CN106745641A - A kind of method of electrolysis production small-micelle water and in air freshener application - Google Patents

A kind of method of electrolysis production small-micelle water and in air freshener application Download PDF

Info

Publication number
CN106745641A
CN106745641A CN201611227531.XA CN201611227531A CN106745641A CN 106745641 A CN106745641 A CN 106745641A CN 201611227531 A CN201611227531 A CN 201611227531A CN 106745641 A CN106745641 A CN 106745641A
Authority
CN
China
Prior art keywords
extract
essence
air freshener
water
small
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611227531.XA
Other languages
Chinese (zh)
Inventor
张晏
万宇
詹宣坤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Shutai Biotechnology Co Ltd
Original Assignee
Guangzhou Shutai Biotechnology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Shutai Biotechnology Co Ltd filed Critical Guangzhou Shutai Biotechnology Co Ltd
Priority to CN201611227531.XA priority Critical patent/CN106745641A/en
Publication of CN106745641A publication Critical patent/CN106745641A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/68Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/012Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Hydrology & Water Resources (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Environmental & Geological Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Botany (AREA)
  • Zoology (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)

Abstract

The present invention provides a kind of method of electrolysis production small-micelle water and in air freshener application, including following steps:Step A:Tourmaline, shot and deionized water are pressed 2:47:10‑4:47:10 mass ratioes are well mixed, the ball milling in ball mill;Step B:By gained raw material drying, grind standby;Step C:Tourmaline after ball milling is added in deionized water, filtering and standing takes supernatant and obtains small-micelle water.In the present invention, the compatibility for realizing small-micelle water and air freshener is combined, for the product of air freshener provides a new direction.

Description

A kind of method of electrolysis production small-micelle water and in air freshener application
Technical field
The invention belongs to air freshener field, and in particular to the production technology for producing small-micelle water by water process should With in air freshener.
Background technology
Water with either as singular molecular entities except existing, if the cluster linked up by hydrogen bond can also form by stem molecule, water this Planting Cluster Structures can cause its viscosity, surface tension, fusing point, boiling point, the change of the aqueous nature such as solvability and pH-value.It is logical A kind of mode is crossed by hydrone point solution, changes the pH-value of water, so as to improve the interfacial activity of water, strengthen water penetration and Dissolving power, obtains first micel water, is with a wide range of applications.
With the high speed development of social material civilization, the particularly indoor air pollution of air pollution is increasingly severe, because And cause the incidence of disease of various breathing problems to improve, threaten the health of the mankind.Therefore how to eliminate or prevent room air Pollution turn into the problem widely paid close attention to.
Domestic patent is consulted result and is found:Various air fresheners have many patents.But, do not have temporarily discovery to have small point Son group water is applied to this aspect.
The content of the invention
Therefore, the present invention provides a kind of method for treating water obtains small-micelle water, it is applied in air freshener.
A kind of method for electrolytically producing small-micelle water, including following steps:
Step A:Tourmaline, shot and deionized water are pressed 2:47:10-4:47:10 mass ratioes are well mixed, in ball mill Middle ball milling;
Step B:By gained raw material drying, grind standby;
Step C:Tourmaline after ball milling is added in deionized water, filtering and standing takes supernatant and obtains subset Water.
Small-micelle water of the present invention is sent out by the nuclear magnetic resonance of oxygen 17 and determined, and the Hz numbers of half breadth high of gained can reflect small point The size of son group water, small-micelle water is smaller, and Hz numbers are smaller, otherwise bigger.Test result is shown in Table 1.
Table 1
Preferably, in the step A, Ball-milling Time is 1.5-2.5 hours.
Preferably, in the step B, drying time is 78-82 DEG C, and the time is 7.5-8.5 hours.
Preferably, in the step C, tourmaline is added in deionized water by 2.5-3.5% of mass fraction, during standing Between be 8-10 minutes.
Preferably, by mass concentration, including:Solubilizer 9-12%, propellant 20-25%, cosolvent 1-3%, spices is carried Take thing 2-5%, essence 0.4-0.8%, balance of obtained small-micelle water.
Preferably, described solubilizer is ethanol, glycerine, one or more the mixture in 1,3 propane diols;
Preferably, described propellant is one or more the mixture in dimethyl ether, normal butane, propane;
Preferably, described cosolvent is Crodaret, AEO, Sorbitan alcohol ester One or more mixture in fat acid ester polyoxyethylene ether;
Preferably, described spice extract includes that Flos Tulipae Gesnerianae extract, Flos Caryophylli extract, Olibanum extract, Chinese cassia tree carry Take thing, chrysanthemum extract, Flos Mume extract, Benzoinum extract, Asiatic sweet leaf extract, cypress extract, rock indigo plant extract, rhizoma nardostachyos The fragrant extract of extract, bubble, shellfish perfume extract, Lignum Aquilariae Resinatum extract, Storax extract, incense wood extract, lotus extract, jasmine One or more mixture in jasmine extract, pine and cypress extract, blue perfume extract, Herba Lysimachiae foenumgraeci extract;
Described essence include flavoring rose essence, cream jasmin france, fragrant citrus essence, Mint Essence, osmanthus flower fragrance, Green tea essence, One or more mixture in lavender oil, lily essence, orchid compound, lemon extract etc..
The present invention also provides a kind of preparation method for preparing air freshener, comprises the following steps:
Step (1):By in spice extract and essence addition solubilizer, it is well mixed, then cosolvent is added by proportioning, mixes Close stirring transparent to solution;
Step (2):Stirring is mixed to get clear solution during (1) is added into aqueous solvent by proportioning;
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, then adds propellant to be made aerosol by proportioning.
Beneficial effect:Whose solvent as air freshener is the present invention roll into a ball with small split, improves spice extract etc. living Property solubility of the thing in water, increase the effect of air freshener.Compared with deionized water, small-micelle water has what is more strengthened Penetration, dissolubility and extension, and the patent and document presently relevant to the research of small-micelle water is all fewer, thus tool Have wide practical use.It is with fresh air and in the present invention, the compatibility for realizing small-micelle water and air freshener is combined The product of agent provides a new direction.
Specific embodiment
Preferably embodiment of the invention is described in further detail below:
Embodiment 1
The aqueous solvent for being used by mass concentration be small-micelle water 59.6%, solubilizer be ethanol 10% and glycerine 2%, Cosolvent is Crodaret 2% and AEO 1%, and propellant is dimethyl ether 18% and propane 5%, spice extract 2%, essence 0.4%.
Comprise the following steps that:
Step (1) adds spice extract and essence in ethanol and glycerine, is well mixed, and adds polyethylene glycol hydrogenated Castor oil and AEO, mix to solution transparent.
Step (2):Stirring is mixed to get clear solution during the solution that (1) step is obtained adds small solvent molecule group water.
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, dimethyl ether, propane propellant is added and is made aerosol Agent.
Comparative example 1:A kind of air freshener, difference substantially the same manner as Example 1 is:The water for being used is deionization Water.
Embodiment 2
The aqueous solvent for being used is small-micelle water 66.4% by mass concentration, and solubilizer is ethanol 8% and 1,3 propane diols 1%, cosolvent is Crodaret 0.5% and sorbitan fatty acid ester APEO 0.5%, propellant It is dimethyl ether 20%, spice extract 3%, essence 0.6%.
Comprise the following steps that:
Step (1):Spice extract and essence are added into ethanol and 1, in 3 propane diols, is well mixed, add polyoxy second Alkene rilanit special and sorbitan fatty acid ester APEO, mix to solution transparent.
Step (2):Stirring is mixed to get clear solution during the solution of step (1) is added into small solvent molecule group water.
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, dimethyl ether propellant is added and is made aerosol.
Comparative example 2:A kind of air freshener, difference substantially the same manner as Example 2 is:The water for being used is deionization Water.
Embodiment 3
The aqueous solvent for being used is small-micelle water 56.4% by mass concentration, and solubilizer is ethanol 12%, and cosolvent is Crodaret 1%, propellant is normal butane 25%, spice extract 5%, essence 0.8%.
Comprise the following steps that:
Step (1):Spice extract and essence are added into ethanol and 1, in 3 propane diols, is well mixed, add polyoxy second Alkene rilanit special, mixes to solution transparent.
Step (2):Stirring is mixed to get clear solution during small solvent molecule group water will be added in the solution of step (1).
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, normal butane propellant is added and is made aerosol.
Comparative example 3:A kind of air freshener, difference substantially the same manner as Example 3 is:The water for being used is deionization
The formula composition of the embodiment 1-3 of table 2 and comparative example 1-3
The evaluation and test of bactericidal effect:
The interior space of the air freshener that will be prepared by plate sedimentation to 20 square metres carries out bactericidal effect Determine, as a result see the table below 3:
Table 3
From above-mentioned table 2 and table 3, compared with the air freshener using deionized water as solvent, subset is used Water has more preferable bactericidal effect as the air freshener of solvent.
Above content is to combine specific preferred embodiment further description made for the present invention, it is impossible to assert Specific implementation of the invention is confined to these explanations.For general technical staff of the technical field of the invention, On the premise of not departing from present inventive concept, some simple deduction or replace can also be made, should be all considered as belonging to of the invention Protection domain.

