CN101130713A - Chinese toon leaf extraction extracted from petroleum ether and application of the same in perfuming cigarette - Google Patents
Chinese toon leaf extraction extracted from petroleum ether and application of the same in perfuming cigarette Download PDFInfo
- Publication number
- CN101130713A CN101130713A CNA2007101897175A CN200710189717A CN101130713A CN 101130713 A CN101130713 A CN 101130713A CN A2007101897175 A CNA2007101897175 A CN A2007101897175A CN 200710189717 A CN200710189717 A CN 200710189717A CN 101130713 A CN101130713 A CN 101130713A
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- CN
- China
- Prior art keywords
- toonae sinensis
- folium toonae
- medicinal extract
- cigarette
- chinese toon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The invention discloses a Chinese toon leaf extract extracted by petroleum ether and the application of the extract in the perfuming cigarette, which comprises the following steps: acquiring the Chinese toon leaf; extracting through petroleum ether; separating liquid from solid; clarifying; filtering; distilling; condensing; obtaining the product under indoor temperature without heating and breaking perfuming component in the Chinese toon leaf. The invention simplifies the extracting technique and operation to ensure the residual in the extract satisfy the safe standard through using medical graded petroleum ether, which adds perfume into the cigarette, reduces stimulation and impure gas and modifies the end taste through adding natural essential oil of Chinese toon leaf into the cut tobacco by spraying, therefore improving the comfort during smoking to provide a new and well natural perfume for the cigarette.
Description
Technical field
The present invention relates to the extraction and the application of natural perfume, be specifically related to a kind of Chinese toon leaf extraction extracted from petroleum ether and the application in perfuming cigarette thereof, the Folium toonae sinensis medicinal extract that utilizes the present invention to obtain has good effect in perfuming cigarette.
Background technology
Essence and flavoring agent is widely used in daily chemical products, food, tobacco, feed and many Industrial products, and natural perfume is because its composition is complicated, fragrance is abundant, fragrance remaining time is the indispensable raw material of preparing essence lastingly.
Chinese toon has another name called Chinese toon, Chinese toon head, Folium toonae sinensis, and section's Cedrela originates in China, is perennial deciduous tree, and trees are the highest to exceed 30 meters, the tender and crisp succulence of Chinese toon tender shoots (leaf), and the color and luster deliciousness has unique strong fragrance; Nutritive value of Chinese toon and economic worth are all high, and China is unique with the country of Chinese toon as vegetables.Now a lot of places have begun the Chinese toon implant mass.
Along with the problem of smoking with health more and more receives publicity, improve the security of sucking of cigarette, the comfort of the objectionable constituent in the reduction cigarette smoke, raising suction is the inevitable development trend of cigarette.
Summary of the invention
Purpose of the present invention just is being based on above-mentioned condition and a kind of Chinese toon leaf extraction extracted from petroleum ether developed and the application in perfuming cigarette thereof, the Folium toonae sinensis medicinal extract that method of the present invention extracted is joined in the cigarette shreds, can increase cigarette flavor, reducing stimulates and assorted gas, improve the mouthfeel pleasant impression, and this The Application of Technology does not change the existing complete processing of cigarette, can improve the interior quality of cigarette.
Purpose of the present invention can realize by following technique measures:
Chinese toon leaf extraction extracted from petroleum ether Folium toonae sinensis medicinal extract of the present invention is to make by the following method: Folium toonae sinensis → petroleum ether extraction → solid-liquid separation → clarification filtration → distillation concentrates → Folium toonae sinensis medicinal extract.
In the present invention, the sherwood oil specification is a medical grade, and boiling point is 30-90 ℃; Folium toonae sinensis fresh flower/sherwood oil (KG/L) is 1: 2-1: 10, and extraction time is 60-360min.
Folium toonae sinensis medicinal extract of the present invention is joined in the cigarette shreds as spices, can increase fragrance, reduce the gas that stimulates, mixes, improve the mouthfeel pleasant impression.Folium toonae sinensis medicinal extract consumption among the present invention is the 0.01-0.1% of pipe tobacco weight; Its concrete addition means is as follows: be that 95% edible ethanol dilutes the Folium toonae sinensis essential oil by dehydrated alcohol or ethanol content earlier, add in the pipe tobacco by spray pattern; Described Folium toonae sinensis medicinal extract and dehydrated alcohol or ethanol content are that 95% edible ethanol is formulated by following weight ratio: wherein Folium toonae sinensis medicinal extract 0.1%～2.0%, and dehydrated alcohol or ethanol content are 95% edible ethanol 98.0%～99.9%.
Effect of the present invention and benefit are that Chinese toon leaf extraction extracted from petroleum ether can carry out under normal temperature condition, do not need heating, and extraction process is simple, and is easy and simple to handle, and adopt the medical grade sherwood oil can guarantee the residual safety standards that meets in the medicinal extract.After the natural Folium toonae sinensis medicinal extract that method of the present invention is extracted adds in the pipe tobacco by spray pattern, can increase cigarette flavor, reducing stimulates and assorted gas, improves the mouthfeel pleasant impression, for tobacco flavoring provides novel, a respond well natural perfume.This The Application of Technology does not change the existing complete processing of cigarette in addition, can improve the interior quality of cigarette.
Embodiment
To method afford further instruction of the present invention, but do not limit the present invention below by example.
Embodiment 1
With electronic balance weighing Folium toonae sinensis 200g, in the flask of packing into equably.Add 30-60 ℃ of sherwood oil 400ml, room temperature condition is immersion 60min down, separates, and filters, and concentrates distillation, gets medicinal extract 0.16g.
Get Folium toonae sinensis medicinal extract by 0.01% of pipe tobacco weight, after with dehydrated alcohol (perhaps ethanol content is 95% edible ethanol) Folium toonae sinensis medicinal extract dissolved dilution being 1.2% (weight ratio), add in the pipe tobacco and roll into cigarette by spray pattern, council's evaluation is thought through smokeing panel test: the perfuming of this product in flue-cured tobacco produces effect, can make smoke alcohol and, there is improvement fine and smooth aspect, and fragrance increases, and pleasant impression is comfortable.
Embodiment 2
With electronic balance weighing Folium toonae sinensis 200g, in the flask of packing into equably.Add 60-90 ℃ of sherwood oil 2000ml, room temperature condition is immersion 360min down, separates, and filters, and concentrates distillation, gets medicinal extract 0.24g.
Get Folium toonae sinensis medicinal extract by 0.1% of pipe tobacco weight, after with dehydrated alcohol (perhaps ethanol content is 95% edible ethanol) Folium toonae sinensis medicinal extract dissolved dilution being 1% (weight ratio), add in the pipe tobacco and roll into cigarette by spray pattern, council's evaluation is thought through smokeing panel test: the perfuming effect of this product in flue-cured tobacco is obvious, can make smoke alcohol and, exquisiteness, fragrance increases, and fragrance matter has raising, and pleasant impression is comparatively comfortable clean.
Claims (5)
1. Chinese toon leaf extraction extracted from petroleum ether, it is characterized in that: it is to make by the following method: Folium toonae sinensis → petroleum ether extraction → solid-liquid separation → clarification filtration → distillation concentrates → Folium toonae sinensis medicinal extract.
2. Folium toonae sinensis medicinal extract according to claim 1 is characterized in that: the sherwood oil specification is a medical grade, and boiling point is 30-90 ℃.
3. Folium toonae sinensis medicinal extract according to claim 1 is characterized in that: Folium toonae sinensis/sherwood oil (KG/L) is 1: 2-1: 10, and extraction time is 60-360min.
4. the application of Folium toonae sinensis medicinal extract according to claim 1 in perfuming cigarette is characterized in that: Folium toonae sinensis medicinal extract of the present invention is joined in the cigarette shreds as spices.
5. the application of Folium toonae sinensis medicinal extract according to claim 4 in perfuming cigarette is characterized in that: Folium toonae sinensis medicinal extract consumption is the 0.01-0.1% of pipe tobacco weight; Its concrete addition means is as follows: be that 95% edible ethanol dilutes the Folium toonae sinensis essential oil by dehydrated alcohol or ethanol content earlier, add in the pipe tobacco by spray pattern.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007101897175A CN101130713A (en) | 2007-09-29 | 2007-09-29 | Chinese toon leaf extraction extracted from petroleum ether and application of the same in perfuming cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007101897175A CN101130713A (en) | 2007-09-29 | 2007-09-29 | Chinese toon leaf extraction extracted from petroleum ether and application of the same in perfuming cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101130713A true CN101130713A (en) | 2008-02-27 |
Family
ID=39128119
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2007101897175A Pending CN101130713A (en) | 2007-09-29 | 2007-09-29 | Chinese toon leaf extraction extracted from petroleum ether and application of the same in perfuming cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101130713A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103461765A (en) * | 2013-08-31 | 2013-12-25 | 徐州绿之野生物食品有限公司 | Preparation method of Chinese toon crisp chips |
| CN104531352A (en) * | 2014-12-12 | 2015-04-22 | 柳州市京阳节能科技研发有限公司 | Technology for extracting essence from natural mallee leaves, little banian leaves and osmanthus tree leaves |
| CN112481033A (en) * | 2020-11-17 | 2021-03-12 | 阜阳师范大学 | Extraction method of cedrela sinensis essential oil |
-
2007
- 2007-09-29 CN CNA2007101897175A patent/CN101130713A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103461765A (en) * | 2013-08-31 | 2013-12-25 | 徐州绿之野生物食品有限公司 | Preparation method of Chinese toon crisp chips |
| CN104531352A (en) * | 2014-12-12 | 2015-04-22 | 柳州市京阳节能科技研发有限公司 | Technology for extracting essence from natural mallee leaves, little banian leaves and osmanthus tree leaves |
| CN112481033A (en) * | 2020-11-17 | 2021-03-12 | 阜阳师范大学 | Extraction method of cedrela sinensis essential oil |
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| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Open date: 20080227 |