CN104382226B - Preparation method of burley tobacco extract - Google Patents
Preparation method of burley tobacco extract Download PDFInfo
- Publication number
- CN104382226B CN104382226B CN201410631271.7A CN201410631271A CN104382226B CN 104382226 B CN104382226 B CN 104382226B CN 201410631271 A CN201410631271 A CN 201410631271A CN 104382226 B CN104382226 B CN 104382226B
- Authority
- CN
- China
- Prior art keywords
- burley tobacco
- extract
- burley tobaccos
- volatile oil
- burley
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 71
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 71
- 239000000284 extract Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000341 volatile oil Substances 0.000 claims abstract description 13
- 238000001914 filtration Methods 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000012141 concentrate Substances 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 5
- 238000010992 reflux Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- -1 and reflux Substances 0.000 claims description 3
- 238000000605 extraction Methods 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000001256 steam distillation Methods 0.000 claims description 3
- 235000019504 cigarettes Nutrition 0.000 abstract description 35
- 230000000694 effects Effects 0.000 abstract description 4
- 235000019441 ethanol Nutrition 0.000 abstract 2
- 239000000779 smoke Substances 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 230000001953 sensory effect Effects 0.000 abstract 1
- 230000000638 stimulation Effects 0.000 abstract 1
- 239000011285 coke tar Substances 0.000 description 10
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 9
- 239000003546 flue gas Substances 0.000 description 9
- 239000000523 sample Substances 0.000 description 8
- 239000003205 fragrance Substances 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 3
- 239000011269 tar Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 235000019506 cigar Nutrition 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Abstract
The invention relates to a preparation method of a burley tobacco extract. The preparation method comprises the following steps of adding water into burley tobacco according to the weight ratio of 1:12, and obtaining volatile oil A by adopting a water vapor distillation method; extracting and filtering the volatile oil, obtaining filter liquor B for standby, adding water into filter residues according to the weight ratio of 1:10 to backflow and extract for 2.0+/-0.1h, filtering while hot, and obtaining filter liquor C for standby, wherein the filter residues can be directly applied in paper-making process reconstituted tobacco production; merging the filter liquor B and C, concentrating to the density of 1.200+/-0.006g/cm<3> at the temperature of 30-45 DEG C, and obtaining the burley tobacco extract D; adding ethyl alcohol with the mass fraction of 95 percent into the burley tobacco extract D, then settling, filtering, vacuum concentrating the filter liquor to the density of 0.930+/-0.006g/cm<3>, and obtaining a burley tobacco concentrate E, wherein the weight of the ethyl alcohol is threes times that of the burley tobacco extract D; adding the burley tobacco volatile oil A into the burley tobacco concentrate E, and uniformly mixing to obtain the burley tobacco extract. The burley tobacco extract prepared by the invention has more obvious effects in stimulation reduction, aroma enhancement, smoke smoothness, smoke concentration increase and the like, the residual taste of cigarettes can be improved, and the low-tar cigarette sensory quality can be obviously improved.
Description
Technical field
The invention belongs to the preparation of tobacco aromatics using and applied technical field, in particular to a kind of system of burley tobaccos essence extract
Preparation Method.
Background technology
Burley tobaccos, Flos Carthami cigarette kind.It is mainly used as the raw material of blended type cigarette it can also be used to cigar, pipe tobacco and chewing tobacco.In vain
Rib cigarette moisture is higher, and blade is thin and light, organizational structure is loose and not coarse, elastic strong, Filling power height, absorbs fragrance performance
Well, nicotine and total nitrogen content are higher than flue-cured tobacco, and flue gas strength is big, and sugar content is low, has very strong absorbability.China mainly plants
Training kind has Hubei Province cigarette series, reaches white series etc..The burley tobaccos extract of burley tobaccos preparation, belongs to burley tobaccos tobacco aroma, can be effective
Supplement cigarette perfume, correct the suction taste of Nicotiana tabacum L. and mouthfeel, improve product quality.But burley tobaccos extract has typical burley tobaccos
Fragrance, is generally used for blended type cigarette charging, is not suitable for flue-cured tobacco and uses.
And the concern further to smoking and health problem along with consumer, low-coke tar cigarette become Medicated cigarette development
Inexorable trend, and while tar content reduces, low-coke tar cigarette fragrance texture dies down, cigarette flavor amount diminishes, and gratification is big
The demand gap having been formed since big reduction, with long term consumer is larger.How under the front topic ensureing reducing cigarette tar and reducing, lift low Jiao
The fragrance of oily Medicated cigarette and gratification are technical problems urgently to be resolved hurrily.For this reason, it is contemplated that preparation one kind can be applicable to
The burley tobaccos essence of low tar flue-cured tobacco is extracted, for increasing fragrance texture and the gratification of Medicated cigarette, the inherence of lifting low-coke tar cigarette
Quality.
Content of the invention
It is an object of the invention to provide a kind of preparation method of burley tobaccos essence extract, gained burley tobaccos extract is added
It is used for improving the organoleptic quality of Medicated cigarette in low-coke tar cigarette.
Technical scheme：A kind of preparation method of burley tobaccos essence extract, comprises the following steps：
(1) burley tobaccos are taken, by weight 1:12 add water, and using extraction by steam distillation volatile oil, obtain burley tobaccos and wave
Hair oil A.
(2) filter after extracting volatile oil, liquor B is standby, filtering residue by weight 1:10 add water reflux, extract, reflux, extract,
2.0 ± 0.1h, filtered while hot, liquor C is standby, and filtering residue can be directly used for papermaking-method reconstituted tobaccos and produces.
(3) it is concentrated into density 1.200 ± 0.006g/cm under the conditions of 30～45 DEG C after liquor B and C merging3, obtain white rib
Tobacco extract D.
(4) add in described burley tobaccos extract D its weight 3.0 times amount mass fraction be 95% ethanol after carry out
Sedimentation, filtration, filtrate reduced in volume to density is 0.930 ± 0.006g/cm3, obtain burley tobaccos concentrate E.
(5) add burley tobaccos volatile oil A in described burley tobaccos concentrate E, mix homogeneously obtains burley tobaccos essence and extracts.
Gained burley tobaccos extract is applied in low-coke tar cigarette leaf group as cigaret additive, the weight being added accounts for
The 0.05～0.08% of cigarette leaf group weight.
The present invention is simple and practical, and operation is implemented easily, and obtained burley tobaccos extract can be coordinated well with Medicated cigarette, carries
The aesthetic quality of high Medicated cigarette, carries out display after contrast is smoked panel test through provincial judging panel with control sample：Burley tobaccos extract has in Medicated cigarette
Play the role of to drop thorn, flavouring, increase flue gas concentration and fine and smooth flue gas.
Specific embodiment：
With reference to specific embodiment, the present invention is further detailed explanation.
Embodiment 1：
A kind of preparation method of burley tobaccos essence extract, comprises the following steps：
(1) burley tobaccos are taken, by weight 1:12 add water, and using extraction by steam distillation volatile oil, obtain burley tobaccos and wave
Hair oil A.
(2) filter after extracting volatile oil, liquor B is standby, filtering residue by weight 1:10 add water reflux, extract, reflux, extract,
2.0h, filtered while hot, liquor C is standby, and filtering residue can be directly used for papermaking-method reconstituted tobaccos and produces.
(3) it is concentrated into density 1.202g/cm under the conditions of 42 DEG C after liquor B and C merging3, obtain burley tobaccos extract D.
(4) add in described burley tobaccos extract D its weight 3.0 times amount mass fraction be 95% ethanol after carry out
Sedimentation, filtration, filtrate reduced in volume to density is 0.926g/cm3, obtain burley tobaccos concentrate E.
(5) add burley tobaccos volatile oil A in described burley tobaccos concentrate E, mix homogeneously obtains burley tobaccos essence and extracts.
Embodiment 2：
Weigh burley tobaccos essence to extract by the 0.06% low-coke tar cigarette tobacco leaf formulation (6mg/ props up) being added to 10 yuan of prices, adjust
Whole moisture in cut tobacco be 12.5% about, roll into cigarette, put into temperature be 22 DEG C ± 1, relative humidity be 60% ± 2% constant temperature
More than constant humidity cabinet inner equilibrium 48h as the sample 1 of the present invention, please the group of smokeing panel test be smoked panel test.Under similarity condition, use same cigarette
Silk spray plus identical deal distilled water, roll into cigarette as the sample 2 of blank.Smoking result asks for an interview table 1 below.
Table 1 sample 1 and sample 2 are smoked panel test contrast
Table 1 result shows, gained burley tobaccos essence of the present invention is extracted to be added in 10 yuan of low-coke tar cigarettes to be had fall thorn, increases
Fragrant, fine and smooth flue gas and the effect increasing flue gas concentration.
Embodiment 3：
Weigh burley tobaccos essence to extract by the 0.06% low-coke tar cigarette tobacco leaf formulation (6mg/ props up) being added to 40 yuan of prices, adjust
Whole moisture in cut tobacco be 12.5% about, roll into cigarette, put into temperature be 22 DEG C ± 1, relative humidity be 60% ± 2% constant temperature
More than constant humidity cabinet inner equilibrium 48h as the sample 3 of the present invention, please the group of smokeing panel test be smoked panel test.Under similarity condition, use same cigarette
Silk spray plus identical deal distilled water, roll into cigarette as the sample 4 of blank.Smoking result asks for an interview table 2 below.
Table 2 sample 3 and sample 4 are smoked panel test contrast
Table 2 result shows, gained burley tobaccos essence of the present invention is extracted to be added in 40 yuan of low-coke tar cigarettes has fall thorn, exquisiteness
Flue gas, the effect improving pleasant impression and increasing flue gas concentration.
Practical application shows：Gained burley tobaccos essence of the present invention is extracted in fall thorn, flavouring, fine and smooth flue gas and increases flue gas concentration
Etc. aspect effect become apparent from, and the pleasant impression of Medicated cigarette can be improved, can significantly improve low-coke tar cigarette aesthetic quality.
Claims (1)
1. a kind of preparation method of burley tobaccos essence extract, comprises the following steps：
(1) burley tobaccos are taken, by weight 1:12 add water, and using extraction by steam distillation volatile oil, obtain burley tobaccos volatile oil
A；
(2) filter after extracting volatile oil, liquor B is standby, filtering residue by weight 1:10 add water reflux, extract, and reflux, extract, 2.0 ±
0.1h, filtered while hot, liquor C is standby, and filtering residue is directly used in papermaking-method reconstituted tobaccos and produces；
(3) it is concentrated into density 1.200 ± 0.006g/cm under the conditions of 30～45 DEG C after liquor B and C merging3, obtain burley tobaccos and carry
Take thing D；
(4) add in described burley tobaccos extract D its weight 3.0 times amount mass fraction be 95% ethanol after sunk
Fall, filtration, filtrate reduced in volume to density is 0.930 ± 0.006g/cm3, obtain burley tobaccos concentrate E；
(5) add burley tobaccos volatile oil A in described burley tobaccos concentrate E, mix homogeneously obtains burley tobaccos essence extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410631271.7A CN104382226B (en) | 2014-11-11 | 2014-11-11 | Preparation method of burley tobacco extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410631271.7A CN104382226B (en) | 2014-11-11 | 2014-11-11 | Preparation method of burley tobacco extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104382226A CN104382226A (en) | 2015-03-04 |
| CN104382226B true CN104382226B (en) | 2017-02-15 |
Family
ID=52600274
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410631271.7A Active CN104382226B (en) | 2014-11-11 | 2014-11-11 | Preparation method of burley tobacco extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104382226B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104905399A (en) * | 2015-06-02 | 2015-09-16 | 湖北中烟工业有限责任公司 | Preparation method of 50% aromatic tobacco extract |
| CN108451003B (en) * | 2018-01-30 | 2020-08-07 | 湖北中烟工业有限责任公司 | Method for preparing burley tobacco reactant by using hydrolase and application |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5381698A (en) * | 1976-12-28 | 1978-07-19 | Japan Tobacco Inc | Tobacco having improved taste |
| JPS60196179A (en) * | 1984-03-16 | 1985-10-04 | 日本たばこ産業株式会社 | Production of tobacco extract |
| CN1025935C (en) * | 1992-03-18 | 1994-09-21 | 湖北省建始县白肋烟复烤厂 | Bailei tobacco extract and producing technology and using method thereof |
| CN1141044C (en) * | 2001-02-26 | 2004-03-10 | 王振锟 | Process and equipment for rectifying tobacco by supercritical multi-element fluid extraction |
| CN100415126C (en) * | 2006-07-24 | 2008-09-03 | 宋光泉 | Method for extracting tobacco essence perfume |
| CN101544927B (en) * | 2008-03-28 | 2011-12-07 | 湖北中烟工业有限责任公司 | Patchouli compound extract and application thereof in cigarette |
| CN101602982A (en) * | 2008-06-11 | 2009-12-16 | 湖北中烟工业有限责任公司 | The step-by-step extracting method of purple perilla and extract obtained application in cigarette |
| CN101731748B (en) * | 2008-11-05 | 2012-07-18 | 湖北中烟工业有限责任公司 | Method for extracting Dendranthema indium leaves and application of extractive thereof in cigarettes |
| CN102823937B (en) * | 2012-08-16 | 2014-12-10 | 湖北中烟工业有限责任公司 | Extracting method of submerged fermentation mycelium extractive of lepista nuda and application thereof in cigarettes |
| CN103385536B (en) * | 2013-07-31 | 2015-09-16 | 浙江中烟工业有限责任公司 | Leaching aqueous solution of a kind of burley tobaccos and its preparation method and application |
-
2014
- 2014-11-11 CN CN201410631271.7A patent/CN104382226B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN104382226A (en) | 2015-03-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102813278B (en) | A kind of mixed type electronic cigarette tobacco liquid | |
| CN104489901B (en) | One grows tobacco taste tobacco juice for electronic smoke | |
| CN103919274B (en) | A kind of electronic cigarette atomizing liquid | |
| CN102559388A (en) | Essential oil of tobaccos as well as preparation method and application thereof to cigarettes | |
| CN102161935A (en) | Endogenous perfume from tobacco as well as preparation method and application thereof | |
| CN106753793B (en) | Preparation method of tea absolute for cigarettes | |
| CN105533793A (en) | Preparation method for tobacco extract of dark sun-cured tobacco | |
| CN103783660A (en) | Supercritical extraction method of aroma substances in tobacco leaf fragments and application of aroma substances | |
| CN105686065A (en) | Tea tobacco and making method thereof | |
| JP7182805B2 (en) | HNB herb aroma bomb flakes, filaments, filament cuts, recipes and production methods for herb aroma bombs | |
| CN108998241B (en) | Cured flue-cured tobacco flavor essence for heating non-combustible cigarettes and preparation method and application thereof | |
| CN109897729B (en) | Preparation method and application of agilawood type tobacco essence | |
| CN104382226B (en) | Preparation method of burley tobacco extract | |
| CN105146740B (en) | The preparation method of a kind of cigarette raisin extract and the application in Medicated cigarette thereof | |
| CN103230093B (en) | Yellow sun-cured tobacco and preparation method and low tar cigarette | |
| CN105394805B (en) | Method for enabling carbon dioxide expanded tobacco to highlight sweet aroma style | |
| CN108991589B (en) | Essence for reducing thorn and covering impurities in non-burning tobacco after heating and preparation method and application thereof | |
| CN106148011A (en) | The preparation method of a kind of cigarette radix valerianae extract and the application in Medicated cigarette thereof | |
| CN103393214B (en) | Aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract and preparation method and application of aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract | |
| CN101138435A (en) | Additive agent for natural polypropylene filter tip cigarette and method of producing the same | |
| CN105747271B (en) | A kind of preparation method of low albumen tobacco extract for novel tobacco | |
| CN104531359A (en) | Preparation method of black tea extractive and application thereof | |
| CN107361398A (en) | A kind of tea extraction in May and preparation method thereof and the application in cigarette | |
| CN109259292B (en) | Tobacco baked fragrant reconstituted tobacco and preparation method thereof | |
| CN108165370A (en) | A kind of fragrance-enhancing tobacco agent containing sandalwood oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |