CN104862077B - Cigarette storax medicinal extract and preparation method thereof - Google Patents
Cigarette storax medicinal extract and preparation method thereof Download PDFInfo
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- CN104862077B CN104862077B CN201510173828.1A CN201510173828A CN104862077B CN 104862077 B CN104862077 B CN 104862077B CN 201510173828 A CN201510173828 A CN 201510173828A CN 104862077 B CN104862077 B CN 104862077B
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- cigarette
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- medicinal extract
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 65
- 235000001361 Styrax officinalis Nutrition 0.000 title claims abstract description 55
- 241001060310 Styracaceae Species 0.000 title claims abstract description 54
- 235000019382 gum benzoic Nutrition 0.000 title claims abstract description 54
- 238000000605 extraction Methods 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229930091371 Fructose Natural products 0.000 claims abstract description 9
- 239000005715 Fructose Substances 0.000 claims abstract description 9
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 238000010992 reflux Methods 0.000 claims abstract description 9
- 239000000706 filtrate Substances 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 239000012141 concentrate Substances 0.000 claims abstract description 3
- 241000208125 Nicotiana Species 0.000 claims description 16
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 16
- 239000007921 spray Substances 0.000 claims description 5
- 238000007654 immersion Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 9
- 239000003546 flue gas Substances 0.000 abstract description 9
- FMMWHPNWAFZXNH-UHFFFAOYSA-N Benz[a]pyrene Chemical compound C1=C2C3=CC=CC=C3C=C(C=C3)C2=C2C3=CC=CC2=C1 FMMWHPNWAFZXNH-UHFFFAOYSA-N 0.000 abstract description 8
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract description 3
- 235000009508 confectionery Nutrition 0.000 abstract description 3
- 230000007794 irritation Effects 0.000 abstract description 3
- 230000035807 sensation Effects 0.000 abstract description 3
- 241001122767 Theaceae Species 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 5
- 239000000779 smoke Substances 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000011269 tar Substances 0.000 description 3
- HEVGGTGPGPKZHF-UHFFFAOYSA-N 1-(1,2-dimethyl-3-methylidenecyclopentyl)-4-methylbenzene Chemical compound CC1C(=C)CCC1(C)C1=CC=C(C)C=C1 HEVGGTGPGPKZHF-UHFFFAOYSA-N 0.000 description 2
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 2
- MOYAFQVGZZPNRA-UHFFFAOYSA-N Terpinolene Chemical compound CC(C)=C1CCC(C)=CC1 MOYAFQVGZZPNRA-UHFFFAOYSA-N 0.000 description 2
- 244000269722 Thea sinensis Species 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 235000019615 sensations Nutrition 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000142952 Hamamelidaceae Species 0.000 description 1
- 235000015511 Liquidambar orientalis Nutrition 0.000 description 1
- 244000303379 Styrax officinalis Species 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229930006722 beta-pinene Natural products 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 231100000206 health hazard Toxicity 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- -1 lauro lene Chemical compound 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000011297 pine tar Substances 0.000 description 1
- 229940068124 pine tar Drugs 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- WTARULDDTDQWMU-UHFFFAOYSA-N β-pinene Chemical compound C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention discloses a kind of cigarette preparation methods of storax medicinal extract, it includes the following steps：1) dry storax is taken, is crushed to 2 10mm bulks；2) broken 50 250 parts by weight of storax, 3 15 parts by weight of fructose are taken, 0.3 1.5 parts by weight of acetic acid are added in 70 95% ethanol solution of 300 1500 parts by weight, impregnate 2 5h of heating and refluxing extraction after 4 8h, and extraction terminates postcooling, filtering；3) concentrate the filtrate to the weight identical with storax to get.The invention also discloses a kind of containing the cigarette cigarette of storax medicinal extract, which enriches, and sweet tea sense is strong, and the dry sensation of flue gas is low, and pungent sense and irritation are weak, and harmful components benzo [a] pyrene, the phenol in flue gas are substantially reduced.
Description
Technical field
The invention belongs to cigarette additive fields, and in particular to a kind of cigarette preparation method of storax medicinal extract.
Background technology
Since Smoking is harmful to your health, smoking has become the social concern of getting worse, and reducing tar and reducing harm has become cigarette industry
Very concern.Its healthhazard can be mitigated, but this frequently can lead to by reducing the content of tar and nicotine in flue gas
Smoke mitigates and insufficient fragrance.In cigarette products, the fragrance and suction taste of cigarette are very important, and additive is cigarette industry
In key link and improve product style and improve one of effective means of cigarette flavor quality, can be carried to consumer
For some fragrance and the cigarette products of suction taste satisfaction.More and more tobacco researchers find cigarette from natural plant raw material
With essence and flavoring agent, application of the natural perfume material in cigarette is more and more extensive.
The storax resin secreted for Hamamelidaceae Plants storax tree, is a kind of common Chinese medicine.Storax is main
Chemical composition contains a- and nopinene, laurene, lauro lene, limonene, 1, 8-Cineole, to P-cymene, terpinolene, fragrant camphor tree
Alcohol, pine tar -4- alcohol and a- terpinols etc..
The utilization of present storax are chiefly used in pharmaceuticals industry, also compare in tobacco business as additive application
It is rare.CN102827696A discloses a kind of preparation method of cigarette Storax extract, it is by storax 0.1-0.5%
Lactic acid aqueous solution extraction, by extract obtained be added in cigarette can promoting or transferring cigarette perfume, reduce stimulation, it is comfortable to improve throat
Sense.But the extract can not reducing tar and reducing harm.
Invention content
The object of the present invention is to provide one kind can improve cigarette smoke panel test effect and reduce flue gas harm storax leaching
The preparation method of cream.
The present invention is achieved by the following technical solutions：
A kind of cigarette preparation method of storax medicinal extract, includes the following steps：
1) dry storax is taken, is crushed to 2-10mm bulks；
2) broken storax 50-250 parts by weight, fructose 3-15 parts by weight are taken, acetic acid 0.3-1.5 parts by weight add in
Into the ethanol solution of the 70-95% of 300-1500 parts by weight, heating and refluxing extraction 2-5h, cold after extraction after immersion 4-8h
But, it filters；
3) concentrate the filtrate to the weight identical with storax to get.
Preferably, broken 150 parts by weight of storax are taken in step 2), 10 parts by weight of fructose, 0.8 parts by weight of acetic acid,
It is added in 80% ethanol solution of 1000 parts by weight, impregnates heating and refluxing extraction 3h after 5h, extraction terminates postcooling, mistake
Filter；
A kind of cigarette, the cigarette storax medicinal extract prepared containing the above method in the pipe tobacco of the cigarette, the cigarette are
It is prepared as follows：It is sprayed into the pipe tobacco of cigarette after the cigarette of preparation is atomized with storax medicinal extract, makes to contain in pipe tobacco
The cigarette storax medicinal extract of 0.01-0.05 weight %, is then made cigarette.
The beneficial effects of the present invention are：
1st, the obtained storax medicinal extract of the present invention is applied in cigarette, can enrich cigarette perfume, increases sweet tea sense, and can reduce
The dry sensation of flue gas, pungent sense and irritation have sense organ humectation effect and sweetening effect, can be obviously improved judging parameter.
2nd, harmful components benzo [a] pyrene in the cigarette smoke obtained by the present invention, phenol are substantially reduced, and illustrate the present invention
The storax medicinal extract of preparation plays the role of reducing flue gas harm.
3rd, raw material sources of the present invention are easy to get, and preparation process is simple, and production cost is low.
Specific embodiment
The present invention is described in detail with reference to embodiments.
Embodiment 1
Dry storax is taken, is crushed to 2-10mm bulks；Take broken storax 150g, fructose 10g, acetic acid
0.8g is added in 80% ethanol water of 1000g, impregnates heating and refluxing extraction 3h after 5h, and extraction terminates postcooling, mistake
Filter；150g is concentrated the filtrate to get cigarette storax medicinal extract.
It sprays into the pipe tobacco of cigarette, makes in pipe tobacco containing 0.03% after cigarette is atomized with storax medicinal extract by atomizer
Cigarette storax medicinal extract, is then made cigarette.
Embodiment 2
Dry storax is taken, is crushed to 2-10mm bulks；Take broken storax 50g, fructose 15g, acetic acid
0.3g is added in 95% ethanol water of 300g, impregnates heating and refluxing extraction 2h after 8h, and extraction terminates postcooling, filtering；
50g is concentrated the filtrate to get cigarette storax medicinal extract.
It sprays into the pipe tobacco of cigarette, makes in pipe tobacco containing 0.01% cigarette storax after cigarette is atomized with storax medicinal extract
Then cigarette is made in medicinal extract.
Embodiment 3
Dry storax is taken, is crushed to 2-10mm bulks；Take broken storax 250g, fructose 3g, acetic acid
1.5g is added in 70% ethanol water of 1500g, impregnates heating and refluxing extraction 5h after 4h, and extraction terminates postcooling, mistake
Filter；250g is concentrated the filtrate to get cigarette storax medicinal extract.
It sprays into the pipe tobacco of cigarette, makes in pipe tobacco containing 0.05% cigarette storax after cigarette is atomized with storax medicinal extract
Then cigarette is made in medicinal extract.
Embodiment 4
Dry storax is taken, is crushed to 2-10mm bulks；Take broken storax 200g, fructose 5g, acetic acid
0.5g is added in 85% ethanol water of 600g, impregnates heating and refluxing extraction 4h after 6h, and extraction terminates postcooling, filtering；
200g is concentrated the filtrate to get cigarette storax medicinal extract.
It sprays into the pipe tobacco of cigarette, makes in pipe tobacco containing 0.04% cigarette storax after cigarette is atomized with storax medicinal extract
Then cigarette is made in medicinal extract.
Effect of smokeing panel test and detection：
Perfumer smokes panel test, and compared with CN102827696A, embodiment 1-4 cigarette perfumes are more abundant, the sense of flue gas sweet tea, moistening
Feel stronger, dry sensation is lighter, and irritation is weaker.It presses《The survey of benzo [a] pyrene in GB/T21130-2007 cigarette smoke condensates
It is fixed》With《The measure high performance liquid chromatography of YC/T255-2008 main phenolic compounds in main stream smoke of cigarette》, detect flue gas
There is drop evil effect.Simultaneously using CN102827696A as control, testing result see the table below.
Table 1 harmful substances in flue gas benzo [a] pyrene, phenol testing result
Claims (4)
1. a kind of cigarette preparation method of storax medicinal extract, it is characterised in that include the following steps：
1) dry storax is taken, is crushed to 2-10mm bulks；
2) broken storax 50-250 parts by weight, fructose 3-15 parts by weight are taken, acetic acid 0.3-1.5 parts by weight are added to
In the ethanol solution of the 70-95% of 300-1500 parts by weight, heating and refluxing extraction 2-5h, cold after extraction after immersion 4-8h
But, it filters；
3) concentrate the filtrate to the weight identical with storax to get.
2. the cigarette as described in claim 1 preparation method of storax medicinal extract, it is characterised in that：In step 2), take after crushing
150 parts by weight of storax, 10 parts by weight of fructose, 0.8 parts by weight of acetic acid are added to 80% ethanol solution of 1000 parts by weight
In, heating and refluxing extraction 3h after 5h is impregnated, extraction terminates postcooling, filtering.
3. the cigarette that preparation method as claimed in claim 1 or 2 obtains storax medicinal extract.
4. a kind of cigarette, containing the storax medicinal extract of the cigarette described in claim 3 in the pipe tobacco of the cigarette, the cigarette be by
Prepared by following methods：It sprays into the pipe tobacco of cigarette, makes in pipe tobacco after cigarette described in claim 3 is atomized with storax medicinal extract
Cigarette storax medicinal extract containing 0.01-0.05 weight %, is then made cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510173828.1A CN104862077B (en) | 2015-04-14 | 2015-04-14 | Cigarette storax medicinal extract and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510173828.1A CN104862077B (en) | 2015-04-14 | 2015-04-14 | Cigarette storax medicinal extract and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104862077A CN104862077A (en) | 2015-08-26 |
| CN104862077B true CN104862077B (en) | 2018-06-08 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510173828.1A Active CN104862077B (en) | 2015-04-14 | 2015-04-14 | Cigarette storax medicinal extract and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN104862077B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109536394B (en) * | 2018-11-09 | 2021-05-18 | 湖北中烟工业有限责任公司 | Preparation method and application of storax extract |
| CN111358035A (en) * | 2020-03-17 | 2020-07-03 | 四川中烟工业有限责任公司 | Cigarette cream fragrance base and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN101940359A (en) * | 2010-09-20 | 2011-01-12 | 湖北中烟工业有限责任公司 | Spice for green tea cigarette and preparation method thereof |
| CN102793264A (en) * | 2012-08-31 | 2012-11-28 | 中国烟草总公司郑州烟草研究院 | Preparation method of magnolia fruit extract and application thereof in cigarette |
| CN102827696A (en) * | 2012-08-16 | 2012-12-19 | 湖北中烟工业有限责任公司 | Preparation method and application of styrax extract for tobacco |
-
2015
- 2015-04-14 CN CN201510173828.1A patent/CN104862077B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN101940359A (en) * | 2010-09-20 | 2011-01-12 | 湖北中烟工业有限责任公司 | Spice for green tea cigarette and preparation method thereof |
| CN102827696A (en) * | 2012-08-16 | 2012-12-19 | 湖北中烟工业有限责任公司 | Preparation method and application of styrax extract for tobacco |
| CN102793264A (en) * | 2012-08-31 | 2012-11-28 | 中国烟草总公司郑州烟草研究院 | Preparation method of magnolia fruit extract and application thereof in cigarette |
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| Publication number | Publication date |
|---|---|
| CN104862077A (en) | 2015-08-26 |
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