CN104531356B - Sweet fragrant additive and the electronic cigarette liquid with sweet perfume - Google Patents
Sweet fragrant additive and the electronic cigarette liquid with sweet perfume Download PDFInfo
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- CN104531356B CN104531356B CN201510026003.7A CN201510026003A CN104531356B CN 104531356 B CN104531356 B CN 104531356B CN 201510026003 A CN201510026003 A CN 201510026003A CN 104531356 B CN104531356 B CN 104531356B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses the sweet fragrant additive of one kind, it is mixed by orris oil by weight or 1~5 part of 2~5 parts of orris absolute, attar of rose or rose absolute, 1~5 part of geranium oil, 1~5 part of citronella oil, 1~2 part of cassie concrete, 1~3 part of osmanthus concrete, 75~93 parts of solvent, the invention also discloses a kind of with sweet fragrant electronic cigarette liquid, it is made up of sweet fragrant additive, tobacco extract, the mixed alkoxide solution of water/glycol/propane three, and the sweet fragrant additive is 1~10 with the mass ratio of the mixed alkoxide solution of water/glycol/propane three：1000, the tobacco extract is 5~20 with the mass ratio of the mixed alkoxide solution of water/glycol/propane three:1000000.Electronic cigarette liquid prepared by the present invention has sweet fragrant characteristic flavor on basis, enriches the suction local flavor of electronic cigarette, and at aspects such as fragrance, mouthfeels, tool is greatly improved compared with existing product, can substantially increase the satisfaction of smoker.
Description
Technical field
Embodiments of the present invention are related to Field of Tobacco, more specifically, embodiments of the present invention are related to a kind of sweet perfume (or spice)
Additive and a kind of electronic cigarette liquid with sweet perfume.
Background technology
Electronic cigarette is a kind of novel tobacco product, and it is typically made up of elements such as lithium battery, atomizer, cigarette bullets, by mist
Change device and nicotine solution is atomized into steam state, consumer meets psychological need by suction.Compared with traditional cigarette, electronic cigarette is not
It is smaller to smoker's actual bodily harm containing harmful substances such as tar, carbon monoxide；In addition, the nicotine of electronic cigarette is formed by atomization
Aerosol, be rapidly diluted in atmosphere, reduce to people around produce harm risk.Electronic cigarette as cigarette replacement
Product, obtain market accreditation in the world, and sales volume is presented ascendant trend year by year.
Tobacco juice for electronic smoke is the key factor for influenceing suction quality.Electronic cigarette by several generations development, although shape, hand
The perceptual image cigarette such as sense, smog, but tobacco juice for these electronic cigarettes remains some shortcomings.Compared with traditional cigarette, electronic cigarette
The smog that liquid is produced has a certain distance in fragrance, mouthfeel with traditional cigarette.Smoker generally feels these electronic cigarettes
Fragrance and mouthfeel do not reach its psychological need, and wherein fragrance is poor, single these problems of mouthfeel will largely effect on the strong of electronic cigarette
Health sustainable development.Different from traditional cigarette, electronic cigarette makes consumer obtain physiology and psychological full without tobacco leaf burning
Foot sense, although the murder by poisoning of brought harmful components of being burnt by tobacco leaf is reduced in aspiration procedure, but decrease simultaneously by cigarette
By the intake for chemically and physically changing the various flavor components for being obtained of a series of complex, therefore electronics in leaf combustion process
In cigarette aspiration procedure generally existing fragrance it is poor, it is single the problems such as.Electronic cigarette is obtained by heating tobacco juice as smoking
" smog " feel, it is basic there is no new chemical change in aspiration procedure by electronic cigarette liquid its chemical composition allocated
(flavor component meeting thermal cracking during cigarette burning), can be very good to be transferred in the smog of electronic cigarette, by electronic cigarette liquid
Allotment perfuming be to solve fragrance is poor, taste is single effective way in electronic cigarette aspiration procedure.
The content of the invention
Instant invention overcomes prior art electronic cigarette liquid the aspects such as fragrance, mouthfeel deficiency, there is provided a kind of sweet perfume (or spice)
Additive and a kind of implementation method with sweet fragrant electronic cigarette liquid, the suction local flavor of electronic cigarette can be enriched with expectation, full
The demand of the foot difference consumer group.
To solve above-mentioned technical problem, one embodiment of the present invention uses following technical scheme：
A kind of sweet fragrant additive, it is mixed by following components by weight：
Orris oil or 1~5 part of 2~5 parts of orris absolute, attar of rose or rose absolute, 1~5 part of geranium oil, citronella oil 1~5
Part, 1~2 part of cassie concrete, 1~3 part of osmanthus concrete, 75~93 parts of solvent.
The main component of orris oil or orris absolute be α-irone and β-irone, irisone, benzylalcohol, geraniol,
Linalool, benzaldehyde, furfural, acetophenone, eugenol, benzoic acid；Fragrant and sweet like gillyflower with sweet perfume (or spice), fragrance is gentle.
The main component of attar of rose or rose absolute is citronellol, geraniol, linalool, benzyl carbinol, fanesol, benzyl
Alcohol, citral, irisone, eugenol, citronellyl acetate, neryl acetate；With fragrant and sweet, fragrance alcohol and.
The main component of geranium oil is rhodinol, geraniol, linalool, terpinol, menthol, leaf-alcohol, citral, different thin
Lotus ketone, laurene, phellandrene, firpene；With sweet note, micro- green grass or young crops, there are rose and leafiness breath, fragrance stabilization is lasting.
The main component of citronella oil be citronellal, citronellol, geraniol, citral, geranyl acetate, citronellyl acetate,
Citronellic acid citronellyl acrylate；Micro- to have the fragrant and sweet of geraniol with the green grass perfume based on citronellal, fragrance is strong and lasting.
The main component fanesol of cassie concrete, geraniol, aromatic alcohol, benzylalcohol, terpinol, anisaldehyde, benzaldehyde,
Benzoic acid, can substantially increase fragrant and sweet.
Osmanthus concrete：Irisone, damascone, linalool, nerol, geraniol, fanesol, terpinol, eugenol,
Can substantially increase fragrant and sweet.
Above-mentioned perfume material more or less all shows certain sweet note according to respective material composition basis, individually makes
Though with certain sweet fragrant effect, the richness of its fragrance is inadequate, in order that the plentiful coordination of the fragrance of electronic cigarette liquid, therefore
Above-mentioned raw material is compounded.
A kind of preferred implementation method is that described sweet fragrant additive is by following components mixing by weight
Into：
Orris oil or 1 part of 2 parts of orris absolute, attar of rose or rose absolute, 1 part of geranium oil, 1 part of citronella oil, Acacia leaching
1 part of cream, 1 part of osmanthus concrete, 93 parts of solvent.
Preferred another embodiment is：Described sweet fragrant additive is by following components mixing by weight
Into：
Orris oil or 5 parts of 5 parts of orris absolute, attar of rose or rose absolute, 5 parts of geranium oil, 5 parts of citronella oil, Acacia leaching
2 parts of cream, 3 parts of osmanthus concrete, 75 parts of solvent.
Further technical scheme is：The solvent is ethyl acetate or glycerine.
Present invention also offers a kind of with sweet fragrant electronic cigarette liquid, it by sweet fragrant additive, tobacco extract,
The mixed alkoxide solution of water/glycol/propane three is constituted, the quality of the sweet fragrant additive and the mixed alkoxide solution of water/glycol/propane three
Than being 1~10：1000, the tobacco extract is 5~20 with the mass ratio of the mixed alkoxide solution of water/glycol/propane three:
1000000。
Preferably, the sweet fragrant additive and the mass ratio of the mixed alkoxide solution of water/glycol/propane three are 1：1000, institute
It is 1 that tobacco extract is stated with the mass ratio of the mixed alkoxide solution of water/glycol/propane three:100000.
Further technical scheme is：The mixed alkoxide solution of water/glycol/propane three is by 10~30 by weight
Part water, 40~80 parts of propane diols and 10~30 parts of glycerine are mixed.
Preferably, the mixed alkoxide solution of water/glycol/propane three by 10 parts of water by weight, 80 parts of propane diols and
10 parts of glycerine are mixed.
Further technical scheme is：The described nicotine content with sweet fragrant electronic cigarette liquid for 10~
30mg/g。
Further technical scheme is：The preparation method of the tobacco extract is：By tobacco leaf in 40~50 DEG C of temperature
Drying, is then comminuted into offal, by ultrasonic extraction 10~30 minutes in offal addition q. s. methylene chloride, stands 2 hours, filtering
Fall offal, collect organic phase, according to tobacco leaf and the mass volume ratio 1g of the dilute sulfuric acid of concentration 5%：2~5mL adds in organic phase
Enter the dilute sulfuric acid of concentration 5%, add in two batches, collect water phase, then the pH value of water phase is adjusted to 8~10, add food-grade acetic acid
Ethyl ester is extracted, and isolates organic phase, is concentrated as 1~5mL obtains tobacco extract.
Compared with prior art, one of beneficial effects of the present invention are：
(1) electronic cigarette liquid prepared by the present invention has sweet fragrant characteristic flavor on basis, enriches the suction local flavor of electronic cigarette, can expire
The demand of the foot difference consumer group.
(2) tool compared with existing product is greatly improved electronic cigarette liquid prepared by the present invention at aspects such as fragrance, mouthfeels,
The satisfaction of smoker can substantially be increased.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
The preparation of tobacco extract
The tobacco leaf of 50g is weighed, is dried in 45 DEG C of baking oven, pulverizer is ground into offal.The two of 300mL will be added in offal
Chloromethanes, ultrasonic extraction 20min, then 2h is stood, and offal is filtered out, organic phase is collected, to the concentration that 100mL is added in organic phase
5% dilute sulfuric acid, adds in two batches, collects water phase.The pH value of water phase is transferred to 10 or so again, the ethyl acetate of food-grade is added
Extraction, isolates organic phase, then organic phase is concentrated into 5mL, obtains tobacco extract, nicotine content 25mg/g.The tobacco
Extract is used for following each embodiments.
Embodiment 1
Weigh orris oil or 1 part of 2 parts of orris absolute, attar of rose or rose absolute, 1 part of geranium oil, 1 part of citronella oil, Jin He
Joyous 93 parts of 1 part of medicinal extract, 1 part of osmanthus concrete and ethyl acetate, are sufficiently mixed uniformly, obtain sweet fragrant additive.Sweet perfume (or spice) is taken to add
Plus agent 10mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：1:8:1)
In, the μ g of tobacco extract 100 are added, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, it is fragrant with obvious sweet fragrant breeze lattice
The plentiful coordination of gas.
Embodiment 2
Weigh orris oil or 1 part of 2 parts of orris absolute, attar of rose or rose absolute, 1 part of geranium oil, 1 part of citronella oil, Jin He
Joyous 93 parts of 1 part of medicinal extract, 1 part of osmanthus concrete and glycerine, are sufficiently mixed uniformly, obtain sweet fragrant additive.Take sweet fragrant addition
Agent 10mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：1:8:1) in,
The addition μ g of tobacco extract 100, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, it is fragrant with obvious sweet fragrant breeze lattice
The plentiful coordination of gas.
Embodiment 3
The comparative example of embodiment 1：Weigh orris oil or 2 parts of orris absolute, attar of rose or 1 part of rose absolute, Jin He
Joyous 95 parts of 1 part of medicinal extract, 1 part of osmanthus concrete and ethyl acetate, are sufficiently mixed uniformly, obtain sweet fragrant additive.Sweet perfume (or spice) is taken to add
Plus agent 10mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：1:8:1)
In, the μ g of tobacco extract 100 are added, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, with sweet fragrant breeze lattice, fragrance owes association
Adjust, richness is slightly worse.
Embodiment 4
Weigh orris oil or 5 parts of 5 parts of orris absolute, attar of rose or rose absolute, 5 parts of geranium oil, 5 parts of citronella oil, Jin He
Joyous 75 parts of 2 parts of medicinal extract, 3 parts of osmanthus concrete and ethyl acetate, are sufficiently mixed uniformly, obtain sweet fragrant additive.Sweet perfume (or spice) is taken to add
Plus agent 10mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：1:8:1),
The addition μ g of tobacco extract 100, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, it is fragrant with obvious sweet fragrant breeze lattice
The plentiful coordination of gas.
Embodiment 5
The comparative example of embodiment 4：Weigh orris oil or 5 parts of orris absolute, attar of rose or 5 parts of rose absolute, spiceleaf
70 parts of 5 parts of oil, 5 parts of citronella oil and ethyl acetate, are sufficiently mixed uniformly, obtain sweet fragrant additive.Take sweet fragrant additive
10mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：1:8:1) in, add
Plus the μ g of tobacco extract 100, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, it is fragrant with obvious sweet fragrant breeze lattice
Gas is plentiful, and harmony is slightly worse.
Embodiment 6
Weigh orris oil or 5 parts of 5 parts of orris absolute, attar of rose or rose absolute, 5 parts of geranium oil, 5 parts of citronella oil, Jin He
Joyous 75 parts of 2 parts of medicinal extract, 3 parts of osmanthus concrete and ethyl acetate, are sufficiently mixed uniformly, obtain sweet fragrant additive.Sweet perfume (or spice) is taken to add
Plus agent 50mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：1:8:1)
In, the μ g of tobacco extract 100 are added, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, it is fragrant with obvious sweet fragrant breeze lattice
The plentiful coordination of gas.
Embodiment 7
Weigh orris oil or 5 parts of 5 parts of orris absolute, attar of rose or rose absolute, 5 parts of geranium oil, 5 parts of citronella oil, Jin He
Joyous 75 parts of 2 parts of medicinal extract, 3 parts of osmanthus concrete and ethyl acetate, are sufficiently mixed uniformly, obtain sweet fragrant additive.Sweet perfume (or spice) is taken to add
Plus agent 100mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：3:4:3)
In, the μ g of tobacco extract 100 are added, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, it is fragrant with obvious sweet fragrant breeze lattice
The plentiful coordination of gas.
Embodiment 8
Weigh orris oil or 5 parts of 5 parts of orris absolute, attar of rose or rose absolute, 5 parts of geranium oil, 5 parts of citronella oil, Jin He
Joyous 75 parts of 2 parts of medicinal extract, 3 parts of osmanthus concrete and ethyl acetate, are sufficiently mixed uniformly, obtain sweet fragrant additive.Sweet perfume (or spice) is taken to add
Plus agent 10mg is added to mixed liquor (water, propane diols, the mass ratio of glycerine of the water/glycol/propane triol of 10g：2:6:2)
In, the μ g of tobacco extract 200 are added, obtain with sweet fragrant electronic cigarette liquid.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, it is fragrant with obvious sweet fragrant breeze lattice
The plentiful coordination of gas.
The blank of embodiment 9 is tested
Be added to instead of sweet fragrant additive with 10mg ethyl acetate or glycerine 10g water/glycol/propane triol it is mixed
Close liquid (water, propane diols, the mass ratio of glycerine：1:8:1) in, the μ g of tobacco extract 100 are added, is obtained with sweet fragrant electricity
Sub- tobacco juice.
Take during 1mL electronic cigarette liquids add atomizer, smoked panel test through the specialty personnel that smoke panel test, without sweet fragrant breeze lattice, fragrance is slightly
Difference, harmony is slightly worse.
Electronic cigarette liquid obtained by the various embodiments described above is carried out into sensory quality assessment：
According to Sensory Quality of Cigarette judgment criteria GB5606.4-2005, with reference to electronic cigarette organoleptic features, according to different weights
6 evaluation indexes and score value are set, 1 is shown in Table.
The electronic cigarette evaluation index of table 1 and score value
The tobacco juice for electronic smoke of embodiment 1~8 is carried out into sensory evaluating smoking, smoking result tries to achieve calculation according to each expert's smoking result
Art average, as a result retains a significant digits, and statistics is shown in Table 2.
Each embodiment electronic cigarette liquid sensory evaluating smoking statistics of table 2
The statistics of table 2 shows, sweet fragrant additive not only allows the electronic cigarette liquid to have the characteristic flavor on basis of sweet perfume, also right
The indexs such as the fragrance of electronic cigarette, miscellaneous gas, excitant, satisfaction, harmony and pleasant impression have certain adjustment effect, add sweet
Fragrant electronic cigarette liquid comprehensive scores of smokeing panel test are high.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that
Those skilled in the art can be designed that a lot of other modification and implementation methods, and these modifications and implementation method will fall in this Shen
Please be within disclosed spirit and spirit.More specifically, in the range of disclosure and claim, can be to master
The building block and/or layout for inscribing composite configuration carry out various variations and modifications.Except what is carried out to building block and/or layout
Outside variations and modifications, to those skilled in the art, other purposes also will be apparent.
Claims (5)
1. it is a kind of with sweet fragrant electronic cigarette liquid, it is characterised in that it is by sweet fragrant additive, tobacco extract, water/the third two
Alcohol/glycerine mixed solution composition, the mass ratio of the sweet fragrant additive and the mixed alkoxide solution of water/glycol/propane three for 1~
10：1000, the tobacco extract is 5~20 with the mass ratio of the mixed alkoxide solution of water/glycol/propane three:1000000；
Sweet fragrant additive is mixed by following components by weight：
Orris oil or 1~5 part of 2~5 parts of orris absolute, attar of rose or rose absolute, 1~5 part of geranium oil, 1~5 part of citronella oil,
1~2 part of cassie concrete, 1~3 part of osmanthus concrete, 75~93 parts of solvent；The solvent is ethyl acetate or glycerine；
The preparation method of the tobacco extract is：By tobacco leaf in 40~50 DEG C of drying of temperature, offal is then comminuted into, by offal
Ultrasonic extraction 10~30 minutes, stands 2 hours in addition q. s. methylene chloride, filters out offal, organic phase is collected, according to tobacco leaf
With the mass volume ratio 1g of the dilute sulfuric acid of concentration 5%：2~5mL adds in two batches to the dilute sulfuric acid that concentration 5% is added in organic phase
Enter, collect water phase, then the pH value of water phase is adjusted to 8~10, add the extraction of food level ethyl acetate, isolate organic phase, concentrate
For 1~5mL obtains tobacco extract.
2. according to claim 1 with sweet fragrant electronic cigarette liquid, it is characterised in that the sweet fragrant additive and water/
The mass ratio of the mixed alkoxide solution of glycol/propane three is 1：1000, the tobacco extract mixes molten with water/glycol/propane triol
The mass ratio of liquid is 1:100000.
3. it is according to claim 1 with sweet fragrant electronic cigarette liquid, it is characterised in that the water/glycol/propane triol
Mixed solution is mixed by 10~30 parts of water by weight, 40~80 parts of propane diols and 10~30 parts of glycerine.
4. it is according to claim 3 with sweet fragrant electronic cigarette liquid, it is characterised in that the water/glycol/propane triol
Mixed solution is mixed by 10 parts of water by weight, 80 parts of propane diols and 10 parts of glycerine.
5. according to claim 1 with sweet fragrant electronic cigarette liquid, it is characterised in that its nicotine content is 10~
30mg/g。
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| CN201510026003.7A CN104531356B (en) | 2015-01-19 | 2015-01-19 | Sweet fragrant additive and the electronic cigarette liquid with sweet perfume |
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| CN201510026003.7A CN104531356B (en) | 2015-01-19 | 2015-01-19 | Sweet fragrant additive and the electronic cigarette liquid with sweet perfume |
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| CN104531356B true CN104531356B (en) | 2017-06-16 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| RU2593964C1 (en) * | 2015-05-20 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| CN104962393B (en) * | 2015-06-18 | 2018-07-03 | 湖北中烟工业有限责任公司 | Cigarette strawberry type cork paper essence |
| CN105124750B (en) * | 2015-07-27 | 2017-10-27 | 浙江中烟工业有限责任公司 | A kind of fragrant and sweet type tobacco juice for electronic smoke and preparation method thereof |
| CN105768198B (en) * | 2016-04-29 | 2017-09-19 | 江苏中烟工业有限责任公司 | Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof |
| CN107513343A (en) * | 2017-09-01 | 2017-12-26 | 陈志年 | A kind of compound spices coating of solidified by ultraviolet ray radiation |
| CN109258370A (en) * | 2018-07-29 | 2019-01-25 | 四川省烟草公司宜宾市公司 | A kind of tobacco planting method improving the sweet fragrant breeze lattice of tobacco leaf |
| CN110655986A (en) * | 2019-09-25 | 2020-01-07 | 武汉黄鹤楼香精香料有限公司 | Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof |
| CN111449282A (en) * | 2020-03-27 | 2020-07-28 | 河南中烟工业有限责任公司 | Replaceable filter stick with sweet fragrance |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101760306A (en) * | 2008-11-24 | 2010-06-30 | 王晓明 | Ylang ylang oil rose essence |
| CN102559388A (en) * | 2012-02-27 | 2012-07-11 | 浙江中烟工业有限责任公司 | Essential oil of tobaccos as well as preparation method and application thereof to cigarettes |
| CN103146482A (en) * | 2013-03-21 | 2013-06-12 | 红云红河烟草(集团)有限责任公司 | Tobacco flavor with sweetening function and application thereof |
| CN103146483A (en) * | 2013-03-21 | 2013-06-12 | 红云红河烟草(集团)有限责任公司 | Pelargonium roseum extract and application thereof in cigarettes |
| CN103881817A (en) * | 2014-03-18 | 2014-06-25 | 黄金珍 | Supercritical extraction method for tobacco essential oil |
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Effective date of registration: 20161222 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Applicant after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Applicant after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610000 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Applicant before: China Tobacco Chuanyu Industry Co., Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170616 Termination date: 20180119 |