CN107034021A - A kind of cigarette quick-fried pearl savory essence of lily and its application in cigarette - Google Patents
A kind of cigarette quick-fried pearl savory essence of lily and its application in cigarette Download PDFInfo
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- CN107034021A CN107034021A CN201710287955.3A CN201710287955A CN107034021A CN 107034021 A CN107034021 A CN 107034021A CN 201710287955 A CN201710287955 A CN 201710287955A CN 107034021 A CN107034021 A CN 107034021A
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- cigarette
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- fried pearl
- lily
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention belongs to cigarette filter rod production technical field, and in particular to a kind of cigarette quick-fried pearl savory essence of lily and its patent application of the application in cigarette.The savory essence of lily is made up of Bulbus Lilii extract, rhodinol, linalool, benzyl carbinol, geranium oil, Glycerin, mixed triester with caprylic acid capric acid.The quick-fried pearl of lily taste cigarette can be prepared using the essence, the quick-fried pearl can be added in filter stick and the quick-fried pearl cigarette application of cigarette is prepared.The application is by providing a kind of savory essence of lily for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried pearl production technology, Forming Quality stabilization, the uniform quick-fried pearl product of cigarette can be prepared, the quick-fried pearl is inserted after cigarette filter, the excitant of cigarette can preferably be weakened, improve and abundant cigarette flavor, the fragrance that is obviously improved cigarette is rich, the interest of aesthetic quality and suction, thus has preferable application value and popularization and application meaning for design, exploitation and the production and sales of quick-fried pearl cigarette.
Description
Technical field
The invention belongs to cigarette filter rod production technical field, and in particular to a kind of quick-fried pearl of cigarette with lily it is savory essence and its
The patent application of application in cigarette.
Background technology
In traditional cigarette perfuming technology, spice liquid is mainly added in pipe tobacco by it, and the feed liquid that this mode is added is past
Toward meeting, partition losses fall during cigarette burning, simultaneously because the reaction of complex material system is difficult to be expected under high temperature, part
Feed liquid can also produce some bad organoleptic effects.Quick-fried pearl perfuming, being capable of necessarily journey as a kind of emerging perfuming cigarette mode
The defect in existing perfuming mode is overcome on degree, its main cause is：Include spices in quick-fried pearl, suck before cigarette, consumer
The first choice quick-fried pearl being contained in filter stick of crumbing burns and sucks cigarette again, and now flue gas is through together acting on and disappearing with quick-fried pearl feed liquid during filter tip
Fei Zhe, so that completing perfuming mends fragrant process；On the one hand this mode can be prevented effectively from feed liquid of the spices during result of combustion of tobacco
Loss, on the other hand, because spices is placed in sealed quick-fried pearl, thus will not be lost, so that really during cigarette is stored
The stabilization of cigarette quality is protected.
" quick-fried pearl ", due to the special delivery mode of its inclusion, is being supplemented, changed as a kind of emerging material in cigarette
Function in terms of kind, coordination smoking property of cigarette quality and lifting, change, cigarette product style is increasingly protruded, and improves cigarette
The interest of suction and aesthetic quality, thus " quick-fried pearl " cigarette is obtaining increasing in Chinese-style cigarette production in recent years
Using also obtaining liking for consumers in general.
In the prior art, although there is the fragrance in a number of quick-fried pearl cigarette, this quick-fried pearl in the market
Because lack of targeted is designed, thus it is relatively poor with flue gas harmony, and the odor characteristic influence on cigarette in itself is larger, because
And have impact on quick-fried pearl cigarette suck impression.
" quick-fried pearl ", although cigarette occurs like the mushrooms after rain, is due to its product relative new, current production standard and
Specification is relative to be lacked, so that the addition of " quick-fried pearl " and use also occur in that many new problems.Especially for cigarette
For the particularity of product, the design of composition formula is included " quick-fried pearl ", inclusion stability discharges, and " quick-fried pearl " filter stick is for cigarette
Rare report in terms of physical index, chemical index, the influence of harm sex index.Therefore " the quick-fried pearl " of different constituents is designed
Inclusion, systematization research " quick-fried pearl " Special inclusion release rule, " quick-fried pearl " inclusion refers to cigarette physical index, flue gas
There is important theory and application value in terms of mark, the influence of harm sex index.
The content of the invention
Present invention aims at a kind of savory essence of lily being targetedly used in cigarette filter rod is provided, so that abundant volume
Smoke product type, to provide the cigarette product of different-style feature.
Details are as follows for the technical scheme that the application is taken.
A kind of cigarette quick-fried pearl savory essence of lily, is calculated in mass percent, composed of the following components：
5.0 ~ 10.0% Bulbus Lilii extract,
1.0 ~ 3.0% rhodinol,
2.0 ~ 5.0% linalool,
8.0 ~ 12.0% benzyl carbinol,
4.0 ~ 8.0% geranium oil,
62.0 ~ 80.0% Glycerin, mixed triester with caprylic acid capric acid.
The Bulbus Lilii extract is the ethanol extract of lily；
The Glycerin, mixed triester with caprylic acid capric acid is medium chain triglyceride (MCT), for the aliphatic acid containing 8-12 carbochain and glycerine esterification
Product.
The Bulbus Lilii extract, specifically refers to following steps and prepares：
（1）After dried lily is crushed, 45 ~ 55 mesh sieves are crossed, lily root flour is prepared；
（2）To step（1）Lily root flour in add the ethanol solution of volume fraction 65 ~ 85%, water-bath heat backflow 4 at 60 ~ 80 DEG C ~
6h；The solid-liquid ratio of lily root flour and ethanol solution is, lily root flour：Ethanol=1g：4~6mL；
（3）By step（2）It is unchanged that middle hot phegma is concentrated under reduced pressure into volume under the conditions of 55 ~ 65 DEG C, 65 ~ 75Kpa, institute
It is Bulbus Lilii extract to obtain extract.
The cigarette quick-fried pearl savory essence of lily, specific formula is, for example,：7.0% Bulbus Lilii extract, 2.0% rose
Alcohol, 3.5% linalool, 10.50% benzyl carbinol, 6.0% geranium oil and 71.0% Glycerin, mixed triester with caprylic acid capric acid.
It is to be understood that different essence are different according to purposes, it, which is formulated, is generally particular design, described herein hundred
Close savory essence be with reference to the quick-fried pearl of cigarette production technology characteristic, while according in final cigarette purposes carry out particular design, from
And regulation flue gas mass can be preferably realized on quick-fried pearl quality base is ensured, improves the result of cigarette sucking quality.
Using the quick-fried pearl of the cigarette with lily it is savory essence prepared by the quick-fried pearl of lily taste cigarette, the quick-fried pearl of cigarette refer to use
Natural macromolecular material or synthesis high polymer material, essence and flavoring agent is wrapped among a closed quick-fried pearl, formed it is a kind of with
Essence content is 20 ~ 25 μ L/ in the quick-fried pearl of sealing of circular different colours in the majority, a diameter of 2.0 ~ 4.0mm of quick-fried pearl, quick-fried pearl
Grain；Specifically for example：The quick-fried a diameter of 3.65mm of pearl, weight are 23mg/；Essence content is 23 μ L/ in quick-fried pearl, in a word, and it has
Body specification can be adjusted according to machinery equipment difference and institute using filter stick specification difference；
Application of the quick-fried pearl of lily taste cigarette in cigarette, the quick-fried pearl of cigarette is made an addition in filter stick, is made an addition to common（Circumference
24.3mm）In cigarette filter rod, it is preferably disposed in the middle part of cigarette filter rod, i.e. quick-fried pearl position is apart from lip end 12.5mm or so place, often
Branch cigarette can add a quick-fried pearl.
The quick-fried pearl of cigarette has obvious draft fragrant with the savory essence of lily provided in the application, and these fragrance are cigarette cigarettes
Most important note feature in gas；It is prepared into " quick-fried pearl " product form and applied to after cigarette, product are inhaled result and shown：Compare
In control sample, after the quick-fried pearl cigarette smoking of lily taste cigarette, the premise of cigarette smoke aromatic style can not only not changed
Under, and can significantly improve that flue gas fragrance is rich, strengthen the satiety of flue gas by with it is rich, and then improve fragrance with
The harmony of product sensory quality, adds the interest of cigarette smoking；Simultaneously because lily has Yin nourishing and lung moistening, clearing away the heart fire and tranquillizing
The effects such as, so that the application has the effect for mitigating smoking property of cigarette harm to a certain degree.
In general, the savory essence of lily employed in the application, by being obtained to be extracted from natural lily, therefore
These aroma substances can reduce the excitant of flue gas after cigarette smoke is entered, and lift soft roundness degree, the perfume (or spice) of cigarette smoke
Gas richness and plumpness, and then improve its sucking quality and sense organ comfort level.
In a word, the application is by providing a kind of savory essence of lily for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried
Pearl production technology, can prepare Forming Quality stabilization, the uniform quick-fried pearl product of cigarette, the quick-fried pearl is inserted into cigarette filter
Afterwards, it can preferably weaken the excitant of cigarette, improve and abundant cigarette flavor, the fragrance for being obviously improved cigarette is rich, sense organ
Quality and the interest of suction, and due to certain Yin nourishing and lung moistening, clearing away the heart fire and tranquillizing, reducing the effects such as cigarette endangers, thus it is right
There is preferable application value and popularization and application meaning in design, exploitation and the production and sales of quick-fried pearl cigarette.
Embodiment
Explanation is further explained to the present invention with reference to embodiment.Before specific embodiment is introduced, first to following
The preparation process of the quick-fried pearl of cigarette described in embodiment is briefly discussed below.
The main preparation process of the quick-fried pearl of cigarette of prior art is as described below：
The mainstream technology of quick-fried pearl production mainly prepares technique using drop method in shunting-liquid and produced, that is, utilizes cooling oil
The shearing force cut-out glue post liquidated, completes quick-fried droplet system；Specifically：Exist first with two different cooling oils of incident angle
Shearing force is formed in solenoid, the wall material during lower drop and core liquid are cut off, finally by surface tension in cooling oil
Effect condenses balling-up, then the quick-fried pearl of final finished product is made after the program such as deoiling, drying, sieve；It is prepared in following embodiments
Quick-fried pearl entrusts company of Shanghai Huabao Biotechnology Co., Ltd. to machine using the method；
It should be noted that, material employed in following embodiments：Rhodinol, linalool, benzyl carbinol, geranium oil, pungent capric acid are sweet
Grease etc. is also Shanghai Huabao Biotechnology Co., Ltd.'s Products；
Bulbus Lilii extract employed in following embodiments, is prepared as follows：
（1）After dried lily is crushed, 50 mesh sieves are crossed, lily root flour is prepared；
（2）To step（1）Lily root flour in add the ethanol solution of volume fraction 75%, water-bath heat backflow 5h at 70 DEG C；Lily root flour
Solid-liquid ratio with ethanol solution is, lily root flour：Ethanol=1g：5mL；
（3）By step（2）Middle hot phegma is concentrated under reduced pressure into volume under the conditions of 60 DEG C, 70Kpa no longer to be changed, extract obtained
As Bulbus Lilii extract.
Embodiment 1
The cigarette quick-fried pearl savory essence of lily in the present embodiment, is calculated in mass percent, composed of the following components：
5.0% Bulbus Lilii extract, 1.0% rhodinol, 2.0% linalool, 8.0% benzyl carbinol, 4.0% geranium oil,
80.0% Glycerin, mixed triester with caprylic acid capric acid.
The savory essence of this lily is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl to contain
Measure as 23 μ L/, the as quick-fried pearl of lily taste cigarette.
By existing filter stick production technology, quick-fried pearl is inserted behind filter stick center by filter-stick forming device, as quick-fried pearl filter stick, and
Cigarette be cigarette sample after be the quick-fried pearl cigarette of lily taste.
To the prepared quick-fried pearl cigarette of lily taste, by 7 professional sensory evaluation personnel to the sample and reference examples blank coil
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the quick-fried pearl of lily taste cigarette, volume
Substantially, the fragrance of flue gas is rich certain lifting to " lily is fragrant " fragrance of cigarette sample, and fresh and sweet fragrant and burnt fragrant and sweet impression enhancing has
Sweet tea sense is returned, excitant reduction, miscellaneous gas is reduced, and flue gas sophistication is improved, and pleasant impression makes moderate progress.
Embodiment 2
The cigarette quick-fried pearl savory essence of lily in the present embodiment, is calculated in mass percent, composed of the following components：
7.0% Bulbus Lilii extract, 2.0% rhodinol, 3.5% linalool, 10.50% benzyl carbinol, 6.0% geranium oil and
71.0% Glycerin, mixed triester with caprylic acid capric acid.
The savory essence of this lily is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl to contain
Measure as 23 μ L/, the as quick-fried pearl of lily taste cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common（Circumference
24.3mm）In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick,
And cigarette be cigarette sample after be the quick-fried pearl cigarette of lily taste.
To the prepared quick-fried pearl cigarette of lily taste, by 7 professional sensory evaluation personnel to the sample and reference examples blank coil
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the quick-fried pearl of lily taste cigarette, volume
" lily is fragrant " of cigarette sample is obvious, and flue gas fragrance is rich to be dramatically increased, and fresh and sweet fragrant and burnt fragrant and sweet impression is remarkably reinforced, and is had
Sweet tea sense is significantly returned, excitant is significantly reduced, miscellaneous gas is reduced, flue gas sophistication is significantly improved, and pleasant impression is obviously improved.
Embodiment 3
The cigarette quick-fried pearl savory essence of lily in the present embodiment, is calculated in mass percent, composed of the following components：
10.0% Bulbus Lilii extract, 3.0% rhodinol, 5.0% linalool, 12.0% benzyl carbinol, 8.0% geranium oil and
62.0%% Glycerin, mixed triester with caprylic acid capric acid.
The savory essence of this lily is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl to contain
Measure as 23 μ L/, the as quick-fried pearl of lily taste cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common（Circumference
24.3mm）In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick,
And cigarette be cigarette sample after be the quick-fried pearl cigarette of lily taste.
To the prepared quick-fried pearl cigarette of lily taste, by 7 professional sensory evaluation personnel to the sample and reference examples blank coil
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the quick-fried pearl of lily taste cigarette, volume
" lily is fragrant " of cigarette sample is fairly obvious, and flue gas fragrance harmony reduction, excitant increase, miscellaneous gas is reduced, flue gas inaccurate coordination
And having uncomfortable sweet sense, pleasant impression is not so good as normal cigarette（Control sample cigarette）.
Quick-fried pearl product prepared by not be the same as Example is detected, while being carried out to prepared cigarette in above-described embodiment
Conventional detection, with to the physical and chemical index of diacetate fiber sample, the physical index of filter stick sample, the reason of cigarette sample in cigarette sample
Change index to be measured, further according to《The conventional analysis of the cigarette of GB/T 19609-2004 determines TPM with smoking machine
And tar》Method determine the index such as TPM, tar, nicotine and moisture in cigarette mainstream flue gas and detected, specifically
As a result it is as shown in the table.
Table 1, not in be the same as Example prepared quick-fried pearl testing result：
。
The testing result of table 2, the not prepared filter stick containing quick-fried pearl of be the same as Example：
。
Table 3, the physical index and main flume testing result of kinds of cigarettes sample：
。
It is can be seen that from the above-mentioned data of table 2 compared with normal diacetate fiber filter stick, the filter stick physics for placing the quick-fried pearl of lily refers to
Mark is without significant difference, and mainly filter stick pressure drop there occurs significant changes.As can be seen from Table 3, with the normal cigarette of reference examples
Compare, the main flume of the quick-fried pearl cigarette of lily taste is varied from, but after quick-fried pearl pinches brokenly, influence the key index of cigarette sense organ burnt
Oil and nicotine do not have significant changes.
Table 4, kinds of cigarettes sample sensory quality assessment result：
。
As can be seen from Table 4, cigarette sensory quality can be made to significantly improve by using the quick-fried pearl of lily, its sense organ
Scoring highest can improve 1.23 points, and cigarette flavor is significantly improved, and pleasant impression improves, and excitant and miscellaneous gas also have larger reduction.
To sum up, it is formulated by targetedly designing the quick-fried pearl of specific fragrance, is applied to after cigarette, can be obviously improved
Impression is sucked in odor characteristic during smoking property of cigarette, abundant and raising, simultaneously because the special efficacy that lily possesses can also reduce volume
Cigarette endangers.Therefore the application highlights cigarette " lily " note as one kind, improves sucking quality, new hundred that reduction cigarette endangers
Quick-fried pearl is closed, in industry with definitely application value.
It is emphasized that above-mentioned quick-fried pearl formula is for being formulated cigarette improvement design, when applied to ramuscule cigarette, equally
With preferable application effect, but need to quick-fried pearl specification and in filter stick, addition enters according to specific tobacco blend and design requirement
The appropriate adjustment of row, will not be described in detail herein.
Claims (6)
1. a kind of cigarette quick-fried pearl savory essence of lily, it is characterised in that be calculated in mass percent, composed of the following components：
5.0 ~ 10.0% Bulbus Lilii extract,
1.0 ~ 3.0% rhodinol,
2.0 ~ 5.0% linalool,
8.0 ~ 12.0% benzyl carbinol,
4.0 ~ 8.0% geranium oil,
62.0 ~ 80.0% Glycerin, mixed triester with caprylic acid capric acid；
The Bulbus Lilii extract is the ethanol extract of lily.
2. the cigarette quick-fried pearl savory essence of lily as claimed in claim 1, it is characterised in that 7.0% Bulbus Lilii extract, 2.0%
Rhodinol, 3.5% linalool, 10.50% benzyl carbinol, 6.0% geranium oil and 71.0% Glycerin, mixed triester with caprylic acid capric acid.
3. the quick-fried pearl of cigarette described in claim 1 is utilized with the quick-fried pearl of lily taste cigarette prepared by the savory essence of lily, it is characterised in that
A diameter of 2.0 ~ 4.0mm of quick-fried pearl；Essence content is 20 ~ 25 μ L/ in quick-fried pearl.
4. the quick-fried pearl of lily taste cigarette as claimed in claim 3, it is characterised in that the quick-fried a diameter of 3.65mm of pearl, weight are 23mg/
Essence content is 23 μ L/ in grain, quick-fried pearl.
5. application of the quick-fried pearl of lily taste cigarette in cigarette described in claim 3, it is characterised in that the quick-fried pearl of cigarette is made an addition into filter
In rod.
6. application of the quick-fried pearl of lily taste cigarette as claimed in claim 5 in cigarette, it is characterised in that the quick-fried pearl of cigarette is located at filter stick
A quick-fried pearl is added in middle part, every cigarette filter rod.
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| CN108359531A (en) * | 2018-03-22 | 2018-08-03 | 甘肃烟草工业有限责任公司 | The quick-fried pearl essence of lily odor type and its application in cigarette |
| CN112175732A (en) * | 2020-09-23 | 2021-01-05 | 甘肃烟草工业有限责任公司 | Rose fragrance type essence for blasting beads and application thereof in cigarettes |
| CN112175731A (en) * | 2020-09-23 | 2021-01-05 | 甘肃烟草工业有限责任公司 | Cordyceps-flavor essence for blasting beads and application of cordyceps-flavor essence in cigarettes |
| CN112924609A (en) * | 2021-01-29 | 2021-06-08 | 福建中烟工业有限责任公司 | Method for analyzing volatile aroma components contained in bead blasting filter stick |
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