CN109846075B - Electronic cigarette liquid with lemon flavor and preparation method thereof - Google Patents

Electronic cigarette liquid with lemon flavor and preparation method thereof Download PDF

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CN109846075B
CN109846075B CN201910005349.7A CN201910005349A CN109846075B CN 109846075 B CN109846075 B CN 109846075B CN 201910005349 A CN201910005349 A CN 201910005349A CN 109846075 B CN109846075 B CN 109846075B
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parts
electronic cigarette
oil
cigarette liquid
lemon
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CN109846075A (en
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丁玉
何书杰
张高峰
陶飞燕
吴志英
胡涛
邓发达
罗诚
黄玉川
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China Tobacco Sichuan Industrial Co Ltd
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China Tobacco Sichuan Industrial Co Ltd
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Abstract

The invention discloses an electronic cigarette liquid with lemon flavor and a preparation method thereof, wherein the electronic cigarette liquid is prepared from the following raw materials in parts by weight: 0.1-10 parts of lemon oil, 0.01-1 part of bergamot oil, 0.01-1 part of lime oil, 0.005-0.25 part of terpineol, 0.005-0.25 part of linalool, 0.001-0.1 part of methyl heptenone, 0.001-0.1 part of octanal, 0.005-0.25 part of geranyl acetate, 1-5 parts of ethanol, 10-30 parts of water, 30-90 parts of propylene glycol and 20-40 parts of glycerol. The electronic cigarette liquid can enrich the smoking flavor of the electronic cigarette, meet the requirements of different consumer groups, and simultaneously effectively reduce the potential harm to the health of consumers.

Description

Electronic cigarette liquid with lemon flavor and preparation method thereof
Technical Field
The invention relates to the technical field of electronic cigarette liquid, in particular to electronic cigarette liquid with lemon flavor and a preparation method thereof.
Background
The direct harm of smoking to smokers and the influence of second-hand smoke on the surrounding environment are increasingly receiving attention from society. The electronic cigarette is a novel tobacco product, and compared with the traditional cigarette, the electronic cigarette does not contain harmful substances such as tar, carbon monoxide and the like, and has less harm to the body of a smoker; in addition, the aerosol formed by atomizing nicotine of the electronic cigarette is quickly diluted in the air, so that the risk of harm to surrounding people is reduced. Electronic cigarettes as a substitute for cigarettes have gained market acceptance worldwide, and sales are on the rising trend year by year.
The electronic cigarette liquid is an important factor influencing the smoking quality. Through the development of several generations, although the electronic cigarettes have the shape, hand feeling, smoke and the like cigarettes, the cigarette liquid used for the electronic cigarettes has some defects. In order to simulate the taste of cigarettes, mainstream electronic cigarettes sold in the market generally adopt tobacco raw material extracts, and then are mixed with tobacco flavors, deionized water and the like to prepare electronic cigarette liquid. The smoke generated by the electronic cigarette liquid can imitate cigarettes to a certain extent, but the released smoke also contains a small amount of harmful substances, smokers generally feel that the fragrance and the taste of the electronic cigarettes do not meet the physiological requirements, the smoking flavor is monotonous, and the health and sustainable development of the electronic cigarettes are greatly influenced by the problems.
Disclosure of Invention
In order to overcome the technical defects, the invention provides the electronic cigarette liquid with the lemon flavor and the preparation method thereof, the electronic cigarette liquid can enrich the smoking flavor of the electronic cigarette and meet the requirements of different consumer groups, and meanwhile, the lemon essential oil has the effects of scavenging free radicals, clearing away heat and toxic materials and the like, has a certain health-care effect and can effectively reduce the potential harm to the health of consumers.
In order to achieve the technical effect, the invention provides an electronic cigarette liquid with lemon flavor, which is prepared from the following raw materials in parts by weight: 0.1-10 parts of lemon oil, 0.01-1 part of bergamot oil, 0.01-1 part of lime oil, 0.005-0.25 part of terpineol, 0.005-0.25 part of linalool, 0.001-0.1 part of methyl heptenone, 0.001-0.1 part of octanal, 0.005-0.25 part of geranyl acetate, 1-5 parts of ethanol, 10-30 parts of water, 30-90 parts of propylene glycol and 20-40 parts of glycerol.
The electronic cigarette liquid is prepared from the following raw materials in parts by weight: 0.5-8 parts of lemon oil, 0.05-1 part of bergamot oil, 0.05-1 part of lime oil, 0.005-0.20 part of terpineol, 0.005-0.20 part of linalool, 0.005-0.1 part of methyl heptenone, 0.005-0.1 part of octanal, 0.01-0.25 part of geranyl acetate, 2-5 parts of ethanol, 10-20 parts of water, 40-80 parts of propylene glycol and 20-40 parts of glycerol.
The electronic cigarette liquid is prepared from the following raw materials in parts by weight: 1-8 parts of lemon oil, 0.1-1 part of bergamot oil, 0.1-1 part of lime oil, 0.01-0.20 part of terpineol, 0.01-0.20 part of linalool, 0.01-0.1 part of methyl heptenone, 0.01-0.1 part of octanal, 0.01-0.2 part of geranyl acetate, 2-5 parts of ethanol, 10-15 parts of water, 50-80 parts of propylene glycol and 20-40 parts of glycerol.
The invention also provides a preparation method of the electronic cigarette liquid with the lemon flavor, which comprises the following steps:
fully mixing the following raw materials in parts by weight to obtain the novel electronic cigarette liquid: 0.1-10 parts of lemon oil, 0.01-1 part of bergamot oil, 0.01-1 part of lime oil, 0.005-0.25 part of terpineol, 0.005-0.25 part of linalool, 0.001-0.1 part of methyl heptenone, 0.001-0.1 part of octanal, 0.005-0.25 part of geranyl acetate, 1-5 parts of ethanol, 10-30 parts of water, 30-90 parts of propylene glycol and 20-40 parts of glycerol.
In the invention, the raw materials for providing the lemon aroma mainly comprise lemon oil, bergamot oil and lime oil, wherein the lemon oil is colorless to light yellow volatile essential oil. Has the special fragrance of fresh lemon, and contains limonene, citral, octanal, nonanal, dodecanal, pinene, camphene, linalool, geranyl acetate and neryl acetate as main ingredients.
The bergamot oil has green and sweet fruity fragrance, and is similar to the refreshing feeling of lemon, and the main components of the bergamot oil comprise linalyl acetate, dihydrodill alcohol, linalool, terpineol, nerol, limonene, bergamotol, limonene, pinene, camphene, limonene, phellandrene, citral and bergamol.
Lime oil: colorless to greenish yellow volatile essential oils. Is in orange fragrance, and contains limonene, citral, linalyl acetate, cumyl alcohol, terpineol, eucalyptol, fatty acid, terpenes, aldehydes and alcohols as main ingredients.
The three raw materials are main raw materials forming the lemon flavor, and have certain lemon flavor when used alone, but the lemon flavor is not skilled enough, has no layering sense, and is not rich in aroma. In the application, terpineol and linalool have lilac flavors, methyl heptenone has fresh faint scent, citrus-like smell, caprylic aldehyde has strong fruit fragrance, geranyl acetate has rose and lavender fragrances, and a certain amount of terpineol, linalool, methyl heptenone, caprylic aldehyde, geranyl acetate and other substances are added into three raw materials with lemon flavor to modify and support the fragrances to a certain degree, so that the lemon flavor is skilled and layered, and therefore the lemon flavor has better satisfaction.
Compared with the prior art, the invention has the following beneficial effects: the electronic cigarette liquid prepared by the invention has strong lemon fragrance, enriches the smoking flavor of the electronic cigarette, and can meet the requirements of different consumer groups. Compared with the existing products, the lemon essential oil has the advantages that the fragrance, the taste and the like are greatly improved, the satisfaction of a smoker can be obviously increased, meanwhile, the lemon essential oil has the effects of clearing free radicals, clearing heat and removing toxicity and the like, has a certain health-care effect, and can effectively reduce the potential harm to the health of the consumer.
Detailed Description
Example 1
The electronic cigarette liquid with the lemon flavor comprises the following raw materials in parts by weight: 8 parts of lemon oil, 0.1 part of bergamot oil, 0.5 part of lime oil, 0.01 part of terpineol, 0.03 part of linalool, 0.005 part of methyl heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethanol, 5 parts of water, 60 parts of propylene glycol and 24.322 parts of glycerol.
The preparation method comprises the following steps:
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious lemon fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 1
The raw materials and preparation method are the same as example 1 except that the raw materials do not contain lemon oil.
Example 2
8 parts of lemon oil, 0.05 part of bergamot oil, 0.02 part of lime oil, 0.01 part of terpineol, 0.03 part of linalool, 0.005 part of methyl heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethanol, 5 parts of water, 60 parts of propylene glycol and 24.852 parts of glycerol.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious lemon fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 2
The procedure of example 2 was followed except that the starting materials contained no lime oil.
Example 3
5 parts of lemon oil, 0.05 part of bergamot oil, 0.02 part of lime oil, 0.01 part of terpineol, 0.03 part of linalool, 0.005 part of methyl heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethanol, 5 parts of water, 60 parts of propylene glycol and 27.852 parts of glycerol.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious lemon fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 3
The raw materials and preparation method are the same as example 2 except that the raw materials do not contain bergamot oil.
Example 4
3 parts of lemon oil, 0.05 part of bergamot oil, 0.02 part of lime oil, 0.01 part of terpineol, 0.03 part of linalool, 0.005 part of methyl heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethanol, 5 parts of water, 60 parts of propylene glycol and 29.852 parts of glycerol.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious lemon fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 4
The procedure of example 4 was followed except that the starting materials contained no terpineol.
Example 5
1 part of lemon oil, 0.05 part of bergamot oil, 0.02 part of lime oil, 0.01 part of terpineol, 0.03 part of linalool, 0.005 part of methyl heptenone, 0.003 part of octanal, 0.03 part of geranyl acetate, 2 parts of ethanol, 5 parts of water, 60 parts of propylene glycol and 31.852 parts of glycerol.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious lemon fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 5
The preparation method of the raw materials is the same as that of example 5 except that the raw materials do not contain methylheptenone.
According to the cigarette sensory quality evaluation standard GB5606.4-2005, in combination with the sensory characteristics of electronic cigarettes, 6 evaluation indexes and scores are set according to different weights, see Table 1
Figure BDA0001935222720000051
TABLE 1
Sensory evaluation is carried out on the electronic cigarette liquid obtained in the embodiment 1 to the embodiment 5 and the comparison example 1 to the comparison example 5, an arithmetic mean value is obtained according to evaluation results of various experts according to the evaluation results, a valid number is reserved in the results, and statistical results are shown in a table 2.
Sample (I) Satisfaction feeling Fragrance Tuning by hand Miscellaneous qi Irritation property Aftertaste
Example 1 22.5 20.5 4.5 8.0 16.0 12.5
Example 2 23.0 21.5 4.5 8.5 16.5 13.0
Example 3 23.0 22.0 4.5 8.5 16.5 13.0
Example 4 23.5 22.5 4.5 8.5 17.0 13.5
Example 5 23.0 22.5 4.5 8.5 16.5 13.5
Comparative example 1 20.0 18.5 3.5 7.5 15.0 11.5
Comparative example 2 21.5 19.0 4.0 8.0 15.5 12.0
Comparative example 3 20.5 18.5 4.0 8.0 16.0 12.5
Comparative example 4 21.0 19.5 3.5 7.5 15.5 11.5
Comparative example 5 21.0 18.0 3.5 7.0 15.5 12.0
TABLE 2
Although the present invention has been described herein with reference to the illustrated embodiments thereof, which are intended to be preferred embodiments of the present invention, it is to be understood that the invention is not limited thereto, and that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the spirit and scope of the principles of this disclosure.

Claims (4)

1. The electronic cigarette liquid with the lemon flavor is characterized by being prepared from the following raw materials in parts by weight: 0.1-10 parts of lemon oil, 0.01-1 part of bergamot oil, 0.01-1 part of lime oil, 0.005-0.25 part of terpineol, 0.005-0.25 part of linalool, 0.001-0.1 part of methyl heptenone, 0.001-0.1 part of octanal, 0.005-0.25 part of geranyl acetate, 1-5 parts of ethanol, 10-30 parts of water, 30-90 parts of propylene glycol and 20-40 parts of glycerol.
2. The electronic cigarette liquid with the lemon flavor according to claim 1, wherein the electronic cigarette liquid is prepared from the following raw materials in parts by weight: 0.5-8 parts of lemon oil, 0.05-1 part of bergamot oil, 0.05-1 part of lime oil, 0.005-0.20 part of terpineol, 0.005-0.20 part of linalool, 0.005-0.1 part of methyl heptenone, 0.005-0.1 part of octanal, 0.01-0.25 part of geranyl acetate, 2-5 parts of ethanol, 10-20 parts of water, 40-80 parts of propylene glycol and 20-40 parts of glycerol.
3. The electronic cigarette liquid with the lemon flavor according to claim 2, wherein the electronic cigarette liquid is prepared from the following raw materials in parts by weight: 1-8 parts of lemon oil, 0.1-1 part of bergamot oil, 0.1-1 part of lime oil, 0.01-0.20 part of terpineol, 0.01-0.20 part of linalool, 0.01-0.1 part of methyl heptenone, 0.01-0.1 part of octanal, 0.01-0.2 part of geranyl acetate, 2-5 parts of ethanol, 10-15 parts of water, 50-80 parts of propylene glycol and 20-40 parts of glycerol.
4. The preparation method of the electronic cigarette liquid with the lemon flavor is characterized in that the electronic cigarette liquid with the lemon flavor is obtained by fully mixing the following raw materials in parts by weight: 0.1-10 parts of lemon oil, 0.01-1 part of bergamot oil, 0.01-1 part of lime oil, 0.005-0.25 part of terpineol, 0.005-0.25 part of linalool, 0.001-0.1 part of methyl heptenone, 0.001-0.1 part of octanal, 0.005-0.25 part of geranyl acetate, 1-5 parts of ethanol, 10-30 parts of water, 30-90 parts of propylene glycol and 20-40 parts of glycerol.
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CN110506979A (en) * 2019-09-12 2019-11-29 深圳雾芯科技有限公司 Flavour compositions and electronic cigarette liquid comprising the flavour compositions
CN110819456A (en) * 2019-12-09 2020-02-21 将军烟草集团有限公司 Green lemon essence for bead blasting and application of green lemon essence in cigarettes
CN113243549B (en) * 2021-04-21 2022-04-05 深圳市真味生物科技有限公司 Lemon-flavor essence extracted from plants for electronic atomized liquid and extraction method
CN114680362B (en) * 2021-12-28 2023-03-21 四川三联新材料有限公司 Electronic cigarette liquid with refreshing function
CN115251450A (en) * 2022-08-22 2022-11-01 东莞市鸿馥生物科技有限公司 Bergamot essential oil applied to electronic cigarette and preparation method thereof

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CN103349353A (en) * 2013-06-20 2013-10-16 王晓凯 Novel application of edible fungus
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CN105124750A (en) * 2015-07-27 2015-12-09 浙江中烟工业有限责任公司 Sweet and fragrant electronic cigarette liquid and preparation method thereof
CN108618192A (en) * 2017-03-22 2018-10-09 赖彦君 A kind of 15 are formulated electronic cigarette tobacco tar and preparation method thereof
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