CN105062682B - A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof - Google Patents

A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof Download PDF

Info

Publication number
CN105062682B
CN105062682B CN201510537622.2A CN201510537622A CN105062682B CN 105062682 B CN105062682 B CN 105062682B CN 201510537622 A CN201510537622 A CN 201510537622A CN 105062682 B CN105062682 B CN 105062682B
Authority
CN
China
Prior art keywords
camphor tree
tree seeds
cigarette
tobacco aromaticss
tobacco
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201510537622.2A
Other languages
Chinese (zh)
Other versions
CN105062682A (en
Inventor
袁超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hunan Industrial Co Ltd
Original Assignee
China Tobacco Hunan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Hunan Industrial Co Ltd filed Critical China Tobacco Hunan Industrial Co Ltd
Priority to CN201510537622.2A priority Critical patent/CN105062682B/en
Publication of CN105062682A publication Critical patent/CN105062682A/en
Application granted granted Critical
Publication of CN105062682B publication Critical patent/CN105062682B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Fats And Perfumes (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The present invention is a kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof, which was that will clean Camphor Tree Seeds, be filtered dry, with 60%-95% edible ethanol natural immersion 5-7 days;Molten juice is squeezed, suction filtration takes filtrate;Filtrate is obtained into extracting solution by steam distillation;Extracting solution is mixed with edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss are to get Camphor Tree Seeds tobacco aromaticss;The quality of the 60%-95% edible ethanol is 2~10 times of Camphor Tree Seeds quality.Application of the invention makes the fragrance natural combination of this perfume of tobacco Yu natural herbal plant camphor tree, enrich the fragrance of cigarette, harmony is good, fragrance is elegant, hair property is good thoroughly, dramatically increases cigarette flavor amount, promotes cigarette rhythm, sets off nature cigarette perfume, the effect for reducing gas drying sense, effectively removing cigarette foreign gas, mitigate irritation, improving cigarette comfort level, flue gas mass is remarkably improved, the significant increase quality of cigarette.

Description

A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof
Technical field
The present invention relates to a kind of tobacco aromaticss, specifically a kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof.
Background technique
Camphor tree is a kind of excellent multipurpose tree species, belongs to aiphyllium plant, is the main tree of the green broad-leaf forest of Subtropic of China One of kind, its fruit Camphor Tree Seeds, also known as camphorwood seed, camphor tree seed distributed more widely in China, grease rich in, virtue in grease Camphor tree alcohol, capric acid content are higher, there is its special physiology and trophism, are widely used in the industries such as medicine, makeup, there is wind-damp dispelling, Degrading the channel, analgesic help digestion, anti-inflammatory, urge sweat and other effects, but application of the camphor tree seed extract in cigarette charging flavoring yet there are no report Road.
As people are to safety cigarette growing interest, tobacco business is to Harm reduction techniques, tar reduction technical research also continuous Deeply, but domestic low tar Less harmful cigarette product still has that fragrance is not thin plentiful, and flue gas concentration is inadequate, and comfort is poor The defects of.Natural perfume material has the advantages that complicated composition, numerous types, fragrance is abundant, and lasting is lasting, extracts from natural plants The fragrance component useful to cigarette quality, has become the development trend of tobacco business.
Summary of the invention
The present invention provides a kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof, and gained camphor tree seed extract is applied and is being rolled up Cigarette feeds in flavoring, and aroma quality, perfume quantity can be improved after, keep fragrance plentiful thick and solid, reduces irritation, reduces miscellaneous gas, Pleasant impression is comfortable, coordinates with flue gas.
To achieve the above object, the present invention takes following technical scheme:
A kind of Camphor Tree Seeds tobacco aromaticss, it is will to clean Camphor Tree Seeds, be filtered dry, and is soaked naturally with 60%~95% edible ethanol Bubble 5~7 days;Molten juice is squeezed, suction filtration takes filtrate;Filtrate is obtained into extracting solution by steam distillation;By extracting solution and edible second Alcohol mixing, the as described Camphor Tree Seeds tobacco aromaticss;The quality of the 60%-95% edible ethanol is the 2~10 of Camphor Tree Seeds quality Times.
The preparation method of the Camphor Tree Seeds tobacco aromaticss includes the following steps:
A. Camphor Tree Seeds cleaned, be filtered dry, with 60%~95% edible ethanol solution natural immersion 5~7 days;
B. molten juice is squeezed, suction filtration takes filtrate;
C. filtrate step B obtained is 665.5~1333Pa by steam distillation, vapour pressure, and distillation speed is to evaporate Flow velocity is 0.5~1 drop/S out;
D. the obtained extracting solution of step C is mixed with edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss.
The quality of the 60%-95% edible ethanol is 2~10 times of Camphor Tree Seeds quality.
Extracting solution in the step C analyzes its chemical component using gas chromatography-mass spectrography, isolates 23 peaks identify 19 compounds, density 0.890-0.906g/cm3
Specific key chemical components see the table below:
Serial number Retention time (min) Components Name
1 10.31 α-thujene
2 11.23 Australene
3 14.59 α-phellandrene
4 14.54 Limonene
5 15.40 1, 8-Cineole
6 15.54 Cineol
7 16.74 γ-terpinene
8 21.30 Camphor
9 21.38 Alpha-terpineol
10 24.58 β-linalool
11 26.06 9- aristolene
12 26.62 Java Cananga Oil alkene
13 27.61 4.7- folium eucalypti diene
14 28.51 Different aromadendrene epoxides)
15 29.45 Aromadendrene epoxides
16 31.06 - 4 alcohol of 6- selinene
17 31.17 The Yilan t- oleyl alcohol
18 31.70 Acetic acid
19 31.96 Bicyclogermacrene
The clear solution is added to pipe tobacco during feeding flavoring according to the 0.01%~0.1% of pipe tobacco total weight In.
The present invention has the advantages that
1, application of the invention makes the fragrance natural combination of this perfume of tobacco Yu natural herbal plant camphor tree, enriches cigarette Fragrance, harmony is good, and fragrance is elegant, and hair property is good thoroughly, dramatically increases cigarette flavor amount, promotes cigarette rhythm, sets off nature cigarette perfume, reduces Gas drying sense, the effect effectively remove cigarette foreign gas, mitigate irritation, improving cigarette comfort level, flue gas mass obtain obviously It improves, the significant increase quality of cigarette.
2, camphor tree seed extract eliminates the impurity such as camphor tree shell, and existing forms are liquid, easy to use.
3. camphor tree seed extract derives from natural plants, any chemicals is not added, highly-safe, low manufacture cost, With actual production and application meaning and value.
Specific embodiment
For a better understanding of the technical solution of the present invention, the technology provided below with reference to embodiment the present invention is described in detail Scheme.
A kind of Camphor Tree Seeds tobacco aromaticss, it is will to clean Camphor Tree Seeds, be filtered dry, and is soaked naturally with 60%~95% edible ethanol Bubble 5~7 days;Molten juice is squeezed, suction filtration takes filtrate;Filtrate is obtained into extracting solution by steam distillation;By extracting solution and edible second Alcohol mixing, the as described Camphor Tree Seeds tobacco aromaticss are to get Camphor Tree Seeds tobacco aromaticss;The quality of the 60%-95% edible ethanol It is 2~10 times of Camphor Tree Seeds quality.
The preparation method of the Camphor Tree Seeds tobacco aromaticss includes the following steps:
A. Camphor Tree Seeds cleaned, be filtered dry, with 60%~95% edible ethanol solution natural immersion 5~7 days;
B. molten juice is squeezed, suction filtration takes filtrate;
C. filtrate step B obtained is 665.5~1333Pa by steam distillation, vapour pressure, and distillation speed is to evaporate Flow velocity is 0.5~1 drop/S out;
D. the obtained extracting solution of step C is mixed with edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss.
The quality of the 60%-95% edible ethanol is 2~10 times of Camphor Tree Seeds quality.
