CN106745641A - A kind of method of electrolysis production small-micelle water and in air freshener application - Google Patents
A kind of method of electrolysis production small-micelle water and in air freshener application Download PDFInfo
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- CN106745641A CN106745641A CN201611227531.XA CN201611227531A CN106745641A CN 106745641 A CN106745641 A CN 106745641A CN 201611227531 A CN201611227531 A CN 201611227531A CN 106745641 A CN106745641 A CN 106745641A
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- extract
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- air freshener
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Hydrology & Water Resources (AREA)
- Dispersion Chemistry (AREA)
- Organic Chemistry (AREA)
- Water Supply & Treatment (AREA)
- Environmental & Geological Engineering (AREA)
- Engineering & Computer Science (AREA)
- Medicinal Chemistry (AREA)
- Botany (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of method of electrolysis production small-micelle water and in air freshener application, including following steps:Step A:Tourmaline, shot and deionized water are pressed 2:47:10‑4:47:10 mass ratioes are well mixed, the ball milling in ball mill;Step B:By gained raw material drying, grind standby;Step C:Tourmaline after ball milling is added in deionized water, filtering and standing takes supernatant and obtains small-micelle water.In the present invention, the compatibility for realizing small-micelle water and air freshener is combined, for the product of air freshener provides a new direction.
Description
Technical field
The invention belongs to air freshener field, and in particular to the production technology for producing small-micelle water by water process should
With in air freshener.
Background technology
Water with either as singular molecular entities except existing, if the cluster linked up by hydrogen bond can also form by stem molecule, water this
Planting Cluster Structures can cause its viscosity, surface tension, fusing point, boiling point, the change of the aqueous nature such as solvability and pH-value.It is logical
A kind of mode is crossed by hydrone point solution, changes the pH-value of water, so as to improve the interfacial activity of water, strengthen water penetration and
Dissolving power, obtains first micel water, is with a wide range of applications.
With the high speed development of social material civilization, the particularly indoor air pollution of air pollution is increasingly severe, because
And cause the incidence of disease of various breathing problems to improve, threaten the health of the mankind.Therefore how to eliminate or prevent room air
Pollution turn into the problem widely paid close attention to.
Domestic patent is consulted result and is found:Various air fresheners have many patents.But, do not have temporarily discovery to have small point
Son group water is applied to this aspect.
The content of the invention
Therefore, the present invention provides a kind of method for treating water obtains small-micelle water, it is applied in air freshener.
A kind of method for electrolytically producing small-micelle water, including following steps:
Step A:Tourmaline, shot and deionized water are pressed 2:47:10-4:47:10 mass ratioes are well mixed, in ball mill
Middle ball milling;
Step B:By gained raw material drying, grind standby;
Step C:Tourmaline after ball milling is added in deionized water, filtering and standing takes supernatant and obtains subset
Water.
Small-micelle water of the present invention is sent out by the nuclear magnetic resonance of oxygen 17 and determined, and the Hz numbers of half breadth high of gained can reflect small point
The size of son group water, small-micelle water is smaller, and Hz numbers are smaller, otherwise bigger.Test result is shown in Table 1.
Table 1
Preferably, in the step A, Ball-milling Time is 1.5-2.5 hours.
Preferably, in the step B, drying time is 78-82 DEG C, and the time is 7.5-8.5 hours.
Preferably, in the step C, tourmaline is added in deionized water by 2.5-3.5% of mass fraction, during standing
Between be 8-10 minutes.
Preferably, by mass concentration, including:Solubilizer 9-12%, propellant 20-25%, cosolvent 1-3%, spices is carried
Take thing 2-5%, essence 0.4-0.8%, balance of obtained small-micelle water.
Preferably, described solubilizer is ethanol, glycerine, one or more the mixture in 1,3 propane diols;
Preferably, described propellant is one or more the mixture in dimethyl ether, normal butane, propane;
Preferably, described cosolvent is Crodaret, AEO, Sorbitan alcohol ester
One or more mixture in fat acid ester polyoxyethylene ether;
Preferably, described spice extract includes that Flos Tulipae Gesnerianae extract, Flos Caryophylli extract, Olibanum extract, Chinese cassia tree carry
Take thing, chrysanthemum extract, Flos Mume extract, Benzoinum extract, Asiatic sweet leaf extract, cypress extract, rock indigo plant extract, rhizoma nardostachyos
The fragrant extract of extract, bubble, shellfish perfume extract, Lignum Aquilariae Resinatum extract, Storax extract, incense wood extract, lotus extract, jasmine
One or more mixture in jasmine extract, pine and cypress extract, blue perfume extract, Herba Lysimachiae foenumgraeci extract;
Described essence include flavoring rose essence, cream jasmin france, fragrant citrus essence, Mint Essence, osmanthus flower fragrance, Green tea essence,
One or more mixture in lavender oil, lily essence, orchid compound, lemon extract etc..
