CN111249181A - Long-acting slow-release perfume and preparation method thereof - Google Patents
Long-acting slow-release perfume and preparation method thereof Download PDFInfo
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- CN111249181A CN111249181A CN201910964652.XA CN201910964652A CN111249181A CN 111249181 A CN111249181 A CN 111249181A CN 201910964652 A CN201910964652 A CN 201910964652A CN 111249181 A CN111249181 A CN 111249181A
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- 239000002304 perfume Substances 0.000 title claims abstract description 98
- 238000002360 preparation method Methods 0.000 title claims abstract description 28
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 185
- 239000000341 volatile oil Substances 0.000 claims abstract description 137
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 123
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 78
- 241000208152 Geranium Species 0.000 claims abstract description 49
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 49
- 244000179970 Monarda didyma Species 0.000 claims abstract description 42
- 235000010672 Monarda didyma Nutrition 0.000 claims abstract description 42
- 240000002505 Pogostemon cablin Species 0.000 claims abstract description 40
- 235000011751 Pogostemon cablin Nutrition 0.000 claims abstract description 40
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000661 sodium alginate Substances 0.000 claims abstract description 26
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 26
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 26
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 25
- 229940072049 amyl acetate Drugs 0.000 claims abstract description 25
- PGMYKACGEOXYJE-UHFFFAOYSA-N anhydrous amyl acetate Natural products CCCCCOC(C)=O PGMYKACGEOXYJE-UHFFFAOYSA-N 0.000 claims abstract description 25
- MNWFXJYAOYHMED-UHFFFAOYSA-M heptanoate Chemical compound CCCCCCC([O-])=O MNWFXJYAOYHMED-UHFFFAOYSA-M 0.000 claims abstract description 25
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 24
- 229930007744 linalool Natural products 0.000 claims abstract description 24
- 229960004106 citric acid Drugs 0.000 claims abstract description 3
- 229960004756 ethanol Drugs 0.000 claims abstract description 3
- 229960005150 glycerol Drugs 0.000 claims abstract description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 36
- 238000003756 stirring Methods 0.000 claims description 32
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 28
- 238000000605 extraction Methods 0.000 claims description 22
- 241001529821 Agastache Species 0.000 claims description 19
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 18
- 239000003208 petroleum Substances 0.000 claims description 18
- 238000010992 reflux Methods 0.000 claims description 16
- 235000021314 Palmitic acid Nutrition 0.000 claims description 14
- 239000000287 crude extract Substances 0.000 claims description 14
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 10
- 239000001569 carbon dioxide Substances 0.000 claims description 9
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 9
- 239000012530 fluid Substances 0.000 claims description 9
- 238000010298 pulverizing process Methods 0.000 claims description 9
- 241000628997 Flos Species 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 8
- 238000001256 steam distillation Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 4
- 239000002671 adjuvant Substances 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 14
- 230000000694 effects Effects 0.000 abstract description 12
- 230000002045 lasting effect Effects 0.000 abstract description 4
- 230000000052 comparative effect Effects 0.000 description 16
- 238000009210 therapy by ultrasound Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 241000700159 Rattus Species 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 230000006399 behavior Effects 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000036651 mood Effects 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
- 235000007173 Abies balsamea Nutrition 0.000 description 1
- 239000004857 Balsam Substances 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- 244000111489 Gardenia augusta Species 0.000 description 1
- 244000018716 Impatiens biflora Species 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 241000219925 Oenothera Species 0.000 description 1
- 235000004496 Oenothera biennis Nutrition 0.000 description 1
- 244000242564 Osmanthus fragrans Species 0.000 description 1
- 235000019083 Osmanthus fragrans Nutrition 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 244000178231 Rosmarinus officinalis Species 0.000 description 1
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 1
- 244000223014 Syzygium aromaticum Species 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 244000273928 Zingiber officinale Species 0.000 description 1
- 235000006886 Zingiber officinale Nutrition 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
- 238000010171 animal model Methods 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000003542 behavioural effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000009194 climbing Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000006397 emotional response Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 235000008397 ginger Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 description 1
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 1
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 1
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- UWKAYLJWKGQEPM-UHFFFAOYSA-N linalool acetate Natural products CC(C)=CCCC(C)(C=C)OC(C)=O UWKAYLJWKGQEPM-UHFFFAOYSA-N 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000001630 malic acid Substances 0.000 description 1
- 235000011090 malic acid Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to the field of perfume preparation, and particularly relates to a long-acting slow-release perfume and a preparation method thereof. The perfume is prepared from bergamot essential oil, geranium essential oil, patchouli essential oil, linalool, amyl acetate, sodium alginate, citric acid, ethanol, glycerol and the like, the preparation method is simple and feasible, the cost is low, and the prepared perfume has good effects of refreshing and relieving pressure, and also has the effects of lasting fragrance and long-acting slow release.
