CN104082855B - Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof - Google Patents
Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof Download PDFInfo
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- CN104082855B CN104082855B CN201410360458.8A CN201410360458A CN104082855B CN 104082855 B CN104082855 B CN 104082855B CN 201410360458 A CN201410360458 A CN 201410360458A CN 104082855 B CN104082855 B CN 104082855B
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Abstract
The invention provides electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof.The electronic cigarette liquid of of the present invention pair of apple local flavor obtains after being mixed in proportion by propane diols, glycerine, 1,3-BDO, xylitol liquid, green apple extract, edible flavoring apple essence etc.; Wherein green apple extract is through alcohol heating reflux extraction, decompression rotary evaporation is concentrated obtains; In the electronic cigarette liquid of two apple local flavor, the parts by weight of each component are: propane diols 1-80 part, glycerine 1-70 part, 1,3-butanediol 1-50 part, xylitol liquid 1-30 part, green apple extract 1-20 part, edible flavoring apple essence 0.1-5 part electronic cigarette liquid of the present invention have two apple fragrance and fresh and sweet mouthfeel preferably, can meet consumer and suck demand to fruity electronic cigarette.
Description
Technical field
The invention belongs to flavouring essence for tobacco field, relate to a kind of electronic cigarette liquid and preparation method thereof, particularly relate to electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof.
Technical background
Electronic cigarette is a kind of Miniature atomized device adopting high-new microelectric technique, is the substitute of conventional cigarette.Electronic cigarette does not have other harmful components such as tar, suspended particulates in cigarette, produces second-hand-cigarette hardly yet.Electronic cigarette is generally made up of three parts: tobacco rod, atomizer and cigarette bullet.When smoker is by cigarette holder air-breathing, the electronic cigarette liquid in cigarette bullet is become the droplet of about 0.5-1.5um in atomizer by heating atomization, forms simulation smoke.
Fragrance and the mouthfeel of electronic cigarette derive from electronic cigarette liquid, the composition mainly essence and flavoring agent of electronic cigarette liquid, tobacco extract and propane diols, glycerine equal solvent.At present, fruity electronic cigarette relies on its fresh and sweet various taste to be subject to the favor of consumers in general.
Summary of the invention
the technical problem solved:apple is liked by consumer deeply as a kind of Common Fruits, market has the product of numerous apple aroma, and apple local flavor electronic cigarette is also one of modal product on electronic cigarette market.But the general fragrance of apple aroma electronic cigarette is in the market single, mouthfeel is sweet greasy, pleasant impression is unclean, can not meet the requirement of sense of consumer.
technical scheme:for above-mentioned technical problem, the invention discloses the electronic cigarette liquid of a kind of pair of apple local flavor, the electronic cigarette liquid of described two apple local flavors consists of the following composition: propane diols, glycerine, 1,3-BDO, xylitol liquid, green apple extract and edible flavoring apple essence.
Preferably, in the electronic cigarette liquid of a kind of pair of described apple local flavor, the parts by weight of each component are: propane diols 1-80 part, glycerine 1-70 part, 1,3-BDO 1-50 part, xylitol liquid 1-30 part, green apple extract 1-20 part, edible flavoring apple essence 0.1-5 part.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor is sundown.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor, described edible flavoring apple essence is composed of the following components: iso-amyl iso-valeriate, ethyl isovalerate, isoamyl butyrate, ethyl acetate, vanillic aldehyde, benzaldehyde, citral, isoamyl formate, geranium oil, allyl hexanoate, caryophyllus oil, 95% ethanol and distilled water.
Iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part, distilled water 10-50 part.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor, in described edible two flavoring apple essence, the parts by weight of each component are: iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part, distilled water 10-50 part.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor, described green apple extract is the green apple extract with obtaining after alcohol extract.
Preferably, described green apple method for preparing extractive comprises the following steps: (1) takes clean green apple, smashs to pieces with tissue mashing machine; (2) add certain density ethanol in proportion, ultrasonic wave extracts three times; (3) merge extract, decompression rotary evaporation is condensed into paste, for subsequent use.
Preferably, in the preparation method of described tomato extract, concentration of alcohol used is 60wt% ~ 90wt%, solid-liquid ratio is 1:8-1:20, supersonic frequency is 50 ~ 400kHz, ultrasonic power is 50 ~ 600W, single ultrasonic extraction time is 10-30min, and the temperature that decompression rotary evaporation concentrates is 50 DEG C, and vacuum is 0.095 Mpa.
A preparation method for the electronic cigarette liquid of pair apple local flavor, comprises the steps: that (1) takes clean green apple, smashs to pieces with tissue mashing machine; (2) add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 60wt% ~ 90wt%, and solid-liquid ratio is 1:8-1:20, and supersonic frequency is 50 ~ 400kHz, and ultrasonic power is 50 ~ 600W, and single ultrasonic extraction time is 10-30min; (3) merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, for subsequent use after concentrated; (4) iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part is got, distilled water 10-50 part, obtains edible flavoring apple essence after being mixed by mentioned component; (5) get propane diols 1-80 part, glycerine 1-70 part, 1,3-BDO 1-50 part, xylitol liquid 1-30 part, green apple extract 1-20 part, edible flavoring apple essence 0.1-5 part, after being mixed by mentioned component, prepare the electronic cigarette liquid of two apple local flavor.