The present invention also provides a kind of preparation method for preparing air freshener, comprises the following steps:
Step (1):By in spice extract and essence addition solubilizer, it is well mixed, then cosolvent is added by proportioning, mixes
Close stirring transparent to solution;
Step (2):Stirring is mixed to get clear solution during (1) is added into aqueous solvent by proportioning;
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, then adds propellant to be made aerosol by proportioning.
Beneficial effect:Whose solvent as air freshener is the present invention roll into a ball with small split, improves spice extract etc. living
Property solubility of the thing in water, increase the effect of air freshener.Compared with deionized water, small-micelle water has what is more strengthened
Penetration, dissolubility and extension, and the patent and document presently relevant to the research of small-micelle water is all fewer, thus tool
Have wide practical use.It is with fresh air and in the present invention, the compatibility for realizing small-micelle water and air freshener is combined
The product of agent provides a new direction.
Specific embodiment
Preferably embodiment of the invention is described in further detail below:
Embodiment 1
The aqueous solvent for being used by mass concentration be small-micelle water 59.6%, solubilizer be ethanol 10% and glycerine 2%,
Cosolvent is Crodaret 2% and AEO 1%, and propellant is dimethyl ether 18% and propane
5%, spice extract 2%, essence 0.4%.
Comprise the following steps that:
Step (1) adds spice extract and essence in ethanol and glycerine, is well mixed, and adds polyethylene glycol hydrogenated
Castor oil and AEO, mix to solution transparent.
Step (2):Stirring is mixed to get clear solution during the solution that (1) step is obtained adds small solvent molecule group water.
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, dimethyl ether, propane propellant is added and is made aerosol
Agent.
Comparative example 1:A kind of air freshener, difference substantially the same manner as Example 1 is:The water for being used is deionization
Water.
Embodiment 2
The aqueous solvent for being used is small-micelle water 66.4% by mass concentration, and solubilizer is ethanol 8% and 1,3 propane diols
1%, cosolvent is Crodaret 0.5% and sorbitan fatty acid ester APEO 0.5%, propellant
It is dimethyl ether 20%, spice extract 3%, essence 0.6%.
Comprise the following steps that:
Step (1):Spice extract and essence are added into ethanol and 1, in 3 propane diols, is well mixed, add polyoxy second
Alkene rilanit special and sorbitan fatty acid ester APEO, mix to solution transparent.
Step (2):Stirring is mixed to get clear solution during the solution of step (1) is added into small solvent molecule group water.
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, dimethyl ether propellant is added and is made aerosol.
Comparative example 2:A kind of air freshener, difference substantially the same manner as Example 2 is:The water for being used is deionization
Water.
Embodiment 3
The aqueous solvent for being used is small-micelle water 56.4% by mass concentration, and solubilizer is ethanol 12%, and cosolvent is
Crodaret 1%, propellant is normal butane 25%, spice extract 5%, essence 0.8%.
Comprise the following steps that:
Step (1):Spice extract and essence are added into ethanol and 1, in 3 propane diols, is well mixed, add polyoxy second
Alkene rilanit special, mixes to solution transparent.
Step (2):Stirring is mixed to get clear solution during small solvent molecule group water will be added in the solution of step (1).
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, normal butane propellant is added and is made aerosol.
Comparative example 3:A kind of air freshener, difference substantially the same manner as Example 3 is:The water for being used is deionization
The formula composition of the embodiment 1-3 of table 2 and comparative example 1-3
The evaluation and test of bactericidal effect:
The interior space of the air freshener that will be prepared by plate sedimentation to 20 square metres carries out bactericidal effect
Determine, as a result see the table below 3:
Table 3
From above-mentioned table 2 and table 3, compared with the air freshener using deionized water as solvent, subset is used
Water has more preferable bactericidal effect as the air freshener of solvent.
Above content is to combine specific preferred embodiment further description made for the present invention, it is impossible to assert
Specific implementation of the invention is confined to these explanations.For general technical staff of the technical field of the invention,
On the premise of not departing from present inventive concept, some simple deduction or replace can also be made, should be all considered as belonging to of the invention
Protection domain.
Claims (6)
1. it is a kind of electrolytically produce small-micelle water method, it is characterised in that including following steps:
Step A:Tourmaline, shot and deionized water are pressed 2:47:10-4:47:10 mass ratioes are well mixed, the ball in ball mill
Mill;
Step B:By gained raw material drying, grind standby;
Step C:Tourmaline after ball milling is added in deionized water, filtering and standing takes supernatant and obtains small-micelle water.
2. the method for claim 1, it is characterised in that in the step B, drying time is 78-82 DEG C, and the time is
7.5-8.5 hours.
3. the method for claim 1, it is characterised in that in the step C, tourmaline is with mass fraction as 2.5-
3.5% is added in deionized water, and time of repose is 8-10 minutes.
4. a kind of air freshener, it is characterised in that by mass concentration, including:Solubilizer 9-12%, propellant 20-25%, helps
Solvent 1-3%, spice extract 2-5%, essence 0.4-0.8%, the balance of small-micelle water as obtained by claim 1.
5. air freshener as claimed in claim 5, it is characterised in that described solubilizer is ethanol, glycerine, 1,3 the third two
One or more mixture in alcohol;
Described propellant is one or more the mixture in dimethyl ether, normal butane, propane;
Described cosolvent is Crodaret, AEO, sorbitan fatty acid ester polyoxy
One or more mixture in vinethene;
Described spice extract includes that Flos Tulipae Gesnerianae extract, Flos Caryophylli extract, Olibanum extract, cinnamomum cassia extract, chrysanthemum are carried
Take thing, Flos Mume extract, Benzoinum extract, Asiatic sweet leaf extract, cypress extract, rock indigo plant extract, Radix Et Rhizoma Nardostachyos extract, bubble fragrant
Extract, shellfish perfume extract, Lignum Aquilariae Resinatum extract, Storax extract, incense wood extract, lotus extract, jasmine extract, pine
One or more mixture in cypress extract, blue perfume extract, Herba Lysimachiae foenumgraeci extract;
Described essence includes flavoring rose essence, cream jasmin france, fragrant citrus essence, Mint Essence, osmanthus flower fragrance, Green tea essence, smokes clothing
One or more mixture in hay-scented essence, lily essence, orchid compound, lemon extract etc..
6. a kind of preparation method for preparing air freshener as claimed in claim 4, comprises the following steps:
Step (1):By in spice extract and essence addition solubilizer, it is well mixed, then cosolvent is added by proportioning, mixing is stirred
Mix transparent to solution;
Step (2):Stirring is mixed to get clear solution during (1) is added into aqueous solvent by proportioning;
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, then adds propellant to be made aerosol by proportioning.
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CN201611227531.XA CN106745641A (en) | 2016-12-27 | 2016-12-27 | A kind of method of electrolysis production small-micelle water and in air freshener application |
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CN201611227531.XA CN106745641A (en) | 2016-12-27 | 2016-12-27 | A kind of method of electrolysis production small-micelle water and in air freshener application |
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CN201611227531.XA Pending CN106745641A (en) | 2016-12-27 | 2016-12-27 | A kind of method of electrolysis production small-micelle water and in air freshener application |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113546206A (en) * | 2021-08-18 | 2021-10-26 | 孙中宝 | Method for preparing liquid capable of releasing far infrared rays, bioelectricity and negative oxygen ions |
CN113648448A (en) * | 2021-08-16 | 2021-11-16 | 魏宇彤 | Preparation method of liquid capable of releasing negative oxygen ions |
CN115006991A (en) * | 2022-05-23 | 2022-09-06 | 陕西一山环保科技有限公司 | High-conversion-rate vehicle urea solution and preparation method thereof |
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CN101711883A (en) * | 2009-10-30 | 2010-05-26 | 台州绿岛化妆品有限公司 | Aerosol air purification freshener and preparation method thereof |
CN105879626A (en) * | 2014-09-22 | 2016-08-24 | 上海四埃美微科技有限公司 | Air cleanser |
CN106219693A (en) * | 2016-08-30 | 2016-12-14 | 李敦武 | Special tourmaline ceramic filter element and preparation method thereof and the strong anti-oxidation obtained by its process, subset reductive water |
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2016
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JP3414707B2 (en) * | 2000-08-10 | 2003-06-09 | 善正 新保 | Drinking water using deep ocean water containing an extract extracted from seeds such as cereals, and a method for producing the same |
KR20030075298A (en) * | 2002-03-18 | 2003-09-26 | 왕수철 | A bad smell removal method |
CN101711883A (en) * | 2009-10-30 | 2010-05-26 | 台州绿岛化妆品有限公司 | Aerosol air purification freshener and preparation method thereof |
CN105879626A (en) * | 2014-09-22 | 2016-08-24 | 上海四埃美微科技有限公司 | Air cleanser |
CN106219693A (en) * | 2016-08-30 | 2016-12-14 | 李敦武 | Special tourmaline ceramic filter element and preparation method thereof and the strong anti-oxidation obtained by its process, subset reductive water |
Non-Patent Citations (1)
Title |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113648448A (en) * | 2021-08-16 | 2021-11-16 | 魏宇彤 | Preparation method of liquid capable of releasing negative oxygen ions |
CN113546206A (en) * | 2021-08-18 | 2021-10-26 | 孙中宝 | Method for preparing liquid capable of releasing far infrared rays, bioelectricity and negative oxygen ions |
CN115006991A (en) * | 2022-05-23 | 2022-09-06 | 陕西一山环保科技有限公司 | High-conversion-rate vehicle urea solution and preparation method thereof |
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Application publication date: 20170531 |