CN101130715A - Peony essential oil abstracted from supercritical CO* fluid and application of the same in perfuming cigarette - Google Patents
Peony essential oil abstracted from supercritical CO* fluid and application of the same in perfuming cigarette Download PDFInfo
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- CN101130715A CN101130715A CNA2007101897211A CN200710189721A CN101130715A CN 101130715 A CN101130715 A CN 101130715A CN A2007101897211 A CNA2007101897211 A CN A2007101897211A CN 200710189721 A CN200710189721 A CN 200710189721A CN 101130715 A CN101130715 A CN 101130715A
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- essential oil
- tree peony
- peony flower
- cigarette
- flower essential
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Abstract
The invention discloses an essential oil of peony flower extracted by hypercritical CO2 flow and the application in the perfuming cigarette, which comprises the following steps: acquiring dried petal of peony as raw material and hypercritical CO2 flow as extracting solvent; setting the extracting pressure at 15-30Mpa, extracting temperature at 35-60 deg. c, separating pressure at 6-9Mpa and separating temperature at 50-65 deg. c; stopping extracting until the extracting and separating autoclave doesn't separate the product. The invention increases the cigarette perfume, reduces stimulation and impure gas and modifies the end taste through adding natural essential oil of essential oil of peony flower into the cut tobacco, which provides a new and well natural perfume for the cigarette.
Description
Technical field
The present invention relates to the extraction and the application of natural perfume, be specifically related to a kind of supercritical CO
2Fluid extraction Tree Peony flower essential oil and the application in perfuming cigarette thereof, the Tree Peony flower essential oil that utilizes the present invention to obtain has good effect in perfuming cigarette.
Background technology
Essence and flavoring agent is widely used in daily chemical products, food, tobacco, feed and many Industrial products, and natural perfume is because its composition is complicated, fragrance is abundant, fragrance remaining time is the indispensable raw material of preparing essence lastingly.
Tree peony is one of China's tradition rare flower, and cultivation history has more than 2000 year history.The tree peony florigen is with beautiful in colour, splendid, and is elegant and poised and solely press beautiful and fragrant flowers, and has the fragrance of strong grace, unusual because of treasure again, the flower type is abundant, and color is multifarious and well-known everywhere.Tree Peony flower is the flower of wealth and rank.The flower of luckiness.Be known as " aromatic ", " king in spending " from ancient times.Tree Peony flower and pharmaceutical use is arranged can promoting blood flow to regulate menstruation.
Along with smoking and healthy problem more and more receive publicity, improve cigarette suck security, improve cigarette interior quality, reduce objectionable constituent in the cigarette smoke, improve the inevitable development trend that the mouthfeel pleasant impression is a cigarette.
Summary of the invention
Purpose of the present invention just is being based on above-mentioned condition and a kind of supercritical CO of developing
2Fluid extraction Tree Peony flower essential oil and the application in perfuming cigarette thereof are applied to the Tree Peony flower essential oil on the cigarette shreds, can increase cigarette flavor, reducing stimulates and assorted gas, improve the mouthfeel pleasant impression, and this The Application of Technology do not change the existing complete processing of cigarette, can improve the interior quality of cigarette.
The objective of the invention is to realize: supercritical CO of the present invention by following scheme
2Fluid extraction Tree Peony flower essential oil is to make by the following method: with the tree peony dry petal is raw material, with supercritical CO
2Fluid is an extraction solvent, extracting pressure 15-30MPa, and extraction temperature: 35-60 ℃, separating pressure 6-9MPa, separation temperature: 50-65 ℃, be extracted to separating still and no longer isolate and stop extraction behind the product, finally obtain the Tree Peony flower essential oil.
Tree Peony flower essential oil of the present invention is joined in the cigarette shreds as spices, can increase fragrance, reduce the gas that stimulates, mixes, improve the mouthfeel pleasant impression, Tree Peony flower essential oil consumption is the 0.01-0.1% of pipe tobacco weight, by dehydrated alcohol essential oil is diluted earlier, adds in the pipe tobacco by the spray add mode again.
Effect of the present invention and benefit are to use supercritical CO
2Fluid extraction Tree Peony flower essential oil, Tree Peony flower essential oil and CO
2Natural separation, the solvent-free pollution of product, and the fragrance of essential oil is abundant, comprehensive, complete.For tobacco flavoring provides novel, a respond well natural perfume.
Embodiment
To method afford further instruction of the present invention, but do not limit the present invention below by example.
Embodiment 1
With electronic balance weighing tree peony dried flower 200g, pack in the stainless steel charging basket of supercritical extraction after the pulverizing equably and add the 20g dehydrated alcohol and carry out CO
2Supercritical extraction.35 ℃ of extracting pressure 15MPa, extraction temperature, separating pressure 6MPa, separation temperature: under 50 ℃ of conditions, use supercritical CO
2Continuous extraction to separating still stops extraction after no longer isolating product, obtains tree peony caul-fat 2.8g.
With dehydrated alcohol or ethanol content is after 95% edible ethanol is 1% (weight ratio) with Tree Peony flower essential oil dissolved dilution, get the Tree Peony flower essential oil by 0.01% of pipe tobacco weight, spray is added in the flue-cured tobacco pipe tobacco, think through smokeing panel test: this product in flue-cured tobacco to add effect obvious, fragrance increases, can make smoke alcohol and, there is improvement fine and smooth aspect, pleasant impression is comparatively comfortable.
Embodiment 2
With electronic balance weighing tree peony dried flower 200g, pack in the stainless steel charging basket of supercritical extraction after the pulverizing equably and add the 20g dehydrated alcohol and carry out CO
2Supercritical extraction.60 ℃ of extracting pressure 30MPa, extraction temperature, separating pressure 9MPa, separation temperature: under 65 ℃ of conditions, use supercritical CO
2Continuous extraction to separating still stops extraction after no longer isolating product, obtains tree peony caul-fat 3g.
With dehydrated alcohol or ethanol content is after 95% edible ethanol is 1% (weight ratio) with Tree Peony flower essential oil dissolved dilution, get the Tree Peony flower essential oil by 0.1% of pipe tobacco weight, spray is added in the flue-cured tobacco pipe tobacco, think through smokeing panel test: this product in flue-cured tobacco to add effect obvious, fragrance increases, can make smoke alcohol and, exquisiteness, pleasant impression is comfortable.
Claims (4)
1. supercritical CO
2Fluid extraction Tree Peony flower essential oil is characterized in that: it is to make by the following method: with the tree peony dry petal is raw material, with supercritical CO
2Fluid is an extraction solvent, extracting pressure 15-30MPa, and extraction temperature: 35-60 ℃, separating pressure 6-9MPa, separation temperature: 50-65 ℃, be extracted to separating still and no longer isolate and stop extraction behind the product, obtain the Tree Peony flower essential oil.
2. the application of Tree Peony flower essential oil according to claim 1 in perfuming cigarette is characterized in that: Tree Peony flower essential oil of the present invention is joined in the cigarette shreds as spices.
3. the application of Tree Peony flower essential oil according to claim 2 in perfuming cigarette, it is characterized in that: Tree Peony flower essential oil consumption is the 0.01-0.1% of pipe tobacco weight, be that 95% edible ethanol dilutes essential oil by dehydrated alcohol or ethanol content earlier, add in the pipe tobacco by the spray add mode again.
4. the application of Tree Peony flower essential oil according to claim 3 in perfuming cigarette is characterized in that: dehydrated alcohol (perhaps 95% edible ethanol) dilutes essential oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101897211A CN101130715B (en) | 2007-09-29 | 2007-09-29 | Peony essential oil abstracted from supercritical CO* fluid and application of the same in perfuming cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101897211A CN101130715B (en) | 2007-09-29 | 2007-09-29 | Peony essential oil abstracted from supercritical CO* fluid and application of the same in perfuming cigarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101130715A true CN101130715A (en) | 2008-02-27 |
| CN101130715B CN101130715B (en) | 2010-10-13 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2007101897211A Expired - Fee Related CN101130715B (en) | 2007-09-29 | 2007-09-29 | Peony essential oil abstracted from supercritical CO* fluid and application of the same in perfuming cigarette |
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| CN (1) | CN101130715B (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2443315C1 (en) * | 2011-01-27 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| CN102391913A (en) * | 2011-10-10 | 2012-03-28 | 杨永庆 | Supercritical extraction method for peony essence and application of method |
| CN102643719A (en) * | 2012-05-09 | 2012-08-22 | 云南烟草科学研究院 | Macadimia nut flower extract and application thereof |
| CN103242960A (en) * | 2013-05-15 | 2013-08-14 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing tobacco flower absolute oil by using supercritical CO2 extraction |
| CN103272008A (en) * | 2013-06-11 | 2013-09-04 | 洛阳建洛生物科技有限公司 | Technology for synergistically extracting peony flavone |
| CN103271860A (en) * | 2013-06-18 | 2013-09-04 | 菏泽尧舜牡丹生物科技有限公司 | Skin care oil containing peony oil and preparation method thereof |
| CN103305344A (en) * | 2013-06-18 | 2013-09-18 | 菏泽尧舜牡丹生物科技有限公司 | Method for extracting peony essence from fresh peony flowers |
| CN103519352A (en) * | 2013-11-07 | 2014-01-22 | 袁恩泽 | Electronic cigarette |
| CN104004589A (en) * | 2013-10-31 | 2014-08-27 | 菏泽中禾健元生物科技有限公司 | Producing method of peony essential oil |
| CN105132181A (en) * | 2015-08-10 | 2015-12-09 | 上海震樨机电科技发展有限公司 | Process for extracting paeonia suffruticosa essential oil from paeonia suffruticosa fresh flower |
| CN105733812A (en) * | 2016-03-17 | 2016-07-06 | 金沙鑫顺农业发展有限公司 | Supercritical CO2 extraction method of peony essence |
| CN106867665A (en) * | 2015-12-10 | 2017-06-20 | 澳华达香料科技(广州)有限公司 | A kind of essential oil containing nicotine tobacco and its preparation method and application less |
-
2007
- 2007-09-29 CN CN2007101897211A patent/CN101130715B/en not_active Expired - Fee Related
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2443315C1 (en) * | 2011-01-27 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| CN102391913A (en) * | 2011-10-10 | 2012-03-28 | 杨永庆 | Supercritical extraction method for peony essence and application of method |
| CN102643719A (en) * | 2012-05-09 | 2012-08-22 | 云南烟草科学研究院 | Macadimia nut flower extract and application thereof |
| CN103242960A (en) * | 2013-05-15 | 2013-08-14 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing tobacco flower absolute oil by using supercritical CO2 extraction |
| CN103272008A (en) * | 2013-06-11 | 2013-09-04 | 洛阳建洛生物科技有限公司 | Technology for synergistically extracting peony flavone |
| CN103305344A (en) * | 2013-06-18 | 2013-09-18 | 菏泽尧舜牡丹生物科技有限公司 | Method for extracting peony essence from fresh peony flowers |
| CN103271860A (en) * | 2013-06-18 | 2013-09-04 | 菏泽尧舜牡丹生物科技有限公司 | Skin care oil containing peony oil and preparation method thereof |
| CN103305344B (en) * | 2013-06-18 | 2014-07-16 | 菏泽尧舜牡丹生物科技有限公司 | Method for extracting peony essence from fresh peony flowers |
| CN103271860B (en) * | 2013-06-18 | 2015-04-15 | 菏泽尧舜牡丹生物科技有限公司 | Skin care oil containing peony oil and preparation method thereof |
| CN104004589A (en) * | 2013-10-31 | 2014-08-27 | 菏泽中禾健元生物科技有限公司 | Producing method of peony essential oil |
| CN104004589B (en) * | 2013-10-31 | 2017-02-08 | 菏泽中禾健元生物科技有限公司 | Producing method of peony essential oil |
| CN103519352A (en) * | 2013-11-07 | 2014-01-22 | 袁恩泽 | Electronic cigarette |
| CN105132181A (en) * | 2015-08-10 | 2015-12-09 | 上海震樨机电科技发展有限公司 | Process for extracting paeonia suffruticosa essential oil from paeonia suffruticosa fresh flower |
| CN106867665A (en) * | 2015-12-10 | 2017-06-20 | 澳华达香料科技(广州)有限公司 | A kind of essential oil containing nicotine tobacco and its preparation method and application less |
| CN105733812A (en) * | 2016-03-17 | 2016-07-06 | 金沙鑫顺农业发展有限公司 | Supercritical CO2 extraction method of peony essence |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101130715B (en) | 2010-10-13 |
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