Described xylitol liquid is the xylitol aqueous solution of 20wt% to 40wt%.
beneficial effect:the electronic cigarette liquid of the two apple local flavors prepared by preparation method of the present invention is sundown, overcome that the general fragrance of apple aroma electronic cigarette is single, mouthfeel is sweet greasy, pleasant impression is unclean, the shortcoming of the requirement of sense of consumer can not be met, electronic cigarette liquid of the present invention can provide salubrious green apple fragrance and sweet apple fragrance when aspirating, mouthfeel is soft and moist and pleasant impression is totally comfortable, and the preparation method of described electronic cigarette liquid is easy, constant product quality, can be widely used in electronic cigarette product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(1) take clean green apple, smash to pieces with tissue mashing machine; Add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 70wt%, and solid-liquid ratio is 1:15, and supersonic frequency is 400kHz, and ultrasonic power is 600W, and single ultrasonic extraction time is 15min; Merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, for subsequent use after concentrated;
(2) iso-amyl iso-valeriate 5 parts, ethyl isovalerate 1.2 parts, isoamyl butyrate 1.5 parts, 1 part, ethyl acetate, vanillic aldehyde 0.1 part, benzaldehyde 0.01 part, citral 0.06 part, isoamyl formate 0.6 part, geranium oil 0.01 part, allyl hexanoate 0.01 part, caryophyllus oil 0.05 part, 95% ethanol 70 parts is got by weight, distilled water 20 parts, obtains edible flavoring apple essence after being mixed by mentioned component;
(3) get propane diols 55 parts by weight, glycerine 15 parts, 1,3-BDO 15 parts, the xylitol liquid 5 parts of 20wt%, green apple extract 9.8 parts, edible flavoring apple essence 0.1 part mix, obtain the electronic cigarette liquid of two apple local flavor.
Embodiment 2
(1) take clean green apple, smash to pieces with tissue mashing machine; Add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 90wt%, and solid-liquid ratio is 1:8, and supersonic frequency is 50kHz, and ultrasonic power is 50W, and single ultrasonic extraction time is 30min; Merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, for subsequent use after concentrated;
(2) iso-amyl iso-valeriate 8 parts, ethyl isovalerate 2 parts, isoamyl butyrate 0.1 part, 0.1 part, ethyl acetate, vanillic aldehyde 0.3 part, benzaldehyde 0.05 part, citral 0.01 part, isoamyl formate 0.1 part, geranium oil 0.5 part, allyl hexanoate 0.05 part, caryophyllus oil 1 part, 95% ethanol 30 parts is got by weight, distilled water 10 parts, obtains edible flavoring apple essence after being mixed by mentioned component;
(3) get propane diols 1 part by weight, glycerine 70 parts, 1,3-BDO 50 parts, 40wt% xylitol liquid 1 part, green apple extract 1 part, edible flavoring apple essence 5 parts mix, obtain the electronic cigarette liquid of two apple local flavor.
Embodiment 3
(1) take clean green apple, smash to pieces with tissue mashing machine; Add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 60wt%, and solid-liquid ratio is 1:20, and supersonic frequency is 200kHz, and ultrasonic power is 300W, and single ultrasonic extraction time is 10min; Merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, for subsequent use after concentrated;
(2) iso-amyl iso-valeriate 1 part, ethyl isovalerate 0.1 part, isoamyl butyrate 2 parts, 2 parts, ethyl acetate, vanillic aldehyde 1 part, benzaldehyde 1 part, citral 1 part, isoamyl formate 2 parts, geranium oil 1 part, allyl hexanoate 1 part, caryophyllus oil 0.01 part, 95% ethanol 90 parts is got by weight, distilled water 50 parts, obtains edible flavoring apple essence after being mixed by mentioned component;
(3) get propane diols 80 parts by weight, glycerine 1 part, 1,3-BDO 1 part, the xylitol liquid 30 parts of 30wt%, green apple extract 20 parts, edible flavoring apple essence 0.5 part mix, obtain the electronic cigarette liquid of two apple local flavor.
Two apple local flavor electronic cigarette liquids of the embodiment 1 prepared, embodiment 2, embodiment 3 are got 0.5mL to be added in electronic cigarette, and separately get after commercially available edible flavoring apple essence propane diols is diluted to 0.3wt%, the commercially available edible flavoring apple essence dilution of 0.3wt% getting 0.5mL is added in electronic cigarette, as a comparison case, integrated sensory's quality evaluation is carried out.Result is as follows:
Embodiment 1: flue gas is full, apple gives off a strong fragrance and be rich in stereovision, mouthfeel sweet soft, pleasant impression is comfortable.
Embodiment 2: flue gas is strong, apple fragrance is soft and moist and be rich in stereovision, mouthfeel is fresh and sweet exquisiteness, pleasant impression be clean.
Embodiment 3: flue gas is strong, apple soft aroma and and be rich in stereovision, delicate mouthfeel, pleasant impression are clean.
Comparative example: flue gas is strong, apple fragrance coordinate, mouthfeel sweet greasy, pleasant impression is not good enough.
Can find out from result, the green apple fragrance that the electronic cigarette liquid of the two apple local flavors prepared by preparation method of the present invention is salubrious and sweet apple fragrance, mouthfeel is soft and moist and pleasant impression is totally comfortable, and the preparation method of described electronic cigarette liquid is easy, constant product quality, can be widely used in electronic cigarette product.
Claims (1)
1. a preparation method for the electronic cigarette liquid of two apple local flavor, is characterized in that comprising the steps: that (1) takes clean green apple, smashs to pieces with tissue mashing machine; (2) add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 60wt% ~ 90wt%, and solid-liquid ratio is 1:8-1:20, and supersonic frequency is 50 ~ 400kHz, and ultrasonic power is 50 ~ 600W, and single ultrasonic extraction time is 10-30min; (3) merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, for subsequent use after concentrated; (4) iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part is got, distilled water 10-50 part, obtains edible flavoring apple essence after being mixed by mentioned component; (5) propane diols 1-80 part, glycerine 1-70 part, 1 is got, 3-butanediol 1-50 part, xylitol liquid 1-30 part, step (1) to (3) obtain green apple extract 1-20 part, step (4) obtains edible flavoring apple essence 0.1-5 part, will mentioned component mix after prepare the electronic cigarette liquid of two apple local flavor.
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| CN201410360458.8A CN104082855B (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof |
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| CN201410360458.8A CN104082855B (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof |
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| CN104082855B true CN104082855B (en) | 2015-10-21 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104382223B (en) * | 2014-10-22 | 2017-03-15 | 浙江中烟工业有限责任公司 | A kind of tobacco juice and electronic cigarette of the solvent and its preparation suitable for preparing Fruity type tobacco juice for electronic smoke |
| CN104585862B (en) * | 2015-01-15 | 2016-03-09 | 云南中烟工业有限责任公司 | A kind of without sweet soapy feeling tobacco juice for electronic smoke |
| CN107460041A (en) * | 2016-06-04 | 2017-12-12 | 沈百祥 | A kind of flavoring apple essence preparation method |
| CN107581655B (en) * | 2017-08-29 | 2020-10-02 | 深圳市真味生物科技有限公司 | Compound sweet-taste-free electronic cigarette tobacco tar and preparation method thereof |
| CN115067540B (en) * | 2022-07-11 | 2023-06-23 | 湖北中烟工业有限责任公司 | Apple extract for cigarettes and preparation method thereof |
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| US4449541A (en) * | 1981-06-02 | 1984-05-22 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
| CN101473999A (en) * | 2009-01-21 | 2009-07-08 | 华健 | Health-care type electronic smoke liquid for preventing and treating decayed tooth |
| CN103070473A (en) * | 2013-01-25 | 2013-05-01 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette tobacco juice prepared from faint scent tobacco leaves |
| CN103622161A (en) * | 2013-11-28 | 2014-03-12 | 刘秋明 | Electronic cigarette tobacco juice solvent and electronic cigarette tobacco juice |
| CN103849465A (en) * | 2014-02-27 | 2014-06-11 | 恩施市锦华生物工程有限责任公司 | Preparation method of essence for electronic cigarette with strawberry flavor |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US7726320B2 (en) * | 2006-10-18 | 2010-06-01 | R. J. Reynolds Tobacco Company | Tobacco-containing smoking article |
| WO2013173469A1 (en) * | 2012-05-17 | 2013-11-21 | Loec, Inc. | Method and compositions to deliver variable quantities of flavor from filtered cigarettes |
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2014
- 2014-07-28 CN CN201410360458.8A patent/CN104082855B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US4449541A (en) * | 1981-06-02 | 1984-05-22 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
| CN101473999A (en) * | 2009-01-21 | 2009-07-08 | 华健 | Health-care type electronic smoke liquid for preventing and treating decayed tooth |
| CN103070473A (en) * | 2013-01-25 | 2013-05-01 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette tobacco juice prepared from faint scent tobacco leaves |
| CN103622161A (en) * | 2013-11-28 | 2014-03-12 | 刘秋明 | Electronic cigarette tobacco juice solvent and electronic cigarette tobacco juice |
| CN103849465A (en) * | 2014-02-27 | 2014-06-11 | 恩施市锦华生物工程有限责任公司 | Preparation method of essence for electronic cigarette with strawberry flavor |
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Inventor after: Wang Xiaoyuan Inventor before: Yin Fei Inventor before: Han Ting Inventor before: Hu Zhonghao |
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Effective date of registration: 20170809 Address after: 741200, No. three, No. 255, Xicheng village, Anyuan Town, Gangu County, Gansu, Tianshui Patentee after: Wang Xiaoyuan Address before: 108 room 1, building 522, 314000 Asia Pacific Road, Zhejiang, Jiaxing Patentee before: Jiaxing City obtains encyclopaedia novel material Science and Technology Ltd. |
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