CN102813278B - A kind of mixed type electronic cigarette tobacco liquid - Google Patents

A kind of mixed type electronic cigarette tobacco liquid Download PDF

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Publication number
CN102813278B
CN102813278B CN201210281706.0A CN201210281706A CN102813278B CN 102813278 B CN102813278 B CN 102813278B CN 201210281706 A CN201210281706 A CN 201210281706A CN 102813278 B CN102813278 B CN 102813278B
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China
Prior art keywords
tobacco
extracting solution
mixed type
electronic cigarette
type electronic
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CN201210281706.0A
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CN102813278A (en
Inventor
姚继徳
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Hengxin Yongji Technology Shenzhen Co Ltd
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Shenzhen Hangsen Star Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes

Abstract

The present invention provides a kind of mixed type electronic cigarette tobacco liquid.This mixed type electronic cigarette tobacco liquid, including the component of following quality proportioning:Zimbabwe's tobacco extract 3 30%, American Burley tobacco leaf extract 2 25%, Maryland tobacco extract 2 15%, Turkey Turkish tobaccos extracting solution 1 10%, Greece Turkish tobaccos extracting solution 1 10%, Baoshan, Yunnan Turkish tobaccos extracting solution 1 10%, Xinjiang cigarette extracting solution 1 10%, Nicotiana tabacum L. ketone 1,035 1 8%, tobacco alcohol 1,036 1 5%, tobacco essence 0.5 5%, natural nicotine 0.1 2.5%, edible glycerol 5 25%, distilled water 1 10%, edible ethanol 1 15%, balance of Propylene Glycol.According to the mixed type electronic cigarette tobacco liquid of the present invention, the mix of flavors tradition substitute of tobacco beneficial to health for meeting smoker's needs is provided, there are international mixed type style and features, the strong satisfaction of flue gas, inhale taste alcohol and coordinate naturally, possess the style and features and taste of mixed type Nicotiana tabacum L., harmful substance is few, healthy beneficial to smoker.

Description

A kind of mixed type electronic cigarette tobacco liquid
Technical field
A kind of the present invention relates to electronic cigarette, more particularly to mixed type electronic cigarette tobacco liquid.
Background technology
In recent years, electronic cigarette is widely recognized as and is achieved great development in the world, and people are to electronics Medicated cigarette generally has more science and objectively judgement, the electronic cigarette product progress of itself also accelerate and promote the industry to Optimum and healthy direction to develop.Electronic cigarette mainly includes smoking set and cigarette bullet, is mounted with tobacco juice, makes cigarette by smoking set in cigarette bullet Liquid mist and produce smoking effect, the larger material of traditional nicotinism can be excluded and have traditional smoking replacement effect Really.But, existing electronic cigarette tobacco liquid, or belonging to the taste that import does not meet Chinese smoker, can not or taste is too single Generally applicable, or being unfavorable for the health of smoker containing more harmful components in tobacco juice.
Content of the invention
The purpose of the present invention is to overcome the deficiencies in the prior art, there is provided a kind of mixed type electronic cigarette ree-oil.
For realizing that object above, the technical solution used in the present invention be:
A kind of flue-cured tobacco type electronic cigarette solution, including the component of following quality proportioning:Zimbabwe tobacco extract 3- 30%, American Burley tobacco leaf extract 2-25%, Maryland tobacco extract 2-15%, Turkey Turkish tobaccos extracting solution 1-10% are wished Cured Turkish tobaccos extracting solution 1-10%, Baoshan, Yunnan Turkish tobaccos extracting solution 1-10%, Xinjiang cigarette extracting solution 1-10%, Nicotiana tabacum L. ketone 1035 1-8%, 1036 1-5% of tobacco alcohol, tobacco essence 0.5-5%, natural nicotine 0.1-2.5%, edible glycerol 5-25%, distillation Water 1-10%, edible ethanol 1-15%, balance of Propylene Glycol.
In a kind of preferred technical scheme, including the component of following quality proportioning:Zimbabwe tobacco extract 5- 15%, American Burley tobacco leaf extract 15-25%, Maryland tobacco extract 10-15%, Turkey Turkish tobaccos extracting solution 2-5% are wished Cured Turkish tobaccos extracting solution 2-5%, Baoshan, Yunnan Turkish tobaccos extracting solution 2-5%, Xinjiang cigarette extracting solution 3-5%, Nicotiana tabacum L. ketone 10355- 8%, tobacco alcohol 10362-3%, tobacco essence 2%, natural nicotine 1-2%, edible glycerol 10-15%, distilled water 3-5%, edible ethanol 2-5%, balance of Propylene Glycol.
The purity of the natural nicotine is more than 98%.
The ethanol content of the edible ethanol is more than or equal to 95%.
The Propylene Glycol is the special Propylene Glycol of food flavor.
Beneficial effects of the present invention:The mix of flavors tradition substitute of tobacco beneficial to health for meeting smoker's needs is provided, There are international mixed type style and features, the strong satisfaction of flue gas to inhale taste alcohol and coordination naturally, the style for possessing mixed type Nicotiana tabacum L. are special Seek peace taste, harmful substance is few, healthy beneficial to smoker.
Specific embodiment
In the present invention, Zimbabwe's tobacco extract, American Burley tobacco leaf extract, Maryland tobacco extract, native ear Its Turkish tobaccos extracting solution, Greece's Turkish tobaccos extracting solution, Baoshan, Yunnan Turkish tobaccos extracting solution, Xinjiang cigarette extracting solution, Nicotiana tabacum L. ketone 1035 and the extraction manufacture method of tobacco alcohol 1036:The above-mentioned Nicotiana tabacum L. being aged naturally for 3 years is taken, according to Nicotiana tabacum L. and mixed solvent(Sweet Oil:Propylene Glycol:Ethanol:Water=1:2:3:4)1:10 ratio feeds intake, using conventional heating(Heating-up temperature 80-85 °C)Backflow is carried Taking technique is extracted in rustless steel container 6 hours, is filtered after being cooled to room temperature, and filtrate is said extracted liquid.Take more than 3 years Naturally the Yunnan Flue-cured Tobacco Nicotiana tabacum L. being aged(Moisture requirement 12.5%), sieve through 100 mesh sieve after crushing, add the stone of 10 times of weight Oily ether(Boiling range 60-90 °C)Heating and refluxing extraction 3 hours(80 ± 2 °C of Extracting temperature), cooled and filtered, filtering residue add 5 times Petroleum ether is extracted by above-mentioned technique and is filtered, and merges petroleum ether extract twice.Mixed petroleum ether extract is concentrated, is obtained oily The tobacco extract A of shape, will freeze 24 hours after dehydrated alcohol back dissolving of the extract A with 10 times(Subzero 10 degree)After took out Filtrate heating is concentrated to give extract B by filter.Extract B is respectively adopted on molecular distillation equipment entering for following process conditions Row molecular distillation:In 0.15Mpa, 175 °C carry out molecular distillation to extract B, and steaming thing is C, and residue is D;Residue D exists 0.10Mpa, 220 °C carry out molecular distillation, and steaming thing is E, and residue is F;In 0.08Mpa, 250 °C carry out molecular distillation to residue F, Steaming thing is G, and residue is H.Through analysis test, steaming thing C main component is natural nicotine, and content >=75% can be used for further Purification obtains more than 98.5% high-purity nicotine.Steaming thing E main component is nerol, linalool, phenethanol etc. rich in alcohols This mixture is named as tobacco alcohol 1036 by mixture, total alcohol content >=30%.Steaming thing G main component is ketone compounds This mixture is named as Nicotiana tabacum L. ketone 1035, wherein Megastigmatrienone content >=2%, damascenone content >=1.5%, oxygen by mixture Change isophorone content >=1%, composition of other contents more than 0.1% also has geranyl acetone, 2,3- diacetyl, damascone Solanone.
Example 1
The formula of mixed type electronic cigarette 1# tobacco juices is(Quality compares content):Zimbabwe's tobacco extract accounts for 15%, the U.S. Burley tobacco leaf extracting solution accounts for 20%, and Maryland tobacco extract accounts for 10%, and Turkey's Turkish tobaccos extracting solution accounts for 5%, and Greece's Turkish tobaccos are carried Take liquid and account for 5%, Baoshan, Yunnan Turkish tobaccos extracting solution accounts for 2%, and Xinjiang cigarette extracting solution accounts for 3%, and Nicotiana tabacum L. ketone 1035 accounts for 5%, tobacco alcohol 1036 account for 3%, and (the electronic cigarette ree-oil that develops used here as De Xin Bioisystech Co., Ltd of Yunnan Yuxi is special for tobacco essence Aromatising prods, product type YN001) 1% is accounted for, natural nicotine(Purity is more than 98%)2% is accounted for, edible glycerol accounts for 10%, and distilled water is accounted for 5%, edible ethanol(Content 95%)2% is accounted for, the special Propylene Glycol of balance of food flavor.Above-mentioned raw materials are according to fixed proportion and elder generation Mix after order is weighed afterwards, 30 minutes post packages of stirring take the supernatant after quiet 72 hours and obtain final product 1# tobacco juices in Brown Glass Brown glass bottles and jars only, Atomization in electronic cigarette device can be directly added on to suck.
Example 2
The formula of mixed type electronic cigarette 2# tobacco juices is(Quality compares content):Zimbabwe's tobacco extract accounts for 10%, the U.S. Burley tobacco leaf extracting solution accounts for 15%, and Maryland tobacco extract accounts for 10%, and Turkey's Turkish tobaccos extracting solution accounts for 2%, and Greece's Turkish tobaccos are carried Take liquid and account for 3%, Baoshan, Yunnan Turkish tobaccos extracting solution accounts for 5%, and Xinjiang cigarette extracting solution accounts for 5%, and Nicotiana tabacum L. ketone 1035 accounts for 5%, tobacco alcohol 1036 account for 3%, and (the electronic cigarette ree-oil that develops used here as De Xin Bioisystech Co., Ltd of Yunnan Yuxi is special for tobacco essence Aromatising prods, product type YN001) 2% is accounted for, natural nicotine(Purity is more than 98%)2% is accounted for, edible glycerol accounts for 15%, and distilled water is accounted for 3%, edible ethanol(Content 95%)5% is accounted for, the special Propylene Glycol of balance of food flavor.Above-mentioned raw materials are according to fixed proportion and elder generation Mix after order is weighed afterwards, 30 minutes post packages of stirring take the supernatant after quiet 72 hours and obtain final product 2# tobacco juices in Brown Glass Brown glass bottles and jars only, Atomization in electronic cigarette device can be directly added on to suck.
Example 3
The formula of mixed type electronic cigarette 3# tobacco juices is(Quality compares content):Zimbabwe's tobacco extract accounts for 5%, the U.S. Burley tobacco leaf extracting solution accounts for 25%, and Maryland tobacco extract accounts for 15%, and Turkey's Turkish tobaccos extracting solution accounts for 5%, and Greece's Turkish tobaccos are carried Take liquid and account for 2%, Baoshan, Yunnan Turkish tobaccos extracting solution accounts for 2%, and Xinjiang cigarette extracting solution accounts for 5%, and Nicotiana tabacum L. ketone 1035 accounts for 8%, tobacco alcohol 1036 account for 2%, and (the electronic cigarette ree-oil that develops used here as De Xin Bioisystech Co., Ltd of Yunnan Yuxi is special for tobacco essence Aromatising prods, product type YN001) 2% is accounted for, natural nicotine(Purity is more than 98%)1% is accounted for, edible glycerol accounts for 10%, and distilled water is accounted for 3%, edible ethanol(Content 95%)2% is accounted for, the special Propylene Glycol of balance of food flavor.Above-mentioned raw materials are according to fixed proportion and elder generation Mix after order is weighed afterwards, 30 minutes post packages of stirring take the supernatant after quiet 72 hours and obtain final product 3# tobacco juices in Brown Glass Brown glass bottles and jars only, Atomization in electronic cigarette device can be directly added on to suck.
Above content is further description made for the present invention with reference to specific preferred implementation, it is impossible to assert The present invention be embodied as be confined to these explanations.For general technical staff of the technical field of the invention, On the premise of without departing from present inventive concept, make specifically being altered or varied and belong to protection scope of the present invention.

Claims (5)

1. a kind of mixed type electronic cigarette tobacco liquid, it is characterised in that including the component of following quality proportioning:Zimbabwe Nicotiana tabacum L. carries Take liquid 3-30%, American Burley tobacco leaf extract 2-25%, Maryland tobacco extract 2-15%, Turkey's Turkish tobaccos extracting solution 1-10%, Greece Turkish tobaccos extracting solution 1-10%, Baoshan, Yunnan Turkish tobaccos extracting solution 1-10%, Xinjiang cigarette extracting solution 1- 10%, 1035 1-8% of Nicotiana tabacum L. ketone, 1036 1-5% of tobacco alcohol, tobacco essence 0.5-5%, natural nicotine 0.1-2.5% eat Glycerol 5-25%, distilled water 1-10%, edible ethanol 1-15%, balance of Propylene Glycol;Wherein, Nicotiana tabacum L. ketone 1035 is main component For the mixture of ketone compounds, Megastigmatrienone content >=2%, damascenone content >=1.5%, oxidation isophorone content >= 1%, composition of other contents more than 0.1% also has geranyl acetone, 2,3- diacetyl, damascone solanone;Wherein, Nicotiana tabacum L. The mixture that alcohol 1036 is main component for nerol, linalool, phenethanol etc. rich in alcohols, total alcohol content >=30%.
2. mixed type electronic cigarette tobacco liquid according to claim 1, it is characterised in that including the component of following quality proportioning: Zimbabwe tobacco extract 5-15%, American Burley tobacco leaf extract 15-25%, Maryland tobacco extract 10-15%, soil Ear its Turkish tobaccos extracting solution 2-5%, Greece Turkish tobaccos extracting solution 2-5%, Baoshan, Yunnan Turkish tobaccos extracting solution 2-5%, Xinjiang are fragrant Material cigarette extracting solution 3-5%, 1035 5-8% of Nicotiana tabacum L. ketone, 1036 2-3% of tobacco alcohol, tobacco essence 1-2%, natural nicotine 1- 2%, edible glycerol 10-15%, distilled water 3-5%, edible ethanol 2-5%, balance of Propylene Glycol.
3. mixed type electronic cigarette tobacco liquid according to claim 1 and 2, it is characterised in that:The purity of the natural nicotine It is more than 98%.
4. mixed type electronic cigarette tobacco liquid according to claim 1 and 2, it is characterised in that:The ethanol of the edible ethanol Content is more than or equal to 95%.
5. mixed type electronic cigarette tobacco liquid according to claim 1 and 2, it is characterised in that:The Propylene Glycol is that food is fragrant The special Propylene Glycol of essence.
CN201210281706.0A 2012-08-09 2012-08-09 A kind of mixed type electronic cigarette tobacco liquid Active CN102813278B (en)

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CN103070473A (en) * 2013-01-25 2013-05-01 红云红河烟草(集团)有限责任公司 Electronic cigarette tobacco juice prepared from faint scent tobacco leaves
CN103054172A (en) * 2013-01-25 2013-04-24 红云红河烟草(集团)有限责任公司 Electronic cigarette liquid prepared from strong-flavor tobacco
CN103070472A (en) * 2013-01-25 2013-05-01 红云红河烟草(集团)有限责任公司 Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette
CN103054171A (en) * 2013-01-25 2013-04-24 红云红河烟草(集团)有限责任公司 Electronic cigarette liquid prepared from flat-flavor tobacco
EP2991510B1 (en) * 2013-05-02 2019-10-16 JT International SA Vaporisable material
CN103610229A (en) * 2013-12-09 2014-03-05 李建伟 Nicotine liquid of electronic cigarette
CN103876273A (en) * 2014-03-12 2014-06-25 红塔烟草(集团)有限责任公司 Mixed type electronic cigarette tobacco juice and preparing method
CN104068469B (en) * 2014-06-25 2016-07-27 湖南中烟工业有限责任公司 A kind of electronic cigarette liquid with sootiness fragrance
CN104026730B (en) * 2014-07-01 2016-02-10 安徽中烟工业有限责任公司 A kind of burnt fragrant and sweet type tobacco juice for electronic smoke
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