, 3.78 parts by weight of acid guaiacyl ester, cyclopentadecylene
78.6 parts by weight of lactone, 0.12 parts by weight of first position hexyl cinnamic aldehyde, 9.3 parts by weight of helional, 0.05 parts by weight of indoles, imperial saliva
88 parts by weight of ketone, 3.9 parts by weight of karanal, green spend fragrant 0.61 parts by weight, 12.2 weight of linalool at 0.53 parts by weight of isoeugenol
Measure part, 26.5 parts by weight of bergamio, 0.2 parts by weight of L- menthones, 0.21 parts by weight of red tangerine aldehyde, 17.88 weight of grapefruit methane
Measure part, 5.24 parts by weight of Moschus ketenes, 92 parts by weight of astrotone, 0.36 parts by weight of neryl acetate, 0.2 weight of octyl aldehyde diethyl acetal
Measure part, 0.07 parts by weight of octyl acetate, 0.08 parts by weight of benzyl carbinol, 2.8 parts by weight of methyl phenyl carbinyl acetate, 2.7 weight of timberol
Measure part, 23.1 parts by weight of triethyl citrate, synthesis 1 parts by weight of oak moss, 1.85 parts by weight of o-tert-butyl cyclohexyl-acetic acid ester, dragon
0.5 parts by weight of saliva acetal, 0.48 parts by weight of first position damascone, 4.9 parts by weight of B position violet ketone, 0.44 weight of second position citronellol
Part, 206.92 parts by weight of composite natral essential oil；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
The mixture that oil, patchouli oil, vetiver oil are formed by weight 50:1:2:105:0.92:2:20:20:6.
Preferably, the cedar wood oil, clove leaf oil and elemi oil are prepared as follows to obtain respectively:
(1) it by after impurity removing, low temperature drying, crushes, obtains raw material powder；
(2) extractant is added in Xiang Suoshu raw material powder, is first impregnated, then carry out subcritical fluids counter-current extraction,
After be evaporated under reduced pressure remove extractant to get.
Preferably, in step (1), the low temperature drying is in the item that vacuum degree is 0.1-0.2MPa, temperature is 25-30 DEG C
Dry 4-8h under part.
Preferably, in step (1), the partial size that is crushed to is less than 40 mesh.
Preferably, in step (2), the extractant is any one in propane and butane；The raw material powder and extraction
The weight ratio for taking solvent is 1:2-1:3；The time of the immersion is 2-6h, carries out the extraction of the subcritical fluids counter-current extraction
Temperature is 35-45 DEG C, and extracting pressure is 0.1~0.4MPa, extraction time 50-70min, carries out extraction 3-4 times；It carries out
The pressure of the reduction vaporization is -0.4~-0.25MPa, and the temperature for carrying out the reduction vaporization is 45-50 DEG C.
A method of preparing the natural essential oil fragrance perfume, specific steps are as follows:
Weigh each raw material component respectively, stirring makes to be uniformly mixed, and aged, filtering is to get arriving the natural essential oil fragrance
Perfume.
Preferably, the speed of the stirring is 40-100r/min, and the time of the stirring is 10-30min.
Preferably, the temperature of the ageing is 15-25 DEG C, and the time of the ageing is 3-5 months, the temperature of the filtering
It is 10 DEG C or less.
The invention has the benefit that
Natural essential oil fragrance perfume of the present invention, by using Neo Heliopan OS, the fluffy ester of lattice, imperial saliva
More than 60 raw material such as furans simultaneously carries out suitable weight proportion, and the natural essential oil fragrance perfume being finally prepared realizes
Natural essential oil is perfectly combined with synthetic perfume fragrance, and more existing perfume fragrance naturally feels that stronger, stereovision is apparent, and fragrance is more
Soft, fragrance is more coordinated, lasting is more longlasting, and the mixing fruity of citrus, lemon is adjusted to before natural essential oil fragrance perfume of the present invention,
In be adjusted to the quiet and beautiful fragrance of a flower of the lily of the valley, jasmine, tail is adjusted to natural ambergris and the mixing sweetness soil property of amber is fragrant, and the present invention is alcohol-free
Sharp aroma, non-stimulated to skin, quality is reliable and stable, and preparation method is simple, and user experience with higher and market push away
Wide application value.
Specific embodiment
Below by specific embodiment, the invention will be further described.
1g is represented in following embodiment with 1 parts by weight.