Extracting solution in the step C analyzes its chemical component using gas chromatography-mass spectrography, isolates 23 peaks identify 19 compounds, density 0.890-0.906g/cm3
Specific key chemical components see the table below:
Serial number Retention time (min) Components Name
1 10.31 α-thujene
2 11.23 Australene
3 14.59 α-phellandrene
4 14.54 Limonene
5 15.40 1, 8-Cineole
6 15.54 Cineol
7 16.74 γ-terpinene
8 21.30 Camphor
9 21.38 Alpha-terpineol
10 24.58 β-linalool
11 26.06 9- aristolene
12 26.62 Java Cananga Oil alkene
13 27.61 4.7- folium eucalypti diene
14 28.51 Different aromadendrene epoxides)
15 29.45 Aromadendrene epoxides
16 31.06 - 4 alcohol of 6- selinene
17 31.17 The Yilan t- oleyl alcohol
18 31.70 Acetic acid
19 31.96 Bicyclogermacrene
The clear solution is added to pipe tobacco during feeding flavoring according to the 0.01%~0.1% of pipe tobacco total weight In.
Embodiment 1:
The Camphor Tree Seeds of 100 parts by weight are cleaned, are filtered dry, with 400 parts by weight, 70% edible ethanol solution natural immersion 7 days; Molten juice is squeezed, clarification is filtered out with qualitative filter paper, obtains extracting solution;Filtrate is by steam distillation, in 100 DEG C of its vapour pressures 665.5-1333Pa, make filtrate lower than 100 DEG C at a temperature of, distillation speed is with 0.5 drop/S, as water vapour distills together Out, when oil droplet when efflux clear no longer containing organic substance, that is, it can conclude that steam distillation terminates, and finally obtains It is colourless or yellowish, pure and fresh slightly to rush nose, band camphor breath extracting solution;By steam distillation separate alcohol obtain uniformly, stablize, Fragrant and sweet liquid perfume additive, removes impurity, constitute the crucial fragrance component relative amount of its odor characteristic 80% with On.Edible ethanol is added in Camphor Tree Seeds extracting solution in 1:1 by volume, obtains clear solution, according to pipe tobacco total weight 0.01% is added to the clear solution in pipe tobacco during feeding flavoring.
Embodiment 2:
The Camphor Tree Seeds of 100 parts by weight are cleaned, are filtered dry, with 800 parts by weight, 80% edible ethanol solution natural immersion 6 days; Molten juice is squeezed, clarification is filtered out with qualitative filter paper, obtains extracting solution;Filtrate is by steam distillation, in 100 DEG C of its vapour pressures 665.5-1333Pa, make filtrate lower than 100 DEG C at a temperature of, distillation speed is with 0.5 drop/S, as water vapour distills together Out, when oil droplet when efflux clear no longer containing organic substance, that is, it can conclude that steam distillation terminates, and finally obtains It is colourless or yellowish, pure and fresh slightly to rush nose, band camphor breath extracting solution;Be separated by distillation alcohol obtain uniformly, it is stable, fragrant and sweet Liquid perfume additive, removes impurity, constitutes the crucial fragrance component relative amount of its odor characteristic 80% or more.Press body Edible ethanol is added in Camphor Tree Seeds extracting solution than 1:1 in product, obtains clear solution, according to the 0.05% of pipe tobacco total weight that this is clear Clear solution is added in pipe tobacco during feeding flavoring.
Embodiment 3:
The Camphor Tree Seeds of 100 parts by weight are cleaned, are filtered dry, with 300 parts by weight, 65% edible ethanol solution natural immersion 5 days; Molten juice is squeezed, clarification is filtered out with qualitative filter paper, obtains extracting solution;Filtrate is by steam distillation, in 100 DEG C of its vapour pressures 665.5-1333Pa, make filtrate lower than 100 DEG C at a temperature of, distillation speed is with 0.5 drop/S, as water vapour distills together Out, when oil droplet when efflux clear no longer containing organic substance, that is, it can conclude that steam distillation terminates, and finally obtains It is colourless or yellowish, pure and fresh slightly to rush nose, band camphor breath extracting solution;Be separated by distillation alcohol obtain uniformly, it is stable, fragrant and sweet Liquid perfume additive, removes impurity, constitutes the crucial fragrance component relative amount of its odor characteristic 80% or more.Press body Edible ethanol is added in Camphor Tree Seeds extracting solution than 1:1 in product, obtains clear solution, according to the 0.1% of pipe tobacco total weight that this is clear Clear solution is added in pipe tobacco.
The control sample used is the blank cigarette without adding any spice additive, by camphor tree seed extract in flavoring and casing mistake It is applied in pipe tobacco in journey according to 0.01%, 0.05% and 0.1%.Cigarette passes through 7 people of judging panel that qualification is commented with tobacco business state It smokes panel test, smoking result is shown in Table 1.
1 blank sample of table and addition camphor tree seed extract cigarette compare smoking result
As can be seen from Table 1, in the embodiment of all addition camphor tree seed extracts, when camphor tree seed extract additive amount is When 0.05%, every Sensory quality index is best.
The present invention has the advantages that
1, application of the invention makes the fragrance natural combination of this perfume of tobacco Yu natural herbal plant camphor tree, enriches cigarette Fragrance, harmony is good, and fragrance is elegant, and hair property is good thoroughly, dramatically increases cigarette flavor amount, promotes cigarette rhythm, sets off nature cigarette perfume, reduces Gas drying sense, the effect effectively remove cigarette foreign gas, mitigate irritation, improving cigarette comfort level, flue gas mass obtain obviously It improves, the significant increase quality of cigarette.
2, camphor tree seed extract eliminates the impurity such as camphor tree shell, and existing forms are liquid, easy to use.
3. camphor tree seed extract derives from natural plants, any chemicals is not added, highly-safe, low manufacture cost, With actual production and application meaning and value.
The foregoing is merely the detailed descriptions of specific embodiments of the present invention, do not limit the present invention with this, all at this Made any modifications, equivalent replacements, and improvements etc. in the mentality of designing of invention, should be included in protection scope of the present invention it It is interior.

Claims (2)

1. a kind of preparation method of Camphor Tree Seeds tobacco aromaticss, it is characterised in that include the following steps:
A. Camphor Tree Seeds cleaned, be filtered dry, with 60% ~ 95% edible ethanol solution natural immersion 5 ~ 7 days;
B. molten juice is squeezed, suction filtration takes filtrate;
C. filtrate step B obtained is 665.5 ~ 1333Pa by steam distillation, vapour pressure, and distillation speed is to distillate liquid stream Speed is 0.5~1 drop/S;
D. the extracting solution that step C is obtained is mixed with 60%-95% edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss, the food With 2 ~ 10 times that the quality of ethyl alcohol is Camphor Tree Seeds quality;
Extracting solution in the step C analyzes its chemical component using gas chromatography-mass spectrography, isolates 23 Peak identifies 19 compounds, including α-thujene, australene, α-phellandrene, limonene, 1,8- Cineole, cineol, γ- Terpinene, camphor, alpha-terpineol, β-linalool, 9- aristolene, Java Cananga Oil alkene, 4.7- folium eucalypti diene, different aromadendrene epoxy Compound, aromadendrene epoxides, -4 alcohol of 6- selinene, the Yilan t- oleyl alcohol, acetic acid and bicyclogermacrene, density 0.890-0.906g/ cm3
2. a kind of application of Camphor Tree Seeds tobacco aromaticss of method preparation as described in claim 1 in cigarette, it is characterised in that: will The ethyl alcohol of Camphor Tree Seeds tobacco aromaticss mass percent 95% dilutes, and clear solution is obtained, according to pipe tobacco total weight 0.01 ~ 0.1% the clear solution is added in pipe tobacco in flavoring process.
CN201510537622.2A 2015-08-27 2015-08-27 A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof Active CN105062682B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510537622.2A CN105062682B (en) 2015-08-27 2015-08-27 A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510537622.2A CN105062682B (en) 2015-08-27 2015-08-27 A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof

Publications (2)

Publication Number Publication Date
CN105062682A CN105062682A (en) 2015-11-18
CN105062682B true CN105062682B (en) 2019-03-19

Family

ID=54492204

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510537622.2A Active CN105062682B (en) 2015-08-27 2015-08-27 A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105062682B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105614947A (en) * 2016-03-28 2016-06-01 云南养瑞科技集团有限公司 Filter stick additive and application thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101671600A (en) * 2009-09-23 2010-03-17 华宝食用香精香料(上海)有限公司 Additives used in compound Chinese herbal medicine cigarette and use thereof
CN102551192A (en) * 2012-01-20 2012-07-11 湖北中烟工业有限责任公司 Method for preparing camphor tree leaf tobacco flavor
CN102899167A (en) * 2012-10-11 2013-01-30 湖北中烟工业有限责任公司 Tobacco flavor with uniform and stable fragrance and preparation method thereof
CN103146483A (en) * 2013-03-21 2013-06-12 红云红河烟草(集团)有限责任公司 Pelargonium roseum extract and application thereof in cigarettes
CN103205314A (en) * 2013-03-21 2013-07-17 红云红河烟草(集团)有限责任公司 Rosemary extract and application thereof in cigarettes
CN104323955A (en) * 2014-11-14 2015-02-04 成都鹏翔生物科技有限公司 Natural moisturizing cream containing Yunnan camphor tree seed oil

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101671600A (en) * 2009-09-23 2010-03-17 华宝食用香精香料(上海)有限公司 Additives used in compound Chinese herbal medicine cigarette and use thereof
CN102551192A (en) * 2012-01-20 2012-07-11 湖北中烟工业有限责任公司 Method for preparing camphor tree leaf tobacco flavor
CN102899167A (en) * 2012-10-11 2013-01-30 湖北中烟工业有限责任公司 Tobacco flavor with uniform and stable fragrance and preparation method thereof
CN103146483A (en) * 2013-03-21 2013-06-12 红云红河烟草(集团)有限责任公司 Pelargonium roseum extract and application thereof in cigarettes
CN103205314A (en) * 2013-03-21 2013-07-17 红云红河烟草(集团)有限责任公司 Rosemary extract and application thereof in cigarettes
CN104323955A (en) * 2014-11-14 2015-02-04 成都鹏翔生物科技有限公司 Natural moisturizing cream containing Yunnan camphor tree seed oil

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
"GC/MS联用技术在烟草香料方面的应用";李广良 等;《烟草科技》;19981231(第5期);22-23
"樟树籽的开发利用";许莉勇;《浙江万里学院学报》;20001231;第13卷(第4期);19-20

Also Published As

Publication number Publication date
CN105062682A (en) 2015-11-18

Similar Documents

Publication Publication Date Title
CN106174683B (en) A kind of composition and the tobacco juice for electronic smoke containing said composition
CN101544927B (en) Patchouli compound extract and application thereof in cigarette
CN108060014A (en) For the preparation method of the Flos Caryophylli extract of quick-fried pearl base oil
CN1875796A (en) Natural flavoring material with perfuming and health caring functions and application thereof
CN102031194A (en) Ginkgo leaf volatile oil extraction method and method for flavoring cigarettes by utilizing volatile oil
CN109852476A (en) A kind of essence for the smoking article that do not burn suitable for low temperature, preparation method and application
CN103146483A (en) Pelargonium roseum extract and application thereof in cigarettes
CN103351950A (en) Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same
CN112795428A (en) Lotus-fragrance-style tobacco essence and preparation method and application thereof
CN110358630B (en) Spice with fresh and spicy flavor for cigarettes, preparation method of spice and application of spice in cigarettes
CN101637303A (en) Lemon extract, preparation method thereof and application thereof in cigarette flavoring
CN101317691B (en) Additive agent for rose fragrance type cigarette, preparation and application thereof
CN105062682B (en) A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof
CN108865437B (en) Preparation method of perilla seed spice for cigarettes and application of perilla seed spice in cigarettes
CN101342018A (en) Green tea mellow wine extract, preparation and application thereof
CN102657375B (en) Method for preparing extract from traditional Chinese medicines and application of extract as tobacco additive
CN103478904B (en) The tobacco auxiliary material of tea flower fragrance and tobacco product
CN115011410B (en) Schisandra chinensis branch spice, preparation method thereof and cigarette
CN105018231A (en) Pericarpium citri reticulatae viride extract for cigarettes and application of extract
CN101342017A (en) Green tea essential oil, preparation and application thereof
CN1202760C (en) Tobacco with low nicotine content and its producing method
CN105029699A (en) Mint glycerol triacetate extract and application thereof in cigarette
CN108851172A (en) A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette
CN101323817A (en) Cooked puerh tea essential oil, preparation and use thereof
CN108359531A (en) The quick-fried pearl essence of lily odor type and its application in cigarette

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant