CN110506979A - Flavour compositions and electronic cigarette liquid comprising the flavour compositions - Google Patents

Flavour compositions and electronic cigarette liquid comprising the flavour compositions Download PDF

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Publication number
CN110506979A
CN110506979A CN201910866656.4A CN201910866656A CN110506979A CN 110506979 A CN110506979 A CN 110506979A CN 201910866656 A CN201910866656 A CN 201910866656A CN 110506979 A CN110506979 A CN 110506979A
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CN
China
Prior art keywords
electronic cigarette
cigarette liquid
parts
weight
flavour compositions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910866656.4A
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Chinese (zh)
Inventor
许静
姜兴涛
熊赞华
李锐
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Relx Technology Co Ltd
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Shenzhen Relx Technology Co Ltd
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Filing date
Publication date
Application filed by Shenzhen Relx Technology Co Ltd filed Critical Shenzhen Relx Technology Co Ltd
Priority to CN201910866656.4A priority Critical patent/CN110506979A/en
Priority to PCT/CN2019/107939 priority patent/WO2021046917A1/en
Publication of CN110506979A publication Critical patent/CN110506979A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Fats And Perfumes (AREA)

Abstract

A kind of electronic cigarette liquid this application involves flavour compositions and comprising the flavour compositions.The flavour compositions of some embodiments of the application include the substance of following parts by weight: 10 to 20 parts of alpha-terpineol, 1 to 5 part of γ-terpinene, 10 to 15 parts of nerol, 15 to 25 parts of dihydrojasmonate, 5 to 10 parts of cis-jasmone, 1 to 5 part of citral and 30 to 40 parts of limonene.The electronic cigarette liquid of the application generates the mouthfeel of lemon and black tea flavor when drawing, and is capable of forming the uniform and strong aerosol of smell, effectively promotes user's experience.

Description

Flavour compositions and electronic cigarette liquid comprising the flavour compositions
Technical field
This application involves the field more particularly to a kind of flavour compositions of electronics aerosol or electronic atomization device and comprising The electronic cigarette liquid of the flavour compositions.
Background technique
Due to the pursuit for personal health, environmental protection and ease of use, electronic cigarette takes as traditional tobacco It is more and more popular with consumers for product.Electronic cigarette or electronic atomizer are by the way that the formation of smoking material low-temperature atomizing to be used to make User sucking aerosol, come replace traditional tobacco in a manner of high-temp combustion caused by flue gas.Wherein, electronic cigarette liquid is for making The experience of user and mouthfeel tool have a certain impact.
Therefore, it is necessary to do further improve and research to the composition of electronic cigarette liquid.
Summary of the invention
The application is also known as flavor additives useful by providing a kind of flavour compositions, can be used in electronic cigarette liquid, the wind Taste composition by atomising device be atomized after be formed by for user sucking aerosol can allow user generate lemon and The flavor of black tea, and the harmful substances such as tar and suspended particulates are not generated.Meanwhile the electronic cigarette liquid can when user aspirates The uniform and strong aerosol of smell is formed, and the aerosol mouthfeel is submissive and does not have residual sense, to promote user's experience.
According to the application level, this application provides a kind of flavour compositions, wherein the flavour compositions packet Substance containing following parts by weight: about 10 to about 20 parts of alpha-terpineol, about 1 to about 5 part of γ-terpinene, about 10 to about 15 parts Nerol, about 15 to about 25 parts of dihydrojasmonate, about 5 to about 10 parts of cis-jasmone, about 1 to about 5 part Citral and about 30 to about 40 parts of limonene.
According to another level of the application, this application provides a kind of electronic cigarette liquids, and it includes above-mentioned flavour compositions.
According to the another level of the application, this application provides a kind of atomising devices, and it includes above-mentioned electronic cigarette liquids.
The additional level and advantage of the embodiment of the present application will be described partly in subsequent instruction, be shown or via this Apply for the implementation of embodiment and illustrates.
Specific embodiment
Embodiments herein will be shown hereinafter by detailed retouch.Embodiments herein does not answer described be interpreted Limitation to the application.
In addition, sometimes herein with range format presentation amount, ratio and other numerical value.It should be understood that such range format It is that and should neatly understand for convenient and for purpose of brevity, not only comprising being expressly specified as the numerical value of scope limitation, but also wraps Containing all individual numbers or the subrange being covered by the range, as explicitly specifying each numerical value and subrange.
As used herein, term " substantially ", " substantially ", " generally ", " essence " and " about " is to describe and illustrate Small variation.When being used in combination with event or situation, the term can be referred to the example that wherein event or situation accurately occur And the example that wherein event or situation pole approximatively occur.For example, when combination numerical value is in use, term can be referred to be less than Or ± 10% variation range equal to the numerical value, e.g., less than or equal to ± 5%, be less than or equal to ± 4%, be less than or wait In ± 3%, be less than or equal to ± 2%, be less than or equal to ± 1%, being less than or equal to ± 0.5%, being less than or equal to ± 0.1%, Or it is less than or equal to ± 0.05%.For example, if the difference between two values is less than or equal to the average value of described value ± 10% (e.g., less than or equal to ± 5%, be less than or equal to ± 4%, be less than or equal to ± 3%, be less than or equal to ± 2%, Less than or equal to ± 1%, it is less than or equal to ± 0.5%, is less than or equal to ± 0.1% or is less than or equal to ± 0.05%), that It is believed that described two numerical value " generally " are identical.
In specific embodiment and claims, by term at least one of at least one of " ", " ", " in At least one " or the list of project that is connected of other term similars may imply that any combination of listed item.For example, such as Fruit lists project A and B, then phrase " at least one of A and B " means only A;Only B;Or A and B.In another example, such as Fruit lists project A, B and C, then phrase " at least one of A, B and C " means only A;Or only B;Only C;A and B (excluding C); A and C (excluding B);B and C (excluding A);Or the whole of A, B and C.Project A may include discrete component or multiple element.Project B can Include discrete component or multiple element.Project C may include discrete component or multiple element.
Herein, term " aerosol for user's sucking " or " aerosol " may include, but be not limited to, aerosol, Suspension liquid, low-temperature steam and escaping gas.
According to the one aspect of the application, the application provides a kind of electronic cigarette liquid, and it includes flavour compositions, wherein described Flavour compositions include following parts by weight substance: about 10 to about 20 parts of alpha-terpineol, about 1 to about 5 part of γ-terpinene, About 10 to about 15 parts of nerol, about 15 to about 25 parts of dihydrojasmonate, about 5 to about 10 parts of cis-jasmone, About 1 to about 5 part of citral and about 30 to about 40 parts of limonene.In some embodiments, the flavour compositions of the application can By the material composition of the above parts by weight.
In the flavour compositions of some embodiments, alpha-terpineol can substantially 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, The range of both any composition in 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts or these parts by weight;γ-terpinene can be substantially For the range of composition both any in 1 part, 2 parts, 3 parts, 4 parts, 5 parts or these parts by weight;Nerol can substantially 10 parts, 11 The range of both any composition in part, 12 parts, 13 parts, 14 parts, 15 parts or these parts by weight;Dihydrojasmonate can be substantially It is in 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts or these parts by weight any two The range of person's composition;Cis-jasmone can be both any in substantially 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts or these parts by weight The range of composition;Citral can in substantially 1 part, 2 parts, 3 parts, 4 parts, 5 parts or these parts by weight both any composition range; And limonene can substantially 30 parts, 31 parts, 32 parts, 33 parts, 34 parts, 35 parts, 36 parts, 37 parts, 38 parts, 39 parts, 40 parts or these The range of both any composition in parts by weight.
Flavour compositions are additive, and when making an addition in electronic cigarette liquid, the electronic cigarette liquid can be made, which to allow when in use, to be made User generates the sense of taste and nasal receptor of lemon and black tea flavor.
In some embodiments, weight of the flavour compositions in the electronic cigarette liquid is with the electronic cigarette liquid gross weight Meter substantially, for example, 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9%, 1.0% or this The range of both any composition in a little weight percent.In some embodiments, the flavour compositions are in electronic cigarette liquid Parts by weight are roughly about 0.1% to about 1.0%, so that its aerosol taste generated is mild, to optimize user's experience.
Electronic cigarette liquid also includes base solvent, wherein the base solvent includes propylene glycol and glycerine (glycerol).One In a little embodiments, with the total restatement of the electronic cigarette liquid, weight of the propylene glycol in electronic cigarette liquid substantially, for example, 15%, 20%, 25%, 30%, 35%, 40%, 50%, 60%, 70% or these weight percent in both any composition range; And weight of the glycerine in electronic cigarette liquid is substantially, for example, 30%, 35%, 40%, 45%, 50%, 55%, 60%, 65%, 70% or these weight percent in both any composition range.In some embodiments, the propylene glycol is in electronics Weight in tobacco juice is about 20% to about 60%, and weight of the glycerine in electronic cigarette liquid is about 40% to about 70%, So that electronic cigarette liquid reaches optimal atomizing effect, user's experience is improved.
It will be understood by those skilled in the art that base solvent can select this field any of molten according to specific requirements Agent, for example, deionized water, propylene glycol, glycerine, and be not limited except as.
In some embodiments, the electronic cigarette liquid further comprises coolant agent.
Coolant agent is additive, for impression and the stimulation that can make product that user be allowed to generate cooling effect when in use The not strong chemicals of property.In some embodiments, the coolant agent includes selected from by menthol, menthones, isomenthone, lactic acid L- menthyl ester, WS-23 (N, 2,3- trimethyl -2- butanamide), WS-3 (N- ethyl-is to menthyl -3- formamide), (N- (4- methoxyphenyl)-is to menthyl -3- carboxylic acyl by WS-5 (N- (ethoxycarbonylmethyl group)-is to alkane -3- formamide), WS-12 Amine) and combinations thereof composed by group.
In some embodiments, with the total restatement of the electronic cigarette liquid, weight of the coolant agent in electronic cigarette liquid is substantially For for example, 0.1%, 0.2%, 0.3%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5%, 5%, 10% or these weight hundred Divide the range of both any composition in ratio.In some embodiments, weight of the coolant agent in electronic cigarette liquid is with the electricity Sub- tobacco juice gross weight is calculated as about 1.0% to about 10%, to improve the electronic cigarette liquid aerosol generated for user's sucking Mouthfeel.
In some embodiments, the electronic cigarette liquid further includes nicotine salt.In some embodiments, with the electronic cigarette The total restatement of liquid, weight of the nicotine salt in electronic cigarette liquid in the electronic cigarette liquid substantially, for example, 0.1%, 0.2%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5%, 5%, 7.5%, 10% or these weight percent in it is both any The range of composition.In some embodiments, weight of the nicotine salt in the electronic cigarette liquid is total with the electronic cigarette liquid Restatement is about 1.8% to about 10.0%.
In some embodiments, the electronic cigarette liquid further includes nicotine.In some embodiments, with the electronic cigarette liquid Total restatement, weight of the nicotine in electronic cigarette liquid in the electronic cigarette liquid substantially, for example, 0.1%, 0.2%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5%, 5% or these weight percent in both any composition range.Some In embodiment, weight of the nicotine in the electronic cigarette liquid is calculated as about 0.9% to about with the electronic cigarette liquid gross weight 5.0%.
In some embodiments, the electronic cigarette liquid further comprises essence, wherein the essence is selected from by Isosorbide-5-Nitrae-folium eucalypti Element, australene, α-terpinene, nopinene, α-phellandrene, laurene, alpha, beta-lonone, benzyl alcohol, benzaldehyde, benzyl carbinol, fourth (1- is p- for fragrant phenol, FoxleneAlkene -8- mercaptan), linalool, n-hexyl alcohol, glyceryl triacetate, terpinyl formate, citronellol, perfume (or spice) Group composed by leaf-alcohol, leaf-alcohol and combinations thereof.
In some embodiments, weight of the essence in the electronic cigarette liquid is calculated as about with the electronic cigarette liquid gross weight 0.01% to about 5.0%, to increase the flavor of the electronic cigarette liquid and optimize the mouthfeel of its aerosol generated.
According to some embodiments of the application, the application provides the preparation method of electronic cigarette liquid, and it includes following steps: by wind The special ratios mixing in range that each composition in taste composition is provided by embodiment, be then added essence, nicotine salt and Then coolant agent is added into basic tobacco juice, mix it uniformly to obtain electronic cigarette liquid.
According to further aspect of the application, the application provides a kind of atomising device, and it includes any of the above-described embodiment institutes The electronic cigarette liquid stated.The electronic cigarette liquid can be atomized the aerosol for generating and sucking for user by the atomising device.
In some embodiments, the atomising device includes electronic cigarette, ultrasonic atomizer or net formula atomizer.
Embodiment
To facilitate a better understanding of the application, it is illustrated by the following examples.These examples belong to the protection of the application Range, but the protection scope of the application is not limited.
The preparation of basic tobacco juice:
By propylene glycol and glycerine by being uniformly mixed after following weight ratio (35:55) allotment, to obtain basic tobacco juice.
The preparation of essence:
According to the weight ratio configuration in the following table 1, mix to obtain essence.
Embodiment 1
By alpha-terpineol, γ-terpinene, nerol, dihydrojasmonate, cis-jasmone, citral and lemon Alkene is mixed by following weight ratio (19:4:12:22:7:2:36) allotment to obtain flavour compositions, then by 0.2 gram of flavor group In the basic tobacco juice for closing 99.8 grams of object addition, stirs evenly, obtain electronic cigarette liquid.
Embodiment 2
By alpha-terpineol, γ-terpinene, nerol, dihydrojasmonate, cis-jasmone, citral and lemon Alkene is mixed by following weight ratio (19:4:12:22:7:2:36) allotment to obtain flavour compositions, then by 0.2 gram of flavor group It closes after object, 3.0 grams of nicotine, 2.2 grams of benzoic acid, 1.2 grams of WS-23 are mixed with 0.9 gram of menthol and is added 92.5 grams Basic tobacco juice in, stir evenly, obtain electronic cigarette liquid.
Embodiment 3
By alpha-terpineol, γ-terpinene, nerol, dihydrojasmonate, cis-jasmone, citral and lemon Alkene is mixed by following weight ratio (19:4:12:22:7:2:36) allotment to obtain flavour compositions, then by 0.2 gram of flavor group It is mixed to close object, 3.0 grams of nicotine, 2.2 grams of benzoic acid, 1.2 grams of WS-23,0.9 gram of menthol and 0.25 gram of essence I It is added after conjunction in 92.25 grams of basic tobacco juice, stirs evenly, obtain electronic cigarette liquid.
Embodiment 4
By alpha-terpineol, γ-terpinene, nerol, dihydrojasmonate, cis-jasmone, citral and lemon Alkene is mixed by following weight ratio (15:4.5:12:23:7.5:3:35) allotment to obtain flavour compositions, then by 0.3 gram of wind Taste composition, 3.0 grams of nicotine, 3.0 grams of benzoic acid, 1.7 grams of WS-23,1.2 grams of menthol and 0.35 gram of essence It is added after II mixing in 90.5 grams of basic tobacco juice, stirs evenly, obtain electronic cigarette liquid.
The composition of essence is as shown in table 1 below in above-described embodiment.
Table 1
After the completion of the electronic cigarette liquid of above-described embodiment 1-4, mouth feel score test is then carried out.
Mouth feel score test method 1
Please 20 evaluation and analysis persons the electronic cigarette aerosol experience of above-described embodiment 1-4 is beaten by each evaluation index in table 2 Point.Evaluation result as shown in table 3 below
Table 2
Table 3
Evaluation index Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4
Flue gas exquisiteness degree 4.2 4.4 4.5 4.4
Fragrance is self-consistent, no segmentation or tomography 4.4 4.4 4.5 4.6
Flue gas and flavor concentration 4.3 4.2 4.3 4.2
Fragrance is rich, the long degree of flue gas 4.0 4.1 4.3 4.5
The sweet degree of mouthfeel, sense of promoting the production of body fluid 4.0 4.5 4.7 4.7
Irritation and burning sensation 4.5 4.8 4.7 4.6
Oral cavity clean level after suction 4.5 4.6 4.8 4.9
Whether there is or not bad breaths 3.8 4.0 4.5 4.6
Hit larynx sense 3.7 4.0 4.1 4.2
The reduction degree and identification of fragrance 4.6 4.7 4.8 4.8
Mouth feel score test mode 2;
Statistical method: randomly select 1000 users is made by electronic cigarette liquid of the electronic cigarette to above-described embodiment 1-4 With test, its taste and mouthfeel are evaluated after test to be used, in terms of wherein evaluation criterion is divided by total score 10, taste it is better or The more good then score of mouthfeel is higher.
Test result is as follows shown in table 4 by mouth feel score test for the electronic cigarette liquid of embodiment 1-4.
Table 4
By data in table 2-4 it is found that the electronic cigarette liquid of the embodiment of the present application 1-4 can be generated after being atomized have lemon and The aerosol for user's sucking of black tea flavor, no matter can effectively promote client's in the performance of mouthfeel or taste Satisfaction.
By the above embodiments of the present application it should be appreciated that this application provides a kind of electronic cigarette liquid, pass through the electronic cigarette liquid In include flavour compositions, user can be allowed to generate the flavor of lemon and black tea, and do not generate tar and suspended particulates etc. Harmful substance.Meanwhile the electronic cigarette liquid is capable of forming the uniform and strong aerosol of smell when user aspirates, and the aerosol mouth Feel submissive and do not have residual sense, to promote user's experience.
Although the specific embodiment for having referred to the application describes and illustrates that the application, these descriptions and instructions are simultaneously unlimited The application processed.Those skilled in the art can be clearly understood from, and not depart from this Shen as defined by the appended patent claims In the case where true spirit please and range, can carry out various changes (such as to the ingredient in the flavour compositions of the application into Row is appropriate to be increased, reduce and changes) so that particular condition, material, material composition, substance, method or process are suitable for the application Target, spirit and scope.All such modifications are intended in this scope of the appended claims.Although having referred to by spy The specific operation that graded executes describes method disclosed herein, it should be appreciated that can be in the teaching for not departing from the application In the case of combine, segment or resequence these operation to form equivalent method.Therefore, unless special instructions herein, otherwise The order of operation and grouping and not this Applicant's Abstract graph limitation.

Claims (11)

1. a kind of flavour compositions, it includes the substances of following parts by weight:
10 to 20 parts of alpha-terpineol, 1 to 5 part of γ-terpinene, 10 to 15 parts of nerol, 15 to 25 parts of dihydro jasmine Ketone acid methyl esters, 5 to 10 parts of cis-jasmone, 1 to 5 part of citral and 30 to 40 parts of limonene.
2. a kind of electronic cigarette liquid, it includes flavour compositions described in claim 1.
3. electronic cigarette liquid according to claim 2, wherein weight of the flavour compositions in the electronic cigarette liquid with The electronic cigarette liquid gross weight is calculated as 0.1% to 1.0%.
4. electronic cigarette liquid according to claim 2 further comprises coolant agent, wherein the coolant agent is selected from by peppermint Brain, menthones, isomenthone, lactic acid l- menthyl ester, WS-23 (N, 2,3- trimethyl -2- butanamide), WS-3 (N- second Base-is to menthyl -3- formamide), WS-5 (N- (ethoxycarbonylmethyl group)-is to alkane -3- formamide), WS-12 (N- (4- methoxyl group Phenyl)-to menthyl -3- carboxylic acid amides) and combinations thereof composed by group.
5. electronic cigarette liquid according to claim 4, wherein weight of the coolant agent in the electronic cigarette liquid is with described Electronic cigarette liquid gross weight is calculated as 1% to 10%.
6. electronic cigarette liquid according to claim 2 further comprises nicotine salt, and the nicotine salt is in the electricity Weight in sub- tobacco juice is calculated as 1.8% to 10.0% with the electronic cigarette liquid gross weight.
7. electronic cigarette liquid according to claim 2 further includes nicotine, and the nicotine is in the electronic cigarette Weight in liquid is calculated as 0.9% to 5.0% with the electronic cigarette liquid gross weight.
8. electronic cigarette liquid according to claim 2 further comprises essence, wherein the essence is selected from by Isosorbide-5-Nitrae-folium eucalypti Element, australene, α-terpinene, nopinene, α-phellandrene, laurene, alpha, beta-lonone, benzyl alcohol, benzaldehyde, benzyl carbinol, fourth Fragrant phenol, Foxlene, linalool, n-hexyl alcohol, glyceryl triacetate, terpinyl formate, citronellol, geraniol, leaf-alcohol and combinations thereof Composed group.
9. electronic cigarette liquid according to claim 8, wherein weight of the essence in the electronic cigarette liquid is with the electricity Sub- tobacco juice gross weight is calculated as 0.01% to 5.0%.
10. a kind of atomising device, it includes any rights in flavour compositions described in claim 1 or claim 2 to 9 to want Seek the electronic cigarette liquid.
11. atomising device according to claim 10, wherein the atomising device includes electronic cigarette, ultrasonic atomizer or net Formula atomizer.
CN201910866656.4A 2019-09-12 2019-09-12 Flavour compositions and electronic cigarette liquid comprising the flavour compositions Pending CN110506979A (en)

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PCT/CN2019/107939 WO2021046917A1 (en) 2019-09-12 2019-09-25 Flavor composition and e-liquid comprising flavor composition

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WO2021128346A1 (en) * 2019-12-27 2021-07-01 深圳雾芯科技有限公司 Flavor composition and electronic cigarette e-liquid containing same

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WO2021128346A1 (en) * 2019-12-27 2021-07-01 深圳雾芯科技有限公司 Flavor composition and electronic cigarette e-liquid containing same

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