CN102827696A - Preparation method and application of styrax extract for tobacco - Google Patents
Preparation method and application of styrax extract for tobacco Download PDFInfo
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- CN102827696A CN102827696A CN2012102933856A CN201210293385A CN102827696A CN 102827696 A CN102827696 A CN 102827696A CN 2012102933856 A CN2012102933856 A CN 2012102933856A CN 201210293385 A CN201210293385 A CN 201210293385A CN 102827696 A CN102827696 A CN 102827696A
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- styrax
- tobacco
- cigarette
- extract
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 34
- 235000000126 Styrax benzoin Nutrition 0.000 title claims abstract description 32
- 235000015511 Liquidambar orientalis Nutrition 0.000 title claims abstract description 31
- 239000004870 Styrax Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 244000028419 Styrax benzoin Species 0.000 title description 3
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 241000208125 Nicotiana Species 0.000 claims abstract description 34
- 241000736148 Styrax Species 0.000 claims abstract description 29
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000007864 aqueous solution Substances 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 7
- 239000004310 lactic acid Substances 0.000 claims abstract description 7
- 238000010992 reflux Methods 0.000 claims abstract description 7
- 235000019504 cigarettes Nutrition 0.000 claims description 48
- 241001060310 Styracaceae Species 0.000 claims description 28
- 235000001361 Styrax officinalis Nutrition 0.000 claims description 28
- 235000019382 gum benzoic Nutrition 0.000 claims description 28
- 238000000605 extraction Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 2
- 230000008569 process Effects 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 8
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000006872 improvement Effects 0.000 abstract description 3
- 238000012986 modification Methods 0.000 abstract description 3
- 230000004048 modification Effects 0.000 abstract description 3
- 239000000779 smoke Substances 0.000 abstract description 2
- 239000000706 filtrate Substances 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 241000411851 herbal medicine Species 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 238000007789 sealing Methods 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 230000001737 promoting effect Effects 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- MOYAFQVGZZPNRA-UHFFFAOYSA-N Terpinolene Chemical compound CC(C)=C1CCC(C)=CC1 MOYAFQVGZZPNRA-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- UAHWPYUMFXYFJY-UHFFFAOYSA-N beta-myrcene Chemical compound CC(C)=CCCC(=C)C=C UAHWPYUMFXYFJY-UHFFFAOYSA-N 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- WTARULDDTDQWMU-RKDXNWHRSA-N (+)-β-pinene Chemical compound C1[C@H]2C(C)(C)[C@@H]1CCC2=C WTARULDDTDQWMU-RKDXNWHRSA-N 0.000 description 1
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- WTARULDDTDQWMU-IUCAKERBSA-N (-)-Nopinene Natural products C1[C@@H]2C(C)(C)[C@H]1CCC2=C WTARULDDTDQWMU-IUCAKERBSA-N 0.000 description 1
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 1
- WUOACPNHFRMFPN-SECBINFHSA-N (S)-(-)-alpha-terpineol Chemical compound CC1=CC[C@@H](C(C)(C)O)CC1 WUOACPNHFRMFPN-SECBINFHSA-N 0.000 description 1
- 206010008190 Cerebrovascular accident Diseases 0.000 description 1
- 206010010071 Coma Diseases 0.000 description 1
- 241000142952 Hamamelidaceae Species 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- WTARULDDTDQWMU-UHFFFAOYSA-N Pseudopinene Natural products C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 description 1
- 208000006011 Stroke Diseases 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- XCPQUQHBVVXMRQ-UHFFFAOYSA-N alpha-Fenchene Natural products C1CC2C(=C)CC1C2(C)C XCPQUQHBVVXMRQ-UHFFFAOYSA-N 0.000 description 1
- 229930006722 beta-pinene Natural products 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 229960005233 cineole Drugs 0.000 description 1
- 239000011280 coal tar Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 206010015037 epilepsy Diseases 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- LCWMKIHBLJLORW-UHFFFAOYSA-N gamma-carene Natural products C1CC(=C)CC2C(C)(C)C21 LCWMKIHBLJLORW-UHFFFAOYSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 231100000206 health hazard Toxicity 0.000 description 1
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 1
- 208000031225 myocardial ischemia Diseases 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 239000006191 orally-disintegrating tablet Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 208000010110 spontaneous platelet aggregation Diseases 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000011269 tar Substances 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a preparation method of a styrax extract for tobacco, and an application in tobacco. The styrax extract for tobacco is prepared by the following steps: soaking 1 part of styrax in a lactic acid aqueous solution with a mass fraction of 0.1-0.5% and a weight being 5-8 times more than that of the styrax for 1 hour, extracting the styrax by heating reflux at normal pressure for 2-4 hours per each time, cooling, filtering, respectively taking 3 filtrates; combining the 3 filtrates, and performing reduced-pressure concentration at 60 DEG C to obtain a weight being 2 times more than the original weight of the styrax. According to the invention, the styrax extract is used in tobacco for the first time, which can improve and adjust tobacco fragrance, reduce irritation, and improve throat comfort. The natural fragrance contained in the styrax extract is harmonized with tobacco; a formula of tobacco added with the styrax extract has good modification effect on the smoke form, and the fragrance is more abundant; good improvement effect on tobacco quality is provided. The preparation method of the invention has easily available raw materials, simple preparation technology, and low cost, and facilitates production conversion.
Description
Technical field
The present invention relates to the preparation method of tobacco aromatics using, refer to of preparation method and the application of a kind of cigarette particularly with Storax extract.
Background technology
Because Smoking is harmful to your health, smoking has become serious social concern day by day, and reducing tar and reducing harm has become the problem that cigarette industry extremely is concerned about.The reduction flue gas is coal-tar middle oil to alleviate its health hazard with content nicotine, but this tends to cause smoke to alleviate and insufficient fragrance.In cigarette products; The fragrance of cigarette is very important with inhaling flavor; Adding spices is the key link in the cigarette industry, also is to improve product style and one of effective means that improves the cigarette flavor quality, can provide some fragrance the cigarette products satisfied with inhaling flavor to the human consumer.
Herbal medicine is the distinct Chinese characteristics products, and tobacco is combined with herbal medicine, is one of " Chinese style cigarette " most characteristic style.Chinese herbal medicine extract is applied to one of the reinforced emphasis that has become the tobacco industry development of perfuming cigarette and focus as additive.Along with the application of herbal medicine class additive in cigarette accepted by consumers in general day by day, existing increasing tobacco researcher is sought essence spice for cigarette from natural Chinese medicinal herb, and the application of natural perfume in cigarette more and more widely.
Styrax is the secreted resin of Hamamelidaceae plant Styrax tree, is a kind of Chinese medicine commonly used.Early summer bark is wounded or cuts and reach woody part deeply, resinoid is infiltrated in the bark.Peel bark autumn, squeeze resinoid, residue squeezes after adding poach again, and the expressed face cream is common Styrax.It is dissolved in the alcohol, filters, boil off alcohol, then become styrax depuratus.Having has one's ideas straightened out wards off dirtyly, opens strongly fragrant open-minded phlegm, the effect of promoting the circulation of QI to relieve pain.Be used for the apoplexy coma due to blocking of the respiratory system clinically, suddenly faint, chest abdomen crymodynia, frightened epilepsy.The modern pharmacology experiment shows that it has platelet aggregation-against, the effect of resisting myocardial ischemia and Azelaic Acid.The Styrax main chemical compositions contains a-and beta-pinene, myrcene, and lauro lene, PC 560,1, the 8-cineole, to P-cymene, terpinolene, phantol, the pure and mild a-Terpineol 350 of pine tar-4-etc.
The development and use of Styrax now are used for pharmaceutical industries more, are orally disintegrating tablets that contains by Styrax and preparation method thereof like patent CN200410039229.2, and CN200810124842.2 is a kind of capsule that contains Styrax and preparation method thereof.In tobacco industry, also do not have relevant report, more do not have application as tobacco aromatics using.
Summary of the invention
The object of the invention will overcome the existing in prior technology deficiency exactly, and a kind of dose preparation method and application are provided.
Cigarette of the present invention may further comprise the steps with the preparation method of Storax extract:
1) getting 1 part of Styrax, is that heating and refluxing extraction was 3 times under normal pressure after 0.1 ~ 0.5% lactic acid aqueous solution soaked 1 hour with the massfraction that is equivalent to 5 ~ 8 times of weight of Styrax, and each 2 ~ 4 hours, cooled and filtered was left and taken filtrating respectively 3 times;
2) merge filtrating three times, be evaporated to 2 times of the former weight of Styrax under 60 ℃, promptly get required cigarette and use Storax extract.
Cigarette of the present invention is with the concrete application of Storax extract: with the Storax extract that makes; Be dissolved in the pure water; The addition that accounts for pipe tobacco dry weight 0.01 ~ 0.1% by Storax extract evenly is sprayed in the blank pipe tobacco; Under 60 ℃ of conditions with shredded tobacco baking to moisture content 14wt%, process cigarette.
Beneficial effect of the present invention is: the present invention is applied to Storax extract in the middle of the cigarette first, and can the promoting or transferring cigarette fragrant, reducing stimulates, and improves throat's comfort.Contained natural fragrance and tobacco are coordinated in the Storax extract, the flue gas form are had modification preferably after joining the tobacco tobacco leaf formulation, make fragrance become abundanter simultaneously, and cigarette quality is had good improvement effect.The starting material source that the present invention adopted is easy to get, and preparation technology is simple, and cost is low, is beneficial to produce to transform.
Embodiment
Further set forth the present invention below in conjunction with specific embodiment.Following examples only are to be used for further specific descriptions of the present invention, rather than are used for the qualification to requirement protection domain of the present invention.
Embodiment 1
Styrax 100g is placed the 2000ml distilling flask; Add the 500g massfraction and be under the 0.5% lactic acid aqueous solution normal pressure heating and refluxing extraction 3 times; Each 2 hours, cooled and filtered merged filtrating 3 times; Be evaporated to 2 times of the former weight of Styrax under 60 ℃, promptly get required cigarette and use Storax extract.
The cigarette of gained uses the addition of Storax extract to be 0.01% of cigarette shreds weight; Cigarette with gained is dissolved in the pure water with Storax extract earlier; Evenly be sprayed on the blank pipe tobacco according to conventional reinforced processing sequence; With shredded tobacco baking to moisture content 14%, sealing was preserved 24 hours, processed cigarette and propped up under 60 ℃ of conditions.
Embodiment 2
Styrax 100g is placed the 2000ml distilling flask; Add the 600g massfraction and be under the 0.2% lactic acid aqueous solution normal pressure heating and refluxing extraction 3 times; Each 3 hours, cooled and filtered merged filtrating 3 times; Be evaporated to 2 times of the former weight of Styrax under 60 ℃, promptly get required cigarette and use Storax extract.
The cigarette of gained uses the addition of Storax extract to be 0.05% of cigarette shreds weight; Cigarette with gained is dissolved in the pure water with Storax extract earlier; Evenly be sprayed on the blank pipe tobacco according to conventional reinforced processing sequence; With shredded tobacco baking to moisture content 14%, sealing was preserved 24 hours, processed cigarette and propped up under 60 ℃ of conditions.
Embodiment 3
Styrax 100g is placed the 2000ml distilling flask; Add the 700g massfraction and be under the 0.3% lactic acid aqueous solution normal pressure heating and refluxing extraction 3 times; Each 2 hours, cooled and filtered merged filtrating 3 times; Be evaporated to 2 times of the former weight of Styrax under 60 ℃, promptly get required cigarette and use Storax extract.
The cigarette of gained uses the addition of Storax extract to be 0.02% of cigarette shreds weight; Cigarette with gained is dissolved in the pure water with Storax extract earlier; Evenly be sprayed on the blank pipe tobacco according to conventional reinforced processing sequence; With shredded tobacco baking to moisture content 14%, sealing was preserved 24 hours, processed cigarette and propped up under 60 ℃ of conditions.
Embodiment 4
Styrax 100g is placed the 2000ml distilling flask; Add the 800g massfraction and be under the 0.1% lactic acid aqueous solution normal pressure heating and refluxing extraction 3 times; Each 4 hours, cooled and filtered merged filtrating 3 times; Be evaporated to 2 times of the former weight of Styrax under 60 ℃, promptly get required cigarette and use Storax extract.
The cigarette of gained uses the addition of Storax extract to be 0.03% of cigarette shreds weight; Cigarette with gained is dissolved in the pure water with Storax extract earlier; Evenly be sprayed on the blank pipe tobacco according to conventional reinforced processing sequence; With shredded tobacco baking to moisture content 14%, sealing was preserved 24 hours, processed cigarette and propped up under 60 ℃ of conditions.
Effect
Select middle-grade blank pipe tobacco for use, the effect that the embodiment of the invention 1 ~ 4 prepared tobacco aromatics using adds in the cigarette is estimated, the result is as shown in table 1.
The sensory evaluating smoking of table 1 embodiment of the invention describes
Shown that by smoking result in the table 1 the prepared cigarette of the present invention is can the promoting or transferring cigarette fragrant with Storax extract, reducing stimulates, and improves throat's comfort.Natural fragrance and tobacco contained in the Storax extract are coordinated, and the flue gas form is had modification preferably, make fragrance become abundanter simultaneously, and cigarette quality is had good improvement effect, can be used as novel tobacco aromatics using and use.
Claims (2)
1. a cigarette may further comprise the steps with the preparation method of Storax extract:
1) getting 1 part of Styrax, is that heating and refluxing extraction was 3 times under normal pressure after 0.1 ~ 0.5% lactic acid aqueous solution soaked 1 hour with the massfraction that is equivalent to 5 ~ 8 times of weight of Styrax, and each 2 ~ 4 hours, cooled and filtered was left and taken filtrating respectively 3 times;
2) merge filtrating three times, be evaporated to 2 times of the former weight of Styrax under 60 ℃, promptly get required cigarette and use Storax extract.
2. according to of the application of the said cigarette of claim 1 with Storax extract; It is characterized in that: with the Storax extract that makes; Be dissolved in the pure water; The addition that accounts for pipe tobacco dry weight 0.01 ~ 0.1% by Storax extract evenly is sprayed in the blank pipe tobacco, under 60 ℃ of conditions with shredded tobacco baking to moisture content 14wt%, process cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012102933856A CN102827696A (en) | 2012-08-16 | 2012-08-16 | Preparation method and application of styrax extract for tobacco |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012102933856A CN102827696A (en) | 2012-08-16 | 2012-08-16 | Preparation method and application of styrax extract for tobacco |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102827696A true CN102827696A (en) | 2012-12-19 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012102933856A Pending CN102827696A (en) | 2012-08-16 | 2012-08-16 | Preparation method and application of styrax extract for tobacco |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102827696A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103131538A (en) * | 2013-03-04 | 2013-06-05 | 湖北中烟工业有限责任公司 | Beer distillation substrate preparation method used for cigarette and application of the preparation method in cigarette |
| CN104862077A (en) * | 2015-04-14 | 2015-08-26 | 湖北中烟工业有限责任公司 | Cigarette-use styrax extract and preparation method thereof |
| CN109105947A (en) * | 2018-07-05 | 2019-01-01 | 湖北中烟工业有限责任公司 | A kind of multistage solvent extraction preparation method and applications of cocoa extract |
| CN109536394A (en) * | 2018-11-09 | 2019-03-29 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of Storax extract |
| CN111849635A (en) * | 2020-08-03 | 2020-10-30 | 湖北中烟工业有限责任公司 | Persicant cigarette flavor and preparation method and application thereof |
Citations (3)
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|---|---|---|---|---|
| CN1189532A (en) * | 1997-01-25 | 1998-08-05 | 杨国祥 | Prodn. tech. of natural plant perfume for cigarette |
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN101940359A (en) * | 2010-09-20 | 2011-01-12 | 湖北中烟工业有限责任公司 | Spice for green tea cigarette and preparation method thereof |
-
2012
- 2012-08-16 CN CN2012102933856A patent/CN102827696A/en active Pending
Patent Citations (3)
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|---|---|---|---|---|
| CN1189532A (en) * | 1997-01-25 | 1998-08-05 | 杨国祥 | Prodn. tech. of natural plant perfume for cigarette |
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN101940359A (en) * | 2010-09-20 | 2011-01-12 | 湖北中烟工业有限责任公司 | Spice for green tea cigarette and preparation method thereof |
Non-Patent Citations (3)
| Title |
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| 张颖璞等: "中草药在中式低危害卷烟中的应用", 《科技信息》 * |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103131538A (en) * | 2013-03-04 | 2013-06-05 | 湖北中烟工业有限责任公司 | Beer distillation substrate preparation method used for cigarette and application of the preparation method in cigarette |
| CN104862077A (en) * | 2015-04-14 | 2015-08-26 | 湖北中烟工业有限责任公司 | Cigarette-use styrax extract and preparation method thereof |
| CN104862077B (en) * | 2015-04-14 | 2018-06-08 | 湖北中烟工业有限责任公司 | Cigarette storax medicinal extract and preparation method thereof |
| CN109105947A (en) * | 2018-07-05 | 2019-01-01 | 湖北中烟工业有限责任公司 | A kind of multistage solvent extraction preparation method and applications of cocoa extract |
| CN109536394A (en) * | 2018-11-09 | 2019-03-29 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of Storax extract |
| CN111849635A (en) * | 2020-08-03 | 2020-10-30 | 湖北中烟工业有限责任公司 | Persicant cigarette flavor and preparation method and application thereof |
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Application publication date: 20121219 |