Claims (6)

1. it is a kind of electrolytically produce small-micelle water method, it is characterised in that including following steps:
Step A:Tourmaline, shot and deionized water are pressed 2:47:10-4:47:10 mass ratioes are well mixed, the ball in ball mill Mill;
Step B:By gained raw material drying, grind standby;
Step C:Tourmaline after ball milling is added in deionized water, filtering and standing takes supernatant and obtains small-micelle water.
2. the method for claim 1, it is characterised in that in the step B, drying time is 78-82 DEG C, and the time is 7.5-8.5 hours.
3. the method for claim 1, it is characterised in that in the step C, tourmaline is with mass fraction as 2.5- 3.5% is added in deionized water, and time of repose is 8-10 minutes.
4. a kind of air freshener, it is characterised in that by mass concentration, including:Solubilizer 9-12%, propellant 20-25%, helps Solvent 1-3%, spice extract 2-5%, essence 0.4-0.8%, the balance of small-micelle water as obtained by claim 1.
5. air freshener as claimed in claim 5, it is characterised in that described solubilizer is ethanol, glycerine, 1,3 the third two One or more mixture in alcohol;
Described propellant is one or more the mixture in dimethyl ether, normal butane, propane;
Described cosolvent is Crodaret, AEO, sorbitan fatty acid ester polyoxy One or more mixture in vinethene;
Described spice extract includes that Flos Tulipae Gesnerianae extract, Flos Caryophylli extract, Olibanum extract, cinnamomum cassia extract, chrysanthemum are carried Take thing, Flos Mume extract, Benzoinum extract, Asiatic sweet leaf extract, cypress extract, rock indigo plant extract, Radix Et Rhizoma Nardostachyos extract, bubble fragrant Extract, shellfish perfume extract, Lignum Aquilariae Resinatum extract, Storax extract, incense wood extract, lotus extract, jasmine extract, pine One or more mixture in cypress extract, blue perfume extract, Herba Lysimachiae foenumgraeci extract;
Described essence includes flavoring rose essence, cream jasmin france, fragrant citrus essence, Mint Essence, osmanthus flower fragrance, Green tea essence, smokes clothing One or more mixture in hay-scented essence, lily essence, orchid compound, lemon extract etc..
6. a kind of preparation method for preparing air freshener as claimed in claim 4, comprises the following steps:
Step (1):By in spice extract and essence addition solubilizer, it is well mixed, then cosolvent is added by proportioning, mixing is stirred Mix transparent to solution;
Step (2):Stirring is mixed to get clear solution during (1) is added into aqueous solvent by proportioning;
Step (3):Clear solution is loaded in inhalator jar, after sealed cans, then adds propellant to be made aerosol by proportioning.
CN201611227531.XA 2016-12-27 2016-12-27 A kind of method of electrolysis production small-micelle water and in air freshener application Pending CN106745641A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611227531.XA CN106745641A (en) 2016-12-27 2016-12-27 A kind of method of electrolysis production small-micelle water and in air freshener application

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611227531.XA CN106745641A (en) 2016-12-27 2016-12-27 A kind of method of electrolysis production small-micelle water and in air freshener application

Publications (1)

Publication Number Publication Date
CN106745641A true CN106745641A (en) 2017-05-31

Family

ID=58922205

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611227531.XA Pending CN106745641A (en) 2016-12-27 2016-12-27 A kind of method of electrolysis production small-micelle water and in air freshener application

Country Status (1)