Embodiment 1
The present embodiment provides a kind of natural essential oil fragrance perfume, raw material components include:
Fluffy 1.2 parts by weight of ester of 5.68 parts by weight of Neo Heliopan OS, lattice, imperial 1.6 parts by weight of saliva furans,
BHT2.4 parts by weight, 25.68 parts by weight of ethoxymethyl) epoxide ring hendecane, 0.176 parts by weight of borneol, wave 0.608 weight of clean big vast aldehyde
It measures part, 0.192 parts by weight of capraldehyde, 0.48 parts by weight of the hendecanal, block imperial 3.2 parts by weight, 0.56 parts by weight of citral, formic acid lemongrass
0.096 parts by weight of ester, coumarin 1 .328 parts by weight, 2.72 parts by weight of cyclamen aldehyde, 150.4 weight of dihydrojasmonate
Part, 49.6 parts by weight of dihydromyrcenol, 32 parts by weight of dipropylene glycol, 17.6 parts by weight of ethyl linalool, acetic virtue camphor tree
7.632 parts by weight of ester, 28 parts by weight of pentadacanolide, 0.544 parts by weight of Jiale muskiness, 0.048 parts by weight of geranyl formate, perfume (or spice)
0.208 parts by weight of leaf-alcohol, 0.8 parts by weight of geranyl acetate, 3.024 parts by weight of acid guaiacyl ester, cyclopentadecylene lactone 62.88
Parts by weight, 0.096 parts by weight of first position hexyl cinnamic aldehyde, 7.44 parts by weight of helional, 0.04 parts by weight of indoles, ambrotone 70.4
Parts by weight, 3.12 parts by weight of karanal, green spend fragrant 0.488 parts by weight, 9.76 weight of linalool at 0.424 parts by weight of isoeugenol
Measure part, 21.2 parts by weight of bergamio, 0.16 parts by weight of L- menthones, 0.168 parts by weight of red tangerine aldehyde, grapefruit methane 14.304
Parts by weight, 4.192 parts by weight of Moschus ketenes, 73.6 parts by weight of astrotone, 0.288 parts by weight of neryl acetate, the contracting of octanal diethyl
0.16 parts by weight of aldehyde, 0.056 parts by weight of octyl acetate, 0.064 parts by weight of benzyl carbinol, 2.24 parts by weight of methyl phenyl carbinyl acetate, spy
2.16 parts by weight of the wooden times alcohol, 18.48 parts by weight of triethyl citrate, synthesis 0.8 parts by weight of oak moss, o-tert-butyl cyclohexyl-acetic acid
1.48 parts by weight of ester, imperial 0.4 parts by weight of saliva acetal, 0.384 parts by weight of first position damascone, 3.92 parts by weight of B position violet ketone,
0.352 parts by weight of second position citronellol, 165.536 parts by weight of composite natral essential oil；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
The mixture that oil, patchouli oil, vetiver oil are formed by weight 40:0.8:1.6:84:0.736:1.6:16:16:4.8；
The cedar wood oil, clove leaf oil and elemi oil are prepared as follows to obtain respectively:
(1) by impurity removing, dry 4h, crushes, obtains partial size under conditions of vacuum degree is 0.1MPa, temperature is 30 DEG C
For the raw material powder of 60 mesh；
(2) propane of 2 times of quality is added in Xiang Suoshu raw material powder, first impregnates 2h, then carries out subcritical fluids adverse current and extracts
Take, extraction temperature be 35 DEG C, extracting pressure 0.4MPa, extraction time 50min, carry out it is described extraction 3 times, after-
0.4MPa, it is evaporated under reduced pressure under the conditions of 45 DEG C and removes extraction propane to get cedar wood oil, clove leaf oil or elemi oil.
Further, a kind of method preparing the natural essential oil fragrance perfume is provided, is included the following steps:
Each raw material component is weighed respectively, is made to be uniformly mixed with 40r/min stirring 30min, is then aged 5 months, 5 DEG C for 15 DEG C
Under the conditions of filtering to get arrive the natural essential oil fragrance perfume.
Embodiment 2
The present embodiment provides a kind of natural essential oil fragrance perfume, raw material components include:
Fluffy 1.8 parts by weight of ester of 8.52 parts by weight of Neo Heliopan OS, lattice, imperial 2.4 parts by weight of saliva furans,
BHT3.6 parts by weight, 38.52 parts by weight of ethoxymethyl) epoxide ring hendecane, 0.264 parts by weight of borneol, wave 0.912 weight of clean big vast aldehyde
It measures part, 0.288 parts by weight of capraldehyde, 0.72 parts by weight of the hendecanal, block imperial 4.8 parts by weight, 0.84 parts by weight of citral, formic acid lemongrass
0.144 parts by weight of ester, coumarin 1 .992 parts by weight, 4.08 parts by weight of cyclamen aldehyde, 225.6 weight of dihydrojasmonate
Part, 74.4 parts by weight of dihydromyrcenol, 48 parts by weight of dipropylene glycol, 26.4 parts by weight of ethyl linalool, acetic virtue camphor tree
11.448 parts by weight of ester, 42 parts by weight of pentadacanolide, 0.816 parts by weight of Jiale muskiness, 0.072 parts by weight of geranyl formate,
0.312 parts by weight of geraniol, 1.2 parts by weight of geranyl acetate, 4.536 parts by weight of acid guaiacyl ester, cyclopentadecylene lactone
94.32 parts by weight, 0.144 parts by weight of first position hexyl cinnamic aldehyde, 11.16 parts by weight of helional, 0.06 parts by weight of indoles, imperial saliva
105.6 parts by weight of ketone, 4.68 parts by weight of karanal, green spend fragrant 0.732 parts by weight, linalool at 0.636 parts by weight of isoeugenol
14.64 parts by weight, 31.8 parts by weight of bergamio, 0.24 parts by weight of L- menthones, 0.252 parts by weight of red tangerine aldehyde, grapefruit first
It is 21.456 parts by weight of alkane, 6.288 parts by weight of Moschus ketenes, 110.4 parts by weight of astrotone, 0.432 parts by weight of neryl acetate, pungent
0.24 parts by weight of aldehyde diethyl acetal, 0.084 parts by weight of octyl acetate, 0.096 parts by weight of benzyl carbinol, 3.36 weight of methyl phenyl carbinyl acetate
Measure part, 3.24 parts by weight of timberol, 27.72 parts by weight of triethyl citrate, synthesis 1.2 parts by weight of oak moss, o-tert-butyl ring
2.22 parts by weight of hexylacetic acid ester, imperial 0.6 parts by weight of saliva acetal, 0.576 parts by weight of first position damascone, B position violet ketone 5.88
Parts by weight, 0.528 parts by weight of second position citronellol, 248.304 parts by weight of composite natral essential oil；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
The mixture that oil, patchouli oil, vetiver oil are formed by weight 60:1.2:2.4:126:1.104:2.4:24:24:7.2；
The cedar wood oil, clove leaf oil and elemi oil are prepared as follows to obtain respectively:
(1) by impurity removing, dry 8h, crushes, obtains partial size under conditions of vacuum degree is 0.2MPa, temperature is 25 DEG C
For the raw material powder of 60 mesh；
(2) propane of 3 times of quality is added in Xiang Suoshu raw material powder, first impregnates 6h, then carries out subcritical fluids adverse current and extracts
Take, extraction temperature be 45 DEG C, extracting pressure 0.1MPa, extraction time 70min, carry out it is described extraction 4 times, after-
0.25MPa, it is evaporated under reduced pressure under the conditions of 50 DEG C and removes extraction propane to get cedar wood oil, clove leaf oil or elemi oil.
Further, a kind of method preparing the natural essential oil fragrance perfume is provided, is included the following steps:
Each raw material component is weighed respectively, makes to be uniformly mixed with 100r/min stirring 10min, then 25 DEG C ageing 3 months, 5
It is filtered under the conditions of DEG C to get the natural essential oil fragrance perfume is arrived.
Embodiment 3
The present embodiment provides a kind of natural essential oil fragrance perfume, raw material components include:
Fluffy 1.35 parts by weight of ester of 6.39 parts by weight of Neo Heliopan OS, lattice, imperial 1.8 parts by weight of saliva furans,
BHT2.7 parts by weight, 28.89 parts by weight of ethoxymethyl) epoxide ring hendecane, 0.198 parts by weight of borneol, wave 0.684 weight of clean big vast aldehyde
It measures part, 0.216 parts by weight of capraldehyde, 0.54 parts by weight of the hendecanal, block imperial 3.6 parts by weight, 0.63 parts by weight of citral, formic acid lemongrass
0.108 parts by weight of ester, coumarin 1 .494 parts by weight, 3.06 parts by weight of cyclamen aldehyde, 169.2 weight of dihydrojasmonate
Part, 55.8 parts by weight of dihydromyrcenol, 36 parts by weight of dipropylene glycol, 19.8 parts by weight of ethyl linalool, acetic virtue camphor tree
8.586 parts by weight of ester, 31.5 parts by weight of pentadacanolide, 0.612 parts by weight of Jiale muskiness, 0.054 parts by weight of geranyl formate,
0.234 parts by weight of geraniol, 0.9 parts by weight of geranyl acetate, 3.402 parts by weight of acid guaiacyl ester, cyclopentadecylene lactone
70.74 parts by weight, 0.108 parts by weight of first position hexyl cinnamic aldehyde, 8.37 parts by weight of helional, 0.045 parts by weight of indoles, imperial saliva
79.2 parts by weight of ketone, 3.51 parts by weight of karanal, green spend fragrant 0.549 parts by weight, linalool at 0.477 parts by weight of isoeugenol
10.98 parts by weight, 23.85 parts by weight of bergamio, 0.18 parts by weight of L- menthones, 0.189 parts by weight of red tangerine aldehyde, grapefruit first
It is 16.092 parts by weight of alkane, 4.716 parts by weight of Moschus ketenes, 82.8 parts by weight of astrotone, 0.324 parts by weight of neryl acetate, pungent
0.18 parts by weight of aldehyde diethyl acetal, 0.063 parts by weight of octyl acetate, 0.072 parts by weight of benzyl carbinol, 2.52 weight of methyl phenyl carbinyl acetate
Measure part, 2.43 parts by weight of timberol, 20.79 parts by weight of triethyl citrate, synthesis 0.9 parts by weight of oak moss, o-tert-butyl ring
1.665 parts by weight of hexylacetic acid ester, imperial 0.45 parts by weight of saliva acetal, 0.432 parts by weight of first position damascone, B position violet ketone
4.41 parts by weight, 0.396 parts by weight of second position citronellol, 186.228 parts by weight of composite natral essential oil；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
The mixture that oil, patchouli oil, vetiver oil are formed by weight 45:0.9:1.8:94.5:0.828:1.8:18:18:5.4；
The cedar wood oil, clove leaf oil and elemi oil are prepared as follows to obtain respectively:
(1) by impurity removing, dry 6h, crushes, obtains grain under conditions of vacuum degree is 0.15MPa, temperature is 30 DEG C
Diameter is the raw material powder of 80 mesh；
(2) propane of 2.6 times of quality is added in Xiang Suoshu raw material powder, first impregnates 3.5h, it is inverse then to carry out subcritical fluids
Stream extraction, extraction temperature are 40 DEG C, extracting pressure 0.3MPa, extraction time 60min, carry out the extraction 3 times, after
It is evaporated under reduced pressure under the conditions of -0.3MPa, 50 DEG C and removes extraction propane to get cedar wood oil, clove leaf oil or elemi oil.
Further, a kind of method preparing the natural essential oil fragrance perfume is provided, is included the following steps:
Each raw material component is weighed respectively, is made to be uniformly mixed with 60r/min stirring 20min, is then aged 4 months, 5 DEG C for 20 DEG C
Under the conditions of filtering to get arrive the natural essential oil fragrance perfume.
Embodiment 4
The present embodiment provides a kind of natural essential oil fragrance perfume, raw material components include:
Fluffy 1.65 parts by weight of ester of 7.81 parts by weight of Neo Heliopan OS, lattice, imperial 2.2 parts by weight of saliva furans,
BHT3.3 parts by weight, 35.31 parts by weight of ethoxymethyl) epoxide ring hendecane, 0.242 parts by weight of borneol, wave 0.836 weight of clean big vast aldehyde
It measures part, 0.264 parts by weight of capraldehyde, 0.66 parts by weight of the hendecanal, block imperial 4.4 parts by weight, 0.77 parts by weight of citral, formic acid lemongrass
0.132 parts by weight of ester, coumarin 1 .826 parts by weight, 3.74 parts by weight of cyclamen aldehyde, 206.8 weight of dihydrojasmonate
Part, 68.2 parts by weight of dihydromyrcenol, 44 parts by weight of dipropylene glycol, 24.2 parts by weight of ethyl linalool, acetic virtue camphor tree
10.494 parts by weight of ester, 38.5 parts by weight of pentadacanolide, 0.748 parts by weight of Jiale muskiness, 0.066 weight of geranyl formate
Part, 0.286 parts by weight of geraniol, 1.1 parts by weight of geranyl acetate, 4.158 parts by weight of acid guaiacyl ester, cyclopentadecylene lactone
86.46 parts by weight, 0.132 parts by weight of first position hexyl cinnamic aldehyde, 10.23 parts by weight of helional, 0.055 parts by weight of indoles, dragon
96.8 parts by weight of saliva ketone, 4.29 parts by weight of karanal, green spend fragrant 0.671 parts by weight, fragrant camphor tree at 0.583 parts by weight of isoeugenol
13.42 parts by weight of alcohol, 29.15 parts by weight of bergamio, 0.22 parts by weight of L- menthones, 0.231 parts by weight of red tangerine aldehyde, grapefruit
19.668 parts by weight of methane, 5.764 parts by weight of Moschus ketenes, 101.2 parts by weight of astrotone, 0.396 parts by weight of neryl acetate,
0.22 parts by weight of octyl aldehyde diethyl acetal, 0.077 parts by weight of octyl acetate, 0.088 parts by weight of benzyl carbinol, methyl phenyl carbinyl acetate 3.08
Parts by weight, 2.97 parts by weight of timberol, 25.41 parts by weight of triethyl citrate, synthesis 1.1 parts by weight of oak moss, o-tert-butyl
2.035 parts by weight of cyclohexyl-acetic acid ester, imperial 0.55 parts by weight of saliva acetal, 0.528 parts by weight of first position damascone, B position violet ketone
5.39 parts by weight, 0.484 parts by weight of second position citronellol, 227.612 parts by weight of composite natral essential oil；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
The mixture that oil, patchouli oil, vetiver oil are formed by weight 55:1.1:2.2:115.5:1.012:2.2:22:22:6.6；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
The mixture that oil, patchouli oil, vetiver oil are formed by weight 45:0.9:1.8:94.5:0.828:1.8:18:18:5.4；
The cedar wood oil, clove leaf oil and elemi oil are prepared as follows to obtain respectively:
(1) by impurity removing, dry 5h, crushes, obtains partial size under conditions of vacuum degree is 0.2MPa, temperature is 30 DEG C
For the raw material powder of 80 mesh；
(2) propane of 3 times of quality is added in Xiang Suoshu raw material powder, first impregnates 5h, then carries out subcritical fluids adverse current and extracts
Take, extraction temperature be 42 DEG C, extracting pressure 0.2MPa, extraction time 60min, carry out it is described extraction 3 times, after-
0.3MPa, it is evaporated under reduced pressure under the conditions of 45 DEG C and removes extraction propane to get cedar wood oil, clove leaf oil or elemi oil.
Further, a kind of method preparing the natural essential oil fragrance perfume is provided, is included the following steps:
Each raw material component is weighed respectively, is made to be uniformly mixed with 50r/min stirring 25min, is then aged 4 months, 5 DEG C for 20 DEG C
Under the conditions of filtering to get arrive the natural essential oil fragrance perfume.
Embodiment 5
The present embodiment provides a kind of natural essential oil fragrance perfume, raw material components include:
Fluffy 1.5 parts by weight of ester of 7.1 parts by weight of Neo Heliopan OS, lattice, imperial 2 parts by weight of saliva furans, BHT3 weight
Part, 32.1 parts by weight of ethoxymethyl) epoxide ring hendecane, 0.22 parts by weight of borneol, 0.76 parts by weight of the clean big vast aldehyde of wave, capraldehyde 0.24
Parts by weight, 0.6 parts by weight of the hendecanal block imperial 4 parts by weight, 0.7 parts by weight of citral, 0.12 parts by weight of citronellyl formate, tonka-bean
Plain 1.66 parts by weight, 3.4 parts by weight of cyclamen aldehyde, 188 parts by weight of dihydrojasmonate, 62 weight of dihydromyrcenol
Part, 40 parts by weight of dipropylene glycol, 22 parts by weight of ethyl linalool, 9.54 parts by weight of ethyl linalyl acetate, pentadacanolide 35
Parts by weight, 0.68 parts by weight of Jiale muskiness, 0.06 parts by weight of geranyl formate, 0.26 parts by weight of geraniol, 1 weight of geranyl acetate
Measure part, 3.78 parts by weight of acid guaiacyl ester, 78.6 parts by weight of cyclopentadecylene lactone, 0.12 parts by weight of first position hexyl cinnamic aldehyde, new
9.3 parts by weight of heliotropin, 0.05 parts by weight of indoles, 88 parts by weight of ambrotone, 0.53 parts by weight of isoeugenol, karanal
3.9 parts by weight green spend fragrant 0.61 parts by weight, 12.2 parts by weight of linalool, 26.5 parts by weight of bergamio, L- menthones 0.2
Parts by weight, 0.21 parts by weight of red tangerine aldehyde, 17.88 parts by weight of grapefruit methane, 5.24 parts by weight of Moschus ketenes, 92 weight of astrotone
Part, 0.36 parts by weight of neryl acetate, 0.2 parts by weight of octyl aldehyde diethyl acetal, 0.07 parts by weight of octyl acetate, 0.08 weight of benzyl carbinol
Measure part, 2.8 parts by weight of methyl phenyl carbinyl acetate, 2.7 parts by weight of timberol, 23.1 parts by weight of triethyl citrate, synthesis oak moss 1
Parts by weight, 1.85 parts by weight of o-tert-butyl cyclohexyl-acetic acid ester, imperial 0.5 parts by weight of saliva acetal, 0.48 parts by weight of first position damascone,
4.9 parts by weight of B position violet ketone, 0.44 parts by weight of second position citronellol, 206.92 parts by weight of composite natral essential oil；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian sweet orange
The mixture that oil, patchouli oil, vetiver oil are formed by weight 50:1:2:105:0.92:2:20:20:6；
The cedar wood oil, clove leaf oil and elemi oil are prepared as follows to obtain respectively:
(1) by impurity removing, dry 7h, crushes, obtains partial size under conditions of vacuum degree is 0.2MPa, temperature is 25 DEG C
For the raw material powder of 60 mesh；
(2) propane of 3 times of quality is added in Xiang Suoshu raw material powder, first impregnates 3h, then carries out subcritical fluids adverse current and extracts
Take, extraction temperature be 38 DEG C, extracting pressure 0.2MPa, extraction time 50min, carry out it is described extraction 3 times, after-
0.3MPa, it is evaporated under reduced pressure under the conditions of 50 DEG C and removes extraction propane to get cedar wood oil, clove leaf oil or elemi oil.
Further, a kind of method preparing the natural essential oil fragrance perfume is provided, is included the following steps:
Each raw material component is weighed respectively, is made to be uniformly mixed with 40r/min stirring 20min, is then aged 4 months, 5 DEG C for 20 DEG C
Under the conditions of filtering to get arrive the natural essential oil fragrance perfume.
Experimental example
1, test specimen
Sample 1: the sample that embodiment 1 is prepared
Sample 2: the sample that embodiment 2 is prepared
Sample 3: the sample that embodiment 3 is prepared
Sample 4: the sample that embodiment 4 is prepared
Sample 5: embodiment: 5 samples being prepared
Sample 6: the sample being prepared by 201510291567.3 embodiment one of number of patent application
2, test method
It takes the 100 above-mentioned test specimens of μ l on glass slide respectively, then glass slide is placed in 32 DEG C of heating plates, with mould
Quasi- skin temperature selects 20 people with aromatic assessment experience, and men and women is fifty-fifty, carries out respectively at 30min, 2h, 4h, 8h, 10h
It smokes panel test and gives a mark, test fragrance stereovision (full marks 25 divide), fragrance harmony (full marks 25 divide) and flavor strength are at any time
Change (full marks 50 divide), each sample retest 5 times is averaged as final testing result.
3, test result is shown in Table 1
1 each sample of table is smoked panel test result of giving a mark
The result shows that 1~5 fragrance stereovision of sample of the present invention is apparent, and whole fragrance is more coordinated, stayed compared with sample 6
It is fragrant more longlasting, illustrate that natural essential oil fragrance perfume of the present invention passes through reasonable compatibility, so that each component plays synergistic effect, thus
The fragrance quality of perfume entirety is improved, there is higher user experience.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of natural essential oil fragrance perfume, which is characterized in that raw material components include:
The fluffy ester 1.2-1.8 parts by weight of Neo Heliopan OS 5.68-8.52 parts by weight, lattice, dragon saliva furans 1.6-2.4 weight
Measure part, BHT2.4-3.6 parts by weight, ethoxymethyl) epoxide ring hendecane 25.68-38.52 parts by weight, borneol 0.176-0.264 weight
Measure part, the clean flood aldehyde 0.608-0.912 parts by weight of wave, capraldehyde 0.192-0.288 parts by weight, hendecanal 0.48-0.72 parts by weight, card
Imperial 3.2-4.8 parts by weight, citral 0.56-0.84 parts by weight, citronellyl formate 0.096-0.144 parts by weight, cumarin
1.328-1.992 parts by weight, cyclamen aldehyde 2.72-4.08 parts by weight, dihydrojasmonate 150.4-225.6 parts by weight,
Dihydromyrcenol 49.6-74.4 parts by weight, dipropylene glycol 32-48 parts by weight, ethyl linalool 17.6-26.4 parts by weight, second
Sour ethyl virtue camphor tree ester 7.632-11.448 parts by weight, pentadacanolide 28-42 parts by weight, Jiale muskiness 0.544-0.816 weight
Part, geranyl formate 0.048-0.072 parts by weight, geraniol 0.208-0.312 parts by weight, geranyl acetate 0.8-1.2 weight
Part, acid guaiacyl ester 3.024-4.536 parts by weight, cyclopentadecylene lactone 62.88-94.32 parts by weight, first position hexyl cinnamic aldehyde
0.096-0.144 parts by weight, helional 7.44-11.16 parts by weight, indoles 0.04-0.06 parts by weight, ambrotone 70.4-
105.6 parts by weight, karanal 3.12-4.68 parts by weight, green spend fragrant 0.488- at isoeugenol 0.424-0.636 parts by weight
0.732 parts by weight, linalool 9.76-14.64 parts by weight, bergamio 21.2-31.8 parts by weight, L- menthones 0.16-
0.24 parts by weight, red tangerine aldehyde 0.168-0.252 parts by weight, grapefruit methane 14.304-21.456 parts by weight, Moschus ketenes 4.192-
6.288 parts by weight, astrotone 73.6-110.4 parts by weight, neryl acetate 0.288-0.432 parts by weight, octyl aldehyde diethyl acetal
0.16-0.24 parts by weight, octyl acetate 0.056-0.084 parts by weight, benzyl carbinol 0.064-0.096 parts by weight, acetic acid storax
Ester 2.24-3.36 parts by weight, timberol 2.16-3.24 parts by weight, triethyl citrate 18.48-27.72 parts by weight, synthesis
Oak moss 0.8-1.2 parts by weight, o-tert-butyl cyclohexyl-acetic acid ester 1.48-2.22 parts by weight, dragon saliva acetal 0.4-0.6 parts by weight,
First position damascone 0.384-0.576 parts by weight, B position violet ketone 3.92-5.88 parts by weight, second position citronellol 0.352-0.528
Parts by weight, composite natral essential oil 165.536-248.304 parts by weight；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian orange oil, wide
Palchouli oil, vetiver oil are by weight (40-60): (0.8-1.2): (1.6-2.4): (84-126): (0.736-1.104): (1.6-
2.4): (16-24): (16-24): the mixture of (4.8-7.2) composition.
2. natural essential oil fragrance perfume according to claim 1, which is characterized in that raw material components include: salicylic acid -2- second
Base hexyl ester 6.39-7.81 parts by weight, the fluffy ester 1.35-1.65 parts by weight of lattice, dragon saliva furans 1.8-2.2 parts by weight, BHT2.7-
3.3 parts by weight, ethoxymethyl) epoxide ring hendecane 28.89-35.31 parts by weight, borneol 0.198-0.242 parts by weight, the clean flood of wave
Aldehyde 0.684-0.836 parts by weight, capraldehyde 0.216-0.264 parts by weight, hendecanal 0.54-0.66 parts by weight, card dragon 3.6-4.4 weight
Measure part, citral 0.63-0.77 parts by weight, citronellyl formate 0.108-0.132 parts by weight, coumarin 1 .494-1.826 weight
Part, cyclamen aldehyde 3.06-3.74 parts by weight, dihydrojasmonate 169.2-206.8 parts by weight, dihydromyrcenol
55.8-68.2 parts by weight, dipropylene glycol 36-44 parts by weight, ethyl linalool 19.8-24.2 parts by weight, ethyl linalyl acetate
8.586-10.494 parts by weight, pentadacanolide 31.5-38.5 parts by weight, Jiale muskiness 0.612-0.748 parts by weight, formic acid are fragrant
Leaf ester 0.054-0.066 parts by weight, geraniol 0.234-0.286 parts by weight, geranyl acetate 0.9-1.1 parts by weight, acetic acid are cured
Create wood ester 3.402-4.158 parts by weight, cyclopentadecylene lactone 70.74-86.46 parts by weight, first position hexyl cinnamic aldehyde 0.108-0.132
Parts by weight, helional 8.37-10.23 parts by weight, indoles 0.045-0.055 parts by weight, ambrotone 79.2-96.8 weight
Part, isoeugenol 0.477-0.583 parts by weight, karanal 3.51-4.29 parts by weight, it is green spend fragrant 0.549-0.671 parts by weight,
Linalool 10.98-13.42 parts by weight, bergamio 23.85-29.15 parts by weight, L- menthones 0.18-0.22 parts by weight,
Red tangerine aldehyde 0.189-0.231 parts by weight, grapefruit methane 16.092-19.668 parts by weight, Moschus ketenes 4.716-5.764 weight
Part, astrotone 82.8-101.2 parts by weight, neryl acetate 0.324-0.396 parts by weight, octyl aldehyde diethyl acetal 0.18-0.22 weight
Measure part, octyl acetate 0.063-0.077 parts by weight, benzyl carbinol 0.072-0.088 parts by weight, methyl phenyl carbinyl acetate 2.52-3.08
Parts by weight, timberol 2.43-2.97 parts by weight, triethyl citrate 20.79-25.41 parts by weight, synthesis oak moss 0.9-1.1
Parts by weight, o-tert-butyl cyclohexyl-acetic acid ester 1.665-2.035 parts by weight, dragon saliva acetal 0.45-0.55 parts by weight, Jia Wei Tujue
Ketone 0.432-0.528 parts by weight, B position violet ketone 4.41-5.39 parts by weight, second position citronellol 0.396-0.484 parts by weight,
Composite natral essential oil 186.228-227.612 parts by weight；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian orange oil, wide
Palchouli oil, vetiver oil are by weight (45-55): (0.9-1.1): (1.8-2.2): and (94.5-115.5): (0.828-1.012):
(1.8-2.2): (18-22): (18-22): the mixture of (5.4-6.6) composition.
3. natural essential oil fragrance perfume according to claim 1, which is characterized in that raw material components include: salicylic acid -2- second
Fluffy 1.5 parts by weight of ester of 7.1 parts by weight of base hexyl ester, lattice, imperial 2 parts by weight of saliva furans, BHT3 parts by weight, ethoxymethyl) epoxide ring ten
0.76 parts by weight of the clean big vast aldehyde of one alkane, 32.1 parts by weight, 0.22 parts by weight of borneol, wave, 0.24 parts by weight of capraldehyde, 0.6 weight of the hendecanal
Part blocks imperial 4 parts by weight, 0.7 parts by weight of citral, 0.12 parts by weight of citronellyl formate, coumarin 1 .66 parts by weight, cyclamen aldehyde
3.4 parts by weight, 188 parts by weight of dihydrojasmonate, 62 parts by weight of dihydromyrcenol, 40 parts by weight of dipropylene glycol, second
22 parts by weight of base linalool, 9.54 parts by weight of ethyl linalyl acetate, 35 parts by weight of pentadacanolide, 0.68 weight of Jiale muskiness
Part, 0.06 parts by weight of geranyl formate, 0.26 parts by weight of geraniol, 1 parts by weight of geranyl acetate, 3.78 weight of acid guaiacyl ester
Measure part, 78.6 parts by weight of cyclopentadecylene lactone, 0.12 parts by weight of first position hexyl cinnamic aldehyde, 9.3 parts by weight of helional, indoles
0.05 parts by weight, 0.53 parts by weight of isoeugenol, 3.9 parts by weight of karanal, green spend fragrant 0.61 weight at 88 parts by weight of ambrotone
Part, 12.2 parts by weight of linalool, 26.5 parts by weight of bergamio, 0.2 parts by weight of L- menthones, 0.21 parts by weight of red tangerine aldehyde,
It is 17.88 parts by weight of grapefruit methane, 5.24 parts by weight of Moschus ketenes, 92 parts by weight of astrotone, 0.36 parts by weight of neryl acetate, pungent
0.2 parts by weight of aldehyde diethyl acetal, 0.07 parts by weight of octyl acetate, 0.08 parts by weight of benzyl carbinol, 2.8 weight of methyl phenyl carbinyl acetate
Part, 2.7 parts by weight of timberol, 23.1 parts by weight of triethyl citrate, synthesis 1 parts by weight of oak moss, o-tert-butyl cyclohexyl second
1.85 parts by weight of acid esters, imperial 0.5 parts by weight of saliva acetal, 0.48 parts by weight of first position damascone, 4.9 parts by weight of B position violet ketone,
0.44 parts by weight of second position citronellol, 206.92 parts by weight of composite natral essential oil；
The composite natral essential oil is cedar wood oil, clove leaf oil, ginger oil, lemon oil, peppermint oil, elemi oil, Brazilian orange oil, wide
The mixture that palchouli oil, vetiver oil are formed by weight 50:1:2:105:0.92:2:20:20:6.
4. natural essential oil fragrance perfume according to claim 1, which is characterized in that the cedar wood oil, clove leaf oil and
Elemi oil is prepared as follows to obtain respectively:
(1) it by after impurity removing, low temperature drying, crushes, obtains raw material powder；
(2) extractant is added in Xiang Suoshu raw material powder, is first impregnated, then carry out subcritical fluids counter-current extraction, finish
Afterwards be evaporated under reduced pressure remove extractant to get.
5. natural essential oil fragrance perfume according to claim 4, which is characterized in that in step (1), the low temperature drying is
Dry 4-8h under conditions of vacuum degree is 0.1-0.2MPa, temperature is 25-30 DEG C.
6. natural essential oil fragrance perfume according to claim 4, which is characterized in that described to be crushed to partial size in step (1)
Less than 40 mesh.
7. natural essential oil fragrance perfume according to claim 4, which is characterized in that in step (2), the extractant is
Any one in propane and butane；The weight ratio of the raw material powder and extractant is 1:2-1:3；The time of the immersion is
2-6h, the extraction temperature for carrying out the subcritical fluids counter-current extraction is 35-45 DEG C, and extracting pressure is 0.1~0.4MPa, extraction
Time is 50-70min, carries out extraction 3-4 times；The pressure for carrying out the reduction vaporization is -0.4~-0.25MPa, is carried out
The temperature of the reduction vaporization is 45-50 DEG C.
8. a kind of method for preparing the described in any item natural essential oil fragrance perfume of claim 1-7, which is characterized in that specific step
Suddenly are as follows:
Weigh each raw material component respectively, stirring makes to be uniformly mixed, and aged, filtering is to get arriving the natural essential oil fragrance perfume.
9. preparation method according to claim 8, which is characterized in that the speed of the stirring is 40-100r/min, described
The time of stirring is 10-30min.
10. preparation method according to claim 8, which is characterized in that the temperature of the ageing is 15-25 DEG C, described old
The time of change is 3-5 months, and the temperature of the filtering is 10 DEG C or less.
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| CN112717184A (en) * | 2019-10-14 | 2021-04-30 | 广州汽车集团股份有限公司 | Vehicle fragrance spice and preparation method thereof |
| CN112717185A (en) * | 2019-10-14 | 2021-04-30 | 广州汽车集团股份有限公司 | Vehicle fragrance spice and preparation method thereof |
| CN113214922A (en) * | 2021-06-17 | 2021-08-06 | 广州馨誉香料有限公司 | Preparation process of long-acting fragrance-retaining composition |
| CN113512467A (en) * | 2021-05-11 | 2021-10-19 | 上海应用技术大学 | Citrus-ginger fragrance air freshener and preparation method thereof |
| CN114712268A (en) * | 2021-01-04 | 2022-07-08 | 广州汽车集团股份有限公司 | Anti-fatigue perfume, and preparation method and application thereof |
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| CN112717185A (en) * | 2019-10-14 | 2021-04-30 | 广州汽车集团股份有限公司 | Vehicle fragrance spice and preparation method thereof |
| CN114712268A (en) * | 2021-01-04 | 2022-07-08 | 广州汽车集团股份有限公司 | Anti-fatigue perfume, and preparation method and application thereof |
| CN113512467A (en) * | 2021-05-11 | 2021-10-19 | 上海应用技术大学 | Citrus-ginger fragrance air freshener and preparation method thereof |
| CN113214922A (en) * | 2021-06-17 | 2021-08-06 | 广州馨誉香料有限公司 | Preparation process of long-acting fragrance-retaining composition |
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| CN110251425B (en) | 2021-11-12 |
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