CN107217518A - A kind of firm elevator of perspiration resistance and preparation method thereof, application - Google Patents
A kind of firm elevator of perspiration resistance and preparation method thereof, application Download PDFInfo
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- CN107217518A CN107217518A CN201710605292.5A CN201710605292A CN107217518A CN 107217518 A CN107217518 A CN 107217518A CN 201710605292 A CN201710605292 A CN 201710605292A CN 107217518 A CN107217518 A CN 107217518A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/06—After-treatment with organic compounds containing nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/30—Material containing basic nitrogen containing amide groups furs feathers, dead hair, furskins, pelts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention provides a kind of firm elevator of perspiration resistance, mainly it is made by following raw material：In terms of mass fraction, 10 200 parts of sulfonylurea, 10 100 parts of organic solvent, 1 10 parts of film forming agent, 20 200 parts of water.Preparation method includes：(A) sulfonylurea and water are mixed until dissolving, temperature control is at 25 30 DEG C；(B) cool the temperature to after 15 20 DEG C, add film forming agent, organic solvent and continue to stir 30 60min, produce.The firm elevator of perspiration resistance of the embodiment of the present invention can be very good to apply in fur dyeing last handling process, perspiration resistance is functional, stability is high, with very strong specific aim, the perspiration fastness of fur dyeing field fur in itself be compensate for generally than relatively low phenomenon, for further expanding fur market scope, improve sales volume and be respectively provided with great meaning.
Description
Technical field
The present invention relates to animal fur manufacture field, in particular to a kind of firm elevator of perspiration resistance and its preparation
Method, application.
Background technology
At present, the fastness to perspiration elevator product of market sale is essentially all using on the textile, just because of living
Property dyed cotton clothes contact human sweat after, through sunlight irradiation be particularly easy to occur become fade (to sweat photoreactivation color fastness：Cause
Acted on by amino acid in human sweat, photooxidation decomposition reaction will be caused to occur to become colour fading), and for the clothes finished product of sale,
Turn into an important indicator of examination quality of textile products with sweat proof light fastness, if not up to standard may influence whether clothes itself
The sales volume of finished product, so the firm elevator application of perspiration resistance is widely.
However, the fastness to perspiration elevator applied to textile sold on the market, it is necessary to post-processing temperature it is general
Higher, majority is more than 100 DEG C, and so high treatment temperature is not particularly suited for fur dyeing industry, because fur dyeing industry
It is that quality of the meeting on dermatotome in itself is influential if post-processing temperature is too high.In addition, conventional fastness to perspiration is carried on the market
Agent is risen, for fur industry, its technique for applying is complicated, condition is harsh, is also not particularly suited for the dyeing of fur dyestuff
Post processing.
Therefore, how to research and develop a kind of fastness to perspiration elevator suitable for fur dyeing sector application is urgently
The technical problem of solution.
In view of this, it is special to propose the present invention.
The content of the invention
The first object of the present invention is to provide a kind of perspiration resistance firm elevator, and the perspiration resistance firmly lifts agent prescription letter
Single, raw material sources are extensively easily obtained, and perspiration resistance is functional, is highly suitable for the after-treatment applications of fur acid dyes, stable
Property it is high, using convenient, the fur perspiration fastness after dyeing can be improved to half grade to one-level, correlation technique blank has been filled up, be worth
Obtain wide popularization and application.
The second object of the present invention is the preparation method for providing the firm elevator of above-mentioned perspiration resistance, the work of the preparation method
Skill is simple, and easy to operate, operating condition is gentleer, and whole processing step is successive close, is produced without any three wastes, green ring
Protect.
The third object of the present invention is the application for providing the firm elevator of above-mentioned perspiration resistance, the firm elevator of the perspiration resistance
It can be very good to apply in fur dyeing last handling process, with very strong specific aim, compensate for fur dyeing field fur
The perspiration fastness of itself is generally than relatively low phenomenon, and for further expanding fur market scope, raising sales volume is respectively provided with great
Meaning.
In order to realize the above-mentioned purpose of the present invention, spy uses following technical scheme：
The invention provides a kind of firm elevator of perspiration resistance, mainly it is made by following raw material：In terms of mass fraction, ureas
10-200 parts of material, 10-100 parts of organic solvent, 1-10 parts of film forming agent, 20-200 parts of water.
The firm elevator of perspiration resistance of the prior art be essentially all using on the textile, it is necessary to post-processing temperature
General higher, majority is more than 100 DEG C, and so high treatment temperature is not particularly suited for fur dyeing industry, because fur dyeing
It is that quality of the meeting on dermatotome in itself is influential if industry post-processing temperature is too high.In addition, conventional perspiration resistance is firm on the market
Elevator is spent, for fur industry, its technique for applying is complicated, condition is harsh, is also not particularly suited for fur dyestuff
Dyeing post processing.
The present invention provides a kind of firm elevator of perspiration resistance suitable for fur industry to solve above technical problem,
The formula of the firm elevator of the perspiration resistance is fairly simple, is mainly made up of four kinds of components, wherein sulfonylurea, organic solvent, into
Film is major ingredient, is to primarily serve the component that perspiration resistance firmly lifts effect, sweat composition：NaCL：5g/L, sodium lactate：5g/L,
Glycine：0.5g/L, urea：0.5g/L, ammoniacal liquor：0.1ml/L (pH is 8 or so), passes through mating reaction and grease, the sweat of three
Stain can form complex compound, to decompose amino acid so as to reach the purpose of removal sweat stain, and can also be in fur goods surface shape
Into protective layer so that fur goods is not infected with grease and sweat stain in use, does not contact with each other, so virtually
The service life of fur goods in itself is improved indirectly, and can also be correspondingly improved the stability of fur after dyeing, including light
Stability, heat endurance and chemical stability.
The firm elevator of sweat stain of the present invention is different from the existing common firm elevator of sweat stain on the market, and it is by with one
After quantitative water formation mixed solution, the inside of fur goods, and stability can be directly penetrated into after being contacted with fur goods
Compare and high be difficult to separate in itself with fur, moreover it is possible to form layer protective layer on the surface of fur, refuse grease, sweat stain in fur it
Outside, the presence of organic solvent can also play a part of hydrotropy, and the materials such as urea can be promoted to be dissolved in water, to reach preferably
Effect to fur goods perspiration resistance.Film forming agent is the thing as its main effect that diaphragm can be formed on fur surface
Matter, by add the material can be formed on fur surface one layer stick together firmly, with certain flexibility, extensibility and elasticity,
The continuous uniform film of rub resistance, water resistance etc..
Preferably, sulfonylurea can include：One in urea, N- methyl ureas, N, N- dimethyl ureas, N- formoxyl ureas
Plant or several mixing, more excellent selection is urea.
In addition, organic solvent can be selected as diethylene glycol dimethyl ether, propandiol butyl ether, propylene glycol methyl ether acetate, the third two
One or more of mixing in alcohol methyl ether, dipropylene.
Film forming agent can include albumen film forming agent, acrylic resin, polyurethane, acrylic resin and be modified casein, propylene
One or more of mixing in acid resin polyurethane copolymerization resin, polyethylene or acrylate modified butadiene resin, as long as
Be the material that can play filming function in protection scope of the present invention, preferably by two or three of film forming agent when actual use
It is used in mixed way, learns from other's strong points to offset one's weaknesses, meets the performance required by the firm elevator of perspiration resistance.
The present inventor have also been made corresponding optimization on the consumption of each raw material, be entered based on the optimum performance reached
The optimization of raw material proportioning is gone, with mass fraction agent, the dosage optimization of each raw material is：50-150 parts of sulfonylurea, organic solvent
50-80 parts, 2-8 parts of film forming agent, 50-150 parts of water, more preferably, 100 parts of sulfonylurea, 70 parts of organic solvent, film forming agent 6
Part, 100 parts of water.
In addition, sulfonylurea can also for 20 parts, 25 parts, 30 parts, 35 parts, 55 parts, 65 parts, 80 parts, 120 parts, 140 parts,
160 parts etc., organic solvent can also be 20 parts, 30 parts, 40 parts, 60 parts, 75 parts, 85 parts etc., film forming agent can also for 1.5 parts,
2.5 parts, 3.5 parts, 4.5 parts, 6 parts, 7 parts, 7.5 parts, 8.5 parts and 9 parts etc., the type of water does not have specific requirement, can be soft
On water, hard water, consumption can for 30 parts, 40 parts, 45 parts, 60 parts, 70 parts, 90 parts, 110 parts, 120 parts, 130 parts, 140
Part, 160 parts, 170 parts, 180 parts etc..
It is noticeable to be, the formula species selection of the firm elevator of perspiration resistance of the invention and adding for each component
Dosage be inventor by the more excellent consumption of creative experiments optimization, it is necessary to these raw materials mutually it is compatible can be only achieved it is final
Purpose, although these raw materials belong to Common materials, but inventor is by dyeing the characteristic of fur in itself, and perspiration resistance jail
Balance between two aspects of degree degree and fur quality itself, it is purposive in numerous materials that can play perspiration resistance effect
Have selected wherein four kinds and enter the conjunction of ranks combo, it is final to cause preparation by the having complementary functions effect of each component from each other
The firm elevator of perspiration resistance gone out can not only have the effect of perspiration resistance, and still want to answer improves the quality of fur in itself, prolongs
The service life of fur goods has been grown, has been to kill two birds with one stone, application is highly used for reference.Belong to especially for the present invention is this
Be formulated the invention of class, between each component it is mutual it is compatible after can play this conspicuousness of synergistic effect, it appears particularly weigh
Will.
As can be seen that these composition of raw materials are to carry out the firm elevator of perspiration resistance of the present invention from each raw material dosage
Addition is had to during making, dosage also shows certain regularity, it is impossible to arbitrarily addition, except other three kinds of things of film forming agent
Matter dosage also compares equalization, if a certain raw material dosage is excessive, may result in that consumption is excessive to play the effect run counter to desire
Really, thus must control it is suitable, final effect could so be performed to it is ultimate attainment, by this several raw material according to each optimal
Consumption compatibility is optimal together, it is especially desirable to it is to be noted that the consumption of film forming agent, much smaller compared to other three kinds of consumptions,
Because if film forming agent dosage is excessive to influence whether the quality of fur goods in itself, fur goods makes with common fibre
With difference in performance than larger, fur gas permeability is bad, and warmth retention property is excellent, so if film forming agent dosage too greatly may be more
It is airtight, or even have influence on the texture of fur in itself etc..
The embodiment of the present invention additionally provides the perspiration resistance firm except the formula there is provided a kind of firm elevator of perspiration resistance
Preferably a kind of preparation method of elevator, specifically includes following steps：
(A) sulfonylurea and water are mixed until dissolving, temperature control is at 25-30 DEG C；
(B) cool the temperature to after 15-20 DEG C, add film forming agent, organic solvent and continue to stir 30-60min, produce.
The preparation method operate in itself it is fairly simple, in operating process also without any waste residue produce, forward/backward operation step rank
Connect close, the firm elevator each side effect of perspiration resistance prepared is all good.
There is clear and definite limitation in charging sequence, first add sulfonylurea and water, film forming agent, You Jirong are then added again
Agent, sulfonylurea is added because if first with the addition of again after film forming agent, organic solvent, possible sulfonylurea can be located on the surface not
Preferably it is integrally formed with film forming agent, immiscible organic solvent, it is therefore desirable to which the operation order disclosed in strict accordance with the present invention is added,
The fusion of preferably interpenetrating of all raw materials can be caused to be integrally formed.
Preferably, the speed control that sulfonylurea and water are mixed is between 300-400rpm, and mixing time control exists
Between 15-30min, more excellent is 20min.Speed control is suitably more conducive to be uniformly mixed.
In the present invention, mix and preferably carry out in the reactor, reactor enamel reaction still is optimum response container,
Because enamel reaction still be by the glass lined containing high silicon dioxide steel vessel inner surface, it is close securely through high temperature sintering
In on metal surface turn into composite product.So, it has the stability of glass and the two-fold advantage of metal strength, is
A kind of excellent corrosion resistant apparatus, corrosion resistance and good.
The firm elevator of perspiration resistance of the present invention has good application, concrete application side in fur dyeing last handling process
Method is：In the aqueous solution that fur after dyeing is soaked in the firm elevator of perspiration resistance, the wherein water of the firm elevator of perspiration resistance
The concentration of solution is 0.3-0.7ml/L, and more excellent is 0.5ml/L, can be also 0.4ml/L, 0.6ml/L etc..
In order to which the firm elevator of perspiration resistance can be enabled preferably to permeate in the fur after dyeing, the time of immersion
Control is in more than 10min, and more excellent is 15-30min, and optimal is 20min.
Compared with prior art, beneficial effects of the present invention are：
(1) the firm elevator of perspiration resistance that the present invention is provided, formula is simple, and raw material sources are extensively easily obtained, perspiration resistance performance
Well, it is highly suitable for the after-treatment applications of fur acid dyes, stability is high, can be by the hair after dyeing using convenience
Skin perspiration fastness improves half grade to one-level, has filled up correlation technique blank, should be widely promoted application；
(2) the preparation method technique of the firm elevator of perspiration resistance of the invention is simple, easy to operate, operating condition temperature
It is successive close with, whole processing step, produced without any three wastes, environmental protection；
(3) the firm elevator of perspiration resistance of the invention can be very good to apply in fur dyeing last handling process, have
Very strong specific aim, dedicated for the perspiration resistance after fur dyeing, firmly lifting is handled, exclusively for the perspiration resistance jail of fur goods
Degree degree and design, be highly suitable for the lifting of the perspiration fastness degree of fur goods, be not particularly suited for other products.
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the present invention.It is unreceipted specific in embodiment
Condition person, the condition advised according to normal condition or manufacturer is carried out.Agents useful for same or the unreceipted production firm person of instrument, be
The conventional products that can be obtained by commercially available purchase.
Embodiment 1
The raw material of the firm elevator of perspiration resistance presses following consumption proportion：
Preparation method is in accordance with the following steps：
1) urea and water are placed in reactor, heat and stir, by temperature control at 25-30 DEG C, treat that it is completely dissolved
Afterwards, stop heating, persistently stir 15-30min；
2) temperature in question response device is down to after 15-20 DEG C, and albumen film forming agent and propandiol butyl ether are added in reactor,
Continue to stir 30-60min, produce.
Embodiment 2
The raw material of the firm elevator of perspiration resistance presses following consumption proportion：
Preparation method is in accordance with the following steps：
1) N- methyl ureas and water are placed in reactor, heat and stirred under the conditions of 300-400rpm, by temperature control
At 25-30 DEG C, after it is completely dissolved, stops heating, persistently stir 20min；
2) temperature in question response device is down to after 15-20 DEG C, and acrylic resin and diethylene glycol dimethyl ether are added into reactor
In, continue to stir 40min, produce.
Embodiment 3
The raw material of the firm elevator of perspiration resistance presses following consumption proportion：
Continuous preparation is consistent with embodiment 2 afterwards.
Embodiment 4
The raw material of the firm elevator of perspiration resistance presses following consumption proportion：
Continuous preparation is consistent with embodiment 2 afterwards.
Embodiment 5
The raw material of the firm elevator of perspiration resistance presses following consumption proportion：
Continuous preparation is consistent with embodiment 2 afterwards.
Application examples 1
Rabbit is dyed using serial R series dyes, the raw material skin of shrinkage temperature >=90 DEG C is chosen.
Bath raio is 20：1 (dry hide), 68 DEG C of temperature,
Fur levelling agent DL 0.5ml/L,
Skin is thrown to add after 15 minutes：
The red R-BR 1.0g/L of uncommon power fur
Two groups add formic acid (85%) 0.5ml/L after 30 minutes
Go out skin after 1 hour, rinse (normal temperature), dry.
Dyeing post processing room temperature, is respectively adopted embodiment 1-2 perspiration fastness elevator：0.3ml/L, by the hair after dyeing
Skin soaks 10min.
Application examples 2
Rabbit is dyed using serial R series dyes, the raw material skin of shrinkage temperature >=90 DEG C is chosen.
Bath raio is 20：1 (dry hide), 68 DEG C of temperature,
Fur levelling agent DL 0.5ml/L,
Skin is thrown to add after 15 minutes：
Uncommon power fur red and black R-BE 5.0g/L
Two groups add formic acid (85%) 0.5ml/L after 30 minutes
Go out skin after 1 hour, rinse (normal temperature), dry.
Dyeing post processing room temperature, is respectively adopted embodiment 3-4 perspiration fastness elevator：0.7ml/L, by the hair after dyeing
Skin soaks 15min.
Application examples 3
Rabbit is dyed using serial R series dyes, the raw material skin of shrinkage temperature >=90 DEG C is chosen.
Bath raio is 20：1 (dry hide), 68 DEG C of temperature,
Fur levelling agent DL 0.5ml/L,
Skin is thrown to add after 15 minutes：
Uncommon power fur red and black R-BE 5.0g/L
Two groups add formic acid (85%) 0.5ml/L after 30 minutes
Go out skin after 1 hour, rinse (normal temperature), dry.
Dyeing post processing room temperature, using the perspiration fastness elevator of embodiment 5：0.5ml/L, the fur after dyeing is soaked
30min.
Experimental example 1
The 5 blocks of furs treated using application examples 1-3 of the present invention are regard as sweat with without the identical fur of any processing
The skin sample to be measured of stain firmness, 3*4cm is cut into by skin sample to be measured2Left and right size, takes formed objects cotton, respectively with sweat by skin
Block and cotton are soaked, after taking-up, are enumerated by the order of glass, skin bit, cloth specimen, glass, are then pressed 450kg mark pounds, are put in baking oven,
2 hours are incubated at 37 DEG C, is then taken out, testing result is as shown in table 1 below：
The testing result of table 1
From table 1 it follows that the sweat stain of the fur after the firm elevator processing of perspiration resistance by the embodiment of the present invention
Firm grade can improve half grade and arrive one-level.
Experimental example 2
By first group of the fur treated using the firm elevator of embodiment 3-4 perspiration resistances of application examples 2 of the present invention to the
Two groups, and without the 3rd group of the identical fur Jing Guo any processing, by observing repeatedly and determining performance, concrete outcome is as follows
Shown in table：
The mechanical performance of the fur of table 2
| Group | Tearing strength | Anti-wear performance | Light resistance | Rub resistance rank |
| First group | ≥40N | 500 turns of nothings come off | >=4 grades | >=4 grades |
| Second group | ≥40N | 500 turns of nothings come off | >=4 grades | >=4 grades |
| 3rd group | 20N | 500 turns have a little come off | 3 grades | 3 grades |
Lifting of the firm elevator of the perspiration resistance of the embodiment of the present invention to the mechanical performance of fur as can be seen from Table 2
There is certain effect.
Although illustrate and describing the present invention with specific embodiment, but it will be appreciated that without departing substantially from the present invention's
Many other changes and modification can be made in the case of spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.
Claims (10)
1. a kind of firm elevator of perspiration resistance, it is characterised in that be mainly made by following raw material：In terms of mass fraction, ureas thing
10-200 parts of matter, 10-100 parts of organic solvent, 1-10 parts of film forming agent, 20-200 parts of water.
2. the firm elevator of perspiration resistance according to claim 1, it is characterised in that 50-150 parts of sulfonylurea, You Jirong
50-80 parts of agent, 2-8 parts of film forming agent, 50-150 parts of water.
3. the firm elevator of perspiration resistance according to claim 2, it is characterised in that 100 parts of sulfonylurea, organic solvent 70
Part, 6 parts of film forming agent, 100 parts of water.
4. the firm elevator of perspiration resistance according to claim any one of 1-3, it is characterised in that the sulfonylurea bag
Include：One or more of mixing in urea, N- methyl ureas, N, N- dimethyl ureas, N- formoxyl ureas, preferably urea.
5. the firm elevator of perspiration resistance according to claim any one of 1-3, it is characterised in that organic solvent includes：Two
One or more in ethylene glycol monomethyl ether, propandiol butyl ether, propylene glycol methyl ether acetate, propylene glycol monomethyl ether, dipropylene
Mixing.
6. the firm elevator of perspiration resistance according to claim any one of 1-3, it is characterised in that the film forming agent includes egg
White film forming agent, acrylic resin, polyurethane, acrylic resin are modified casein, acrylic resin polyurethane copolymerization resin, poly- second
One or more of mixing in alkene or acrylate modified butadiene resin.
7. the preparation method of the firm elevator of perspiration resistance described in claim any one of 1-6, it is characterised in that including following step
Suddenly：
(A) sulfonylurea and water are mixed until dissolving, temperature control is at 25-30 DEG C；
(B) cool the temperature to after 15-20 DEG C, add film forming agent, organic solvent and continue to stir 30-60min, produce.
8. the preparation method of the firm elevator of perspiration resistance according to claim 7, it is characterised in that in the step (A),
The speed control that sulfonylurea and water are mixed is between 300-400rpm, and mixing time is controlled in 15-30min.
9. the preparation method of the firm elevator of perspiration resistance according to claim 7, it is characterised in that mix in reaction
Carried out in device, the reactor is enamel reaction still.
10. application of the firm elevator of perspiration resistance in fur dyeing last handling process described in claim any one of 1-6；
Preferably, the fur after dyeing is soaked in the aqueous solution of the firm elevator of perspiration resistance；
Preferably, the concentration of the aqueous solution of the firm elevator of perspiration resistance is 0.3-0.7ml/L, and more excellent is 0.5ml/L；
Preferably, the time control of immersion is in more than 10min, and more excellent is 15-30min.
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| CN107217518B (en) | 2019-06-07 |
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Effective date of registration: 20230626 Address after: No. 2, Hengjing Yanglian Farm, Ganduo, Gaoyou City, Yangzhou City, Jiangsu Province 225600 Patentee after: Fanbo (Jiangsu) Jinghua Technology Co.,Ltd. Address before: 100000 Building 3, Yard 7, Ronghua Middle Road, Beijing Economic-Technological Development Area Patentee before: BEIJING FANBO CHEMICALS CO.,LTD. |