Country Link
CN (1) CN106745641A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113546206A (en) * 2021-08-18 2021-10-26 孙中宝 Method for preparing liquid capable of releasing far infrared rays, bioelectricity and negative oxygen ions
CN113648448A (en) * 2021-08-16 2021-11-16 魏宇彤 Preparation method of liquid capable of releasing negative oxygen ions
CN115006991A (en) * 2022-05-23 2022-09-06 陕西一山环保科技有限公司 High-conversion-rate vehicle urea solution and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3414707B2 (en) * 2000-08-10 2003-06-09 善正 新保 Drinking water using deep ocean water containing an extract extracted from seeds such as cereals, and a method for producing the same
KR20030075298A (en) * 2002-03-18 2003-09-26 왕수철 A bad smell removal method
CN101711883A (en) * 2009-10-30 2010-05-26 台州绿岛化妆品有限公司 Aerosol air purification freshener and preparation method thereof
CN105879626A (en) * 2014-09-22 2016-08-24 上海四埃美微科技有限公司 Air cleanser
CN106219693A (en) * 2016-08-30 2016-12-14 李敦武 Special tourmaline ceramic filter element and preparation method thereof and the strong anti-oxidation obtained by its process, subset reductive water

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3414707B2 (en) * 2000-08-10 2003-06-09 善正 新保 Drinking water using deep ocean water containing an extract extracted from seeds such as cereals, and a method for producing the same
KR20030075298A (en) * 2002-03-18 2003-09-26 왕수철 A bad smell removal method
CN101711883A (en) * 2009-10-30 2010-05-26 台州绿岛化妆品有限公司 Aerosol air purification freshener and preparation method thereof
CN105879626A (en) * 2014-09-22 2016-08-24 上海四埃美微科技有限公司 Air cleanser
CN106219693A (en) * 2016-08-30 2016-12-14 李敦武 Special tourmaline ceramic filter element and preparation method thereof and the strong anti-oxidation obtained by its process, subset reductive water

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
姚鼎山等编著: "《走进长寿村》", 31 January 2004 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113648448A (en) * 2021-08-16 2021-11-16 魏宇彤 Preparation method of liquid capable of releasing negative oxygen ions
CN113546206A (en) * 2021-08-18 2021-10-26 孙中宝 Method for preparing liquid capable of releasing far infrared rays, bioelectricity and negative oxygen ions
CN115006991A (en) * 2022-05-23 2022-09-06 陕西一山环保科技有限公司 High-conversion-rate vehicle urea solution and preparation method thereof

Similar Documents

Publication Publication Date Title
CN106310906B (en) A kind of room air eliminating smell agent and preparation method thereof having both sterilizing function
CN106665700B (en) Plant-source disinfection composition, disinfectant and preparation method thereof
CN111887264A (en) Natural plant essential oil microemulsion antibacterial spray and preparation method thereof
CN104164301B (en) A kind of effect lavender oil and compound method thereof
CN107801738A (en) A kind of plant composition and preparation method thereof, application
CN106039361B (en) Air freshener and preparation method thereof
CN108158869A (en) A kind of antibacterial wet tissue liquid, wet tissue and preparation method thereof
CN104644499A (en) Composition with powerful preservative effect and application of composition in cosmetics
CN106745641A (en) A kind of method of electrolysis production small-micelle water and in air freshener application
CN105342932B (en) A kind of all natural multifunctional liquid soap and its production method containing carboxymethyl chitosan
CN102349547B (en) Composite argy wormwood leaf low-alcohol mosquito-repellent liquid and preparation method thereof
CN101954107B (en) Solid aromatic sleep aid and preparation method thereof
CN103690449B (en) Without alcohol mosquito-repellent perfume and preparation method thereof
CN110215532A (en) A kind of plants essential oil water solvent combinations object and preparation method thereof
CN104368026A (en) Environmental-friendly indoor environment purifying agent and preparation method thereof
CN105797189A (en) Preparation method of plant-extract air cleaning agent
CN104688637A (en) Red sage root acne-removing repairing cream
CN103405359A (en) Natural chionanthus retusus flower perfume and preparation method thereof
CN112220824A (en) Antibacterial nano microemulsion system, preparation method, application and application method
CN108094446B (en) Traditional Chinese medicine air purification spray based on microemulsion technology and preparation method thereof
KR101437336B1 (en) Natural cleansing composition for improving hair and scalp comprising fermented needle-leaf extracts
KR101898060B1 (en) Natural aroma essential oil water soluble composition for humidifier disinfectant and the method of manufaturing the same
CN110075339A (en) A kind of natural air scavenging solution and preparation method thereof
CN112891259B (en) Plant perfume and preparation method thereof
CN106983691A (en) A kind of anti-oxidant pore refining sleep mask of the polyphenol containing lotus and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170531