CN109248112A - A kind of lasting refreshing perfume and preparation method thereof - Google Patents
A kind of lasting refreshing perfume and preparation method thereof Download PDFInfo
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- CN109248112A CN109248112A CN201811317464.XA CN201811317464A CN109248112A CN 109248112 A CN109248112 A CN 109248112A CN 201811317464 A CN201811317464 A CN 201811317464A CN 109248112 A CN109248112 A CN 109248112A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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Abstract
The invention discloses a kind of lasting refreshing perfumes and preparation method thereof, belong to perfume technical field.The lasting refreshing perfume, including following raw material: tasselled flower natural essential oil, sandalwood essential oil, Rosemary Oil, tea oil, Geranium Essential, Bergamot, orange oil, ethyl alcohol, Glucomannan, zytase, apple pectin；The preparation method of the lasting refreshing perfume be by mixing, low-temperature preservation, impurity elimination and etc. be made.The present invention is reinforcement system by using Glucomannan, zytase, apple pectin, improves the compatibility and persistence of lasting refreshing perfume.
Description
Technical field
The invention belongs to perfume areas, and in particular to a kind of lasting refreshing perfume and preparation method thereof.
Background technique
Chionanthus retusus is Oleaceae tasselled platymiscium, defoliation small arbor or shrub, and Chinese Second Class Key Protected Plant is excellent ornamental
Species.Time early summer, completely tree white flower a thousand li drifting fragrance such as cover frost lid snow, luicd and elegant pleasant, are suitable for planting in building surrounding or park
By the side Zhong Chi and trade.Tasselled tender leaf can make beverage for tealeaves, and fruit rich in oil can extract oil, and confession is industrial, and timber heavily fortified point weight is thin
It causes, it can manufacturing appliance.Bud, the leaf of Chionanthus retusus also have medical value.Tasselled are chiefly used in folk medicine at medicinal aspect, relieve summer heat only
Thirsty effect, the tender leaf and flower of tasselled can also be used to prevent and treat chronic liver disease in civil brewed for drinking.Therefore cultivated plant tasselled,
The great Development volue in China.
The volatile oil aroma of pure of middle extraction is spent from tasselled, for the typical fragrance of a flower, contains tens kinds of fragrance components after measured, it is main
There are benzyl alcohol, benzyl carbinol, p- methoxybenzene ethyl alcohol, p-hydroxyphenylethanol, ethyl anisate, trans- (+)-flores aurantii
The tertiary alcohol, hexyl-benzoate, (E) -2- hexyl-benzoate, myristic aldehyde, fanesol, Ergol, linalool oxide, cloves
A large amount of natural flavoring ingredients such as phenol, p- methoxybenzene ethyl alcohol, trans--jasmone, dehydrogenation ionol, can not only be used for essence again
It can be used as natural perfume material application, be used especially in the preparation of specific single floral type perfume.Current single floral type perfume
Be mostly the fragrance of a flower perfume such as common rose, jasmine, and with tasselled flower for main note natural single floral type perfume so far still
It has not been reported.
Chinese patent application document " a kind of natural tasselled flower perfume and preparation method thereof (publication number: CN103405359B) "
A kind of natural tasselled flower perfume and preparation method thereof and its production method are disclosed, consisting of: tasselled flower based on volume parts
1.4-2.8 parts of natural essential oil, 0.05-0.12 parts of sandalwood essential oil, 0.05-0.13 parts of Rosemary Oil, tea oil 0.05-0.10
Part, 0.08-0.2 parts of Geranium Essential, 0.08-0.17 parts of Bergamot, 0.15-0.23 parts of orange oil and volumetric concentration are
96.25-98.14 parts of 95% ethyl alcohol, above-mentioned each component is uniformly mixed and aged, the natural tasselled fragrance of a flower can be obtained in filtering
Water.The natural tasselled flower perfume color of the invention is limpid, and fragrance exquisiteness is soft, and formula is reasonable, each fragrance component fragrance in perfume
Distribute it is harmonious, stablize, remain tasselled and spend distinctive foundation for heavy florals breath, highlight the main note taste of single floral type perfume,
Fragrance remaining time is but insufficient to there is compatibility, persistence up to 3-5 days.
Summary of the invention
The object of the present invention is to provide a kind of lasting refreshing perfumes and preparation method thereof, to solve in Patent Application Publication
On the basis of welding material disclosed in " a kind of natural tasselled flower perfume and preparation method thereof (publication number: CN103405359B) ",
How to optimize component, dosage, method etc., solves the problems, such as that compatibility, persistence are insufficient.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of lasting refreshing perfume, including following raw material: tasselled flower natural essential oil, sandalwood essential oil, Rosemary Oil, tea tree
Oil, Geranium Essential, Bergamot, orange oil, ethyl alcohol, Glucomannan, zytase, apple pectin；
The Glucomannan, zytase, the ratio of apple pectin are (0.02-0.04): (0.06-0.08): (0.01-
0.03)。
Further, the Glucomannan, zytase, the ratio of apple pectin are 0.03:0.07:0.02.
Further, the lasting refreshing perfume is as unit of parts by weight, including following raw material: tasselled flower natural essential oil
2.0-2.4 parts, 0.05-0.07 parts of sandalwood essential oil, 0.05-0.08 parts of Rosemary Oil, 0.1-0.2 parts of tea oil, fish pelargonium essence
It is 0.01-0.03 parts oily, 0.08-0.1 parts of Bergamot, 0.1-0.2 parts of orange oil, 94-96 parts of ethyl alcohol, Glucomannan 0.02-
0.04 part, 0.06-0.08 parts of zytase, 0.01-0.03 parts of apple pectin.
Further, the lasting refreshing perfume is as unit of parts by weight, including following raw material: tasselled flower natural essential oil
2.2 parts, 0.06 part of sandalwood essential oil, 0.07 part of Rosemary Oil, 0.15 part of tea oil, 0.05 part of Geranium Essential, bergamot essence
0.09 part of oil, 0.15 part of orange oil, alcohol 95 part, 0.03 part of Glucomannan, 0.07 part of zytase, 0.02 part of apple pectin.
Further, the ethyl alcohol is the ethyl alcohol that concentration is 95%.
Further, the described tasselled flower natural essential oil the preparation method comprises the following steps: spending nature to dry in the shade tasselled, crushing and be placed on
It distills in container, is distilled 6-7 hours using steam distillation, gained distillate obtains tasselled flower day after being extracted, being filtered
Right essential oil.
Further, the apple pectin is natural apple pectin, and molecular weight is 2-4 ten thousand.
A kind of preparation method according to above-mentioned lasting refreshing perfume, comprising the following steps: (1) press recipe ratio, stream will be taken
It revives and spends natural essential oil, Rosemary Oil, Geranium Essential, Bergamot and orange oil, above-mentioned fragrance is uniformly mixed and is kept away
Light saves 3-5 days；(2) above-mentioned fragrance is uniformly mixed and is kept in dark place 3-5 days, then add sandalwood essential oil, tea oil, Portugal
Sweet glycan, zytase, apple pectin and ethyl alcohol, obtain mixed liquor after mixing, and above-mentioned mixed liquor is placed at 0-5 DEG C
40-60 days, it is then filtered to remove sediment, gained filtrate is lasting refreshing perfume.
The invention has the following advantages:
(1) as the data of embodiment 1-3 and comparative example 5 as it can be seen that the compatibility of lasting refreshing perfume made from embodiment 1-3
It is significantly higher than compatibility made from comparative example 5 and persistence with persistence；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1
For optimum embodiment.
(2) by embodiment 1 and the data of comparative example 1-4 as it can be seen that Glucomannan, zytase, apple pectin are held in preparation
Synergistic effect is played in long refreshing perfume, collaboration improves the compatibility and persistence of lasting refreshing perfume；This is:
Natural tasselled flower perfume color of the invention is limpid, and fragrance exquisiteness is soft, and formula is reasonable, each fragrance component in perfume
Distributing for fragrance is harmonious, stablizes, and remains tasselled and spends distinctive foundation for heavy florals breath, highlights the main note of single floral type perfume
Taste, fragrance remaining time was up to 3-5 days.In perfume of the present invention, select fragrance orange oil as head perfume, addition have it is happy, nice and cool,
The Bergamot of aromatic odour is used to modify head perfume.Natural tasselled flower essential oil as body note, and with fish pelargonium and rosemary come
Reconciliation body note, to protrude the main note taste of tasselled flower, while rosemary also acts as corrosion-resistant function.The wingceltis of bottom note selection woody note
Perfume (or spice) had not only remained the strong of the tasselled fragrance of a flower but also had increased wooden pure and fresh, and formed a kind of unique fresh scent, and and tea oil
Play the role of slow-release fragrance together, to coordinate the volatility of each fragrance, each fragrance fragrance emission is made to become slow, harmonious steady
It is fixed, while keeping perfume fragrance more lasting, extend fragrance remaining time.But by comparative example 1 it is found that only add above-mentioned component cannot
Realize satisfactory compatibility and persistence effect, therefore applicant, by repetition test, discovery is added to Glucomannan, wood
Dextranase, apple pectin play synergistic effect in preparing lasting refreshing perfume.
Speculate that its possible mechanism is Glucomannan to belong to soluble hemicellulose, thicken, stablize with water-soluble, water holding,
Suspension, gelling, bonding, film forming etc. are specific, can play slow-release fragrance, and have good compatibility to skin, on the skin
Moisture can be locked, moisture is avoided to rinse out essence, increases duration；Zytase reduces the viscosity of material, promotes to have
The release for imitating substance after being administered to skin surface, under low temperature and certain water function, can cross the release played and promote fragrance,
It avoids the water lock effect bring of Glucomannan from discharging slow effect, while improving viscosity, increase film-formation result and stability,
Promote persistence；Apple pectin is natural acidic polysaccharide vegetable fiber, and the hydroxyl of Glucomannan can interact therewith,
Realize cross-linking effect, the stability of promotion system and on a skin surface film forming stability, and it has higher glue to skin
Conjunction property improves compatibility, and zytase is added as distintegrant, is destroying the process for decomposing apple pectin and Glucomannan
In, discharge fragrance gradually, to realize persistence.
(3) by the data of comparative example 6-8 as it can be seen that Glucomannan, zytase, the weight ratio of apple pectin is not in (0.02-
0.04): (0.06-0.08): when in (0.01-0.03) range, the compatibility and persistence numerical value and embodiment of perfume obtained
The numerical value of 1-3 is very different, suitable with the numerical value of the prior art (comparative example 5) much smaller than the numerical value of embodiment 1-3.The present invention
Glucomannan, zytase, apple pectin is as reinforcement system, by adding when embodiment 1-3 prepares lasting refreshing perfume
Add Glucomannan, zytase, the weight ratio of apple pectin is (0.02-0.04): (0.06-0.08): (0.01-0.03), real
Glucomannan slow-release fragrance is utilized in present reinforcement system, and there is good compatibility to skin, can lock water on the skin
Point, it avoids moisture from rinsing out essence, increases duration；Zytase reduces the viscosity of material, promotes active principle
Release after being administered to skin surface, under low temperature and certain water function, can cross the release played and promote fragrance；Apple pectin
For natural acidic polysaccharide vegetable fiber, and the hydroxyl of Glucomannan can interact therewith, and realize cross-linking effect, promote body
The stability of system and on a skin surface film forming stability, and it has higher adhesiveness to skin, improves compatibility, and it is wooden
Dextranase is added as distintegrant, during destroying decomposition apple pectin and Glucomannan, discharges fragrance gradually, thus
Realize persistence, so that Glucomannan, zytase, the reinforcement system that apple pectin is constituted is in lasting refreshing perfume of the invention
In, collaboration improves the compatibility and persistence of lasting refreshing perfume.
Specific embodiment
To facilitate a better understanding of the present invention, it is illustrated by the following examples, these examples belong to protection of the invention
Range, but do not limit the scope of the invention.
In embodiment, lasting refreshing perfume is as unit of parts by weight, including following raw material: tasselled flower natural essential oil 2.0-
2.4 parts, 0.05-0.07 parts of sandalwood essential oil, 0.05-0.08 parts of Rosemary Oil, 0.1-0.2 parts of tea oil, Geranium Essential
0.01-0.03 parts, 0.08-0.1 parts of Bergamot, 0.1-0.2 parts of orange oil, 94-96 parts of ethyl alcohol, Glucomannan 0.02-
0.04 part, 0.06-0.08 parts of zytase, 0.01-0.03 parts of apple pectin.
The ethyl alcohol is the ethyl alcohol that concentration is 95%.The described tasselled flower natural essential oil the preparation method comprises the following steps: by tasselled flower
Naturally it dries in the shade, crush to be placed on and distill in container, distilled 6-7 hours using steam distillation, gained distillate is through extraction, mistake
Tasselled flower natural essential oil is obtained after filter.The apple pectin is natural apple pectin, and molecular weight is 2-4 ten thousand.
A kind of preparation method according to above-mentioned lasting refreshing perfume, which comprises the following steps: (1) by matching
Square ratio will take tasselled flower natural essential oil, Rosemary Oil, Geranium Essential, Bergamot and orange oil, above-mentioned fragrance mixed
It closes uniformly and is kept in dark place 3-5 days；(2) above-mentioned fragrance is uniformly mixed and is kept in dark place 3-5 days, then add santal essence
Oil, tea oil, Glucomannan, zytase, apple pectin and ethyl alcohol, obtain mixed liquor after mixing, by above-mentioned mixed liquor
It is placed 40-60 days at 0-5 DEG C, is then filtered to remove sediment, gained filtrate is lasting refreshing perfume.
Embodiment 1
A kind of lasting refreshing perfume is as unit of parts by weight, including following raw material: tasselled 2.2 parts of natural essential oil of flower, santal
0.06 part of essential oil, 0.07 part of Rosemary Oil, 0.15 part of tea oil, 0.05 part of Geranium Essential, 0.09 part of Bergamot, sweet tea
0.15 part of orange oil, alcohol 95 part, 0.03 part of Glucomannan, 0.07 part of zytase, 0.02 part of apple pectin.
The ethyl alcohol is the ethyl alcohol that concentration is 95%.The described tasselled flower natural essential oil the preparation method comprises the following steps: by tasselled flower
Naturally it dries in the shade, crush to be placed on and distill in container, distilled 6.5 hours using steam distillation, gained distillate is through extraction, mistake
Tasselled flower natural essential oil is obtained after filter.The apple pectin is natural apple pectin, and molecular weight is 30,000.
A kind of preparation method according to above-mentioned lasting refreshing perfume, which comprises the following steps: (1) by matching
Square ratio will take tasselled flower natural essential oil, Rosemary Oil, Geranium Essential, Bergamot and orange oil, above-mentioned fragrance mixed
It closes uniformly and is kept in dark place 4 days；(2) above-mentioned fragrance is uniformly mixed and is kept in dark place 4 days, then add sandalwood essential oil, tea
Oil, Glucomannan, zytase, apple pectin and ethyl alcohol are set, mixed liquor is obtained after mixing, by above-mentioned mixed liquor at 0 DEG C
It is lower to place 50 days, it is then filtered to remove sediment, gained filtrate is lasting refreshing perfume.
Embodiment 2
A kind of lasting refreshing perfume is as unit of parts by weight, including following raw material: tasselled 2.0 parts of natural essential oil of flower, santal
0.07 part of essential oil, 0.05 part of Rosemary Oil, 0.2 part of tea oil, 0.01 part of Geranium Essential, 0.1 part of Bergamot, sweet orange
0.1 part, 96 parts of ethyl alcohol, 0.02 part of Glucomannan, 0.08 part of zytase, 0.01 part of apple pectin of oil.
The ethyl alcohol is the ethyl alcohol that concentration is 95%.The described tasselled flower natural essential oil the preparation method comprises the following steps: by tasselled flower
Naturally it dries in the shade, crush to be placed on and distill in container, distilled 6 hours using steam distillation, gained distillate is extracted, filtered
Tasselled flower natural essential oil is obtained afterwards.The apple pectin is natural apple pectin, and molecular weight is 40,000.
A kind of preparation method according to above-mentioned lasting refreshing perfume, which comprises the following steps: (1) by matching
Square ratio will take tasselled flower natural essential oil, Rosemary Oil, Geranium Essential, Bergamot and orange oil, above-mentioned fragrance mixed
It closes uniformly and is kept in dark place 3 days；(2) above-mentioned fragrance is uniformly mixed and is kept in dark place 5 days, then add sandalwood essential oil, tea
Oil, Glucomannan, zytase, apple pectin and ethyl alcohol are set, mixed liquor is obtained after mixing, by above-mentioned mixed liquor at 0 DEG C
It is lower to place 60 days, it is then filtered to remove sediment, gained filtrate is lasting refreshing perfume.
Embodiment 3
A kind of lasting refreshing perfume is as unit of parts by weight, including following raw material: tasselled 2.4 parts of natural essential oil of flower, santal
0.05 part of essential oil, 0.08 part of Rosemary Oil, 0.1 part of tea oil, 0.03 part of Geranium Essential, 0.08 part of Bergamot, sweet tea
0.2 part of orange oil, 94 parts of ethyl alcohol, 0.04 part of Glucomannan, 0.06 part of zytase, 0.03 part of apple pectin.
The ethyl alcohol is the ethyl alcohol that concentration is 95%.The described tasselled flower natural essential oil the preparation method comprises the following steps: by tasselled flower
Naturally it dries in the shade, crush to be placed on and distill in container, distilled 7 hours using steam distillation, gained distillate is extracted, filtered
Tasselled flower natural essential oil is obtained afterwards.The apple pectin is natural apple pectin, and molecular weight is 20,000.
A kind of preparation method according to above-mentioned lasting refreshing perfume, which comprises the following steps: (1) by matching
Square ratio will take tasselled flower natural essential oil, Rosemary Oil, Geranium Essential, Bergamot and orange oil, above-mentioned fragrance mixed
It closes uniformly and is kept in dark place 5 days；(2) above-mentioned fragrance is uniformly mixed and is kept in dark place 3 days, then add sandalwood essential oil, tea
Oil, Glucomannan, zytase, apple pectin and ethyl alcohol are set, mixed liquor is obtained after mixing, by above-mentioned mixed liquor at 5 DEG C
It is lower to place 40 days, it is then filtered to remove sediment, gained filtrate is lasting refreshing perfume.
Comparative example 1
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare and lack in the raw material of lasting refreshing perfume
Glucomannan, zytase, apple pectin.
Comparative example 2
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare and lack in the raw material of lasting refreshing perfume
Glucomannan.
Comparative example 3
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare and lack in the raw material of lasting refreshing perfume
Zytase.
Comparative example 4
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare and lack in the raw material of lasting refreshing perfume
Apple pectin.
Comparative example 5
Using Chinese patent application document " a kind of natural tasselled flower perfume and preparation method thereof (publication number:
CN103405359B method described in specific embodiment 1 prepares welding material in) ".
Comparative example 6
It is essentially identical with the preparation process of embodiment 1, have only unlike to prepare Portugal in the raw material of lasting refreshing perfume sweet
Glycan is 0.01 part, zytase is 0.1 part, apple pectin is 0.04 part.
Comparative example 7
It is essentially identical with the preparation process of embodiment 1, have only unlike to prepare Portugal in the raw material of lasting refreshing perfume sweet
Glycan is 0.05 part, zytase is 0.04 part, apple pectin is 0.05 part.
Comparative example 8
It is essentially identical with the preparation process of embodiment 1, have only unlike to prepare Portugal in the raw material of lasting refreshing perfume sweet
Glycan is 0.05 part, zytase is 0.1 part, apple pectin is 0.005 part.
To product made from embodiment 1-3 and comparative example 1-8, lasting fragrance time, compatibility test method are tested are as follows:
The back of the hand smears identical perfume, is put into each 5s in clear water, takes out and calculates which time can't smell fragrance.As a result such as following table institute
Show.
| Experimental project | Compatibility (number) | Lasting fragrance time h |
| Embodiment 1 | 5 | 13 |
| Embodiment 2 | 5 | 12.5 |
| Embodiment 3 | 4 | 12 |
| Comparative example 1 | 2 | 8 |
| Comparative example 2 | 3 | 11.5 |
| Comparative example 3 | 3 | 12 |
| Comparative example 4 | 4 | 11 |
| Comparative example 5 | 2 | 7 |
| Comparative example 6 | 3 | 8 |
| Comparative example 7 | 3 | 8 |
| Comparative example 8 | 3 | 9 |
As seen from the above table: (1) as the data of embodiment 1-3 and comparative example 5 as it can be seen that persistently refreshing oneself made from embodiment 1-3
The compatibility and persistence of perfume are significantly higher than compatibility made from comparative example 5 and persistence；Simultaneously by the data of embodiment 1-3
As it can be seen that embodiment 1 is optimum embodiment.
(2) by embodiment 1 and the data of comparative example 1-4 as it can be seen that Glucomannan, zytase, apple pectin are held in preparation
Synergistic effect is played in long refreshing perfume, collaboration improves the compatibility and persistence of lasting refreshing perfume；This is:
Natural tasselled flower perfume color of the invention is limpid, and fragrance exquisiteness is soft, and formula is reasonable, each fragrance component in perfume
Distributing for fragrance is harmonious, stablizes, and remains tasselled and spends distinctive foundation for heavy florals breath, highlights the main note of single floral type perfume
Taste, fragrance remaining time was up to 3-5 days.In perfume of the present invention, select fragrance orange oil as head perfume, addition have it is happy, nice and cool,
The Bergamot of aromatic odour is used to modify head perfume.Natural tasselled flower essential oil as body note, and with fish pelargonium and rosemary come
Reconciliation body note, to protrude the main note taste of tasselled flower, while rosemary also acts as corrosion-resistant function.The wingceltis of bottom note selection woody note
Perfume (or spice) had not only remained the strong of the tasselled fragrance of a flower but also had increased wooden pure and fresh, and formed a kind of unique fresh scent, and and tea oil
Play the role of slow-release fragrance together, to coordinate the volatility of each fragrance, each fragrance fragrance emission is made to become slow, harmonious steady
It is fixed, while keeping perfume fragrance more lasting, extend fragrance remaining time.But by comparative example 1 it is found that only add above-mentioned component cannot
Realize satisfactory compatibility and persistence effect, therefore applicant, by repetition test, discovery is added to Glucomannan, wood
Dextranase, apple pectin play synergistic effect in preparing lasting refreshing perfume.
Speculate that its possible mechanism is Glucomannan to belong to soluble hemicellulose, thicken, stablize with water-soluble, water holding,
Suspension, gelling, bonding, film forming etc. are specific, can play slow-release fragrance, and have good compatibility to skin, on the skin
Moisture can be locked, moisture is avoided to rinse out essence, increases duration；Zytase reduces the viscosity of material, promotes to have
The release for imitating substance after being administered to skin surface, under low temperature and certain water function, can cross the release played and promote fragrance,
It avoids the water lock effect bring of Glucomannan from discharging slow effect, while improving viscosity, increase film-formation result and stability,
Promote persistence；Apple pectin is natural acidic polysaccharide vegetable fiber, and the hydroxyl of Glucomannan can interact therewith,
Realize cross-linking effect, the stability of promotion system and on a skin surface film forming stability, and it has higher glue to skin
Conjunction property improves compatibility, and zytase is added as distintegrant, is destroying the process for decomposing apple pectin and Glucomannan
In, discharge fragrance gradually, to realize persistence.
(3) by the data of comparative example 6-8 as it can be seen that Glucomannan, zytase, the weight ratio of apple pectin is not in (0.02-
0.04): (0.06-0.08): when in (0.01-0.03) range, the compatibility and persistence numerical value and embodiment of perfume obtained
The numerical value of 1-3 is very different, suitable with the numerical value of the prior art (comparative example 5) much smaller than the numerical value of embodiment 1-3.The present invention
Glucomannan, zytase, apple pectin is as reinforcement system, by adding when embodiment 1-3 prepares lasting refreshing perfume
Add Glucomannan, zytase, the weight ratio of apple pectin is (0.02-0.04): (0.06-0.08): (0.01-0.03), real
Glucomannan slow-release fragrance is utilized in present reinforcement system, and there is good compatibility to skin, can lock water on the skin
Point, it avoids moisture from rinsing out essence, increases duration；Zytase reduces the viscosity of material, promotes active principle
Release after being administered to skin surface, under low temperature and certain water function, can cross the release played and promote fragrance；Apple pectin
For natural acidic polysaccharide vegetable fiber, and the hydroxyl of Glucomannan can interact therewith, and realize cross-linking effect, promote body
The stability of system and on a skin surface film forming stability, and it has higher adhesiveness to skin, improves compatibility, and it is wooden
Dextranase is added as distintegrant, during destroying decomposition apple pectin and Glucomannan, discharges fragrance gradually, thus
Realize persistence, so that Glucomannan, zytase, the reinforcement system that apple pectin is constituted is in lasting refreshing perfume of the invention
In, collaboration improves the compatibility and persistence of lasting refreshing perfume.
The above content is it cannot be assumed that present invention specific implementation is only limited to these instructions, for the technical field of the invention
Those of ordinary skill for, under the premise of not departing from present inventive concept, a number of simple deductions or replacements can also be made, all answers
When being considered as belonging to present invention scope of patent protection determined by the appended claims.
Claims (8)
1. a kind of lasting refreshing perfume, which is characterized in that including following raw material: tasselled flower natural essential oil, sandalwood essential oil, rosemary
Essential oil, tea oil, Geranium Essential, Bergamot, orange oil, ethyl alcohol, Glucomannan, zytase, apple pectin；
The Glucomannan, zytase, the ratio of apple pectin are (0.02-0.04): (0.06-0.08): (0.01-
0.03)。
2. lasting refreshing perfume according to claim 1, which is characterized in that the Glucomannan, zytase, Apples
The ratio of glue is 0.03:0.07:0.02.
3. lasting refreshing perfume according to claim 1, which is characterized in that the lasting refreshing perfume is single with parts by weight
Position, including following raw material: natural essential oil 2.0-2.4 parts of tasselled flower, 0.05-0.07 parts of sandalwood essential oil, Rosemary Oil 0.05-
0.08 part, 0.1-0.2 parts of tea oil, 0.01-0.03 parts of Geranium Essential, 0.08-0.1 parts of Bergamot, orange oil 0.1-
0.2 part, 94-96 parts of ethyl alcohol, 0.02-0.04 parts of Glucomannan, 0.06-0.08 parts of zytase, apple pectin 0.01-0.03
Part.
4. lasting refreshing perfume according to claim 1, which is characterized in that the lasting refreshing perfume is single with parts by weight
Position, including following raw material: tasselled 2.2 parts of natural essential oil of flower, 0.06 part of sandalwood essential oil, 0.07 part of Rosemary Oil, tea oil
0.15 part, 0.05 part of Geranium Essential, 0.09 part of Bergamot, 0.15 part of orange oil, alcohol 95 part, Glucomannan 0.03
Part, 0.07 part of zytase, 0.02 part of apple pectin.
5. lasting refreshing perfume according to claim 1, which is characterized in that the ethyl alcohol is the ethyl alcohol that concentration is 95%.
6. lasting refreshing perfume according to claim 1, which is characterized in that the preparation side of the tasselled flower natural essential oil
Method are as follows: spend nature to dry in the shade tasselled, crush to be placed on and distill in container, distilled 6-7 hours using steam distillation, gained evaporates
Tasselled flower natural essential oil is obtained after liquid is extracted, filtered out.
7. lasting refreshing perfume according to claim 1, which is characterized in that the apple pectin is natural apple pectin,
Its molecular weight is 2-4 ten thousand.
8. a kind of preparation method of lasting refreshing perfume according to claim 1-7, which is characterized in that including with
Lower step: (1) pressing recipe ratio, will take tasselled flower natural essential oil, Rosemary Oil, Geranium Essential, Bergamot and sweet orange
Above-mentioned fragrance is uniformly mixed and is kept in dark place 3-5 days by oil；(2) above-mentioned fragrance is uniformly mixed and is kept in dark place 3-5 days, so
After add sandalwood essential oil, tea oil, Glucomannan, zytase, apple pectin and ethyl alcohol, mixed after mixing
Liquid places above-mentioned mixed liquor 40-60 days at 0-5 DEG C, is then filtered to remove sediment, and gained filtrate is as persistently refreshed oneself perfume (or spice)
Water.
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| CN201811317464.XA CN109248112A (en) | 2018-11-07 | 2018-11-07 | A kind of lasting refreshing perfume and preparation method thereof |
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| CN201811317464.XA CN109248112A (en) | 2018-11-07 | 2018-11-07 | A kind of lasting refreshing perfume and preparation method thereof |
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| CN109248112A true CN109248112A (en) | 2019-01-22 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115322831A (en) * | 2022-08-15 | 2022-11-11 | 泉州威士登香精香料有限公司 | Mint essence with lasting cool feeling release function and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103405359A (en) * | 2013-07-16 | 2013-11-27 | 河南科技大学 | Natural chionanthus retusus flower perfume and preparation method thereof |
| CN105380837A (en) * | 2015-11-03 | 2016-03-09 | 金玛瑙香水（明光）有限公司 | Anti-fatigue grapefruit perfume |
| CN106109273A (en) * | 2016-07-06 | 2016-11-16 | 唐虎 | Natural syringa microphylla flower perfume |
| CN106580746A (en) * | 2016-12-24 | 2017-04-26 | 杭州心悦化妆品有限公司 | Perfume with long fragrance holding time |
-
2018
- 2018-11-07 CN CN201811317464.XA patent/CN109248112A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103405359A (en) * | 2013-07-16 | 2013-11-27 | 河南科技大学 | Natural chionanthus retusus flower perfume and preparation method thereof |
| CN105380837A (en) * | 2015-11-03 | 2016-03-09 | 金玛瑙香水（明光）有限公司 | Anti-fatigue grapefruit perfume |
| CN106109273A (en) * | 2016-07-06 | 2016-11-16 | 唐虎 | Natural syringa microphylla flower perfume |
| CN106580746A (en) * | 2016-12-24 | 2017-04-26 | 杭州心悦化妆品有限公司 | Perfume with long fragrance holding time |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115322831A (en) * | 2022-08-15 | 2022-11-11 | 泉州威士登香精香料有限公司 | Mint essence with lasting cool feeling release function and preparation method thereof |
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Application publication date: 20190122 |