CN105768198B - Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof - Google Patents

Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof Download PDF

Info

Publication number
CN105768198B
CN105768198B CN201610280399.2A CN201610280399A CN105768198B CN 105768198 B CN105768198 B CN 105768198B CN 201610280399 A CN201610280399 A CN 201610280399A CN 105768198 B CN105768198 B CN 105768198B
Authority
CN
China
Prior art keywords
molecular distillation
level
tree moss
acetate
tobacco
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201610280399.2A
Other languages
Chinese (zh)
Other versions
CN105768198A (en
Inventor
朱怀远
庄亚东
张媛
沈晓晨
曹毅
尤晓娟
万敏
朱龙杰
刘献军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Jiangsu Industrial Co Ltd
Original Assignee
China Tobacco Jiangsu Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Jiangsu Industrial Co Ltd filed Critical China Tobacco Jiangsu Industrial Co Ltd
Priority to CN201610280399.2A priority Critical patent/CN105768198B/en
Publication of CN105768198A publication Critical patent/CN105768198A/en
Application granted granted Critical
Publication of CN105768198B publication Critical patent/CN105768198B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Confectionery (AREA)
  • Bakery Products And Manufacturing Methods Therefor (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The present invention provides a kind of tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof, is made up of each component of following mass percent:The molecular distillation cut 0.005~5% of tree moss concrete, tobacco extract 1%~15%, malt extract 2~5%, geranyl acetate 0.2~2%, Leaf Acetate 0.5~2.5%, menthyl acetate 0.4~2%, cinnamyl acetate 0.6~2.2%, 1% bread ketone 0.1~1.5%, 1% damascone 0.8~5%, the 2 of 1%, 3,5 trimethylpyrazines 0.2~1.5%, 1% geranium oil 0.9~3%, edible alcohol 1~5%, propane diols 20~60%, glycerine 10~40%.Tobacco juice for electronic smoke prepared by the present invention has graceful tongue delicate fragrance fragrance, and the atomizing effect of tobacco juice is good, and physiology satisfaction is strong, while there is flue gas without greasy feeling, the advantage such as clean noresidue in oral cavity, with preferable market application foreground.

Description

Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof.
Background technology
As the public is to smoking and the growing interest of health problem, low temperature cigarette, heating do not burn cigarette, electronic cigarette etc. newly Type tobacco product is quickly grown, and BAT, the luxuriant and rich with fragrance not international large-scale tobacco company such as tobacco actively research and develop, promote novel tobacco system Product.One entitled CHIC Group of Poland electronic cigarette group company has just been purchased by September, 2015, British American Tobacco.At present The product of CHIC Group electronic cigarettes group company has occupied the market share of Polish similar market 60%.British American Tobacco It is expected that using electronics smoke product as the new generation product of representative, in addition to the U.S. and Chinese market, its sales volume is estimated to the year two thousand twenty Up to 8,400,000,000 pounds.
Electronic cigarette profile is similar to common cigarette, and current electronic cigarette will contain cigarette mainly by a kind of atomising device The electronic cigarette liquid atomization of alkali, by pulmonary absorption, makes consumer obtain the similar satisfaction for sucking traditional cigarette.In electronic cigarette Tobacco juice, also referred to as tobacco tar, more with propane diols, glycerine, ethanol etc. for solvent, pass through the flavouring essence for tobacco compatibility group with certain content Into.The A of Chinese patent CN 105011351 disclose a kind of electronic cigarette liquid with bitter buckwheat local flavor, and the A of CN 105361237 are disclosed It is a kind of that there is electronic cigarette liquid of reduction cholesterol effect and preparation method thereof.
The electronic cigarette liquid and the Gas phase Smoke ratio of traditional cigarette developed at present, flavor component differs greatly, and smoker is very Hardly possible obtains the physiology satisfaction similar to traditional cigarette, moreover, the higher-boiling compound such as carbohydrate, protein in electronic cigarette liquid compared with Many, the oral coatings sense in aspiration procedure is larger, and residual phenomena is serious, has a strong impact on the sucking quality of electronic cigarette.Tongue delicate fragrance is fragrant Expect, due to the natural delicate fragrance with unique liverwort material, to be well received by consumers, in food, cosmetic field application more Extensively, very important effect is also played in cigarette blending.Some domestic Cigarette Industrial Enterprises are successfully opened with tongue delicate fragrance spices Many cigarette brands are sent out.In view of this, the problem of present invention exists for electronic cigarette liquid, develops one kind and is easily atomized, raw Manage that satisfaction is strong, fragrance the is fresh and sweet electronic cigarette liquid without soapy feeling, oral cavity noresidue
The content of the invention
The present invention provides a kind of tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, overcomes the electronics of prior art preparation The aroma quality and perfume quantity that tobacco juice is present can not meet the psychological need of consumer, and oral cavity residual is heavier, and suction greasy feeling is again etc. Problem has tongue delicate fragrance odor characteristic, the electronic cigarette liquid that flue gas is fresh and sweet, physiology satisfaction is strong there is provided a kind of.
The present invention technical solution be:
A kind of tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, is made up of each component of following mass percent:Tree moss The molecular distillation cut 0.005~5% of medicinal extract, tobacco extract 1%~15%, malt extract 2~5%, geranyl acetate 0.2 ~2%, Leaf Acetate 0.5~2.5%, menthyl acetate 0.4~2%, cinnamyl acetate 0.6~2.2%, 1% bread ketone 0.1~1.5%, 1% damascone 0.8~5%, the 2 of 1%, 3,5- trimethylpyrazines 0.2~1.5%, 1% geranium oil 0.9 ~3%, edible alcohol 1~5%, propane diols 20~60%, glycerine 10~40%.
Further, the molecular distillation cut of the tree moss concrete is made by following steps:
It is 1 to weigh mass ratio:4 tree moss concrete and the common 200g of absolute ethyl alcohol, uniform system is dispersed into through refiner, will The degassing of system ultrasound is added after 4 minutes in the feed liquid bottle of wiped film molecular distillation device, opens cooling circulating water, by the first order and The temperature of second level condensed water is set to 2 DEG C, and the third level uses liquid nitrogen condensation, and parameter to the vapo(u)rizing temperature of adjusting apparatus is 50~ 100 DEG C, blade applicator rotating speed is 50~300r/min, and absolute pressure starts to add with 1~4ml/min speed when being 0.1~30Pa Material, collects the second level and third level cut, and by the second level and third level cut according to mass ratio 1-5:Obtained after 1 mixing.
Further, the relative amount sum of single aryl compound is not less than in the molecular distillation cut of the tree moss concrete 40%, the relative amount of terpene compound is not less than 10% in the molecular distillation cut of tree moss concrete.
Further, the tobacco extract is Zimbabwe's pure tobacco oil, cloud and mist absolute oil, Turkish tobaccos absolute oil, Sun cured tobacco One or more in absolute oil, Dark sun-cured absolute oil.
Further, described 1% bread ketone, 1% damascone, the 2 of 1%, 3,5- trimethylpyrazines and 1% spiceleaf Oil is respectively the ethanol solution that respective monomer essence mass fraction is 1%.
Further, it is formulated by following component according to mass percent:The molecular distillation cut of tree moss concrete 0.01%, tobacco extract 7.5%, malt extract 2.24%, geranyl acetate 1.5%, Leaf Acetate 0.6%, acetic acid is thin Lotus ester 0.5%, cinnamyl acetate 0.8%, 1% bread ketone 1%, 1% damascone 1.5%, the 2 of 1%, 3,5- trimethylpyrazines 0.6%, 1% geranium oil 1.25%, edible alcohol 2.5%, propane diols 45%, glycerine 35%.
A kind of preparation method of the tobacco juice for electronic smoke of any of the above-described tongue delicate fragrance aromatic style feature, including:
The molecular distillation cut of tree moss concrete is prepared, it is 1 to weigh mass ratio:4 tree moss concrete and the common 200g of absolute ethyl alcohol, Uniform system is dispersed into through refiner, the feed liquid bottle of wiped film molecular distillation device is added after system ultrasound is deaerated 4 minutes In, cooling circulating water is opened, the temperature of the first order and second level condensed water 2 DEG C are set to, the third level uses liquid nitrogen condensation, adjusted The parameter of device to vapo(u)rizing temperature is 50~100 DEG C, and blade applicator rotating speed is 50~300r/min, and absolute pressure is 0.1~30Pa When start, with the charging of 1~4ml/min speed, to collect the second level and third level cut, and the second level and third level cut are pressed According to mass ratio 1-5:The molecular distillation cut of stand-by tree moss concrete is prepared after 1 mixing;
The molecular distillation cut for preparing stand-by tree moss concrete is mixed to get with following mass percent:Tree moss soaks The molecular distillation cut 0.005~5% of cream, tobacco extract 1%~15%, malt extract 2~5%, geranyl acetate 0.2~ 2%, Leaf Acetate 0.5~2.5%, menthyl acetate 0.4~2%, cinnamyl acetate 0.6~2.2%, 1% bread ketone 0.1 ~1.5%, 1% damascone 0.8~5%, the 2 of 1%, 3,5- trimethylpyrazines 0.2~1.5%, 1% geranium oil 0.9~ 3%, edible alcohol 1~5%, propane diols 20~60%, glycerine 10~40%.
The beneficial effects of the invention are as follows:Tobacco juice for electronic smoke of this kind of tongue delicate fragrance aromatic style feature and preparation method thereof, tool Have the following advantages:
First, the tobacco juice for electronic smoke of this kind of tongue delicate fragrance aromatic style feature, clarification, uniform, raw materials used middle high boiling substance It is less, it is ensured that the atomizing effect of tobacco juice.
2nd, by Zimbabwe tobacco, cloud and mist, Turkish tobaccos and the compatibility for shining the pure tobacco oils such as Huang, turn to red because of sun burn, without additional biology The composition such as alkali and nicotine, it is ensured that the natural attribute of electronic cigarette liquid, while the physiology need of consumer's smoking cigarette can be met again Ask.
3rd, make by the selection of the molecular distillation cut of tree moss concrete and with the cooperation of the monomer perfume such as burnt odor, fragrant and sweet With the electronic cigarette liquid of preparation has graceful, elegant tongue delicate fragrance fragrance, and flue gas is fresh and sweet, and oral cavity is clean, pure and fresh without residual after suction Stay, overcome after the suction of conventional electrical tobacco juice, flue gas is greasy, the inferior position of oral coatings sense weight.
Embodiment
The following detailed description of the preferred embodiments of the present invention.According to following embodiments, the present invention may be better understood.So And, as it will be easily appreciated by one skilled in the art that be merely to illustrate the present invention described by embodiment, without should also without limitation on The present invention described in detail in claims.
The tobacco juice for electronic smoke of the tongue delicate fragrance aromatic style feature of embodiment, the tongue delicate fragrance fragrance for having gracefulness, the atomization of tobacco juice Effect is good, and physiology satisfaction is strong, while there is flue gas without greasy feeling, the advantage such as clean noresidue in oral cavity, with preferable market Application prospect.
The tobacco juice for electronic smoke of this kind of tongue delicate fragrance aromatic style feature, is made up of each component of following mass percent:Tree moss The molecular distillation cut 0.005~5% of medicinal extract, tobacco extract 1%~15%, malt extract 2~5%, geranyl acetate 0.2 ~2%, Leaf Acetate 0.5~2.5%, menthyl acetate 0.4~2%, cinnamyl acetate 0.6~2.2%, 1% bread ketone 0.1~1.5%, 1% damascone 0.8~5%, the 2 of 1%, 3,5- trimethylpyrazines 0.2~1.5%, 1% geranium oil 0.9 ~3%, edible alcohol 1~5%, propane diols 20~60%, glycerine 10~40%.
The molecular distillation cut of tree moss concrete is made by following steps:It is 1 to weigh mass ratio:4 tree moss concrete with it is anhydrous The common 200g of ethanol, uniform system is dispersed into through refiner, and wiped film molecular distillation dress is added after system ultrasound is deaerated 4 minutes In the feed liquid bottle put, cooling circulating water is opened, the temperature of the first order and second level condensed water 2 DEG C are set to, the third level uses liquid Nitrogen is condensed, and parameter to the vapo(u)rizing temperature of adjusting apparatus is 50~100 DEG C, and blade applicator rotating speed is 50~300r/min, absolute pressure Start during for 0.1~30Pa with the charging of 1~4ml/min speed, collect the second level and third level cut, and by the second level and the Three-level cut is according to mass ratio 1-5:Obtained after 1 mixing.
The relative amount sum of single aryl compound is not less than 40%, tree moss concrete in the molecular distillation cut of tree moss concrete Molecular distillation cut in the relative amount of terpene compound be not less than 10%.
According to influence of the Parameter Conditions such as vapo(u)rizing temperature, vacuum, blade applicator rotating speed to molecular distillation cut, according to Dan Yin Element and Orthogonal Experiment and Design, it is preferable that the conditional parameter of molecular distillation instrument is:Feed rate 3ml/min, vapo(u)rizing temperature 70 DEG C, absolute pressure 5Pa, blade applicator rotating speed 200r/min, the first order and second level cut use condensation cycle water condensation, condensed water Temperature be 2 DEG C, third level cut is cooled down using liquid nitrogen, collection second level cut and third level cut.
By second level cut and third level cut in mass ratio 1~5:1 mixing is used as the tree moss concrete in tobacco juice for electronic smoke Molecular distillation cut.
Embodiment 1
It is 1 to weigh mass ratio:4 tree moss concrete and the common 200g of absolute ethyl alcohol, uniform system is dispersed into through refiner, will The degassing of system ultrasound is added after 4 minutes in the feed liquid bottle of wiped film molecular distillation device, opens cooling circulating water, by the first order and The temperature of second level condensed water is set to 2 DEG C, and the third level uses liquid nitrogen condensation, and parameter to the vapo(u)rizing temperature of adjusting apparatus is 70 DEG C, Blade applicator rotating speed is 200r/min, and absolute pressure starts the speed charging with 3ml/min, collects the second level and the 3rd when being 5Pa Level cut, and by the second level and third level cut according to mass ratio 1:1 mixing.
Table 1 gives the analysis result of the Gc/ms Analyser device of tree moss concrete molecular distillation cut.As a result show Show, the relative amount of the ter penoidses such as alloaromadendrene, aromadendrene, ledene is 15.485%, and the ter penoidses of high level are assigned Delicate fragrance style and volatility that electronic cigarette liquid is good are given, it is ensured that flue gas has preferable fresh and sweet sense, divaricatic acid second The relative amount of the list aryl compound such as ester, red star clothing acetoacetic ester, everninic acid ethyl ester is 74.197%, is retained to greatest extent The tongue delicate fragrance aromatic style feature of tree moss concrete.
The composition of the tree moss concrete molecular distillation cut of table 1
The tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, each group of mass percentage is divided into:The molecule of tree moss concrete Distillation fraction 0.05%, tobacco extract 9.5%, malt extract 3%, geranyl acetate 1.6%, Leaf Acetate 1.4%, second Sour menthyl ester 1.4%, cinnamyl acetate 1.5%, 1% bread ketone 1.5%, 1% damascone 2.5%, the 2 of 1%, 3,5- front threes Base pyrazine 0.85%, 1% geranium oil 2.2%, edible alcohol 4.5%, propane diols 45%, glycerine 25%.
Embodiment 2
It is 1 to weigh mass ratio:4 tree moss concrete and the common 200g of absolute ethyl alcohol, uniform system is dispersed into through refiner, will The degassing of system ultrasound is added after 4 minutes in the feed liquid bottle of wiped film molecular distillation device, opens cooling circulating water, by the first order and The temperature of second level condensed water is set to 2 DEG C, and the third level uses liquid nitrogen condensation, and parameter to the vapo(u)rizing temperature of adjusting apparatus is 80 DEG C, Blade applicator rotating speed is 200r/min, and absolute pressure starts the speed charging with 3ml/min, collects the second level and the 3rd when being 10Pa Level cut, and by the second level and third level cut according to mass ratio 3:1 mixing.
Table 2 gives the analysis result of the Gc/ms Analyser device of tree moss concrete molecular distillation cut.As a result show Show, the relative amount of the ter penoidses such as alloaromadendrene, aromadendrene, ledene is 14.633%, and the ter penoidses of high level are assigned Delicate fragrance style and volatility that electronic cigarette liquid is good are given, it is ensured that flue gas has preferable fresh and sweet sense, divaricatic acid second The relative amount of the list aryl compound such as ester, red star clothing acetoacetic ester, everninic acid ethyl ester is 74.986%, is retained to greatest extent The tongue delicate fragrance aromatic style feature of tree moss concrete.
The composition of the tree moss concrete molecular distillation cut of table 2
The tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, each group of mass percentage is divided into:The molecule of tree moss concrete Distillation fraction 0.035%, tobacco extract 7.9%, malt extract 2.25%, geranyl acetate 1.25%, Leaf Acetate 1.5%, menthyl acetate 0.85%, cinnamyl acetate 1.25%, 1% bread ketone 0.75%, 1% damascone 1.235%, The 2 of 1%, 3,5- trimethylpyrazines 0.7%, 1% geranium oil 2%, edible alcohol 3.28%, propane diols 47%, glycerine 30%.
Embodiment 3
It is 1 to weigh mass ratio:4 tree moss concrete and the common 200g of absolute ethyl alcohol, uniform system is dispersed into through refiner, will The degassing of system ultrasound is added after 4 minutes in the feed liquid bottle of wiped film molecular distillation device, opens cooling circulating water, by the first order and The temperature of second level condensed water is set to 2 DEG C, and the third level uses liquid nitrogen condensation, and parameter to the vapo(u)rizing temperature of adjusting apparatus is 80 DEG C, Blade applicator rotating speed is 200r/min, and absolute pressure starts when being 2.5Pa with the charging of 3ml/min speed, collects the second level and the Three-level cut, and by the second level and third level cut according to mass ratio 5:1 mixing.
Table 3 gives the analysis result of the Gc/ms Analyser device of tree moss concrete molecular distillation cut.As a result show Show, the relative amount of the ter penoidses such as alloaromadendrene, aromadendrene, ledene is 14.127%, and the ter penoidses of high level are assigned Delicate fragrance style and volatility that electronic cigarette liquid is good are given, it is ensured that flue gas has preferable fresh and sweet sense, divaricatic acid second The relative amount of the list aryl compound such as ester, red star clothing acetoacetic ester, everninic acid ethyl ester is 76.737%, is retained to greatest extent The tongue delicate fragrance aromatic style feature of tree moss concrete.
The composition of the tree moss concrete molecular distillation cut of table 3
The tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, each group of mass percentage is divided into:The molecule of tree moss concrete Distillation fraction 1.75%, tobacco extract 15%, malt extract 4.25%, geranyl acetate 1.75%, Leaf Acetate 2%, Menthyl acetate 1%, cinnamyl acetate 2%, 1% bread ketone 1%, 1% damascone 2.25%, the 2 of 1%, 3,5- trimethyls Pyrazine 1.2%, 1% geranium oil 2.8%, edible alcohol 3%, propane diols 35%, glycerine 27%.
The above embodiment of the present invention is only intended to clearly illustrate example of the present invention, not to the reality of the present invention Apply the restriction of mode.For those of ordinary skill in the field, it can also make other on the basis of the above description Various forms of changes or variation.Here all embodiments can not be exhaustive.Every technical side for belonging to the present invention Row of the obvious changes or variations that case is extended out still in protection scope of the present invention.

Claims (5)

1. a kind of tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, it is characterised in that by each component of following mass percent Composition:The molecular distillation cut 0.005~5% of tree moss concrete, tobacco extract 1%~15%, malt extract 2~5%, geranyl Ester 0.2~2%, Leaf Acetate 0.5~2.5%, menthyl acetate 0.4~2%, cinnamyl acetate 0.6~2.2%, 1% bread ketone 0.1~1.5%, 1% damascone 0.8~5%, the 2 of 1%, 3,5- trimethylpyrazines 0.2~1.5%, 1% geranium oil 0.9~3%, Edible alcohol 1~5%, propane diols 20~60%, glycerine 10~40%;Single arylation in the molecular distillation cut of the tree moss concrete The relative amount sum of compound is not less than the relative amount of terpene compound in 40%, the molecular distillation cut of tree moss concrete not Less than 10%;The molecular distillation cut of the tree moss concrete is made by following steps:
It is 1 to weigh mass ratio:4 tree moss concrete and the common 200g of absolute ethyl alcohol, are dispersed into uniform system, by system through refiner Ultrasound degassing is added after 4 minutes in the feed liquid bottle of wiped film molecular distillation device, cooling circulating water is opened, by the first order and second The temperature of level condensed water is set to 2 DEG C, and the third level uses liquid nitrogen condensation, and parameter to the vapo(u)rizing temperature of adjusting apparatus is 50~100 DEG C, Blade applicator rotating speed is 50~300r/min, and absolute pressure starts the speed charging with 1~4ml/min, collected when being 0.1~30Pa The second level and third level cut, and by the second level and third level cut according to mass ratio 1-5:Obtained after 1 mixing.
2. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature as claimed in claim 1, it is characterised in that:The tobacco extract For the one or more in Zimbabwe's pure tobacco oil, cloud and mist absolute oil, Turkish tobaccos absolute oil, Sun cured tobacco absolute oil, Dark sun-cured absolute oil.
3. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature as claimed in claim 1, it is characterised in that:Described 1% bread Ketone, 1% damascone, 1% 2,3,5- trimethylpyrazines and 1% geranium oil are respectively that respective monomer essence mass fraction is 1% Ethanol solution.
4. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature as claimed in claim 1, it is characterised in that:By following component according to Mass percent is formulated:The molecular distillation cut 0.01% of tree moss concrete, tobacco extract 7.5%, malt extract 2.24%, Geranyl acetate 1.5%, Leaf Acetate 0.6%, menthyl acetate 0.5%, cinnamyl acetate 0.8%, 1% bread ketone 1%, 1% it is prominent Faint ketone 1.5%, the 2 of 1%, 3,5- trimethylpyrazines 0.6%, 1% geranium oil 1.25%, edible alcohol 2.5%, propane diols 45%, glycerine 35%。
5. a kind of preparation method of the tobacco juice for electronic smoke of any one of claim 1-4 tongue delicate fragrance aromatic style features, it is special Levy and be, including:
The molecular distillation cut of tree moss concrete is prepared, it is 1 to weigh mass ratio:4 tree moss concrete and the common 200g of absolute ethyl alcohol, through even Pulp grinder is dispersed into uniform system, in the feed liquid bottle that wiped film molecular distillation device is added after system ultrasound is deaerated 4 minutes, beats Cooling circulating water is opened, the temperature of the first order and second level condensed water 2 DEG C are set to, the third level uses liquid nitrogen condensation, adjusting apparatus Parameter to vapo(u)rizing temperature be 50~100 DEG C, blade applicator rotating speed be 50~300r/min, absolute pressure be 0.1~30Pa when open Begin to feed with 1~4ml/min speed, collect the second level and third level cut, and by the second level and third level cut according to matter Amount compares 1-5:The molecular distillation cut of stand-by tree moss concrete is prepared after 1 mixing;The molecular distillation of the tree moss concrete evaporates The relative amount sum of single aryl compound is not less than terpene compound in 40%, the molecular distillation cut of tree moss concrete in point Relative amount be not less than 10%;
The molecular distillation cut for preparing stand-by tree moss concrete is mixed to get with following mass percent:Tree moss concrete Molecular distillation cut 0.005~5%, tobacco extract 1%~15%, malt extract 2~5%, geranyl acetate 0.2~2%, acetic acid Leaf-alcohol ester 0.5~2.5%, menthyl acetate 0.4~2%, cinnamyl acetate 0.6~2.2%, 1% bread ketone 0.1~1.5%, 1% Damascone 0.8~5%, the 2 of 1%, 3,5- trimethylpyrazines 0.2~1.5%, 1% geranium oil 0.9~3%, edible alcohol 1~5%, Propane diols 20~60%, glycerine 10~40%.
CN201610280399.2A 2016-04-29 2016-04-29 Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof Active CN105768198B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610280399.2A CN105768198B (en) 2016-04-29 2016-04-29 Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610280399.2A CN105768198B (en) 2016-04-29 2016-04-29 Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof

Publications (2)

Publication Number Publication Date
CN105768198A CN105768198A (en) 2016-07-20
CN105768198B true CN105768198B (en) 2017-09-19

Family

ID=56400202

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610280399.2A Active CN105768198B (en) 2016-04-29 2016-04-29 Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105768198B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106490674A (en) * 2016-11-30 2017-03-15 湖北中烟工业有限责任公司 A kind of electronics tobacco tar of fresh breath and preparation method thereof
CN106706794B (en) * 2017-01-04 2018-12-11 江苏中烟工业有限责任公司 A kind of method of main tongue fur faint scent characteristic chicken flavor substance in quantitative analysis ramuscule cigarette mainstream flue gas
CN108936791B (en) * 2018-08-28 2022-03-15 云南恒罡科技有限公司 Method for preparing flue gas condensate by high-temperature thermal cracking

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102041174A (en) * 2011-01-07 2011-05-04 江苏中烟工业有限责任公司 Preparation method of moss-scented tobacco flavor and application of moss-scented cigarette flavor in cigarette flavoring
CN104531356A (en) * 2015-01-19 2015-04-22 川渝中烟工业有限责任公司 Honeyed-sweet additive and electronic cigarette liquid with same
CN104531351A (en) * 2014-12-03 2015-04-22 河南中烟工业有限责任公司 Additive for electronic cigarette liquid, and preparation method thereof
CN104856216A (en) * 2015-05-31 2015-08-26 中国烟草总公司郑州烟草研究院 Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette
CN104946390A (en) * 2015-05-31 2015-09-30 中国烟草总公司郑州烟草研究院 Method for processing natural perfume used for electronic cigarette
CN104983063A (en) * 2015-05-31 2015-10-21 中国烟草总公司郑州烟草研究院 Improved preparation method for electronic cigarette smoke solution
CN105249524A (en) * 2015-08-14 2016-01-20 贵州中烟工业有限责任公司 Fragrance type heating nonflammable tobacco product and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150181924A1 (en) * 2013-10-31 2015-07-02 Michael R. Llamas Cannabidiol liquid composition for smoking

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102041174A (en) * 2011-01-07 2011-05-04 江苏中烟工业有限责任公司 Preparation method of moss-scented tobacco flavor and application of moss-scented cigarette flavor in cigarette flavoring
CN104531351A (en) * 2014-12-03 2015-04-22 河南中烟工业有限责任公司 Additive for electronic cigarette liquid, and preparation method thereof
CN104531356A (en) * 2015-01-19 2015-04-22 川渝中烟工业有限责任公司 Honeyed-sweet additive and electronic cigarette liquid with same
CN104856216A (en) * 2015-05-31 2015-08-26 中国烟草总公司郑州烟草研究院 Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette
CN104946390A (en) * 2015-05-31 2015-09-30 中国烟草总公司郑州烟草研究院 Method for processing natural perfume used for electronic cigarette
CN104983063A (en) * 2015-05-31 2015-10-21 中国烟草总公司郑州烟草研究院 Improved preparation method for electronic cigarette smoke solution
CN105249524A (en) * 2015-08-14 2016-01-20 贵州中烟工业有限责任公司 Fragrance type heating nonflammable tobacco product and preparation method thereof

Also Published As

Publication number Publication date
CN105768198A (en) 2016-07-20

Similar Documents

Publication Publication Date Title
CN103923747B (en) Essence on cigarette tissue
CN106174683B (en) A kind of composition and the tobacco juice for electronic smoke containing said composition
CN104087415B (en) Electronic cigarette liquid of a kind of grape flavor and preparation method thereof
CN104839883A (en) Electronic cigarette liquid with characteristics of tobaccos for tobacco pipes
CN111671134A (en) Mint flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid
CN104041935A (en) Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette
CN103478894A (en) Camellia extract composition with spicy fragrance and application of same to cigarettes
CN101633864A (en) Apple-flavored essence for tobacco, preparation method and application thereof
CN103468410A (en) Tea flower extract composition and its use in cigarette
CN105768198B (en) Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof
CN109135924A (en) A kind of orange flavor and its preparation method and application for cigarette mouth stick
CN103783660A (en) Supercritical extraction method of aroma substances in tobacco leaf fragments and application of aroma substances
CN106010797A (en) Malt coke-sweet flavor prepared from coked malt and application thereof in electronic cigarettes
KR20210018948A (en) Delayed Release Flavoring and Its Application in Chinese Flavored Tobacco Products
CN112457914A (en) Spicy base for improving smoking comfort of heated cigarettes and application thereof
CN108497544A (en) It a kind of coating medium, coating fluid and its does not burn with the application in dry process reproduction tobacco leaf preparing heating
CN104082855B (en) Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof
CN106978258A (en) Enzymatic flavouring improves the preparation method and application of the FLOS CHRYSANTHEMI ALBA from Haizhou of China volatile oil of flavouring essence quality
CN108618192A (en) A kind of 15 are formulated electronic cigarette tobacco tar and preparation method thereof
CN111329103B (en) Electronic cigarette spice composition with Tie Guanyin tea aroma characteristics, electronic cigarette liquid and application of electronic cigarette spice composition and electronic cigarette liquid
CN108949347A (en) Increase the essence and its preparation method and application for heating the new cigarette flue gas moist feeling that do not burn
CN102994229B (en) Cigarette flavor prepared by utilizing red date extract and preparation and application method thereof
CN110295088B (en) Cumquat-flavored essence and application thereof
CN108185512A (en) A kind of perfume material for the fragrant section of cigarette production of not burning for mixed type heating and preparation method thereof
CN101342018A (en) Green tea mellow wine extract, preparation and application thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant