CN101317692B - Additive agent for jasmine fragrance type cigarette, preparation and application thereof - Google Patents
Additive agent for jasmine fragrance type cigarette, preparation and application thereof Download PDFInfo
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- CN101317692B CN101317692B CN2008100736630A CN200810073663A CN101317692B CN 101317692 B CN101317692 B CN 101317692B CN 2008100736630 A CN2008100736630 A CN 2008100736630A CN 200810073663 A CN200810073663 A CN 200810073663A CN 101317692 B CN101317692 B CN 101317692B
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Abstract
The invention relates to a jasmine flower additive for tobacco and the preparation method and applications thereof. The jasmine flower additive essentially consists of the jasmine flowers. The preparation method includes the steps that the jasmine flowers are extracted by heating and refluxing petroleum ether or ethanol solution or by soaking at ambient temperature; the extracted fluid is filtered and then decompressed and condensed into jasmine flower soaking cream which is mixed with honey in certain proportion to obtain the jasmine flower additive for tobacco. The jasmine flower additive is dissolved in the solution of ethanol and propanediol with certain concentration to form saturated solution, which is then evenly sprayed on cut tobacco, tobacco stems or tobacco sheets which are then prepared into cigarette. The dosage of the jasmine flower additive accounts for 0.01percent to 5percent of the weight of the cut tobacco, the tobacco stems or the tobacco sheets. The jasmine flower additive is characterized by the harmony of the jasmine flower fragrance and the tobacco fragrance and can soften the cigarette smoke and reduce the irritation of the cigarette fragrance to the respiratory system and the harm of smoking.
Description
Technical field
The present invention relates to a kind of extraction and application of natural perfume material, especially a kind of additive agent for jasmine fragrance type cigarette and preparation method thereof and the application in perfuming cigarette.
Background technology
China is first big country of World tobacco production and consumption, and the annual leaf tobacco production amount of China accounts for 35% of world's total amount, and the cigarette volume of production and marketing accounts for 32% of world's total amount.Because factor affecting such as the defective of tobacco itself is big as assorted gas, bitter taste, fiber taste objectively need to improve or cover, so tobacco industry will be used a large amount of perfume additives in its product.With regard to the cigarette flavors additive, countries in the world all take much count of its research.Comparatively speaking, China is relatively weak in cigarette flavors additive industrial system, and the cigarette flavors additive product is of poor quality, the kind of Gong selecting for use is more limited, also these perfume additive major controls in supplier's hand, the overwhelming majority is a composite, product composition is indeterminate, the quality instability.For a long time, this is a bottleneck problem of restriction cigarette industry enterprise.
Jasmine originates in western part of China, and existing extensively planting planted in the subtropical zone.Jasmine is Guangxi characteristic crops, and not only raw material sources are abundant but also fragrance is dense, clearing heat and detoxicating in addition in addition, the medical value of anti-inflammation etc.Therefore, research is effective component extracting from Jasmine, development Chinese style cigarette flavors additive green, pure natural, make the fragrant jealous improvement of cigarette, fragrance is coordinated, and pleasant impression is comfortable, flue gas exquisiteness, soft, and effectively reduce the pungent stimulation of flue gas to smoker's respiratory system, and alleviate harm of smoking, will have remarkable economical and social benefit.
Summary of the invention
The objective of the invention is: a kind of additive agent for jasmine fragrance type cigarette and preparation method thereof and the application in perfuming cigarette are provided.
The purpose of foregoing invention is to be achieved through the following technical solutions:
The used primary raw material of preparation additive agent for jasmine fragrance type cigarette is: Jasmine.
The preparation method of additive agent for jasmine fragrance type cigarette is:
(1) with the Jasmine raw material of 100 weight portions, with the solution of 30～90 ℃ of benzinums of 500～1000 weight portions or 50～100% ethanolic solution, heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, each 1～5 hour, filter, leach the Jasmine slag, merge extract, under 40～80 ℃ condition, be evaporated to paste, store for future use.
(2) get a certain amount of Jasmine medicinal extract (10～50% percentage by weight) and proper honey (50～90% percentage by weight) mixes the formation additive agent for jasmine fragrance type cigarette.
The application of additive agent for jasmine fragrance type cigarette: get an amount of additive agent for jasmine fragrance type cigarette, be dissolved in 80% ethanol and the propane diols and form saturated solution, and be sprayed at cigarette shreds uniformly, on stem or the reconstituted tobacoo and roll into cigarette and prop up.The additive agent for jasmine fragrance type cigarette consumption is 0.01～5% of cigarette shreds, stem or a reconstituted tobacoo weight.
The invention has the beneficial effects as follows: Jasmine has effects such as clearing heat and detoxicating, anti-inflammation, the additive agent for jasmine fragrance type cigarette that makes is added in the cigarette, can make cigarette have jasmin and the fragrant fragrance style of coordinating of cigarette, the fragrant jealous improvement of cigarette, fragrance is coordinated, pleasant impression is comfortable, flue gas exquisiteness, soft, effectively reduce the pungent stimulation of flue gas to smoker's respiratory system, alleviate harm of smoking, and this cigarette additive preparation technology is simple, cost is low, has good market prospects and using value.
The specific embodiment
For ease of understanding the present invention better, be illustrated by following examples, embodiment only is to best implementation of the present invention, not should be understood to limitation of the present invention.
Embodiment 1
Get Jasmine raw material 100 grams and place the 2000ml distilling flask, add 30～60 ℃ of petroleum ether solution 800ml, soaking at room temperature is extracted 3 times, each 3 hours, leach the Jasmine slag with the filter paper suction filtration, merge extract, under 40 ℃ water bath condition, be evaporated to paste.Prepared Jasmine medicinal extract (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for jasmine fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed on the finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 2
Get Jasmine raw material 100 grams and place the 2000ml distilling flask, add 60～90 ℃ of petroleum ether solution 1000ml, refluxing extraction 2 times, each 2 hours, leach the Jasmine slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared Jasmine medicinal extract (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for jasmine fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.2%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 3
Get Jasmine raw material 100 grams and place the 2000ml distilling flask, add 95% ethanolic solution 1000ml, soaking at room temperature is extracted 3 times, and each 3 hours, leach the Jasmine slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared Jasmine medicinal extract (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for jasmine fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed on the finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 4
Get Jasmine raw material 100 grams and place the 2000ml distilling flask, add 70% ethanolic solution 800ml, refluxing extraction 2 times, each 2 hours, leach the Jasmine slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared Jasmine medicinal extract (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for jasmine fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.4%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 5
Get Jasmine raw material 100 grams and place the 2000ml distilling flask, add 95% ethanol and the petroleum ether solution 1000ml of equivalent, refluxing extraction 2 times, each 2 hours, leach the Jasmine slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared Jasmine medicinal extract (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for jasmine fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed at finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 6
Get Jasmine raw material 100 grams and place the 2000ml distilling flask, add ethanol solution 1000ml, refluxing extraction 2 times, each 2 hours, leach the Jasmine slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared Jasmine medicinal extract (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for jasmine fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Claims (3)
1. additive agent for jasmine fragrance type cigarette, primary raw material is a Jasmine, it is characterized in that: extract Jasmine medicinal extract from Jasmine, and be made up of Jasmine medicinal extract 10-50% percentage by weight and honey 50～90% percentage by weights.
2. the preparation method of additive agent for jasmine fragrance type cigarette according to claim 1 is characterized in that may further comprise the steps:
(1) with the Jasmine raw material of 100 weight portions, with the solution of 30～90 ℃ of benzinums of 500～1000 weight portions or 50～100% ethanolic solution, heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, each 1～5 hour, filter, leach the Jasmine slag, merge extract, under 40～80 ℃ condition, be evaporated to paste, obtain Jasmine medicinal extract;
(2) get a certain amount of Jasmine medicinal extract 10～50% percentage by weights and honey 50～90% percentage by weights and mix the formation additive agent for jasmine fragrance type cigarette.
3. the application of additive agent for jasmine fragrance type cigarette according to claim 1 and 2, it is characterized in that: get an amount of additive agent for jasmine fragrance type cigarette, be dissolved in 80% ethanol and the propane diols and form saturated solution, and be sprayed on cigarette shreds, stem or the reconstituted tobacoo uniformly and roll into cigarette and prop up, the additive agent for jasmine fragrance type cigarette consumption is 0.01～5% of cigarette shreds, stem or a reconstituted tobacoo weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100736630A CN101317692B (en) | 2008-07-03 | 2008-07-03 | Additive agent for jasmine fragrance type cigarette, preparation and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100736630A CN101317692B (en) | 2008-07-03 | 2008-07-03 | Additive agent for jasmine fragrance type cigarette, preparation and application thereof |
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| Publication Number | Publication Date |
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| CN101317692A CN101317692A (en) | 2008-12-10 |
| CN101317692B true CN101317692B (en) | 2011-06-15 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101624555B (en) * | 2009-07-30 | 2012-10-10 | 无锡嘉华香精香料有限公司 | Preparation method of tobacco extract and product thereof |
| CN102334748B (en) * | 2010-07-20 | 2013-10-09 | 湖北中烟工业有限责任公司 | Application of Desmodium styracifolium in papermaking-reconstituted slices |
| CN102150948B (en) * | 2011-05-19 | 2012-10-03 | 湖北中烟工业有限责任公司 | Method for preparing jasmine extract for tobacco |
| CN105713842B (en) * | 2016-04-18 | 2019-04-05 | 云南中烟工业有限责任公司 | A method of cigarette perfume of jasmines is prepared using trichoderma aureoviride fermentation |
| CN106381224A (en) * | 2016-11-01 | 2017-02-08 | 湖北中烟工业有限责任公司 | Preparation method of cigarette essence with jasmine flower smelling fragrance and application |
| CN109105948A (en) * | 2018-07-05 | 2019-01-01 | 湖北中烟工业有限责任公司 | A kind of stage extraction preparation method and applications of jasmine flower extract |
| CN111254749A (en) * | 2020-02-28 | 2020-06-09 | 广西中烟工业有限责任公司 | Jasmine flower fragrance type cigarette lining paper spice and preparation method thereof |
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Owner name: GUANGXI CHINA TOBACCO INDUSTRIAL LCC Free format text: FORMER NAME: CHINA TOBACCO GUANGXI INDUSTRIAL CORPORATION |
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Address after: 530000 No. 28 Beihu South Road, the Guangxi Zhuang Autonomous Region, Nanning Patentee after: China Tobacco Guangxi Industrial Co., Ltd. Address before: 530000 No. 28 Beihu South Road, the Guangxi Zhuang Autonomous Region, Nanning Patentee before: China Tobacco Guangxi Industrial Corporation |