CN110283662B - Ice-feeling tea-flavored essence and application thereof - Google Patents

Ice-feeling tea-flavored essence and application thereof Download PDF

Info

Publication number
CN110283662B
CN110283662B CN201910694259.3A CN201910694259A CN110283662B CN 110283662 B CN110283662 B CN 110283662B CN 201910694259 A CN201910694259 A CN 201910694259A CN 110283662 B CN110283662 B CN 110283662B
Authority
CN
China
Prior art keywords
parts
tea
ice
essence
cigarette
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201910694259.3A
Other languages
Chinese (zh)
Other versions
CN110283662A (en
Inventor
钟家威
张建平
钟洪祥
谢金栋
邓小华
苏明亮
林黎生
陈小明
黄朝章
陈昆焱
邓梅忠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Fujian Industrial Co Ltd
Original Assignee
China Tobacco Fujian Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Fujian Industrial Co Ltd filed Critical China Tobacco Fujian Industrial Co Ltd
Priority to CN201910694259.3A priority Critical patent/CN110283662B/en
Publication of CN110283662A publication Critical patent/CN110283662A/en
Application granted granted Critical
Publication of CN110283662B publication Critical patent/CN110283662B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0003Compounds of unspecified constitution defined by the chemical reaction for their preparation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention relates to an ice tea flavor essence and application thereof. The ice tea flavor essence contains the following aroma components in parts by weight: 3.06-3.74 parts of ice essence; 1.17-1.43 parts of jasmine essence; 0.32 to 0.41 portion of flower fragrance essence; 0.21 to 0.27 portion of tea essence; and 0.05 to 0.08 portion of auxiliary essence. The ice tea flavor essence has pleasant ice feeling and remarkable matcha fragrance.

Description

Ice-feeling tea-flavored essence and application thereof
Technical Field
The invention belongs to the field of essence, and particularly relates to ice-feeling tea-flavor essence and application thereof.
Background
The essence and the spice are widely applied to the fields of tobacco, food, daily chemicals and the like. In the tobacco field, the essence and the spice not only can endow the cigarette products with unique style characteristics, but also can improve the taste of the cigarettes. The international tobacco industry highly attaches importance to the development and application of flavors and fragrances, and the technology for producing and applying high-quality flavors and fragrances is taken as the core technology of the international tobacco industry.
The matcha is tea powder with smaller particle size, which is prepared by taking high-quality fresh tea leaves as raw materials and adopting the technologies of steaming, rolling, drying and the like, has natural and green appearance, reserves more than 500 components in the tea leaves, has the advantages of drinking and eating the tea, and has higher nutritional value and health care value than the tea leaves. The traditional Chinese matcha has been used for more than one thousand years, but unfortunately, the traditional Chinese matcha is not popular since the Ming dynasty, but the traditional Chinese matcha is lost after the tea is used, soup is brewed and drunk and tea residues are discarded, so that the historical deputy is formed.
Disclosure of Invention
The inventor finds that by reasonably compounding ice essence, jasmine essence, flower fragrance essence, tea essence and auxiliary essence, the essence with pleasant 'ice feeling' and remarkable 'green tea fragrance' characteristics can be obtained.
Based on the above findings, the present invention provides the following aspects:
the invention provides an ice tea flavor essence which comprises the following aroma components in parts by weight:
3.06-3.74 parts of ice essence;
1.17-1.43 parts of jasmine essence;
0.32 to 0.41 portion of flower fragrance essence;
0.21 to 0.27 portion of tea essence;
0.05 part to 0.08 part of auxiliary essence;
wherein,
the ice essence is selected from one or more of peppermint oil, menthol, menthone and menthyl acetate;
the jasmine essence is selected from one or more of jasmine essential oil, methyl dihydrojasmonate, jasmone and phenethyl alcohol;
the floral essence is selected from one or more of geranium oil, bergamot oil, hexanoic acid leaf alcohol ester, alpha-ionone and alpha-damascenone;
the tea-flavored essence is selected from one or more of linalool, tea-scented ketone, indole, benzyl alcohol, tea-scented spirane, and Tieguanyin tea leaf essential oil;
the auxiliary essence is one or more selected from dihydroactinidiolide, gamma-caprolactone and peru extract.
In some embodiments, the ice-tea flavourant further comprises a solvent.
In some embodiments, the solvent is selected from one or more of propylene glycol, water, and ethanol.
In some embodiments, the ice tea flavor includes 4 to 6 parts by weight of a fragrant component and 94 to 96 parts by weight of a solvent.
In some embodiments, the ice tea flavor comprises the following ingredients:
0.45-0.55 part of peppermint oil;
1.8-2.2 parts of menthol;
0.36-0.44 parts of menthone;
0.45-0.55 part of menthyl acetate;
0.18-0.22 part of jasmine essential oil;
0.36-0.44 parts of methyl dihydrojasmonate;
0.27-0.33 part of cis-jasmone;
0.36-0.44 parts of phenethyl alcohol;
0.09-0.11 part of geranium oil;
0.18-0.22 part of bergamot oil;
0.045-0.055 part of hexanoic acid leaf alcohol ester;
0.009-0.011 part of alpha-ionone;
0.0045-0.0055 part of alpha-damascenone;
0.09-0.11 part of linalool;
0.045-0.055 parts of tea scented ketone;
0.018-0.022 parts of indole;
0.045-0.055 part of benzyl alcohol;
0.009-0.011 part of tea-scented spirane;
0.009-0.011 part of Tieguanyin tea essential oil;
0.036-0.044 parts of dihydroactinidiolide;
0.018-0.022 parts of gamma-caprolactone; and
0.0045-0.0055 part of Peru extract.
In some embodiments, the ice tea flavor further comprises:
47.6-48.1 parts of propylene glycol;
13.1-14.3 parts of water; and
32.9-33.3 parts of ethanol.
In a second aspect the invention provides the use of an ice-tasting tea flavour according to any of the invention in the manufacture of a smoking article.
In some embodiments, the smoking article comprises: burning cigarettes, heating non-burning cigarettes or electronic cigarettes.
In some embodiments, the ice-tea flavourant is applied to one or more of the following in the preparation of the smoking article: cut tobacco, thin sheets, cigarette paper, cigarette lining paper, filter sticks and electronic cigarette liquid.
In a third aspect, the invention provides a smoking article comprising an ice tea flavour according to any one of the invention.
In some embodiments, the smoking article comprises one or more of: burning cigarettes, heating non-burning cigarettes, electronic cigarettes.
In a preferred embodiment, the ice tea flavour of any one of the present invention is applied in a proportion of 0.01-0.1% by weight of the cut tobacco in the tobacco product.
In a preferred embodiment, the ice tea flavor is added as a cigarette (burning cigarette or heating non-burning cigarette) additive in the following way: the ice tea flavor essence is uniformly sprayed on the tobacco shreds according to 1 percent of the weight of the tobacco shreds to prepare the cigarette.
In some aspects, a preparation method of ice tea flavor is provided, which comprises the following steps:
1) obtaining raw materials according to a formula;
2) putting menthol, peru extract, tea spirane and Tieguanyin tea essential oil into a closed container, adding water, placing on an ultrasonic oscillator, and carrying out ultrasonic treatment under the condition of water bath at 6-10 ℃ until all components are uniformly mixed;
3) and adding the rest raw material components in the formula into the product obtained in the last step, and stirring uniformly under the water bath condition of 5-10 ℃.
The term "ice feel" refers to the cooling sensation imparted to the flavor by peppermint oil, menthol, menthone, menthyl acetate, or a combination thereof, including a cooling olfactory sensation and/or a cooling gustatory sensation.
The term "burning cigarette" refers to a type of tobacco product in which the cigarette remains lit during use.
The term "heated non-burning cigarette" refers to a type of tobacco product in which the cigarette remains heated but not lit during use.
The term "electronic cigarette" refers to a type of tobacco product that, when in use, generates an aerosol by atomizing an electronic cigarette liquid.
The essence or the cigarette has the following beneficial effects:
1) the matcha has obvious faint scent;
2) has pleasant cool feeling, namely 'ice feeling'.
3) After the essence is used for tobacco products, the special ice feeling is achieved, and the matcha fragrance, the flower fragrance and the tobacco fragrance are coordinated, so that satisfactory smoking feeling is obtained;
4) the essence is harmonious with the smoke of the cigarette, and has no smell of wood gas, earthy smell and the like, and no stimulation and dry feeling of mouth, nose and throat;
5) the essence has moderate volatility, can stably exist in the cigarettes before the cigarettes are combusted, and can migrate along with the smoke when the cigarettes are combusted;
6) the essence, the essence thermal cracking product and the essence combustion product can meet the requirement of safe smoking.
Detailed Description
The technical solution of the present invention is further described in detail by the following examples. The exemplary embodiments of the present invention and the description thereof are provided for the purpose of explanation and are not to be construed as limiting the invention.
The fragrances described in the examples are provided by the tobacco industry, llc in fujian.
Examples 1 to 3 and comparative examples 1 to 3
The ice tea flavor of examples 1 to 3 were numbered A1 to A3.
The ice tea flavor of comparative examples 1 to 3 were numbered B1 to B3.
The raw material formula of the ice tea flavor essence is shown in table 1.
The preparation method of the essence comprises the following steps:
1) obtaining raw materials according to a formula;
2) placing menthol, Peru extract, tea spirane, and Tieguanyin tea essential oil in a sealed container, adding water, placing on an ultrasonic oscillator, and performing ultrasonic treatment in water bath at 8 deg.C until the components are mixed uniformly;
3) adding the rest raw materials into the product of the last step, and stirring uniformly by using a spiral stirrer under the condition of water bath at 7 ℃ to obtain the ice tea flavor essence;
4) storing at 5 ℃ for later use.
Figure BDA0002148847980000061
Figure BDA0002148847980000071
Figure BDA0002148847980000081
Fragrance smelling test:
the fragrance smelling judgment is carried out on the matcha flavor note and the fragrance holding capacity of the A1-A3 and B1-B3 ice tea flavor essence in the table 1, and the specific judgment result is shown in the table 2:
TABLE 2 judgment results of aroma smelling of ice tea flavor
Figure BDA0002148847980000091
As can be seen from Table 2, the matcha flavor note and the aroma-holding capacity of the A1-A3 ice-feeling tea flavor are better than those of B1-B3. The B1-B3 essence is separated from the formula of the ice tea essence, and the green tea flavor note and the fragrance lasting are poor.
Cigarette aroma/smoking evaluation test:
respectively applying the A1-A3 and the B1-B3 ice tea flavor essence to the tobacco shreds with the application amount of 0.2 percent, and preparing the cigarette. Obtaining cigarette samples with the numbers of A1-A3 and B1-B3.
A blank solvent (propylene glycol: water: ethanol: 47.6: 14.3: 33.3 by mass) was added to the tobacco shreds in an amount of 0.2%, and cigarettes were prepared. A blank sample was obtained.
I. The cigarette aroma characteristic evaluation (cigarette aroma test) is carried out on the cigarette samples A1-A3 and B1-B3 and the blank samples, and the specific evaluation results are shown in Table 3:
TABLE 3 evaluation results of cigarette aroma characteristics
Figure BDA0002148847980000092
As can be seen from Table 3, the matcha flavor characteristics of the A1-A3 cigarettes were all stronger than those of the B1-B3 cigarettes and the blank samples. The B1-B3 essence is separated from the formula of the ice tea essence, and the matcha taste has poor characteristic expression.
II, cigarette sensory quality evaluation is carried out on blank cigarette samples and cigarette samples A1-A3 and B1-B3 according to the national standard GB5606.4-2005, and the evaluation results are shown in Table 4.
TABLE 4 cigarette sensory quality evaluation results
Figure BDA0002148847980000101
As can be seen from Table 4, the sensory quality scores of the A1-A3 cigarette samples are higher than those of the B1-B3 cigarette samples and the blank cigarette samples.
The smoking feeling of the A1-A3 cigarette samples is as follows: has outstanding 'ice feeling' and 'matcha flavor'. The ice feeling, the matcha fragrance, the flower fragrance and the cigarette fragrance are coordinated, and the satisfactory smoking feeling is obtained. The essence is harmonious with cigarette smoke, and has no smell of wood gas, earthy smell and the like, and no irritation and dry feeling to mouth, nose and throat. In addition, the essence of the A1-A3 cigarette sample has moderate volatility, can stably exist in the cigarette before the cigarette is burnt, and can migrate along with the smoke when the cigarette is burnt. In addition, the essence, thermal cracking products and combustion products of the A1-A3 cigarette sample can meet the smoking safety requirement.
The B1-B3 essence is separated from the formula of the ice tea essence, the sensory quality scores of the cigarette samples B1-B3 are low, the excellent matcha fragrance is not reflected, and the whole fragrance is not harmonious.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the present invention and not to limit it; although the present invention has been described in detail with reference to preferred embodiments, those skilled in the art will understand that: modifications to the specific embodiments of the invention or equivalent substitutions for parts of the technical features may be made; without departing from the spirit of the present invention, it is intended to cover all aspects of the invention as defined by the appended claims.

Claims (7)

1. The ice tea flavor essence comprises the following components in parts by weight:
0.45-0.55 part of peppermint oil;
1.8-2.2 parts of menthol;
0.36-0.44 parts of menthone;
0.45-0.55 part of menthyl acetate;
0.18-0.22 part of jasmine essential oil;
0.36-0.44 parts of methyl dihydrojasmonate;
0.27-0.33 part of cis-jasmone;
0.36-0.44 parts of phenethyl alcohol;
0.09-0.11 part of geranium oil;
0.18-0.22 part of bergamot oil;
0.045-0.055 part of hexanoic acid leaf alcohol ester;
0.009-0.011 part of alpha-ionone;
0.004-0.0055 part of alpha-damascenone;
0.09-0.11 part of linalool;
0.045-0.055 parts of tea scented ketone;
0.018-0.022 parts of indole;
0.045-0.055 part of benzyl alcohol;
0.009-0.011 part of tea-scented spirane;
0.009-0.011 part of Tieguanyin tea essential oil;
0.036-0.044 parts of dihydroactinidiolide;
0.018-0.022 parts of gamma-caprolactone;
0.0044-0.0055 part of Peru extract;
47.6-48.1 parts of propylene glycol;
13.15-14.28 parts of water; and
32.9-33.3 parts of ethanol.
2. Use of the ice tea flavour of claim 1 in the manufacture of a tobacco product.
3. Use according to claim 2, the tobacco product comprising: burning cigarettes or heating non-burning cigarettes.
4. Use according to claim 2, wherein the ice tea flavour is applied to one or more of the following in the preparation of a smoking article: tobacco shreds, sheets, cigarette paper, cigarette lining paper and filter sticks.
5. A tobacco product comprising the ice tea flavor of claim 1.
6. A smoking article according to claim 5, comprising one or more of: burning cigarette, heating non-burning cigarette.
7. A method of preparing the ice tea flavour of claim 1 comprising the steps of:
1) obtaining raw materials according to a formula;
2) putting menthol, peru extract, tea spirane and Tieguanyin tea essential oil into a closed container, adding water, placing on an ultrasonic oscillator, and carrying out ultrasonic treatment under the condition of water bath at 6-10 ℃ until all components are uniformly mixed;
3) and adding the rest raw material components in the formula into the product obtained in the previous step, and stirring uniformly under the water bath condition of 5-10 ℃.
CN201910694259.3A 2019-07-30 2019-07-30 Ice-feeling tea-flavored essence and application thereof Active CN110283662B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910694259.3A CN110283662B (en) 2019-07-30 2019-07-30 Ice-feeling tea-flavored essence and application thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910694259.3A CN110283662B (en) 2019-07-30 2019-07-30 Ice-feeling tea-flavored essence and application thereof

Publications (2)

Publication Number Publication Date
CN110283662A CN110283662A (en) 2019-09-27
CN110283662B true CN110283662B (en) 2022-08-02

Family

ID=68024353

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910694259.3A Active CN110283662B (en) 2019-07-30 2019-07-30 Ice-feeling tea-flavored essence and application thereof

Country Status (1)

Country Link
CN (1) CN110283662B (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3996505A4 (en) * 2019-10-08 2023-08-02 Bedoukian Research, Inc. Synergistic formulations for control and repellency of biting arthropods
EP3996506A4 (en) * 2019-10-08 2023-08-02 Bedoukian Research, Inc. Formulations for control and repellency of biting arthropods
CN111000288A (en) * 2019-12-30 2020-04-14 福建中烟工业有限责任公司 Gel for cigarettes and tobacco products
CN113372994A (en) * 2021-07-23 2021-09-10 广州芬豪香精有限公司 Preparation method of cool essence
WO2023089938A1 (en) * 2021-11-18 2023-05-25 日本たばこ産業株式会社 Fragrance composition

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105231479A (en) * 2015-10-21 2016-01-13 河南中烟工业有限责任公司 Faint scent tobacco essence and application
CN105962426A (en) * 2016-07-29 2016-09-28 福建中烟工业有限责任公司 Composition containing Tie Guanyin tea extracts and electronic cigarette fluid
CN107629876A (en) * 2017-10-31 2018-01-26 鹰潭中投科技有限公司 Improve flavouring essence for tobacco and its preparation and the application of reconstituted tobacco cigarette quality

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0568526A (en) * 1991-09-12 1993-03-23 T Hasegawa Co Ltd Preparation of extract for tobacco flavoring
CN105286080B (en) * 2015-11-12 2021-05-28 贵州中烟工业有限责任公司 Buccal smokeless tobacco product and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105231479A (en) * 2015-10-21 2016-01-13 河南中烟工业有限责任公司 Faint scent tobacco essence and application
CN105962426A (en) * 2016-07-29 2016-09-28 福建中烟工业有限责任公司 Composition containing Tie Guanyin tea extracts and electronic cigarette fluid
CN107629876A (en) * 2017-10-31 2018-01-26 鹰潭中投科技有限公司 Improve flavouring essence for tobacco and its preparation and the application of reconstituted tobacco cigarette quality

Also Published As

Publication number Publication date
CN110283662A (en) 2019-09-27

Similar Documents

Publication Publication Date Title
CN110283662B (en) Ice-feeling tea-flavored essence and application thereof
KR101742249B1 (en) Filter containing built-in capsule, cigarette provided with filter and cigarette substitute provide with filter
CN106174683B (en) A kind of composition and the tobacco juice for electronic smoke containing said composition
CN105249524A (en) Fragrance type heating nonflammable tobacco product and preparation method thereof
CN103923747B (en) Essence on cigarette tissue
CN102349699A (en) Preparation method for electronic cigarette liquid
CN103266014B (en) Spicy sweet flue-cured tobacco essence and application thereof
CN102002440A (en) Essence for tonka bean odor type cigarettes
CN107586616A (en) One grows tobacco with tea perfume essence
CN110771947A (en) Spice functional module for cigarette thickening and increasing
CN108618192A (en) A kind of 15 are formulated electronic cigarette tobacco tar and preparation method thereof
CN110295088B (en) Cumquat-flavored essence and application thereof
CN111329103B (en) Electronic cigarette spice composition with Tie Guanyin tea aroma characteristics, electronic cigarette liquid and application of electronic cigarette spice composition and electronic cigarette liquid
JP5771697B2 (en) Method for enhancing useful components of flavor for tobacco products, tobacco materials, cigarettes and cigars
KR101332596B1 (en) Manufacturing method of electronic cigarette liquid
JP5235044B1 (en) Capsule built-in filter, cigarettes with this filter, and tobacco substitutes
CN102304427A (en) Formula of fresh and sweet tobacco flavoring essence
CN110295087B (en) Hami melon essence and application thereof
EP2888951A1 (en) Product comprising kratom
CN111000288A (en) Gel for cigarettes and tobacco products
CN109234011A (en) A kind of fragrance-enhancing tobacco agent containing sage clary oil
CN106675784A (en) Charging essence for embellishing aroma style cigarettes
CN111671133A (en) Tea-flavored flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid
CN105686084A (en) Manufacturing method of cigarette aromatic flavoring rods
CN111269753A (en) Essence, cigarette leaf group formula and application of essence and cigarette leaf group formula in tobacco products

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant