CN101317690A - Additive agent for osmanthus fragrance type cigarette, preparation and application thereof - Google Patents
Additive agent for osmanthus fragrance type cigarette, preparation and application thereof Download PDFInfo
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- CN101317690A CN101317690A CNA2008100736611A CN200810073661A CN101317690A CN 101317690 A CN101317690 A CN 101317690A CN A2008100736611 A CNA2008100736611 A CN A2008100736611A CN 200810073661 A CN200810073661 A CN 200810073661A CN 101317690 A CN101317690 A CN 101317690A
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Abstract
The invention relates to an osmanthus flower additive for tobacco and the preparation method and applications thereof. The osmanthus flower additive essentially consists of the osmanthus flowers. The preparation method includes the steps that the osmanthus flowers are extracted by heating and refluxing of petroleum ether or ethanol solution or by soaking at ambient temperature; the extracted fluid is filtered and then decompressed and condensed into osmanthus flower soaking cream which is mixed with honey in certain proportion to obtain the osmanthus flower additive for tobacco. The osmanthus flower additive is dissolved in the solution of ethanol and propanediol with certain concentration to form saturated solution, which is then evenly sprayed on cut tobacco, tobacco stems or tobacco sheets which are then prepared into cigarette. The dosage of the osmanthus flower additive accounts for 0.01 to 5 percent of the weight of the cut tobacco, the tobacco stems or the tobacco sheets. The osmanthus flower additive is characterized by the harmony of the osmanthus flower fragrance and the tobacco fragrance and can soften the cigarette fragrance and reduce the irritation of the cigarette smoke to the respiratory system and the harm of smoking.
Description
Technical field
The present invention relates to a kind of extraction and application of natural perfume material, especially a kind of additive agent for osmanthus fragrance type cigarette and preparation method thereof and the application in perfuming cigarette.
Background technology
China is first big country of World tobacco production and consumption, and the annual leaf tobacco production amount of China accounts for 35% of world's total amount, and the cigarette volume of production and marketing accounts for 32% of world's total amount.Because factor affecting such as the defective of tobacco itself is big as assorted gas, bitter taste, fiber taste objectively need to improve or cover, so tobacco industry will be used a large amount of perfume additives in its product.With regard to the cigarette flavors additive, countries in the world all take much count of its research.Comparatively speaking, China is relatively weak in cigarette flavors additive industrial system, and the cigarette flavors additive product is of poor quality, the kind of Gong selecting for use is more limited, also these perfume additive major controls in supplier's hand, the overwhelming majority is a composite, product composition is indeterminate, the quality instability.For a long time, this is a bottleneck problem of restriction cigarette industry enterprise.
Sweet osmanthus originates in western part of China, is Guangxi characteristic crops, and not only raw material sources are abundant but also fragrance is dense, and are lasting, can make cake, candy, and can make wine, and reduces phlegm in addition in addition, cough-relieving, promotes the production of body fluid, ends effect such as toothache.Therefore, research is effective component extracting from sweet osmanthus, development Chinese style cigarette flavors additive green, pure natural, make the fragrant jealous improvement of cigarette, fragrance is coordinated, and pleasant impression is comfortable, flue gas exquisiteness, soft, and effectively reduce the pungent stimulation of flue gas to smoker's respiratory system, and alleviate harm of smoking, will have remarkable economical and social benefit.
Summary of the invention
The objective of the invention is: a kind of additive agent for osmanthus fragrance type cigarette and preparation method thereof and the application in perfuming cigarette are provided.
The purpose of foregoing invention is to be achieved through the following technical solutions:
The used primary raw material of preparation additive agent for osmanthus fragrance type cigarette is: sweet osmanthus.
The preparation method of additive agent for osmanthus fragrance type cigarette is:
(1) with the sweet osmanthus raw material of 100 weight portions, with the solution of 30～90 ℃ of benzinums of 500～1000 weight portions or 50～100% ethanolic solution, heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, each 1～5 hour, filter, leach the sweet osmanthus slag, merge extract, under 40～80 ℃ condition, be evaporated to paste, store for future use.
(2) get a certain amount of osmanthus concrete (10～50% percentage by weight) and proper honey (50～90% percentage by weight) mixes the formation additive agent for osmanthus fragrance type cigarette.
The application of additive agent for osmanthus fragrance type cigarette: get an amount of additive agent for osmanthus fragrance type cigarette, be dissolved in 80% ethanol and the propane diols and form saturated solution, and be sprayed at cigarette shreds uniformly, on stem or the reconstituted tobacoo and roll into cigarette and prop up.The additive agent for osmanthus fragrance type cigarette consumption is 0.01～5% of cigarette shreds, stem or a reconstituted tobacoo weight.
The invention has the beneficial effects as follows: sweet osmanthus has reduces phlegm, cough-relieving, promotes the production of body fluid, ends effect such as toothache, the additive agent for osmanthus fragrance type cigarette that makes is added in the cigarette, can make cigarette have fragrance of osmanthus and the fragrant fragrance style of coordinating of cigarette, the fragrant jealous improvement of cigarette, fragrance is coordinated, pleasant impression is comfortable, flue gas exquisiteness, soft, effectively reduce the pungent stimulation of flue gas to smoker's respiratory system, alleviate harm of smoking, and this cigarette additive preparation technology is simple, cost is low, has good market prospects and using value.
The specific embodiment
For ease of understanding the present invention better, be illustrated by following examples, embodiment only is to best implementation of the present invention, not should be understood to limitation of the present invention.
Embodiment 1
Get sweet osmanthus raw material 100 grams and place the 2000ml distilling flask, add 30～60 ℃ of petroleum ether solution 800ml, soaking at room temperature is extracted 3 times, and each 3 hours, leach the sweet osmanthus slag with the filter paper suction filtration, merge extract, under 40 ℃ water bath condition, be evaporated to paste.Prepared osmanthus concrete (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for osmanthus fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.15%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, and the process of complying with conventional perfuming is sprayed on the finished cut tobacco, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 2
Get sweet osmanthus raw material 100 grams and place the 2000ml distilling flask, add 60～90 ℃ of petroleum ether solution l000ml, refluxing extraction 2 times, each 2 hours, leach the sweet osmanthus slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared osmanthus concrete (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for osmanthus fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.2%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 3
Get sweet osmanthus raw material 100 grams and place the 2000ml distilling flask, add 95% ethanolic solution 1000ml, soaking at room temperature is extracted 3 times, and each 3 hours, leach the sweet osmanthus slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared osmanthus concrete (20% percentage by weight) and honey (80% percentage by weight) are mixed the formation additive agent for osmanthus fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed on the finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 4
Get sweet osmanthus raw material 100 grams and place the 2000ml distilling flask, add 70% ethanolic solution 800ml, refluxing extraction 2 times, each 2 hours, leach the sweet osmanthus slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared osmanthus concrete (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for osmanthus fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.4%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 5
Get sweet osmanthus raw material 100 grams and place the 2000ml distilling flask, add 95% ethanol and the petroleum ether solution 1000ml of equivalent, refluxing extraction 2 times, each 2 hours, leach the sweet osmanthus slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared osmanthus concrete (40% percentage by weight) and honey (60% percentage by weight) are mixed the formation additive agent for osmanthus fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, is dissolved in this ratio to form in 80% ethanol and the propane diols in the saturated solution, is sprayed at finished cut tobacco according to the process of conventional perfuming, and sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 6
Get sweet osmanthus raw material 100 grams and place the 2000ml distilling flask, add ethanol solution 1000ml, refluxing extraction 2 times, each 2 hours, leach the sweet osmanthus slag with the filter paper suction filtration, merge extract, under 60 ℃ water bath condition, be evaporated to paste.Prepared osmanthus concrete (30% percentage by weight) and honey (70% percentage by weight) are mixed the formation additive agent for osmanthus fragrance type cigarette.The use amount of this cigarette additive is a cigarette shreds weight 0.3%, be dissolved in this ratio and form in the saturated solution in 80% ethanol and the propane diols, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%) according to the process of conventional perfuming, sealing was preserved 24 hours, made cigarette and propped up.
Claims (3)
1, a kind of additive agent for osmanthus fragrance type cigarette, primary raw material is a sweet osmanthus, it is characterized in that: extract osmanthus concrete from sweet osmanthus, and be made up of osmanthus concrete (10-50% percentage by weight) and honey (50～90% percentage by weight).
2, the preparation method of additive agent for osmanthus fragrance type cigarette according to claim 1 is characterized in that may further comprise the steps:
(1) with the sweet osmanthus raw material of 100 weight portions, with the solution of 30～90 ℃ of benzinums of 500～1000 weight portions or 50～100% ethanolic solution, heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, each 1～5 hour, filter, leach the sweet osmanthus slag, merge extract, under 40～80 ℃ condition, be evaporated to paste, obtain osmanthus concrete;
(2) get a certain amount of osmanthus concrete (10～50% percentage by weight) and honey (50～90% percentage by weight) mixes the formation additive agent for osmanthus fragrance type cigarette.
3, the application of additive agent for osmanthus fragrance type cigarette according to claim 1 and 2, it is characterized in that: get an amount of additive agent for osmanthus fragrance type cigarette, be dissolved in 80% ethanol and the propane diols and form saturated solution, and be sprayed on cigarette shreds, stem or the reconstituted tobacoo uniformly and roll into cigarette and prop up, the additive agent for osmanthus fragrance type cigarette consumption is 0.01～5% of cigarette shreds, stem or a reconstituted tobacoo weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2008100736611A CN101317690A (en) | 2008-07-03 | 2008-07-03 | Additive agent for osmanthus fragrance type cigarette, preparation and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2008100736611A CN101317690A (en) | 2008-07-03 | 2008-07-03 | Additive agent for osmanthus fragrance type cigarette, preparation and application thereof |
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| CN101317690A true CN101317690A (en) | 2008-12-10 |
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| CNA2008100736611A Pending CN101317690A (en) | 2008-07-03 | 2008-07-03 | Additive agent for osmanthus fragrance type cigarette, preparation and application thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102551195A (en) * | 2012-02-17 | 2012-07-11 | 张婷婷 | Extract of common coltsfoot flower extracted with petroleum ether and preparation method and application thereof |
| CN103184100A (en) * | 2013-04-12 | 2013-07-03 | 红云红河烟草(集团)有限责任公司 | Method for extracting and preparing tobacco flavors by using pistacia weinmannifolia |
| CN104762134A (en) * | 2015-04-27 | 2015-07-08 | 湖北中烟工业有限责任公司 | Sweet osmanthus fermentation type cigarette perfume and preparation method thereof |
| CN104818114A (en) * | 2015-03-05 | 2015-08-05 | 云南中烟工业有限责任公司 | Preparation method and applications of indigofera stachyodes extract |
| CN105124736A (en) * | 2015-09-02 | 2015-12-09 | 云南中烟工业有限责任公司 | Method of promoting moisturizing and aroma enhancement effects of cigarettes by means of cloves |
| CN105154232A (en) * | 2015-09-15 | 2015-12-16 | 江苏锦宇环境工程有限公司 | Preparation method of tobacco flavor for refreshment |
| CN111117768A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarette, preparation method thereof and application of composition in tobacco products |
| CN111887469A (en) * | 2019-05-05 | 2020-11-06 | 贵州中烟工业有限责任公司 | Preparation method of burley tobacco additive |
| CN112226280A (en) * | 2020-10-09 | 2021-01-15 | 湖北中烟工业有限责任公司 | Spice based on key aroma components of osmanthus fragrans and application of spice in cigarettes |
| CN113897244A (en) * | 2021-10-14 | 2022-01-07 | 深圳市兰科植物保护研究中心 | Preparation method and application of healthy cigarette spice |
-
2008
- 2008-07-03 CN CNA2008100736611A patent/CN101317690A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102551195A (en) * | 2012-02-17 | 2012-07-11 | 张婷婷 | Extract of common coltsfoot flower extracted with petroleum ether and preparation method and application thereof |
| CN102551195B (en) * | 2012-02-17 | 2014-04-02 | 张婷婷 | Extract of common coltsfoot flower extracted with petroleum ether and preparation method and application thereof |
| CN103184100A (en) * | 2013-04-12 | 2013-07-03 | 红云红河烟草(集团)有限责任公司 | Method for extracting and preparing tobacco flavors by using pistacia weinmannifolia |
| CN104818114A (en) * | 2015-03-05 | 2015-08-05 | 云南中烟工业有限责任公司 | Preparation method and applications of indigofera stachyodes extract |
| CN104762134A (en) * | 2015-04-27 | 2015-07-08 | 湖北中烟工业有限责任公司 | Sweet osmanthus fermentation type cigarette perfume and preparation method thereof |
| CN105124736A (en) * | 2015-09-02 | 2015-12-09 | 云南中烟工业有限责任公司 | Method of promoting moisturizing and aroma enhancement effects of cigarettes by means of cloves |
| CN105154232A (en) * | 2015-09-15 | 2015-12-16 | 江苏锦宇环境工程有限公司 | Preparation method of tobacco flavor for refreshment |
| CN111887469A (en) * | 2019-05-05 | 2020-11-06 | 贵州中烟工业有限责任公司 | Preparation method of burley tobacco additive |
| CN111117768A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarette, preparation method thereof and application of composition in tobacco products |
| CN112226280A (en) * | 2020-10-09 | 2021-01-15 | 湖北中烟工业有限责任公司 | Spice based on key aroma components of osmanthus fragrans and application of spice in cigarettes |
| CN113897244A (en) * | 2021-10-14 | 2022-01-07 | 深圳市兰科植物保护研究中心 | Preparation method and application of healthy cigarette spice |
| CN113897244B (en) * | 2021-10-14 | 2023-10-27 | 深圳市兰科植物保护研究中心 | Preparation method and application of cigarette spice |
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Open date: 20081210 |