CN101317691B - Additive agent for rose fragrance type cigarette, preparation and application thereof - Google Patents
Additive agent for rose fragrance type cigarette, preparation and application thereof Download PDFInfo
- Publication number
- CN101317691B CN101317691B CN2008100736626A CN200810073662A CN101317691B CN 101317691 B CN101317691 B CN 101317691B CN 2008100736626 A CN2008100736626 A CN 2008100736626A CN 200810073662 A CN200810073662 A CN 200810073662A CN 101317691 B CN101317691 B CN 101317691B
- Authority
- CN
- China
- Prior art keywords
- rose
- cigarette
- tobacco
- additive agent
- fragrance type
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Abstract
The invention relates to a rose flower additive for tobacco and the preparation method and applications thereof. The rose flower additive essentially consists of the rose flowers. The preparation method includes the steps that the rose flowers are extracted by heating and refluxing petroleum ether or ethanol solution or by soaking at ambient temperature; the extracted fluid is filtered and then decompressed and condensed into rose flower soaking cream which is mixed with honey in certain proportion to obtain the rose flower additive for tobacco. The rose flower additive is dissolved in the solution of ethanol and propanediol with certain concentration to form saturated solution, which is then evenly sprayed on cut tobacco, tobacco stems or tobacco sheets which are then prepared into cigarette. The dosage of the rose flower additive accounts for 0.01 to 5percent of the weight of the cut tobacco, the tobacco stems or the tobacco sheets. The rose flower additive is characterized by the harmony of the rose flower fragrance and the tobacco fragrance and can soften the cigarette smoke and reduce the irritation of the cigarette fragrance to the respiratory system and the harm of smoking.
Description
Technical field
The present invention relates to a kind of extraction and application of natural perfume material, especially a kind of additive agent for rose fragrance type cigarette and preparation method thereof and the application in perfuming cigarette.
Background technology
China is first big country of World tobacco production and consumption, and the annual leaf tobacco production amount of China accounts for 35% of world's total amount, and the cigarette volume of production and marketing accounts for 32% of world's total amount.Because factor affecting such as the defective of tobacco itself is big as assorted gas, bitter taste, fiber taste objectively need to improve or cover, so tobacco industry will be used a large amount of perfume additives in its product.With regard to the cigarette flavors additive, countries in the world all take much count of its research.Comparatively speaking, China is relatively weak in cigarette flavors additive industrial system, and the cigarette flavors additive product is of poor quality, the kind of Gong selecting for use is more limited, also these perfume additive major controls in supplier's hand, the overwhelming majority is a composite, product composition is indeterminate, the quality instability.For a long time, this is a bottleneck problem of restriction cigarette industry enterprise.
Rose, not only raw material sources are abundant but also fragrance is dense, the diffusing stasis of blood effect of regulate the flow of vital energy in addition Xie Yu and blood.Cure mainly stomachache due to emotional depression and the hyperactive liver-qi attacking the stomach, new wandering arthritis for a long time, the spitting of blood of spitting blood, irregular menstruation, leukorrhea with reddish discharge, dysentery, acute mastitis, pyogenic infections." food book on Chinese herbal medicine " calls it, and " main sharp lung spleen, beneficial liver and gall, the fragrance of food is sweet and refreshing, makes us refreshing refreshing." take for a long time, cosmetic result is excellent, can remove free radical effectively, eliminates pigmentation, makes us calling out pastiness spring vigor.Therefore, research is effective component extracting from rose, development Chinese style cigarette flavors additive green, pure natural, make the fragrant jealous improvement of cigarette, fragrance is coordinated, and pleasant impression is comfortable, flue gas exquisiteness, soft, and effectively reduce the pungent stimulation of flue gas to smoker's respiratory system, and alleviate harm of smoking, will have remarkable economical and social benefit.
Summary of the invention
The objective of the invention is: a kind of additive agent for rose fragrance type cigarette and preparation method thereof and the application in perfuming cigarette are provided.
The purpose of foregoing invention is to be achieved through the following technical solutions:
The used primary raw material of preparation additive agent for rose fragrance type cigarette is: rose.
The preparation method of additive agent for rose fragrance type cigarette is:
(1) with the rose raw material of 100 weight portions, with the solution of 30～90 ℃ of benzinums of 500～1000 weight portions or 50～100% ethanolic solution, heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, each 1～5 hour, filter, leach rose slag, merge extract, under 40～80 ℃ condition, be evaporated to paste, store for future use.
(2) get a certain amount of rose medicinal extract (10～50% percentage by weight) and proper honey (50～90% percentage by weight) mixes the formation additive agent for rose fragrance type cigarette.
The application of additive agent for rose fragrance type cigarette: get an amount of additive agent for rose fragrance type cigarette, be dissolved in 80% ethanol and the propane diols and form saturated solution, and be sprayed at cigarette shreds uniformly, on stem or the reconstituted tobacoo and roll into cigarette and prop up.The additive agent for rose fragrance type cigarette consumption is 0.01～5% of cigarette shreds, stem or a reconstituted tobacoo weight.
The invention has the beneficial effects as follows: rose has the Xie Yu of regulating the flow of vital energy and the diffusing stasis of blood effect of blood, cures mainly stomachache due to emotional depression and the hyperactive liver-qi attacking the stomach, new wandering arthritis for a long time, the spitting of blood of spitting blood, irregular menstruation, leukorrhea with reddish discharge, dysentery, acute mastitis, pyogenic infections.The additive agent for rose fragrance type cigarette that makes is added in the cigarette, can make cigarette have Rose Essentielle and the fragrant fragrance style of coordinating of cigarette, the fragrant jealous improvement of cigarette, fragrance is coordinated, and pleasant impression is comfortable, flue gas exquisiteness, soft, effectively reduce the pungent stimulation of flue gas to smoker's respiratory system, alleviate harm of smoking, and this cigarette additive preparation technology is simple, cost is low, has good market prospects and using value.
The specific embodiment
For ease of understanding the present invention better, be illustrated by following examples, embodiment only is to best implementation of the present invention, not should be understood to limitation of the present invention.
Embodiment 1
Get rose raw material 100 grams and place the 2000ml distilling flask, add 30～60 ℃ of petroleum ether solution 800ml, soaking at room temperature is extracted 3 times, each 3 hours, leach rose slag with the filter paper suction filtration, merge extract, under 40 ℃ water bath condition, be evaporated to paste.Prepared rose medicinal extract (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for rose fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.15%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed on the finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 2
Get rose raw material 100 grams and place the 2000ml distilling flask, add 60～90 ℃ of petroleum ether solution 1000ml, refluxing extraction 2 times, each 2 hours, leach rose slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared rose medicinal extract (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for rose fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.2%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 3
Get rose raw material 100 grams and place the 2000ml distilling flask, add 95% ethanolic solution 1000ml, soaking at room temperature is extracted 3 times, and each 3 hours, leach rose slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared rose medicinal extract (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for rose fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed on the finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 4
Get rose raw material 100 grams and place the 2000ml distilling flask, add 70% ethanolic solution 800ml, refluxing extraction 2 times, each 2 hours, leach rose slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared rose medicinal extract (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for rose fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.4%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 5
Get rose raw material 100 grams and place the 2000ml distilling flask, add 95% ethanol and the petroleum ether solution 1000ml of equivalent, refluxing extraction 2 times, each 2 hours, leach rose slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared rose medicinal extract (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for rose fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed at finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 6
Get rose raw material 100 grams and place the 2000ml distilling flask, add ethanol solution 1000ml, refluxing extraction 2 times, each 2 hours, leach rose slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared rose medicinal extract (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for rose fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Claims (3)
1. additive agent for rose fragrance type cigarette, primary raw material is a rose, it is characterized in that: extract rose medicinal extract from rose, and be made up of rose medicinal extract 10-50% percentage by weight and honey 50～90% percentage by weights.
2. the preparation method of additive agent for rose fragrance type cigarette according to claim 1 is characterized in that may further comprise the steps:
(1) with the rose raw material of 100 weight portions, with the solution of 30～90 ℃ of benzinums of 500～1000 weight portions or 50～100% ethanolic solution, heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, each 1～5 hour, filter, leach rose slag, merge extract, under 40～80 ℃ condition, be evaporated to paste, obtain rose medicinal extract;
(2) get a certain amount of rose medicinal extract 10～50% percentage by weights and honey 50～90% percentage by weights and mix the formation additive agent for rose fragrance type cigarette.
3. the application of additive agent for rose fragrance type cigarette according to claim 1 and 2, it is characterized in that: get an amount of additive agent for rose fragrance type cigarette, be dissolved in 80% ethanol and the propane diols and form saturated solution, and be sprayed on cigarette shreds, stem or the reconstituted tobacoo uniformly and roll into cigarette and prop up, the additive agent for rose fragrance type cigarette consumption is 0.01～5% of cigarette shreds, stem or a reconstituted tobacoo weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100736626A CN101317691B (en) | 2008-07-03 | 2008-07-03 | Additive agent for rose fragrance type cigarette, preparation and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100736626A CN101317691B (en) | 2008-07-03 | 2008-07-03 | Additive agent for rose fragrance type cigarette, preparation and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101317691A CN101317691A (en) | 2008-12-10 |
| CN101317691B true CN101317691B (en) | 2011-06-15 |
Family
ID=40178167
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100736626A Active CN101317691B (en) | 2008-07-03 | 2008-07-03 | Additive agent for rose fragrance type cigarette, preparation and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101317691B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102823940A (en) * | 2012-09-18 | 2012-12-19 | 江苏中烟工业有限责任公司 | Cigarette aroma-enhancement humectant as well as preparation method and application thereof |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102499428A (en) * | 2011-11-20 | 2012-06-20 | 红云红河烟草(集团)有限责任公司 | Rose blended tobacco baking and flavoring method |
| CN105124737A (en) * | 2015-09-02 | 2015-12-09 | 云南中烟工业有限责任公司 | Method of promoting moisturizing and aroma enhancement effects of cigarettes by means of Damask roses |
| CN105441195A (en) * | 2015-12-03 | 2016-03-30 | 李嘉 | Purifying method for rose essential oil |
| CN105713846B (en) * | 2016-04-18 | 2019-04-05 | 云南中烟工业有限责任公司 | A kind of trichoderma aureoviride bacterial strain and the method with its preparation rose tobacco aromatics |
| CN110959904B (en) * | 2019-11-28 | 2022-03-25 | 四川中烟工业有限责任公司 | Method for improving quality of domestic cigars by using rose tea |
-
2008
- 2008-07-03 CN CN2008100736626A patent/CN101317691B/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102823940A (en) * | 2012-09-18 | 2012-12-19 | 江苏中烟工业有限责任公司 | Cigarette aroma-enhancement humectant as well as preparation method and application thereof |
| CN102823940B (en) * | 2012-09-18 | 2014-05-07 | 江苏中烟工业有限责任公司 | Cigarette aroma-enhancement humectant as well as preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101317691A (en) | 2008-12-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101317690A (en) | Additive agent for osmanthus fragrance type cigarette, preparation and application thereof | |
| CN101606753B (en) | Flavoring essence for tobacco | |
| CN101317691B (en) | Additive agent for rose fragrance type cigarette, preparation and application thereof | |
| CN101317692B (en) | Additive agent for jasmine fragrance type cigarette, preparation and application thereof | |
| CN101496638B (en) | Additive agent for Chinese herbal medicine tobacco as well as preparation method and application | |
| CN101810367A (en) | Tobacco additive for increasing smoke concentration and preparation method and application thereof | |
| CN108179066A (en) | It is a kind of for honeysuckle Peppermint essential oil of the quick-fried pearl of cigarette and its preparation method and application | |
| CN101156711A (en) | Additive for tea odor type tobacco and method for making same | |
| CN110205200B (en) | Myrtle-flavored essence and myrtle-flavored electronic cigarette liquid and preparation method thereof | |
| CN104450192A (en) | Tobacco flavor prepared by taking fructus terminaliae immaturus, dendrobium nobile, tobacco and the like as raw materials and application thereof | |
| CN101637303A (en) | Lemon extract, preparation method thereof and application thereof in cigarette flavoring | |
| CN105011353B (en) | Natural bio-chemical agent used for cigar fermentation and quality improvement and application thereof | |
| CN101455442B (en) | Grape extractum and preparation method thereof and use thereof in cigarette performing | |
| CN101606756A (en) | Green tea cigarette and production method thereof | |
| CN106858705A (en) | A kind of tobacco juice for electronic smoke for containing 3 oxo-alpha violet alcohol radical β D glucopyranosides | |
| CN103497836A (en) | Tea flower essence, preparation method and application of essence to cigarette | |
| CN102408944A (en) | Tobacco additive capable of reducing irritation and increasing tobacco fragrance and preparation method thereof | |
| CN102657375B (en) | Method for preparing extract from traditional Chinese medicines and application of extract as tobacco additive | |
| CN103060090B (en) | Tobacco spice with faint scent style, preparing and using methods thereof, and cigarettes | |
| CN101327041B (en) | Pu'er cooked tea alcohol extract and preparation and use thereof | |
| CN110358630A (en) | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette | |
| CN114085711B (en) | Plant essence for electronic atomized liquid and preparation method thereof | |
| CN104862077B (en) | Cigarette storax medicinal extract and preparation method thereof | |
| CN103622150A (en) | Additive for golden camellia cigarette, preparation method of additive for golden camellia cigarette and application of additive for golden camellia cigarette | |
| CN103451020B (en) | Preparation and application of natural cabo flavor-correcting synergist |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: GUANGXI CHINA TOBACCO INDUSTRIAL LCC Free format text: FORMER NAME: CHINA TOBACCO GUANGXI INDUSTRIAL CORPORATION |
|
| CP01 | Change in the name or title of a patent holder |
Address after: 530000 No. 28 Beihu South Road, the Guangxi Zhuang Autonomous Region, Nanning Patentee after: China Tobacco Guangxi Industrial Co., Ltd. Address before: 530000 No. 28 Beihu South Road, the Guangxi Zhuang Autonomous Region, Nanning Patentee before: China Tobacco Guangxi Industrial Corporation |