CN109846075A - A kind of electronic cigarette liquid and preparation method thereof with lemon flavor - Google Patents

A kind of electronic cigarette liquid and preparation method thereof with lemon flavor Download PDF

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Publication number
CN109846075A
CN109846075A CN201910005349.7A CN201910005349A CN109846075A CN 109846075 A CN109846075 A CN 109846075A CN 201910005349 A CN201910005349 A CN 201910005349A CN 109846075 A CN109846075 A CN 109846075A
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parts
electronic cigarette
oil
lemon
cigarette liquid
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CN201910005349.7A
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CN109846075B (en
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丁玉
何书杰
张高峰
陶飞燕
吴志英
胡涛
邓发达
罗诚
黄玉川
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China Tobacco Sichuan Industrial Co Ltd
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China Tobacco Sichuan Industrial Co Ltd
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Abstract

The invention discloses a kind of electronic cigarette liquid and preparation method thereof with lemon flavor, the electronic cigarette liquid are prepared from the following raw materials in parts by weight: 0.1~10 part of lemon oil, 0.01~1 part of bergamot oil, 0.01~1 part of limette oil, 0.005~0.25 part of terpinol, 0.005~0.25 part of linalool, 0.001~0.1 part of methyl heptenone, 0.001~0.1 part of octanal, 0.005~0.25 part of geranyl acetate, 1~5 part of ethyl alcohol, 10~30 parts of water, 30~90 parts of propylene glycol, 20~40 parts of glycerine.The electronic cigarette liquid can enrich the suction flavor of electronic cigarette, meet the needs of different consumer groups, while can effectively reduce the potential hazard to consumer health.

Description

A kind of electronic cigarette liquid and preparation method thereof with lemon flavor
Technical field
The present invention relates to electronic cigarette liquid technical fields, and in particular to a kind of electronic cigarette liquid and its preparation with lemon flavor Method.
Background technique
Smoking directly endangers smoker's bring and secondhand smoke influences increasingly by society ambient enviroment Pay attention to.Electronic cigarette is a kind of new tobacco products, and compared with traditional cigarette, electronic cigarette is without nuisances such as tar, carbon monoxide Matter is smaller to smoker's actual bodily harm;In addition, the aerosol that the nicotine of electronic cigarette is formed by atomization, rapid in air Dilution reduces the risk that harm is generated to people around.Substitute of the electronic cigarette as cigarette, obtains market in the world Approve, sales volume presentation rises year by year trend.
Tobacco juice for electronic smoke is an important factor for influencing suction quality.Electronic cigarette passes through the development of several generations, although shape, hand The perceptual images cigarette such as sense, smog, but the tobacco juice for these electronic cigarettes remains some shortcomings.Nowadays sale is managed in the market Mainstream electronic cigarette generally uses tobacco material extract, then mixed with tobacco aromaticss, deionized water etc. to imitate the mouthfeel of cigarette Tobacco juice for electronic smoke is made in conjunction.The mist that the smog that such tobacco juice for electronic smoke generates can imitate cigarette to a certain extent, but be discharged Gas also contains a small amount of harmful substance, and smoker generally feels that the fragrance of these electronic cigarettes and mouthfeel are not achieved its physiology and need It asks, suction flavor is more dull, and the above problem will largely effect on the sustainable health development of electronic cigarette.
Summary of the invention
In order to overcome the above technical defects, the present invention provides a kind of with the electronic cigarette liquid of lemon flavor and its preparation side Method, the electronic cigarette liquid can enrich the suction flavor of electronic cigarette, meet the needs of different consumer groups, while the essential oil of lemon class Have and remove free radical, clearing heat and detoxicating and other effects, there is certain health-care effect, can effectively reduce the potential danger to consumer health Evil.
In order to reach above-mentioned technical effect, the present invention provides a kind of electronic cigarette liquid with lemon flavor, the electronics Tobacco juice is prepared from the following raw materials in parts by weight: 0.1~10 part of lemon oil, 0.01~1 part of bergamot oil, limette oil 0.01~1 part, 0.005~0.25 part of terpinol, 0.005~0.25 part of linalool, 0.001~0.1 part of methyl heptenone, octanal 0.001~0.1 part, 0.005~0.25 part of geranyl acetate, 1~5 part of ethyl alcohol, 10~30 parts of water, 30~90 parts of propylene glycol, third 20~40 parts of triol.
Further technical solution is that the electronic cigarette liquid is prepared from the following raw materials in parts by weight: lemon oil 0.5 ~8 parts, 0.05~1 part of bergamot oil, 0.05~1 part of limette oil, 0.005~0.20 part of terpinol, linalool 0.005~ 0.20 part, 0.005~0.1 part of methyl heptenone, 0.005~0.1 part of octanal, 0.01~0.25 part of geranyl acetate, ethyl alcohol 2~ 5 parts, 10~20 parts of water, 40~80 parts of propylene glycol, 20~40 parts of glycerine.
Further technical solution is that the electronic cigarette liquid is prepared from the following raw materials in parts by weight: lemon oil 1~ 8 parts, 0.1~1 part of bergamot oil, 0.1~1 part of limette oil, 0.01~0.20 part of terpinol, 0.01~0.20 part of linalool, 0.01~0.1 part of methyl heptenone, 0.01~0.1 part of octanal, 0.01~0.2 part of geranyl acetate, 2~5 parts of ethyl alcohol, water 10~ 15 parts, 50~80 parts of propylene glycol, 20~40 parts of glycerine.
The present invention also provides a kind of preparation methods of electronic cigarette liquid with lemon flavor, comprising the following steps:
Novel electron tobacco juice: 0.1~10 part of lemon oil, bergamot is sufficiently mixed and obtained according to the raw material of following parts by weight 0.01~1 part of oil, 0.01~1 part of limette oil, 0.005~0.25 part of terpinol, 0.005~0.25 part of linalool, methyl heptan 0.001~0.1 part of ketenes, 0.001~0.1 part of octanal, 0.005~0.25 part of geranyl acetate, 1~5 part of ethyl alcohol, water 10~30 Part, 30~90 parts of propylene glycol, 20~40 parts of glycerine.
In the present invention, the raw material for providing citris aromas is mainly lemon oil, bergamot oil and limette oil, wherein lemon oil For colourless to faint yellow volatile essential oil.With fragrance specific to Fresh Lemon, main component You limonene, citral, octanal, Aldehyde C-9, lauric aldehyde, firpene, amphene, linalool, geranyl acetate and neryl acetate.
Bergamot oil has the fruity of green perfumed ribbon sweet tea, and like the cooling-freshness of lemon sample, main component includes acetic acid virtue camphor tree Ester, dihydro pillapiol, linalool, terpinol, nerol, limonene, bergaptene, limonene, firpene, amphene, limonene, Chinese celery Alkene, citral, bergaptol.
Limette oil: colourless to green-yellow volatile essential oil.In citrus fragrance, main component has limonene, citral, second Sour virtue camphor tree ester, fenchanol, terpineol, Cineole and fatty acid, terpene, aldehydes and alcohols.
Three of the above raw material is the primary raw material for constituting lemon, and exclusive use has certain lemon, but lemon Not enough skillfully, there is no stereovision, note also owes abundant.In the application, terpinol and linalool have lilac taste, methyl heptenyl Ketone has fresh faint scent, citrus sample breath, and octanal has very strong fruit aroma, and geranyl acetate has rose and lavender fragrant Gas adds a certain amount of terpinol, linalool, methyl heptenone, octanal, geranyl in three kinds of raw materials with lemon The substances such as ester, which carry out certain modification and setting off to fragrance, could make that lemon is skilled, has a sense of hierarchy, to have better Satisfaction.
Compared with prior art, the present invention it is strong to have the following beneficial effects: that electronic cigarette liquid prepared by the present invention has Citrus scented enriches the suction flavor of electronic cigarette, can meet the needs of different consumer groups.Fragrance, in terms of with Existing product is greatly improved compared to tool, can obviously increase the satisfaction of smoker, while the essential oil of lemon class has removing certainly By base, clearing heat and detoxicating and other effects, there is certain health-care effect, can effectively reduce the potential hazard to consumer health.
Specific embodiment
Embodiment 1
A kind of electronic cigarette liquid with lemon flavor, raw material composition include: 8 parts of lemon oil, perfume in parts by weight 0.1 part of lemon oil, 0.5 part of limette oil, 0.01 part of terpinol, 0.03 part of linalool, 0.005 part of methyl heptenone, octanal 0.003 part, 0.03 part of geranyl acetate, 2 parts of ethyl alcohol, 5 parts of water, 60 parts of propylene glycol, 24.322 parts of glycerine.
Preparation method are as follows:
It takes 1mL electronic cigarette liquid to be added in atomizer, smokes panel test through the profession personnel that smoke panel test, there are apparent Lemon fruit fragrant breeze lattice.
Reference examples 1
Raw material except without containing in addition to lemon oil, other raw materials with the preparation method is the same as that of Example 1.
Embodiment 2
8 parts of lemon oil, 0.05 part of bergamot oil, 0.02 part of limette oil, 0.01 part of terpinol, 0.03 part of linalool, first 0.005 part of base heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethyl alcohol, 5 parts of water, 60 parts of propylene glycol, glycerine 24.852 parts.
It takes 1mL electronic cigarette liquid to be added in atomizer, smokes panel test through the profession personnel that smoke panel test, there are apparent Lemon fruit fragrant breeze lattice.
Reference examples 2
Raw material is in addition to without containing limette oil, other raw materials and preparation method are the same as embodiment 2.
Embodiment 3
5 parts of lemon oil, 0.05 part of bergamot oil, 0.02 part of limette oil, 0.01 part of terpinol, 0.03 part of linalool, first 0.005 part of base heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethyl alcohol, 5 parts of water, 60 parts of propylene glycol, glycerine 27.852 parts.
It takes 1mL electronic cigarette liquid to be added in atomizer, smokes panel test through the profession personnel that smoke panel test, there are apparent Lemon fruit fragrant breeze lattice.
Reference examples 3
Raw material is in addition to without containing bergamot oil, other raw materials and preparation method are the same as embodiment 2.
Embodiment 4
3 parts of lemon oil, 0.05 part of bergamot oil, 0.02 part of limette oil, 0.01 part of terpinol, 0.03 part of linalool, first 0.005 part of base heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethyl alcohol, 5 parts of water, 60 parts of propylene glycol, glycerine 29.852 parts.
It takes 1mL electronic cigarette liquid to be added in atomizer, smokes panel test through the profession personnel that smoke panel test, there are apparent Lemon fruit fragrant breeze lattice.
Reference examples 4
Raw material is in addition to without containing terpinol, other raw materials and preparation method are the same as embodiment 4.
Embodiment 5
1 part of lemon oil, 0.05 part of bergamot oil, 0.02 part of limette oil, 0.01 part of terpinol, 0.03 part of linalool, first 0.005 part of base heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethyl alcohol, 5 parts of water, 60 parts of propylene glycol, glycerine 31.852 parts.
It takes 1mL electronic cigarette liquid to be added in atomizer, smokes panel test through the profession personnel that smoke panel test, there are apparent Lemon fruit fragrant breeze lattice.
Reference examples 5
Raw material is in addition to without containing methyl heptenone, other raw materials and preparation method are the same as embodiment 5.
According to Sensory Quality of Cigarette judgment criteria GB5606.4-2005, in conjunction with electronic cigarette organoleptic features, according to different weights 6 evaluation indexes and score value are set, are shown in Table 1
Table 1
The tobacco juice for electronic smoke of 1~embodiment of embodiment 5 and 1~reference examples of reference examples 5 is subjected to sensory evaluation, evaluation and analysis knot Fruit evaluates and analyses result according to each expert and acquires arithmetic equal value, as a result retains an effective digital, and statistical result is shown in Table 2.
Sample Satisfaction Fragrance Harmony Miscellaneous gas Irritation Pleasant impression
Embodiment 1 22.5 20.5 4.5 8.0 16.0 12.5
Embodiment 2 23.0 21.5 4.5 8.5 16.5 13.0
Embodiment 3 23.0 22.0 4.5 8.5 16.5 13.0
Embodiment 4 23.5 22.5 4.5 8.5 17.0 13.5
Embodiment 5 23.0 22.5 4.5 8.5 16.5 13.5
Reference examples 1 20.0 18.5 3.5 7.5 15.0 11.5
Reference examples 2 21.5 19.0 4.0 8.0 15.5 12.0
Reference examples 3 20.5 18.5 4.0 8.0 16.0 12.5
Reference examples 4 21.0 19.5 3.5 7.5 15.5 11.5
Reference examples 5 21.0 18.0 3.5 7.0 15.5 12.0
Table 2
Although reference be made herein to invention has been described for explanatory embodiment of the invention, and above-described embodiment is only this hair Bright preferable embodiment, embodiment of the present invention are not limited by the above embodiments, it should be appreciated that those skilled in the art Member can be designed that a lot of other modification and implementations, these modifications and implementations will fall in principle disclosed in the present application Within scope and spirit.

Claims (4)

1. a kind of electronic cigarette liquid with lemon flavor, which is characterized in that the electronic cigarette liquid is in parts by weight by following Raw material is made: 0.1~10 part of lemon oil, 0.01~1 part of bergamot oil, 0.01~1 part of limette oil, terpinol 0.005~ 0.25 part, 0.005~0.25 part of linalool, 0.001~0.1 part of methyl heptenone, 0.001~0.1 part of octanal, geranyl acetate 0.005~0.25 part, 1~5 part of ethyl alcohol, 10~30 parts of water, 30~90 parts of propylene glycol, 20~40 parts of glycerine.
2. the electronic cigarette liquid according to claim 1 with lemon flavor, which is characterized in that the electronic cigarette liquid is according to weight Amount number meter is prepared from the following raw materials: 0.5~8 part of lemon oil, 0.05~1 part of bergamot oil, 0.05~1 part of limette oil, pine 0.005~0.20 part of oleyl alcohol, 0.005~0.20 part of linalool, 0.005~0.1 part of methyl heptenone, octanal 0.005~0.1 Part, 0.01~0.25 part of geranyl acetate, 2~5 parts of ethyl alcohol, 10~20 parts of water, 40~80 parts of propylene glycol, glycerine 20~40 Part.
3. the electronic cigarette liquid according to claim 2 with lemon flavor, which is characterized in that the electronic cigarette liquid is according to weight Amount number meter is prepared from the following raw materials: 1~8 part of lemon oil, 0.1~1 part of bergamot oil, 0.1~1 part of limette oil, terpinol 0.01~0.20 part, 0.01~0.20 part of linalool, 0.01~0.1 part of methyl heptenone, 0.01~0.1 part of octanal, acetic acid perfume 0.01~0.2 part of leaf ester, 2~5 parts of ethyl alcohol, 50~80 parts, 20~40 parts of glycerine of 10~15 propylene glycol of water.
4. a kind of preparation method of the electronic cigarette liquid with lemon flavor, which is characterized in that the raw material of following parts by weight is abundant The electronic cigarette liquid with lemon flavor: 0.1~10 part of lemon oil, 0.01~1 part of bergamot oil, limette oil can be obtained in mixing 0.01~1 part, 0.005~0.25 part of terpinol, 0.005~0.25 part of linalool, 0.001~0.1 part of methyl heptenone, octanal 0.001~0.1 part, 0.005~0.25 part of geranyl acetate, 1~5 part of ethyl alcohol, 10~30 parts of water, 30~90 parts of propylene glycol, third 20~40 parts of triol.
CN201910005349.7A 2019-01-03 2019-01-03 Electronic cigarette liquid with lemon flavor and preparation method thereof Active CN109846075B (en)

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Cited By (5)

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CN110506979A (en) * 2019-09-12 2019-11-29 深圳雾芯科技有限公司 Flavour compositions and electronic cigarette liquid comprising the flavour compositions
CN110819456A (en) * 2019-12-09 2020-02-21 将军烟草集团有限公司 Green lemon essence for bead blasting and application of green lemon essence in cigarettes
CN113243549A (en) * 2021-04-21 2021-08-13 深圳市真味生物科技有限公司 Lemon-flavor essence extracted from plants for electronic atomized liquid and extraction method
CN114680362A (en) * 2021-12-28 2022-07-01 四川三联新材料有限公司 Electronic cigarette liquid with refreshing function
CN115251450A (en) * 2022-08-22 2022-11-01 东莞市鸿馥生物科技有限公司 Bergamot essential oil applied to electronic cigarette and preparation method thereof

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CN108165371A (en) * 2018-01-10 2018-06-15 湖北中烟工业有限责任公司 A kind of preparation method and applications of iris extract
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110506979A (en) * 2019-09-12 2019-11-29 深圳雾芯科技有限公司 Flavour compositions and electronic cigarette liquid comprising the flavour compositions
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CN110819456A (en) * 2019-12-09 2020-02-21 将军烟草集团有限公司 Green lemon essence for bead blasting and application of green lemon essence in cigarettes
CN113243549A (en) * 2021-04-21 2021-08-13 深圳市真味生物科技有限公司 Lemon-flavor essence extracted from plants for electronic atomized liquid and extraction method
CN113243549B (en) * 2021-04-21 2022-04-05 深圳市真味生物科技有限公司 Lemon-flavor essence extracted from plants for electronic atomized liquid and extraction method
CN114680362A (en) * 2021-12-28 2022-07-01 四川三联新材料有限公司 Electronic cigarette liquid with refreshing function
CN115251450A (en) * 2022-08-22 2022-11-01 东莞市鸿馥生物科技有限公司 Bergamot essential oil applied to electronic cigarette and preparation method thereof

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