CN104382226A - Preparation method of burley tobacco extract - Google Patents
Preparation method of burley tobacco extract Download PDFInfo
- Publication number
- CN104382226A CN104382226A CN201410631271.7A CN201410631271A CN104382226A CN 104382226 A CN104382226 A CN 104382226A CN 201410631271 A CN201410631271 A CN 201410631271A CN 104382226 A CN104382226 A CN 104382226A
- Authority
- CN
- China
- Prior art keywords
- burley tobacco
- extract
- burley tobaccos
- volatile oil
- burley
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 75
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 74
- 239000000284 extract Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 239000000341 volatile oil Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000012141 concentrate Substances 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims abstract description 5
- 238000000605 extraction Methods 0.000 claims description 11
- 238000010992 reflux Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000004062 sedimentation Methods 0.000 claims description 3
- 238000001256 steam distillation Methods 0.000 claims description 3
- 235000019504 cigarettes Nutrition 0.000 abstract description 33
- 230000000694 effects Effects 0.000 abstract description 5
- 239000000779 smoke Substances 0.000 abstract description 4
- 235000019441 ethanol Nutrition 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 230000001953 sensory effect Effects 0.000 abstract 1
- 230000000638 stimulation Effects 0.000 abstract 1
- 239000011285 coke tar Substances 0.000 description 11
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 9
- 239000003546 flue gas Substances 0.000 description 9
- 239000000523 sample Substances 0.000 description 8
- 239000003205 fragrance Substances 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 3
- 239000011269 tar Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 244000020518 Carthamus tinctorius Species 0.000 description 1
- 235000003255 Carthamus tinctorius Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 235000019506 cigar Nutrition 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to a preparation method of a burley tobacco extract. The preparation method comprises the following steps of adding water into burley tobacco according to the weight ratio of 1:12, and obtaining volatile oil A by adopting a water vapor distillation method; extracting and filtering the volatile oil, obtaining filter liquor B for standby, adding water into filter residues according to the weight ratio of 1:10 to backflow and extract for 2.0+/-0.1h, filtering while hot, and obtaining filter liquor C for standby, wherein the filter residues can be directly applied in paper-making process reconstituted tobacco production; merging the filter liquor B and C, concentrating to the density of 1.200+/-0.006g/cm<3> at the temperature of 30-45 DEG C, and obtaining the burley tobacco extract D; adding ethyl alcohol with the mass fraction of 95 percent into the burley tobacco extract D, then settling, filtering, vacuum concentrating the filter liquor to the density of 0.930+/-0.006g/cm<3>, and obtaining a burley tobacco concentrate E, wherein the weight of the ethyl alcohol is threes times that of the burley tobacco extract D; adding the burley tobacco volatile oil A into the burley tobacco concentrate E, and uniformly mixing to obtain the burley tobacco extract. The burley tobacco extract prepared by the invention has more obvious effects in stimulation reduction, aroma enhancement, smoke smoothness, smoke concentration increase and the like, the residual taste of cigarettes can be improved, and the low-tar cigarette sensory quality can be obviously improved.
Description
Technical field
The invention belongs to the preparations and applicatio technical field of tobacco aromatics, refer to a kind of preparation method of burley tobaccos essence extract particularly.
Background technology
Burley tobaccos, safflower cigarette kind.The main raw material being used as blended type cigarette, also can be used for cigar, pipe tobacco and chewing tobacco.Burley tobaccos moisture is higher, and blade is thin and light, institutional framework loose and not coarse, and elasticity is strong, and Filling power is high, absorbs fragrance performance good, nicotine and total nitrogen content higher than flue-cured tobacco, flue gas strength is large, and sugar content is low, has very strong absorbability.China's Main Cultivars has Hubei Province cigarette series, reaches white series etc.Burley tobaccos extract prepared by burley tobaccos, belongs to burley tobaccos tobacco aroma, can effectively augment cigarette perfume (or spice), corrects suction taste and the mouthfeel of tobacco, improves the quality of products.But burley tobaccos extract has typical burley tobaccos fragrance, be generally applied to blended type cigarette and feed in raw material, be not suitable for flue-cured tobacco and use.
And along with the further concern of consumer to smoking and health problem, low-coke tar cigarette has become the inexorable trend of cigarette development, and while tar content reduces, low-coke tar cigarette fragrance texture dies down, cigarette flavor amount diminishes, satisfaction reduces greatly, larger with the demand gap formed since long term consumer.Under how inscribing before guarantee reducing cigarette tar and reducing, the fragrance of lifting low-coke tar cigarette and satisfaction are technical problems urgently to be resolved hurrily.For this reason, the present invention is intended to prepare a kind of burley tobaccos essence that can be applicable to low tar flue-cured tobacco and extracts, and for increasing fragrance texture and the satisfaction of cigarette, promotes the inherent quality of low-coke tar cigarette.
Summary of the invention
The object of this invention is to provide a kind of preparation method of burley tobaccos essence extract, add in low-coke tar cigarette gained burley tobaccos extract to be used for improving cigarette organoleptic quality.
Technical scheme of the present invention: a kind of preparation method of burley tobaccos essence extract, comprises the following steps:
(1) get burley tobaccos, add water by weight 1:12, adopt extraction by steam distillation volatile oil, obtain burley tobaccos volatile oil A.
(2) extract after volatile oil and filter, liquor B is for subsequent use, and filter residue to add water refluxing extraction by weight 1:10, and refluxing extraction 2.0 ± 0.1h, filters while hot, and liquor C is for subsequent use, and filter residue can be directly used in papermaking-method reconstituted tobaccos and produce.
(3) liquor B and C are concentrated into density 1.200 ± 0.006g/cm after merging under 30 ~ 45 DEG C of conditions
3, obtain burley tobaccos extract D.
(4) mass fraction adding its weight 3.0 times amount in described burley tobaccos extract D carries out sedimentation, filtration after being the ethanol of 95%, and filtrate reduced in volume to density is 0.930 ± 0.006g/cm
3, obtain burley tobaccos concentrate E.
(5) in described burley tobaccos concentrate E, add burley tobaccos volatile oil A, mix and namely obtain the extraction of burley tobaccos essence.
Be applied in low-coke tar cigarette leaf group as cigarette additive by gained burley tobaccos extract, the weight added accounts for 0.05 ~ 0.08% of cigarette leaf group weight.
The present invention is simple and practical, operation is implemented easily, the burley tobaccos extract obtained well can be coordinated with cigarette, improve the aesthetic quality of cigarette, carry out showing after contrast is smoked panel test through provincial judging panel and control sample: burley tobaccos extract have in cigarette fall sting, the effect of flavouring, increase flue gas concentration and fine and smooth flue gas.
Detailed description of the invention:
Below in conjunction with specific embodiment, the present invention is further detailed explanation.
Embodiment 1:
A preparation method for burley tobaccos essence extract, comprises the following steps:
(1) get burley tobaccos, add water by weight 1:12, adopt extraction by steam distillation volatile oil, obtain burley tobaccos volatile oil A.
(2) extract after volatile oil and filter, liquor B is for subsequent use, and filter residue to add water refluxing extraction by weight 1:10, and refluxing extraction 2.0h, filters while hot, and liquor C is for subsequent use, and filter residue can be directly used in papermaking-method reconstituted tobaccos and produce.
(3) liquor B and C are concentrated into density 1.202g/cm after merging under 42 DEG C of conditions
3, obtain burley tobaccos extract D.
(4) mass fraction adding its weight 3.0 times amount in described burley tobaccos extract D carries out sedimentation, filtration after being the ethanol of 95%, and filtrate reduced in volume to density is 0.926g/cm
3, obtain burley tobaccos concentrate E.
(5) in described burley tobaccos concentrate E, add burley tobaccos volatile oil A, mix and namely obtain the extraction of burley tobaccos essence.
Embodiment 2:
Take burley tobaccos essence and extract the low-coke tar cigarette tobacco leaf formulation (6mg/ props up) joining 10 yuan of prices by 0.06%, adjustment moisture in cut tobacco is about 12.5%, roll into cigarette, put into that temperature is 22 DEG C ± 1, relative humidity be more than the climatic chamber inner equilibrium 48h of 60% ± 2% as sample 1 of the present invention, please the group of smokeing panel test smoke panel test.Under similarity condition, add identical deal distilled water with same pipe tobacco spray, roll into the sample 2 of cigarette as blank.Smoking result asks for an interview following table 1.
Table 1 sample 1 and sample 2 are smoked panel test contrast
Table 1 result shows, and gained burley tobaccos essence of the present invention extracts the effect joining in 10 yuan of low-coke tar cigarettes and have and fall thorn, flavouring, fine and smooth flue gas and increase flue gas concentration.
Embodiment 3:
Take burley tobaccos essence and extract the low-coke tar cigarette tobacco leaf formulation (6mg/ props up) joining 40 yuan of prices by 0.06%, adjustment moisture in cut tobacco is about 12.5%, roll into cigarette, put into that temperature is 22 DEG C ± 1, relative humidity be more than the climatic chamber inner equilibrium 48h of 60% ± 2% as sample 3 of the present invention, please the group of smokeing panel test smoke panel test.Under similarity condition, add identical deal distilled water with same pipe tobacco spray, roll into the sample 4 of cigarette as blank.Smoking result asks for an interview following table 2.
Table 2 sample 3 and sample 4 are smoked panel test contrast
Table 2 result shows, and gained burley tobaccos of the present invention essence is extracted to join in 40 yuan of low-coke tar cigarettes to have and fallen thorn, fine and smooth flue gas, improves the effect of pleasant impression and increase flue gas concentration.
Practical application shows: gained burley tobaccos essence of the present invention is extracted in falls thorn, flavouring, fine and smooth flue gas and increases the aspect effects such as flue gas concentration more obviously, and can improve the pleasant impression of cigarette, can improve low-coke tar cigarette aesthetic quality significantly.
Claims (1)
1. a preparation method for burley tobaccos essence extract, comprises the following steps:
(1) get burley tobaccos, add water by weight 1:12, adopt extraction by steam distillation volatile oil, obtain burley tobaccos volatile oil A;
(2) extract after volatile oil and filter, liquor B is for subsequent use, and filter residue to add water refluxing extraction by weight 1:10, and refluxing extraction 2.0 ± 0.1h, filters while hot, and liquor C is for subsequent use, and filter residue is directly used in papermaking-method reconstituted tobaccos and produces;
(3) liquor B and C are concentrated into density 1.200 ± 0.006g/cm after merging under 30 ~ 45 DEG C of conditions
3, obtain burley tobaccos extract D;
(4) mass fraction adding its weight 3.0 times amount in described burley tobaccos extract D carries out sedimentation, filtration after being the ethanol of 95%, and filtrate reduced in volume to density is 0.930 ± 0.006g/cm
3, obtain burley tobaccos concentrate E;
(5) in described burley tobaccos concentrate E, add burley tobaccos volatile oil A, mix and namely obtain burley tobaccos essence extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410631271.7A CN104382226B (en) | 2014-11-11 | 2014-11-11 | Preparation method of burley tobacco extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410631271.7A CN104382226B (en) | 2014-11-11 | 2014-11-11 | Preparation method of burley tobacco extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104382226A true CN104382226A (en) | 2015-03-04 |
| CN104382226B CN104382226B (en) | 2017-02-15 |
Family
ID=52600274
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410631271.7A Active CN104382226B (en) | 2014-11-11 | 2014-11-11 | Preparation method of burley tobacco extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104382226B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104905399A (en) * | 2015-06-02 | 2015-09-16 | 湖北中烟工业有限责任公司 | Preparation method of 50% aromatic tobacco extract |
| CN108451003A (en) * | 2018-01-30 | 2018-08-28 | 湖北中烟工业有限责任公司 | The methods and applications of burley tobaccos reactant are prepared using hydrolase |
Citations (10)
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|---|---|---|---|---|
| JPS5381698A (en) * | 1976-12-28 | 1978-07-19 | Japan Tobacco Inc | Tobacco having improved taste |
| JPS60196179A (en) * | 1984-03-16 | 1985-10-04 | 日本たばこ産業株式会社 | Production of tobacco extract |
| CN1064793A (en) * | 1992-03-18 | 1992-09-30 | 湖北省建始县白肋烟复烤厂 | Bailei tobacco extract and production technology thereof and using method |
| CN1302568A (en) * | 2001-02-26 | 2001-07-11 | 王振锟 | Process and equipment for rectifying tobacco by supercritical multi-element fluid extraction |
| CN1899141A (en) * | 2006-07-24 | 2007-01-24 | 宋光泉 | Method for extracting tobacco essence perfume |
| CN101544927A (en) * | 2008-03-28 | 2009-09-30 | 湖北中烟工业有限责任公司 | Patchouli compound extract and application thereof in cigarette |
| CN101602982A (en) * | 2008-06-11 | 2009-12-16 | 湖北中烟工业有限责任公司 | The step-by-step extracting method of purple perilla and extract obtained application in cigarette |
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| CN102823937A (en) * | 2012-08-16 | 2012-12-19 | 湖北中烟工业有限责任公司 | Extracting method of submerged fermentation mycelium extractive of lepista nuda and application thereof in cigarettes |
| CN103385536A (en) * | 2013-07-31 | 2013-11-13 | 浙江中烟工业有限责任公司 | Leaching aqueous solution of burley tobacco as well as preparation method and application thereof |
-
2014
- 2014-11-11 CN CN201410631271.7A patent/CN104382226B/en active Active
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5381698A (en) * | 1976-12-28 | 1978-07-19 | Japan Tobacco Inc | Tobacco having improved taste |
| JPS60196179A (en) * | 1984-03-16 | 1985-10-04 | 日本たばこ産業株式会社 | Production of tobacco extract |
| CN1064793A (en) * | 1992-03-18 | 1992-09-30 | 湖北省建始县白肋烟复烤厂 | Bailei tobacco extract and production technology thereof and using method |
| CN1302568A (en) * | 2001-02-26 | 2001-07-11 | 王振锟 | Process and equipment for rectifying tobacco by supercritical multi-element fluid extraction |
| CN1899141A (en) * | 2006-07-24 | 2007-01-24 | 宋光泉 | Method for extracting tobacco essence perfume |
| CN101544927A (en) * | 2008-03-28 | 2009-09-30 | 湖北中烟工业有限责任公司 | Patchouli compound extract and application thereof in cigarette |
| CN101602982A (en) * | 2008-06-11 | 2009-12-16 | 湖北中烟工业有限责任公司 | The step-by-step extracting method of purple perilla and extract obtained application in cigarette |
| CN101731748A (en) * | 2008-11-05 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for extracting Dendranthema indium leaves and application of extractive thereof in cigarettes |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104905399A (en) * | 2015-06-02 | 2015-09-16 | 湖北中烟工业有限责任公司 | Preparation method of 50% aromatic tobacco extract |
| CN108451003A (en) * | 2018-01-30 | 2018-08-28 | 湖北中烟工业有限责任公司 | The methods and applications of burley tobaccos reactant are prepared using hydrolase |
| CN108451003B (en) * | 2018-01-30 | 2020-08-07 | 湖北中烟工业有限责任公司 | Method for preparing burley tobacco reactant by using hydrolase and application |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104382226B (en) | 2017-02-15 |
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