Description
Technical Field
The invention belongs to the field of perfume preparation, and particularly relates to a long-acting slow-release perfume and a preparation method thereof.
Background
The perfume is a mixture of alcohol solution of essence and proper amount of perfume. Has aromatic and rich fragrance, is mainly sprayed on the parts such as lappets, handkerchiefs, hairlines and the like to emit pleasant fragrance, and is one of important cosmetics.
With the gradual improvement of living standard, people have higher and higher demands on living goods, and the perfume is changed from the previous rare article to the common article of the public. The perfume is a cosmetic made of perfume, alcohol and distilled water, and can give off strong, lasting and pleasant fragrance, and improve the aesthetic feeling and attraction of users. However, the perfume sold in the market has not very strong persistence, and the fragrance of the sprayed perfume gradually disappears in a short time.
Most of the existing perfume processes are composed of a balsam material and a solvent, the perfume has a strong taste at the beginning, but the fragrance gradually becomes lighter or even disappears along with the emission of the solvent, and the lasting fragrance of the existing perfume is between 2 and 3 hours. Prolonging the volatilization time of the perfume and keeping the fragrance to be released persistently are the hot spots of the current perfume process research and the demands of the consumers.
Chinese patent application CN 103405357 a discloses a process for preparing a long-acting slow-release perfume, which comprises jasmine essence, violet essence, citric acid, hydroxypropyl methylcellulose, ethanol, polyethylene glycol, tartaric acid, sodium chloride and other components, and has a good fragrance-retaining effect, but the variety of the components affects the original taste and efficacy of the perfume, and is not a good choice.
The Chinese patent application CN 106491398A discloses a slow-release long-acting perfume, which comprises rosemary, sweet osmanthus flower, Jinlu plum, gardenia, evening primrose, clove, roasted ginger, malic acid, nano platinum, slow-release solvent, antioxidant and other components, and has a certain slow-release effect, but the use of the nano platinum greatly increases the manufacturing cost of the perfume and is not beneficial to the use of common consumers.
In the prior art, the long-acting slow-release perfume which does not affect the taste and the efficacy of the perfume, has a good long-acting slow-release effect and reduces the production cost is difficult to find.
Particularly, the problem of fragrance retention of the refreshing and pressure-relieving perfume which is greatly demanded by the current consumers is not successfully solved.
Disclosure of Invention
In order to overcome the technical problems, the invention provides the long-acting slow-release perfume which has better refreshing and pressure relieving effects, and meanwhile, the perfume has lasting fragrance and is simple to prepare.
In order to achieve the above purpose, the technical scheme provided by the invention is as follows:
the long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
preferably, the long-acting slow-release perfume comprises the following components: bergamot essential oil, geranium essential oil, and patchouli essential oil;
preferably, the long-acting slow-release perfume further comprises the following auxiliary materials: linalool, amyl acetate, sodium alginate, citric acid, ethanol and glycerol;
preferably, the long-acting slow-release perfume comprises the following components in parts by weight: 0.1-3 parts of bergamot essential oil, 0.1-3 parts of geranium essential oil, 0.1-6 parts of patchouli essential oil, 1-10 parts of linalool, 10-25 parts of amyl acetate, 1-3 parts of sodium alginate, 1-10 parts of citric acid, 80-140 parts of ethanol and 10-30 parts of glycerol;
preferably, the long-acting slow-release perfume comprises the following components in parts by weight: 0.5-1 part of bergamot essential oil, 0.5-1 part of geranium essential oil, 0.5-2 parts of patchouli essential oil, 2-5 parts of linalool, 15-20 parts of amyl acetate, 1.5-2 parts of sodium alginate, 2-5 parts of citric acid, 120 parts of 100 parts of ethanol and 15-25 parts of glycerol;
preferably, the mass ratio of the bergamot essential oil to the geranium essential oil to the patchouli essential oil is 1:1: 1-2;
preferably, the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 15 parts of amyl acetate, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
preferably, the preparation method of the essential oil comprises the following steps:
(1) pulverizing fructus Citri Sarcodactylis and herba Agastaches respectively, adding ethanol and palmitic acid, extracting with supercritical carbon dioxide fluid, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil respectively;
(2) putting geranium into petroleum ether for reflux extraction, and obtaining a crude extract after reduced pressure distillation;
(3) and (3) carrying out steam distillation extraction on the crude extract, and adding reflux to obtain the geranium essential oil.
Preferably, in the step (1), the extraction temperature is 37-38 ℃, the extraction pressure is 8-10MPa, the flow rate is 8-12kg/h, and the extraction time is 1-2 h;
preferably, the ethanol and the palmitic acid are essential oil extraction promoters, and the addition amount of the ethanol is 10-30% of the mass of the bergamot or the pogostemon cablin respectively; the addition amount of the palmitic acid is 1-5% of the mass of the bergamot or the patchouli respectively;
preferably, in the step (2), the amount of the petroleum ether is 3-5 times of the mass of the geranium; the boiling range of the petroleum ether is 30-60 ℃;
preferably, in the step (3), the heating and refluxing are carried out until the essential oil is not increased any more;
the invention also aims to provide a preparation method of the long-acting slow-release perfume, which comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution, adding bergamot essential oil, patchouli essential oil and geranium essential oil, and stirring to obtain the long-acting slow-release perfume.
Preferably, in step (1) or (2), the stirring is carried out under the conditions of 300-500 rpm;
preferably, step (3) is carried out at 15-30 ℃;
preferably, in the step (3), the stirring is performed under the conditions of 100-200 rpm;
preferably, the step (3) further comprises performing ultrasound under the conditions of 80-100HZ, 200-500W.
Compared with the prior art, the invention has the technical advantages that:
(1) the essential oil of bergamot, patchouli and geranium is used together, so that the health care tea has good functions of refreshing and relieving pressure;
(2) the linalool and the amyl acetate used in the perfume have good synergistic effect, and can better promote the refreshing effect of the perfume and relieve the mood;
(3) according to the perfume, the volatilization of perfume essential oil can be effectively controlled by the sodium alginate, the citric acid, the ethanol and the glycerol, so that the perfume has a long-acting slow-release effect;
(4) in the invention, ethanol and palmitic acid are used as extraction promoters in the process of extracting the bergamot essential oil and the pogostemon cablin essential oil, so that the essential oil in the bergamot and the pogostemon cablin can be effectively extracted, the utilization rate of raw materials is effectively improved, and the production cost of the perfume is reduced.
Detailed Description
Example 1
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 15 parts of amyl acetate, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol and 2% palmitic acid, extracting with supercritical carbon dioxide fluid at 37 deg.C under 9MPa and flow rate of 10kg/h for 1.5h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 4 times of that of the geranium for reflux extraction, and obtaining a crude extract after reduced pressure distillation; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Example 2
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.1 part of bergamot essential oil, 0.1 part of geranium essential oil, 0.1 part of patchouli essential oil, 1 part of linalool, 10 parts of amyl acetate, 1 part of sodium alginate, 1 part of citric acid, 80 parts of ethanol and 10 parts of glycerol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 10% ethanol and 1% palmitic acid, extracting with supercritical carbon dioxide fluid at 37 deg.C under 8MPa and flow rate of 8kg/h for 1h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 3 times, performing reflux extraction, and performing reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 300rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 300rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 15 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 100rpm, and performing ultrasonic treatment at 80HZ and 200W to obtain the long-acting slow-release perfume.
Example 3
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 3 parts of bergamot essential oil, 3 parts of geranium essential oil, 6 parts of patchouli essential oil, 10 parts of linalool, 25 parts of amyl acetate, 3 parts of sodium alginate, 10 parts of citric acid, 140 parts of ethanol and 30 parts of glycerol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 30% ethanol and 5% palmitic acid, extracting with supercritical carbon dioxide fluid at 38 deg.C under 10MPa and flow rate of 12kg/h for 2 hr, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass 5 times of that of the geranium for reflux extraction, and obtaining a crude extract after reduced pressure distillation; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 500rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 500rpm to form an ethanol solution;
(3) mixing glycerol solution and ethanol solution at 30 deg.C, adding bergamot essential oil, herba Pogostemonis essential oil, and flos Pelargonii Hortori essential oil, stirring at 200rpm, and performing ultrasonic treatment at 100Hz and 500W to obtain the long-acting slow-release perfume.
Example 4
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.5 part of bergamot essential oil, 0.5 part of geranium essential oil, 0.5 part of patchouli essential oil, 2 parts of linalool, 15 parts of amyl acetate, 2 parts of sodium alginate, 5 parts of citric acid, 100 parts of ethanol and 15 parts of glycerol;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol and 3% palmitic acid, extracting with supercritical carbon dioxide fluid at 38 deg.C under 10MPa and flow rate of 9kg/h for 1h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 3 times, performing reflux extraction, and performing reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing glycerol solution and ethanol solution at 20 deg.C, adding bergamot essential oil, herba Pogostemonis essential oil, and flos Pelargonii Hortori essential oil, stirring at 200rpm, and performing ultrasonic treatment at 100Hz and 500W to obtain the long-acting slow-release perfume.
Example 5
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 1 part of bergamot essential oil, 1 part of geranium essential oil, 2 parts of patchouli essential oil, 5 parts of linalool, 20 parts of amyl acetate, 1.5 parts of sodium alginate, 2 parts of citric acid, 120 parts of ethanol and 25 parts of glycerol;
the mass ratio of the bergamot essential oil to the geranium essential oil to the patchouli essential oil is 1:1: 1-2;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 15% ethanol and 1-5% palmitic acid, extracting with supercritical carbon dioxide fluid at 38 deg.C under 10MPa and flow rate of 12kg/h for 2 hr, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 3 times, performing reflux extraction, and performing reduced pressure distillation to obtain a crude extract; the boiling range of the petroleum ether is 30-60 ℃;
(3) extracting the crude extract by steam distillation, and adding reflux until the essential oil is not increased to obtain flos Pelargonii Hortori essential oil.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 300rpm to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring at 300rpm to form an ethanol solution;
mixing the glycerol solution and the ethanol solution at 15 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 100rpm, and performing ultrasonic treatment at 80HZ and 250W to obtain the long-acting slow-release perfume.
Comparative example 1
Compared with example 1, amyl acetate was not included.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
the essential oil was prepared as in example 1.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool and citric acid in ethanol, and stirring at 400rpm to form ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Comparative example 2
In comparison with example 1, linalool was not included.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 15 parts of amyl acetate, 1.5 parts of sodium alginate, 3 parts of citric acid and 120 parts of ethanol;
the preparation method of the essential oil is the same as that of the example 1;
the preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving amyl acetate and citric acid in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Comparative example 3
Compared with example 1, no palmitic acid was added during extraction of the essential oil.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the components of the long-acting slow-release perfume are the same as those in the embodiment 1;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol, extracting with supercritical carbon dioxide fluid at 37 deg.C under 9MPa and flow rate of 10kg/h for 1.5h, and separating to obtain essential oil of fructus Citri Sarcodactylis and herba Agastaches;
(2) - (3) same as in example 1.
The preparation method of the long-acting slow-release perfume is the same as that of the example 1.
Comparative example 4
The essential oil extraction process was different compared to example 1.
The raw materials of the long-acting slow-release perfume are the same as those in the embodiment 1;
the components of the long-acting slow-release perfume are the same as those in the embodiment 1;
the preparation method of the essential oil comprises the following steps:
(1) respectively pulverizing fructus Citri Sarcodactylis and herba Agastaches, adding 20% ethanol and 2% palmitic acid, extracting with supercritical carbon dioxide fluid at 37 deg.C under 9MPa and flow rate of 10kg/h for 1.5h, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil;
(2) putting the geranium into petroleum ether with the mass of 4 times, performing reflux extraction, and performing reduced pressure distillation to obtain geranium essential oil; the boiling range of the petroleum ether is 30-60 ℃;
the preparation method of the long-acting slow-release perfume is the same as that of the example 1.
Comparative example 5
Compared to example 1, no citric acid was included.
The long-acting slow-release perfume comprises the following raw materials: bergamot, geranium, patchouli;
the long-acting slow-release perfume comprises the following components in parts by weight: 0.8 part of bergamot essential oil, 0.8 part of geranium essential oil, 0.8 part of patchouli essential oil, 3 parts of linalool, 15 parts of amyl acetate, 1.5 parts of sodium alginate and 120 parts of ethanol;
the essential oil was prepared as in example 1.
The preparation method of the long-acting slow-release perfume comprises the following steps:
(1) dissolving sodium alginate in glycerol, and stirring at 400rpm to form glycerol solution;
(2) dissolving linalool and amyl acetate in ethanol, and stirring at 400rpm to form an ethanol solution;
(3) mixing the glycerol solution and the ethanol solution at 25 ℃, adding bergamot essential oil, patchouli essential oil and geranium essential oil, stirring at 150rpm, and performing ultrasonic treatment at 90HZ and 300W to obtain the long-acting slow-release perfume.
Examples of effects
(I) testing the effect of the long-acting sustained release:
the absorbent tissue paper was soaked in the perfume of the groups of examples 1, 3, 5 and comparative examples 1 to 4 for 6 hours, and naturally dried in the shade in a closed space at a constant temperature of 30 ℃ to obtain a fragrant sheet. The obtained incense tablet is placed in a place with good indoor air fluidity, and tested by smelling at 15 days, 30 days, and 45 days for whether it has fragrance (+ +: normal fragrance; + light fragrance; -: no fragrance). The results are shown in the following table:
test group | 15 days | 30 days | 45 days |
Example 1 | ++ | + | + |
Example 2 | ++ | + | + |
Example 3 | ++ | + | + |
Comparative example 1 | + | + | - |
Comparative example 2 | ++ | - | - |
Comparative example 3 | + | - | - |
Comparative example 4 | + | - | - |
Comparative example 5 | + | - |
Therefore, the perfume prepared by the invention has a long-acting slow-release effect.
(II) emotional response animal model test:
100 Wister rats with the weight of 180-. The behavior of the rats in the angry model group is divided into fighting times, threatening times, climbing times, winning interest times and failure times, three persons observe and record the video and then score, and the average value of the score is taken; the results are shown in Table 1.
TABLE 1 Total behavioral score in rats
Test group | Total score of behavior |
Control group | 75.36±8.32a |
Example 1 | 43.21±5.89b |
Example 3 | 45.23±7.44b |
Example 5 | 43.87±10.21b |
Comparative example 1 | 64.45±9.46c |
Comparative example 2 | 68.23±13.62c |
Comparative example 3 | 62.56±9.58c |
Comparative example 4 | 52.32±6.45d |
Comparative example 5 | 56.67±11.23d |
Remarking: the significant difference p < 0.05 is found between different letters in the same list.
Therefore, the perfume provided by the invention has a certain mood relieving effect, and the perfume composition and the extraction method of the essential oil have great influence on the perfume.
The above detailed description is specific to one possible embodiment of the present invention, and the embodiment is not intended to limit the scope of the present invention, and all equivalent implementations or modifications without departing from the scope of the present invention should be included in the technical scope of the present invention.
Claims (10)
1. The long-acting slow-release perfume is characterized by comprising the following raw materials: bergamot, geranium and patchouli.
2. The long-acting slow-release perfume according to claim 1, comprising the following components: bergamot essential oil, geranium essential oil and patchouli essential oil.
3. The long-acting slow-release perfume according to claim 2, further comprising adjuvants: linalool, amyl acetate, sodium alginate, citric acid, ethanol and glycerol.
4. The long-acting slow-release perfume according to claim 3, wherein the long-acting slow-release perfume comprises the following components in parts by weight: 0.1-3 parts of bergamot essential oil, 0.1-3 parts of geranium essential oil, 0.1-6 parts of patchouli essential oil, 1-10 parts of linalool, 10-25 parts of amyl acetate, 1-3 parts of sodium alginate, 1-10 parts of citric acid, 80-140 parts of ethanol and 10-30 parts of glycerol.
5. The long-acting slow-release perfume according to claim 4, wherein the mass ratio of the bergamot essential oil to the geranium essential oil to the patchouli essential oil is 1:1: 1-2.
6. The long-acting slow-release perfume according to claim 2, wherein the essential oil is prepared by a method comprising the steps of:
(1) pulverizing fructus Citri Sarcodactylis and herba Agastaches respectively, adding ethanol and palmitic acid, extracting with supercritical carbon dioxide fluid, and separating to obtain fructus Citri Sarcodactylis essential oil and herba Agastaches essential oil respectively;
(2) putting geranium into petroleum ether for reflux extraction, and obtaining a crude extract after reduced pressure distillation;
(3) and (3) carrying out steam distillation extraction on the crude extract, and adding reflux to obtain the geranium essential oil.
7. The long-acting slow-release perfume according to claim 6, wherein in the step (1), the temperature of the extraction is 37-38 ℃, the pressure of the extraction is 8-10MPa, the flow rate is 8-12kg/h, and the extraction time is 1-2 h.
8. The long-acting slow-release perfume according to claim 6, wherein in the step (1), the ethanol and the palmitic acid are essential oil extraction promoters, and the addition amount of the ethanol is 10-30% of the mass of the bergamot or the pogostemon cablin respectively; the addition amount of the palmitic acid is 1-5% of the mass of the bergamot or the patchouli respectively.
9. The long-acting slow-release perfume according to claim 6, wherein in the step (2), the amount of the petroleum ether is 3 to 5 times of the mass of the geranium; the boiling range of the petroleum ether is 30-60 ℃.
10. A process for the preparation of a long-acting slow-release perfume according to any of claims 3 to 9 comprising the steps of:
(1) dissolving sodium alginate in glycerol, and stirring to form glycerol solution;
(2) dissolving linalool, amyl acetate and citric acid in ethanol, and stirring to form an ethanol solution;
(3) mixing glycerol solution and ethanol solution, adding fructus Citri Sarcodactylis essential oil, herba Agastaches essential oil, and flos Pelargonii Hortori essential oil,
stirring to obtain the long-acting slow-release perfume.
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