CN113214922A - Preparation process of long-acting fragrance-retaining composition - Google Patents
Preparation process of long-acting fragrance-retaining composition Download PDFInfo
- Publication number
- CN113214922A CN113214922A CN202110670977.4A CN202110670977A CN113214922A CN 113214922 A CN113214922 A CN 113214922A CN 202110670977 A CN202110670977 A CN 202110670977A CN 113214922 A CN113214922 A CN 113214922A
- Authority
- CN
- China
- Prior art keywords
- raw materials
- vessel
- equal
- less
- digital display
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 213
- 238000000034 method Methods 0.000 claims abstract description 75
- 239000003205 fragrance Substances 0.000 claims abstract description 25
- YPZUZOLGGMJZJO-LQKXBSAESA-N ambroxan Chemical compound CC([C@@H]1CC2)(C)CCC[C@]1(C)[C@@H]1[C@]2(C)OCC1 YPZUZOLGGMJZJO-LQKXBSAESA-N 0.000 claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 14
- 239000001147 (3aR,5aS,9aS,9bR)-3a,6,6,9a-tetramethyl-2,4,5,5a,7,8,9,9b-octahydro-1H-benzo[e][1]benzofuran Substances 0.000 claims abstract description 11
- 238000005303 weighing Methods 0.000 claims description 57
- 238000003756 stirring Methods 0.000 claims description 45
- 238000003860 storage Methods 0.000 claims description 43
- 239000007787 solid Substances 0.000 claims description 15
- 230000005923 long-lasting effect Effects 0.000 claims description 11
- JBDGDEWWOUBZPM-XYPYZODXSA-N ambroxol Chemical compound NC1=C(Br)C=C(Br)C=C1CN[C@@H]1CC[C@@H](O)CC1 JBDGDEWWOUBZPM-XYPYZODXSA-N 0.000 claims description 9
- 229960005174 ambroxol Drugs 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 9
- 150000002576 ketones Chemical class 0.000 claims description 7
- 238000007789 sealing Methods 0.000 claims description 7
- 239000011521 glass Substances 0.000 claims description 6
- 210000001503 joint Anatomy 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 abstract description 13
- YPZUZOLGGMJZJO-UHFFFAOYSA-N ambrofix Natural products C1CC2C(C)(C)CCCC2(C)C2C1(C)OCC2 YPZUZOLGGMJZJO-UHFFFAOYSA-N 0.000 abstract description 12
- 230000014759 maintenance of location Effects 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 5
- 230000002045 lasting effect Effects 0.000 abstract description 3
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 26
- 239000000686 essence Substances 0.000 description 12
- 239000003599 detergent Substances 0.000 description 10
- 150000001875 compounds Chemical class 0.000 description 6
- 238000005352 clarification Methods 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 238000007605 air drying Methods 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 230000004584 weight gain Effects 0.000 description 1
- 235000019786 weight gain Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a process for preparing a long-acting fragrance-retaining composition, which comprises the following raw materials in parts by weight: z11 is less than or equal to 10, ambrox is less than or equal to 10, amber core is less than or equal to 20, ambrox is less than or equal to 30 and ambroxone is less than or equal to 30, firstly, the raw material preparation procedure is carried out, and Z11, ambrox, amber core and ambrox are firstly prepared; according to the invention, Z11, ambergris costustoot, ambroxone, amber core and ambroxan are mixed and dissolved together to form a composition, and the composition can cover the odor of a washing aid component and a washing liquid base material in the washing liquid and can emit fragrance after being mixed with the washing liquid by utilizing the high-strength lasting fragrance retention property and high-strength fragrance stability of the composition.
Description
Technical Field
The invention relates to the technical field of essence and spice manufacturing, in particular to a manufacturing process of a long-acting fragrance-retaining composition.
Background
The essence is a mixture which is prepared by manual work and contains more than two or dozens of spices, and sometimes contains proper solvent or carrier, and has certain fragrance. In order to increase the fragrance of clothes, people can mix the laundry detergent and the essence, clean the clothes after mixing, and then when the existing essence and the laundry detergent are mixed for use, the fragrance in the essence can be covered by the washing assistant components in the laundry detergent and the odor emitted by the laundry detergent base material, and the boiling point of the existing essence is low, so that the fragrance retention of the essence is low, the effect of long-acting fragrance retention cannot be achieved, and the cost performance of the essence is greatly reduced.
Disclosure of Invention
The invention aims to provide a process for preparing a long-acting fragrance-retaining composition, which solves the problem that the fragrance in the existing essence can be covered by the odor emitted by the washing assistant components and the base materials of the laundry detergent.
In order to achieve the purpose, the invention provides the following technical scheme: the long-acting fragrance-retaining composition comprises the following raw materials in parts by weight:
z11 is less than or equal to 10, ambrofuran is less than or equal to 10, amber core is less than or equal to 20, ambergris root is less than or equal to 30, and ambergris ketone is less than or equal to 30.
A process for preparing a long-lasting fragrance-retaining composition, comprising the steps of:
step 1: preparing raw materials: firstly, preparing Z11, ambroxan, amber core and ambroxol, and then weighing the Z11, the ambroxan, the amber core and the ambroxol by using a weighing device according to the proportioning requirement;
step 2: storing raw materials: after the raw materials are weighed, the weighed Z11, ambroxan, amber core and ambroxol are all poured into a vessel to wait for the next procedure;
and step 3: mixing raw materials: after the raw materials are poured into the vessel, putting a rotor into the vessel, then placing the vessel on a digital display constant-temperature magnetic stirrer, setting the revolution of the digital display constant-temperature magnetic stirrer according to the requirement after the vessel is placed, and starting the digital display constant-temperature magnetic stirrer to stir uniformly after the revolution is set;
and 4, step 4: and (3) storing the mixture: after the raw materials are stirred and mixed, the raw materials are poured into a storage bottle and then stored, and the preparation of the raw materials is finished.
Preferably, in step 1, before the raw materials are weighed, the raw materials are cleaned to ensure that the purity of the raw materials is free from errors, after the raw materials are cleaned, the raw materials are checked again to check whether the raw materials deteriorate or not, the raw materials are immediately replaced if the raw materials deteriorate, and the raw materials are normally subjected to the next process.
Preferably, in the step 1, the bottom of the weighing device is kept flat in the raw material weighing process, so that the deviation of the precision of the weighing process caused by the inclination of the weighing device is avoided, and the top of the heavy device is cleaned before weighing, so that the influence of impurities on the weighing precision is avoided.
Preferably, in step 2, before the household utensils were poured into to the raw materials, use funnel and household utensils butt joint, in the raw materials passed through funnel entering household utensils, the raw materials was emptyd the in-process, guaranteed that the raw materials can not appear the water clock, and the raw materials is deposited household utensils and is adopted transparent glass bottle, conveniently observes the raw materials stirring condition.
Preferably, in the step 3, before the raw material is poured into the vessel, the funnel is used for butt joint with the vessel, the raw material enters the vessel through the funnel, and the raw material is prevented from dripping and leaking in the pouring process.
Preferably, in step 3, the digital display constant temperature magnetic stirrer sets corresponding revolution numbers according to different weights, the revolution number of the digital display constant temperature magnetic stirrer increases along with the increase of the weights, the digital display constant temperature magnetic stirrer ensures the uniform rotation of the liquid in the stirring process, and a vortex is preferably arranged in the middle of a horizontal plane.
Preferably, in step 3, the stirring time of the digital display constant temperature magnetic stirrer is based on that after the raw materials are stirred to be clear and transparent without solids, the stirring is carried out for 10 minutes, the stirring time cannot be too much or too little, and the raw materials are stirred to be clear and transparent without solids and then are timed by a timer.
Preferably, in step 3, when the solid which is not dissolved in the raw material for a long time is encountered during the stirring process, the raw material may be heated at a constant temperature of 55 ℃ until the raw material is completely dissolved.
Preferably, in the step 4, after the raw materials are filled into the corresponding storage bottles, the corresponding numbers, names, dates and the like are attached to the storage bottles, then sealing is performed, whether the storage bottles have air leakage conditions or not is checked after sealing, the storage bottles are immediately blocked if the air leakage conditions exist, the air circulation phenomenon of the storage bottles is avoided, and the storage bottles need to be placed in cool and dry places for storage after being sealed.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, Z11, ambergris costustoot, ambroxone, amber core and ambroxan are mixed to be completely dissolved and mixed together to form a composition, and the composition can cover the odor of a washing aid component and a washing liquid base material in the washing liquid after being mixed with the washing liquid by utilizing the high-strength lasting fragrance retention property and the high-strength fragrance stability of the composition, so that the fragrance can be released, and the composition can keep the lasting fragrance by utilizing the characteristic of high boiling point of the composition, so that the fragrance retention property is prolonged, the cost performance is improved, and the problem that the fragrance in essence can be covered by the odor of the washing aid component and the washing liquid base material in the washing liquid is effectively solved.
Detailed Description
The present invention will now be described in more detail by way of examples, which are given by way of illustration only and are not intended to limit the scope of the present invention in any way.
The invention provides a technical scheme that: the long-acting fragrance-retaining composition comprises the following raw materials in parts by weight:
z11 is less than or equal to 10, ambrofuran is less than or equal to 10, amber core is less than or equal to 20, ambergris root is less than or equal to 30, and ambergris ketone is less than or equal to 30.
A process for preparing a long-lasting fragrance-retaining composition, comprising the steps of:
step 1: preparing raw materials: firstly, preparing Z11, ambroxan, amber core and ambroxol, and then weighing the Z11, the ambroxan, the amber core and the ambroxol by using a weighing device according to the proportioning requirement;
step 2: storing raw materials: after the raw materials are weighed, the weighed Z11, ambroxan, amber core and ambroxol are all poured into a vessel to wait for the next procedure;
and step 3: mixing raw materials: after the raw materials are poured into the vessel, putting a rotor into the vessel, then placing the vessel on a digital display constant-temperature magnetic stirrer, setting the revolution of the digital display constant-temperature magnetic stirrer according to the requirement after the vessel is placed, and starting the digital display constant-temperature magnetic stirrer to stir uniformly after the revolution is set;
and 4, step 4: and (3) storing the mixture: after the raw materials are stirred and mixed, the raw materials are poured into a storage bottle and then stored, and the preparation of the raw materials is finished.
The first embodiment is as follows:
z11 is less than or equal to 10, ambrox is less than or equal to 10, amber core is less than or equal to 20, ambrox is less than or equal to 30 and ambroxone is less than or equal to 30, firstly, a raw material preparation procedure is carried out, Z11, ambrox, amber core and ambrox are prepared, then Z11, ambrox, amber core and ambrox are weighed by using a weighing device according to the needs of mixture ratio, then a raw material storage procedure is carried out, after the raw materials are weighed, Z11, ambrox, amber core and ambrox are all poured into a vessel, the next procedure is waited, then a raw material mixing procedure is carried out, after the raw materials are poured into the vessel, a rotor is placed in the vessel, then the vessel is placed on a digital display constant temperature magnetic stirrer, the revolution number of the digital display constant temperature magnetic stirrer is set according to needs, the digital display constant temperature magnetic stirrer is started for uniform stirring after the revolution number of the vessel is set, finally, a mixture storage procedure is carried out, after the raw materials are stirred and mixed, and pouring the raw materials into a storage bottle, and then storing to finish the preparation of the raw materials.
Example two:
in the first embodiment, the following steps are added:
in step 1, the raw materials is cleared up before weighing, guarantees that raw materials purity is error-free, checks the raw materials again after the clearance, and whether the inspection raw materials appear rotten, and the raw materials is rotten and is then changed immediately, and the raw materials is normal then carries out next process, and the raw materials is weighed in-process and will be kept weighing device bottom level and smooth, avoids weighing device slope to lead to weighing process precision to the deviation appears to clear up heavy device top before weighing, avoids having impurity to influence the weighing precision.
Z11 is less than or equal to 10, ambergris furan is less than or equal to 10, amber core is less than or equal to 20, ambergris aucklandia root is less than or equal to 30 and ambergris ketone is less than or equal to 30, raw material preparation is firstly carried out, Z11, ambergris furan, amber core and ambergris aucklandia root are firstly prepared, then Z11, ambergris furan, amber core and ambergris aucklandia root are weighed by using a weighing device according to the proportion requirement, the raw materials are cleaned before being weighed, the purity of the raw materials is ensured to be free from error, the raw materials are inspected again after being cleaned, whether the raw materials are deteriorated or not is checked, the raw materials are immediately replaced when being deteriorated, the next procedure is carried out when the raw materials are normal, the bottom of the weighing device is kept flat in the weighing process of the raw materials, the deviation of the weighing process caused by the inclination of the weighing device is avoided, the top of the heavy device is cleaned before being weighed, the weighing is prevented from influencing the weighing precision, then the raw materials are stored and put in the procedure, after the weighing of the raw materials is completed, the method comprises the following steps of pouring weighed Z11, ambergris furan, amber core and ambergris costustoot into a vessel, waiting for the next process, then performing a raw material mixing process, pouring raw materials into the vessel, putting a rotor into the vessel, then placing the vessel on a digital display constant-temperature magnetic stirrer, setting the revolution number of the digital display constant-temperature magnetic stirrer as required after the vessel is placed, opening the digital display constant-temperature magnetic stirrer for uniform stirring after the revolution number is set, and finally performing a mixture storage process, pouring the raw materials into a storage bottle after the raw materials are stirred and mixed, and then storing to finish the raw material preparation.
Example three:
in the second embodiment, the following steps are added:
in step 2, before the household utensils were poured into to the raw materials, use funnel and household utensils butt joint, in the raw materials got into the household utensils through the funnel, the raw materials was emptyd the in-process, guaranteed that the water clock can not appear in the raw materials, and the household utensils are deposited to the raw materials and are adopted the clear glass bottle, conveniently observe the raw materials stirring condition, before the household utensils was poured into to the raw materials, use funnel and household utensils butt joint, the raw materials passed through in the funnel gets into the household utensils, the raw materials was emptyd the in-process, guaranteed that the water clock can not appear in the raw materials.
Z11 is less than or equal to 10, ambergris furan is less than or equal to 10, amber core is less than or equal to 20, ambergris aucklandia root is less than or equal to 30 and ambergris ketone is less than or equal to 30, raw material preparation is firstly carried out, Z11, ambergris furan, amber core and ambergris aucklandia root are firstly prepared, then Z11, ambergris furan, amber core and ambergris aucklandia root are weighed by using a weighing device according to the proportion requirement, the raw materials are cleaned before being weighed, the purity of the raw materials is ensured to be free from error, the raw materials are inspected again after being cleaned, whether the raw materials are deteriorated or not is checked, the raw materials are immediately replaced when being deteriorated, the next procedure is carried out when the raw materials are normal, the bottom of the weighing device is kept flat in the weighing process of the raw materials, the deviation of the weighing process caused by the inclination of the weighing device is avoided, the top of the heavy device is cleaned before being weighed, the weighing is prevented from influencing the weighing precision, then the raw materials are stored and put in the procedure, after the weighing of the raw materials is completed, the method comprises the steps of pouring weighed Z11, ambrofuran, amber cores and ambergris costustoot into a vessel, waiting for the next process, before pouring raw materials into the vessel, butting the raw materials with the vessel by using a funnel, enabling the raw materials to enter the vessel through the funnel, ensuring that the raw materials do not leak during pouring of the raw materials, adopting a transparent glass bottle as a raw material storage vessel, conveniently observing the stirring condition of the raw materials, before pouring the raw materials into the vessel, butting the raw materials with the vessel by using the funnel, enabling the raw materials to enter the vessel through the funnel, ensuring that the raw materials do not leak during pouring of the raw materials, then performing a raw material mixing process, after pouring the raw materials into the vessel, putting a rotor into the vessel, then placing the vessel on a digital display constant temperature magnetic stirrer, setting the revolution number of the digital display constant temperature magnetic stirrer according to needs after placing the vessel, starting the digital display constant temperature magnetic stirrer to uniformly stir after setting the revolution number, and finally performing a mixture storage process, after the raw materials are stirred and mixed, the raw materials are poured into a storage bottle and then stored, and the preparation of the raw materials is finished.
Example four:
in the third embodiment, the following steps are added:
in step 3, the corresponding revolution of digital display constant temperature magnetic stirrers sets up according to different weight, the revolution of digital display constant temperature magnetic stirrers increases along with weight increase, the even rotation of liquid is guaranteed to the stirring in-process of digital display constant temperature magnetic stirrers, and it is suitable to have the swirl in the middle of the horizontal plane, the time of digital display constant temperature magnetic stirrers stirring is according to the raw materials stirring to the transparent no solid back of clarification, it is accurate to carry out 10 minutes stirring again, stirring time can not be too much, also can not be too little, the raw materials stirring is regularly with the timer after the transparent no solid of clarification, when meeting the long-time undissolved solid of raw materials in the stirring, can carry out constant temperature heating 55 ℃, until the raw materials dissolves completely.
Z11 is less than or equal to 10, ambergris furan is less than or equal to 10, amber core is less than or equal to 20, ambergris aucklandia root is less than or equal to 30 and ambergris ketone is less than or equal to 30, raw material preparation is firstly carried out, Z11, ambergris furan, amber core and ambergris aucklandia root are firstly prepared, then Z11, ambergris furan, amber core and ambergris aucklandia root are weighed by using a weighing device according to the proportion requirement, the raw materials are cleaned before being weighed, the purity of the raw materials is ensured to be free from error, the raw materials are inspected again after being cleaned, whether the raw materials are deteriorated or not is checked, the raw materials are immediately replaced when being deteriorated, the next procedure is carried out when the raw materials are normal, the bottom of the weighing device is kept flat in the weighing process of the raw materials, the deviation of the weighing process caused by the inclination of the weighing device is avoided, the top of the heavy device is cleaned before being weighed, the weighing is prevented from influencing the weighing precision, then the raw materials are stored and put in the procedure, after the weighing of the raw materials is completed, the method comprises the steps of pouring weighed Z11, ambrofuran, amber cores and ambergris costustoot into a vessel, waiting for the next process, before pouring raw materials into the vessel, butting the raw materials with the vessel by using a funnel, enabling the raw materials to enter the vessel through the funnel, ensuring that the raw materials do not leak during pouring of the raw materials, adopting a transparent glass bottle as a raw material storage vessel, facilitating observation of the stirring condition of the raw materials, before pouring the raw materials into the vessel, butting the raw materials with the vessel by using the funnel, enabling the raw materials to enter the vessel through the funnel, ensuring that the raw materials do not leak during pouring of the raw materials, then performing a raw material mixing process, after pouring the raw materials into the vessel, placing a rotor in the vessel, then placing the vessel on a digital display constant temperature magnetic stirrer, setting the revolution number of the digital display constant temperature magnetic stirrer according to needs after placing the vessel, starting the digital display constant temperature magnetic stirrer to uniformly stir, setting corresponding revolution numbers by the digital display constant temperature magnetic stirrer according to different weights, the revolution of digital display constant temperature magnetic stirrers increases along with weight gain, the even rotation of liquid is guaranteed to digital display constant temperature magnetic stirrers stirring in-process, and it is advisable to have the swirl in the middle of the horizontal plane, the time of digital display constant temperature magnetic stirrers stirring is after the transparent nothing solid of clarification according to the raw materials stirring, it is accurate to carry out the 10 minutes stirring again, the churning time can not be too much, also can be too little, the raw materials stirring is regularly with the timer after the transparent nothing solid of clarification, when the long-time undissolved solid of raw materials of chance raw materials is met in the stirring process, can carry out constant temperature heating 55 ℃, until the raw materials dissolves completely, carry out mixture storage process at last, treat the raw materials stirring and mix the back, pour the storage bottle into the raw materials, accomplish the raw materials preparation promptly after storing afterwards.
Example five:
in the fourth example, the following steps were added:
in step 4, after the raw materials are filled into the corresponding storage bottles, the corresponding numbers, names, dates and the like are pasted on the storage bottles, then sealing is carried out, whether the storage bottles have air leakage conditions or not is checked after sealing, air leakage is immediately blocked, the storage bottles are guaranteed not to have air circulation, and the storage bottles are required to be placed in shady and cool places and dry places for storage after being sealed.
Z11 is less than or equal to 10, ambergris furan is less than or equal to 10, amber core is less than or equal to 20, ambergris aucklandia root is less than or equal to 30 and ambergris ketone is less than or equal to 30, raw material preparation is firstly carried out, Z11, ambergris furan, amber core and ambergris aucklandia root are firstly prepared, then Z11, ambergris furan, amber core and ambergris aucklandia root are weighed by using a weighing device according to the proportion requirement, the raw materials are cleaned before being weighed, the purity of the raw materials is ensured to be free from error, the raw materials are inspected again after being cleaned, whether the raw materials are deteriorated or not is checked, the raw materials are immediately replaced when being deteriorated, the next procedure is carried out when the raw materials are normal, the bottom of the weighing device is kept flat in the weighing process of the raw materials, the deviation of the weighing process caused by the inclination of the weighing device is avoided, the top of the heavy device is cleaned before being weighed, the weighing is prevented from influencing the weighing precision, then the raw materials are stored and put in the procedure, after the weighing of the raw materials is completed, the method comprises the steps of pouring weighed Z11, ambrofuran, amber cores and ambergris costustoot into a vessel, waiting for the next process, before pouring raw materials into the vessel, butting the raw materials with the vessel by using a funnel, enabling the raw materials to enter the vessel through the funnel, ensuring that the raw materials do not leak during pouring of the raw materials, adopting a transparent glass bottle as a raw material storage vessel, facilitating observation of the stirring condition of the raw materials, before pouring the raw materials into the vessel, butting the raw materials with the vessel by using the funnel, enabling the raw materials to enter the vessel through the funnel, ensuring that the raw materials do not leak during pouring of the raw materials, then performing a raw material mixing process, after pouring the raw materials into the vessel, placing a rotor in the vessel, then placing the vessel on a digital display constant temperature magnetic stirrer, setting the revolution number of the digital display constant temperature magnetic stirrer according to needs after placing the vessel, starting the digital display constant temperature magnetic stirrer to uniformly stir, setting corresponding revolution numbers by the digital display constant temperature magnetic stirrer according to different weights, the revolution number of the digital display constant-temperature magnetic stirrer is increased along with the increase of the weight, the digital display constant-temperature magnetic stirrer ensures the uniform rotation of liquid in the stirring process, and is suitable for a vortex in the middle of a horizontal plane, the stirring time of the digital display constant-temperature magnetic stirrer is based on that the raw material is stirred to be clear and transparent and has no solid, then the stirring is carried out for 10 minutes, the stirring time cannot be too much or too little, the raw material is timed by a timer after being stirred to be clear and transparent and has no solid, the constant-temperature heating at 55 ℃ can be carried out when the raw material meets the solid which is not dissolved for a long time in the stirring process until the raw material is completely dissolved, finally, a mixture storage procedure is carried out, after the raw material is stirred and mixed, the raw material is poured into a storage bottle, then the raw material preparation is completed by storage, after the raw material is filled into the corresponding storage bottle, the storage bottle is pasted with the corresponding number, name, date and the like, and then the sealing is carried out, whether there is the gas leakage condition in sealed back inspection storage bottle, the shutoff immediately then exists gas leakage, guarantees that the circulation of air phenomenon can not appear in the storage bottle, and the storage bottle is sealed the back and need be placed in shady and cool and dry department and preserve.
Experimental procedure
Firstly, experimental comparison:
1. preparing the long-acting fragrance-retaining compound.
2. The long-acting fragrance-retaining compound is compared with each single component in the long-acting fragrance-retaining compound and the double components respectively, and the fragrance-retaining effect is verified.
Secondly, a verification method:
1. dipping equal amount of liquid with fragrance-smelling paper respectively, placing for 0h, 2h, 5h, 8h, 1t, 2t, 3t, 5t, 10t, 12t, 15t, 21t and 28t, then performing fragrance evaluation, multi-person test, comprehensive grading, and selecting the result of the best long-acting fragrance-retaining compound.
2. The long-acting fragrance-retaining compound is applied to the laundry detergent essences, and a certain amount of long-acting fragrance-retaining compound is added to different laundry detergent essences and mixed and stirred.
3. Respectively adding the non-lengthened effective fragrance-retaining composition and the essence added with the long-acting fragrance-retaining composition into the laundry detergent, adding 3 percent of the added amount of the mixture, fully stirring and emulsifying, adding the same amount of the laundry detergent into 1000ml of water with the same amount, uniformly stirring, putting the same towel, marking, kneading the same person with the same hand power under 30 parts of the front surface and 30 parts of the back surface, fully contacting the laundry detergent with the hand power, standing for 30 minutes, taking out, and airing in a ventilated place.
4. After air-drying, evaluation was performed by the evaluation department.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (10)
1. A long-lasting fragrance composition characterized by: the raw materials are as follows:
z11 is less than or equal to 10, ambrofuran is less than or equal to 10, amber core is less than or equal to 20, ambergris root is less than or equal to 30, and ambergris ketone is less than or equal to 30.
2. A manufacturing process of a long-acting fragrance-retaining composition is characterized in that: the method comprises the following steps:
step 1: preparing raw materials: firstly, preparing Z11, ambroxan, amber core and ambroxol, and then weighing the Z11, the ambroxan, the amber core and the ambroxol by using a weighing device according to the proportioning requirement;
step 2: storing raw materials: after the raw materials are weighed, the weighed Z11, ambroxan, amber core and ambroxol are all poured into a vessel to wait for the next procedure;
and step 3: mixing raw materials: after the raw materials are poured into the vessel, putting a rotor into the vessel, then placing the vessel on a digital display constant-temperature magnetic stirrer, setting the revolution of the digital display constant-temperature magnetic stirrer according to the requirement after the vessel is placed, and starting the digital display constant-temperature magnetic stirrer to stir uniformly after the revolution is set;
and 4, step 4: and (3) storing the mixture: after the raw materials are stirred and mixed, the raw materials are poured into a storage bottle and then stored, and the preparation of the raw materials is finished.
3. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in the step 1, the raw materials are cleaned before being weighed, so that the purity of the raw materials is ensured to be free from errors, the raw materials are checked again after being cleaned, whether the raw materials deteriorate or not is checked, the raw materials are immediately replaced when the raw materials deteriorate, and the next procedure is carried out when the raw materials are normal.
4. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in the step 1, the bottom of the weighing device is kept flat in the raw material weighing process, deviation of precision in the weighing process caused by inclination of the weighing device is avoided, the top of the heavy device is cleaned before weighing, and the weighing precision is prevented from being influenced by impurities.
5. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in step 2, before the household utensils were poured into to the raw materials, use funnel and household utensils butt joint, in the raw materials got into the household utensils through the funnel, the raw materials was emptyd the in-process, guaranteed that the water clock can not appear in the raw materials, and the raw materials is deposited the household utensils and is adopted transparent glass bottle, and the convenience is observed the raw materials stirring condition.
6. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in step 3, before the raw materials are poured into the vessel, the funnel is used for being in butt joint with the vessel, the raw materials enter the vessel through the funnel, and the raw materials are prevented from dripping and leaking in the pouring process.
7. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in the step 3, the digital display constant-temperature magnetic stirrer is provided with corresponding revolution according to different weights, the revolution of the digital display constant-temperature magnetic stirrer is increased along with the increase of the weights, the uniform rotation of the liquid is ensured in the stirring process of the digital display constant-temperature magnetic stirrer, and a vortex is preferably arranged in the middle of a horizontal plane.
8. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in the step 3, the stirring time of the digital display constant temperature magnetic stirrer is based on that the stirring is carried out for 10 minutes after the raw materials are stirred to be clear and transparent without solids, the stirring time cannot be too much or too little, and the raw materials are stirred to be clear and transparent without solids and then are timed by a timer.
9. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in the step 3, when the raw materials meet the solid which is not dissolved for a long time in the stirring process, the raw materials can be heated at a constant temperature of 55 ℃ until the raw materials are completely dissolved.
10. A process for the manufacture of a long lasting fragrance composition according to claim 2, wherein: in step 4, after the raw materials are loaded into the corresponding storage bottles, the corresponding numbers, names, dates and the like are pasted on the storage bottles, then sealing is carried out, whether the storage bottles have air leakage conditions or not is checked after sealing, the storage bottles are immediately blocked if the air leakage conditions exist, the air circulation phenomenon of the storage bottles is guaranteed, and the storage bottles need to be placed in shady and cool places and dry places for storage after being sealed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110670977.4A CN113214922A (en) | 2021-06-17 | 2021-06-17 | Preparation process of long-acting fragrance-retaining composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110670977.4A CN113214922A (en) | 2021-06-17 | 2021-06-17 | Preparation process of long-acting fragrance-retaining composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113214922A true CN113214922A (en) | 2021-08-06 |
Family
ID=77080428
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110670977.4A Pending CN113214922A (en) | 2021-06-17 | 2021-06-17 | Preparation process of long-acting fragrance-retaining composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113214922A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114053894A (en) * | 2021-10-27 | 2022-02-18 | 广州馨誉香料有限公司 | Method for manufacturing essence with good fragrance retaining effect special for spinning |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108368450A (en) * | 2015-12-11 | 2018-08-03 | 奇华顿股份有限公司 | In organic compound or associated improvement |
| CN110251425A (en) * | 2019-06-19 | 2019-09-20 | 广州市珍馨香精香料有限公司 | A kind of natural essential oil fragrance perfume and preparation method thereof |
-
2021
- 2021-06-17 CN CN202110670977.4A patent/CN113214922A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108368450A (en) * | 2015-12-11 | 2018-08-03 | 奇华顿股份有限公司 | In organic compound or associated improvement |
| CN110251425A (en) * | 2019-06-19 | 2019-09-20 | 广州市珍馨香精香料有限公司 | A kind of natural essential oil fragrance perfume and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114053894A (en) * | 2021-10-27 | 2022-02-18 | 广州馨誉香料有限公司 | Method for manufacturing essence with good fragrance retaining effect special for spinning |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN113214922A (en) | Preparation process of long-acting fragrance-retaining composition | |
| CN102802595A (en) | Hair dye, dyeing hair product combination and its use method | |
| CN106039361A (en) | Air freshener and preparation method thereof | |
| CN104448927B (en) | A kind of composite reactive blue dye | |
| US3056644A (en) | Dyeing compositions | |
| JP6259217B2 (en) | Liquid detergent composition for clothing | |
| US4060505A (en) | Compositions for souring and softening laundered textile materials and stock solutions prepared therefrom | |
| CN106568719A (en) | Chili oil color fast detection and adjustment method | |
| CN109322159A (en) | A kind of antioxidative method for cleaning of raising fishing net | |
| CN113736576A (en) | Washing gel bead and preparation method thereof | |
| CN107596933A (en) | A kind of compounding and production process of essence | |
| CN209406337U (en) | A kind of liquid detergent pipeline hybrid system | |
| KR101479008B1 (en) | Preparation method for softener | |
| CN110610854A (en) | Preparation method of diffused phosphorus source | |
| JP2006232798A (en) | Gelatin hard capsule having enhanced film strength | |
| CN108524321A (en) | A kind of reduction cutaneous pigmentation topical composition and preparation method thereof | |
| JP2011055749A (en) | Method for producing amazake | |
| CN202124751U (en) | High-precision color blending and copying dyeing device | |
| US26271A (en) | Berfthakd koegel | |
| JP2939769B2 (en) | Solid detergent for flush toilet | |
| CN107217518A (en) | A kind of firm elevator of perspiration resistance and preparation method thereof, application | |
| CN116602930A (en) | Preparation method of hydroxypropyl starch hollow capsules | |
| US493460A (en) | Moses wool | |
| US1289968A (en) | Dye. | |
| UA149642U (en) | METHOD OF OBTAINING A SOLID SHAMPOO FOR OILY HAIR |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |