CN105768198A - Electronic cigarette juice with moss faint scent feature and preparation method thereof - Google Patents
Electronic cigarette juice with moss faint scent feature and preparation method thereof Download PDFInfo
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- CN105768198A CN105768198A CN201610280399.2A CN201610280399A CN105768198A CN 105768198 A CN105768198 A CN 105768198A CN 201610280399 A CN201610280399 A CN 201610280399A CN 105768198 A CN105768198 A CN 105768198A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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Abstract
The invention provides electronic cigarette juice with a moss faint scent feature and a preparation method thereof. The electronic cigarette juice is prepared from the following components in percentage by mass: 0.005-5 percent of molecular distillation cut of tree moss extract, 1-15 percent of tobacco extract, 2-5 percent of malt extract, 0.2-2 percent of geranyl acetate, 0.5-2.5 percent of hexenyl acetate, 0.4-2 percent of menthyl acetate, 0.6-2.2 percent of cinnamyl acetate, 0.1-1.5 percent of 1 percent 2- methyl -tetrahydrofuran-3-ketone, 0.8-5 percent of 1 percent damascenone, 0.2-1.5 percent 1 percent 2,3,5-trimethylpyrazine, 0.9-3 percent of 1 percent geranium oil, 1-5 percent of edible alcohol, 20-60 percent of propylene glycol and 10-40 percent of glycerinum. The prepared electronic cigarette juice has the advantages of faint scent moss fragrance, good tobacco juice atomizing effect, good physical satisfaction, no greasy feel of smoke gas, no residues in oral cavity and the like, and has good market application prospect.
Description
Technical field
The present invention relates to tobacco juice for electronic smoke of a kind of tongue delicate fragrance aromatic style feature and preparation method thereof.
Background technology
Along with public's growing interest to smoking Yu health problem, low temperature cigarette, heating are not burnt Medicated cigarette, electronics
The international large-scale tobacco companies such as the novel tobacco goods such as cigarette quickly grow, BAT, phenanthrene not Nicotiana tabacum L. actively research and develop,
Promote novel tobacco goods.In JIUYUE, 2015, one entitled CHIC of Poland has just purchased in British American Tobacco
The electronic cigarette group company of Group.The product of CHIC Group electronic cigarette group company has occupied ripple at present
The market share of blue similar market 60%.The anticipated a new generation's product with electronic cigarette product as representative of British American Tobacco
Product, in addition to the U.S. and Chinese market, its sales volume is estimated to the year two thousand twenty up to 8,400,000,000 pounds.
Electronic cigarette profile is similar to common cigarette, and current electronic cigarette mainly by a kind of atomising device, will contain
The electronic cigarette liquid having nicotine is atomized, and by pulmonary absorption, makes consumer's acquisition be similar to and sucks meeting of traditional cigarette
Sense.Tobacco juice in electronic cigarette, also referred to as ree-oil, how with propylene glycol, glycerol, ethanol etc. as solvent, by with
The flavouring essence for tobacco compatibility composition of certain content.Chinese patent CN 105011351 A discloses one and has Radix Et Rhizoma Fagopyri Tatarici
The electronic cigarette liquid of local flavor, CN 105361237 A discloses a kind of electronic cigarette liquid having and reducing cholesterol effect
And preparation method thereof.
The Gas phase Smoke ratio of the electronic cigarette liquid developed at present and traditional cigarette, flavor component differs greatly, smoking
Person is difficult to obtain the physiology gratification similar to traditional cigarette, and, saccharide in electronic cigarette liquid, protein etc.
Higher-boiling compound is more, and the oral coatings sense in aspiration procedure is relatively big, and residual phenomena is serious, has a strong impact on electricity
The sucking quality of sub-cigarette.Tongue delicate fragrance spice is owing to having the natural delicate fragrance of the liverwort material of uniqueness, deeply by consumer
Like, food, cosmetic field application relatively broad, Medicated cigarette perfumery also plays very important work
With.More domestic Cigarette Industrial Enterprises successfully develop a lot of cigarette brand with tongue delicate fragrance spice.In view of this,
The present invention is directed to the problem that electronic cigarette liquid exists, develop one and be easily atomized, physiology gratification is strong, and fragrance is clear
Sweet without soapy feeling, the electronic cigarette liquid of oral cavity noresidue
Summary of the invention
The present invention provides the tobacco juice for electronic smoke of a kind of tongue delicate fragrance aromatic style feature, overcomes prepared by prior art
The aroma quality of electronic cigarette liquid existence and perfume quantity can not meet the psychological need of consumer, and oral cavity residual is heavier, takes out
The oil suction soapy feeling problem such as heavily, it is provided that one has tongue delicate fragrance odor characteristic, flue gas is fresh and sweet, physiology gratification is strong
Electronic cigarette liquid.
The technical solution of the present invention is:
The tobacco juice for electronic smoke of a kind of tongue delicate fragrance aromatic style feature, is made up of each component of following mass percent:
The molecular distillation fraction 0.005～5% of tree moss concrete, tobacco extract 1%～15%, malt extract 2～5%,
Geranyl acetate 0.2～2%, Leaf Acetate 0.5～2.5%, menthyl acetate 0.4～2%, cinnamyl acetate
0.6～2.2%, the bread ketone 0.1～1.5% of 1%, the damascone 0.8～5% of 1%, the 2 of 1%, 3,5-trimethyls
Pyrazine 0.2～1.5%, the Oleum Pelargonii Graveolentis 0.9～3% of 1%, edible ethanol 1～5%, propylene glycol 20～60%, sweet
Oil 10～40%.
Further, the molecular distillation fraction of described tree moss concrete is prepared by following steps:
Weigh tree moss concrete and dehydrated alcohol 200g altogether that mass ratio is 1:4, be dispersed into uniformly through refiner
System, by the feed liquid bottle adding wiped film molecular distillation device after ultrasonic for system degassing 4 minutes, opens cooling
Recirculated water, is set to 2 DEG C by the temperature of the first order and second level condensed water, and the third level uses liquid nitrogen condensation, adjusts
The parameter of device to vapo(u)rizing temperature is 50～100 DEG C, and blade applicator rotating speed is 50～300r/min, and absolute pressure is
Start when 0.1～30Pa to feed with the speed of 1～4ml/min, collect the second level and third level fraction, and by the
Two grades obtain according to after mass ratio 1-5:1 mixing with third level fraction.
Further, in the molecular distillation fraction of described tree moss concrete, the relative amount sum of single aryl compound is not
Less than 40%, in the molecular distillation fraction of tree moss concrete, the relative amount of terpene compound is not less than 10%.
Further, described tobacco extract be Zimbabwe's pure tobacco oil, cloud and mist absolute oil, Turkish tobaccos absolute oil,
One or more in Sun cured tobacco absolute oil, Dark sun-cured absolute oil.
Further, described 1% bread ketone, the damascone of 1%, the 2，3，5-trimethylpyrazine of 1% and 1%
Oleum Pelargonii Graveolentis to be respectively respective monomer essence mass fraction be the ethanol solution of 1%.
Further, formulated according to mass percent by following component: the molecular distillation fraction of tree moss concrete
0.01%, tobacco extract 7.5%, malt extract 2.24%, geranyl acetate 1.5%, Leaf Acetate 0.6%,
Menthyl acetate 0.5%, cinnamyl acetate 0.8%, the bread ketone 1% of 1%, the damascone 1.5% of 1%, 1%
2，3，5-trimethylpyrazine 0.6%, the Oleum Pelargonii Graveolentis 1.25% of 1%, edible ethanol 2.5%, propylene glycol 45%, sweet
Oil 35%.
A kind of preparation method of the tobacco juice for electronic smoke of any of the above-described tongue delicate fragrance aromatic style feature, including:
Prepare the molecular distillation fraction of tree moss concrete, weigh tree moss concrete and dehydrated alcohol that mass ratio is 1:4
Altogether 200g, is dispersed into uniform system through refiner, ultrasonic for system degassing is added scraped film type after 4 minutes and divides
In the feed liquid bottle of sub-distilling apparatus, open cooling circulating water, the temperature of the first order and second level condensed water is set to
2 DEG C, the third level uses liquid nitrogen condensation, and the parameter of adjusting apparatus to vapo(u)rizing temperature is 50～100 DEG C, blade applicator
Rotating speed is 50～300r/min, and absolute pressure is to start when 0.1～30Pa to feed with the speed of 1～4ml/min,
Collect the second level and third level fraction, and after the second level and third level fraction are mixed according to mass ratio 1-5:1
Prepare the molecular distillation fraction of stand-by tree moss concrete；
The molecular distillation fraction preparing stand-by tree moss concrete is mixed to get with following mass percent: tree
The molecular distillation fraction 0.005～5% of tongue extractum, tobacco extract 1%～15%, malt extract 2～5%,
Geranyl acetate 0.2～2%, Leaf Acetate 0.5～2.5%, menthyl acetate 0.4～2%, cinnamyl acetate
0.6～2.2%, the bread ketone 0.1～1.5% of 1%, the damascone 0.8～5% of 1%, the 2 of 1%, 3,5-trimethyls
Pyrazine 0.2～1.5%, the Oleum Pelargonii Graveolentis 0.9～3% of 1%, edible ethanol 1～5%, propylene glycol 20～60%, sweet
Oil 10～40%.
The invention has the beneficial effects as follows: tobacco juice for electronic smoke of this kind of tongue delicate fragrance aromatic style feature and preparation method thereof,
Have the advantage that
One, the tobacco juice for electronic smoke of this kind of tongue delicate fragrance aromatic style feature, clarification, uniformly, raw materials used middle height
Boilers is less, it is ensured that the atomizing effect of tobacco juice.
Two, by Zimbabwe Nicotiana tabacum L., cloud and mist, Turkish tobaccos and solarization are yellow, shine the compatibility of the pure tobacco oil such as red, nothing
The compositions such as additional alkaloid and nicotine, it is ensured that the natural attribute of electronic cigarette liquid, can meet again consumer simultaneously
The psychological need of smoking cigarette.
Three, by the selection of the molecular distillation fraction of tree moss concrete and with burnt odor, the joining of the monomer perfume such as fragrant and sweet
Closing and use, the electronic cigarette liquid of preparation has gracefulness, elegant tongue delicate fragrance fragrance, and flue gas is fresh and sweet, oral cavity after suction
Totally, pure and fresh noresidue, overcome conventional electrical tobacco juice suction after, flue gas is greasy, oral coatings sense weight bad
Gesture.
Detailed description of the invention
The following detailed description of the preferred embodiments of the present invention.According to following embodiment, this be may be better understood
Bright.But, as it will be easily appreciated by one skilled in the art that the present invention that is merely to illustrate described by embodiment, and
Should be without limitation on the present invention described in detail in claims yet.
The tobacco juice for electronic smoke of the tongue delicate fragrance aromatic style feature of embodiment, has the tongue delicate fragrance fragrance of gracefulness, tobacco juice
Atomizing effect is good, and physiology gratification is strong, has flue gas without advantages such as greasy feeling, the clean noresidues in oral cavity simultaneously,
There is preferable market application foreground.
The tobacco juice for electronic smoke of this kind of tongue delicate fragrance aromatic style feature, is made up of each component of following mass percent:
The molecular distillation fraction 0.005～5% of tree moss concrete, tobacco extract 1%～15%, malt extract 2～5%,
Geranyl acetate 0.2～2%, Leaf Acetate 0.5～2.5%, menthyl acetate 0.4～2%, cinnamyl acetate
0.6～2.2%, the bread ketone 0.1～1.5% of 1%, the damascone 0.8～5% of 1%, the 2 of 1%, 3,5-trimethyls
Pyrazine 0.2～1.5%, the Oleum Pelargonii Graveolentis 0.9～3% of 1%, edible ethanol 1～5%, propylene glycol 20～60%, sweet
Oil 10～40%.
The molecular distillation fraction of tree moss concrete is prepared by following steps: weigh the tree moss concrete that mass ratio is 1:4
With dehydrated alcohol altogether 200g, it is dispersed into uniform system through refiner, ultrasonic for system degassing is added after 4 minutes
Enter in the feed liquid bottle of wiped film molecular distillation device, open cooling circulating water, by the first order and second level condensed water
Temperature be set to 2 DEG C, the third level use liquid nitrogen condensation, the parameter of adjusting apparatus to vapo(u)rizing temperature is 50～100 DEG C,
Blade applicator rotating speed is 50～300r/min, and absolute pressure is to start with the speed of 1～4ml/min when 0.1～30Pa
Charging, collects the second level and third level fraction, and by the second level and third level fraction according to mass ratio 1-5:1
Obtain after mixing.
In the molecular distillation fraction of tree moss concrete, the relative amount sum of single aryl compound is not less than 40%, tree moss
In the molecular distillation fraction of extractum, the relative amount of terpene compound is not less than 10%.
According to Parameter Conditions impacts on molecular distillation fraction such as vapo(u)rizing temperature, vacuum, blade applicator rotating speeds, depend on
According to single factor test and Orthogonal Experiment and Design, it is preferable that the conditional parameter of molecular distillation instrument is: feed rate
3ml/min, vapo(u)rizing temperature 70 DEG C, absolute pressure 5Pa, blade applicator rotating speed 200r/min, the first order and second
Level fraction uses condensation cycle water-cooled to coagulate, and the temperature of condensed water is 2 DEG C, and third level fraction uses liquid nitrogen to carry out cold
But, second level fraction and third level fraction are collected.
Second level fraction and third level fraction in mass ratio 1～5:1 are mixed as the tree moss in tobacco juice for electronic smoke
The molecular distillation fraction of extractum.
Embodiment 1
Weigh tree moss concrete and dehydrated alcohol 200g altogether that mass ratio is 1:4, be dispersed into uniformly through refiner
System, by the feed liquid bottle adding wiped film molecular distillation device after ultrasonic for system degassing 4 minutes, opens cooling
Recirculated water, is set to 2 DEG C by the temperature of the first order and second level condensed water, and the third level uses liquid nitrogen condensation, adjusts
The parameter of device to vapo(u)rizing temperature is 70 DEG C, and blade applicator rotating speed is 200r/min, and absolute pressure is to open during 5Pa
Begin to feed with the speed of 3ml/min, collect the second level and third level fraction, and by the second level and third level fraction
Mix according to mass ratio 1:1.
Table 1 gives the analysis result of the Gc/ms Analyser device of tree moss concrete molecular distillation fraction.
Result shows, the relative amount of the ter penoids such as alloaromadendrene, aromadendrene, ledene is 15.485%, higher
The ter penoids of content imparts the good delicate fragrance style of electronic cigarette liquid and volatility, it is ensured that flue gas has relatively
Good fresh and sweet sense, single aryl compound such as divaricatic acid ethyl ester, red star clothing acetoacetic ester, everninic acid ethyl ester
Relative amount is 74.197%, remains the tongue delicate fragrance aromatic style feature of tree moss concrete to greatest extent.
The composition of table 1 tree moss concrete molecular distillation fraction
The tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, each component of mass percentage is: tree moss concrete
Molecular distillation fraction 0.05%, tobacco extract 9.5%, malt extract 3%, geranyl acetate 1.6%, acetic acid
Folic alcohol ester 1.4%, menthyl acetate 1.4%, cinnamyl acetate 1.5%, the bread ketone 1.5% of 1%, Tujue of 1%
Ketone 2.5%, the 2，3，5-trimethylpyrazine 0.85% of 1%, the Oleum Pelargonii Graveolentis 2.2% of 1%, edible ethanol 4.5%, third
Glycol 45%, glycerol 25%.
Embodiment 2
Weigh tree moss concrete and dehydrated alcohol 200g altogether that mass ratio is 1:4, be dispersed into uniformly through refiner
System, by the feed liquid bottle adding wiped film molecular distillation device after ultrasonic for system degassing 4 minutes, opens cooling
Recirculated water, is set to 2 DEG C by the temperature of the first order and second level condensed water, and the third level uses liquid nitrogen condensation, adjusts
The parameter of device to vapo(u)rizing temperature is 80 DEG C, and blade applicator rotating speed is 200r/min, and absolute pressure is to open during 10Pa
Begin to feed with the speed of 3ml/min, collect the second level and third level fraction, and by the second level and third level fraction
Mix according to mass ratio 3:1.
Table 2 gives the analysis result of the Gc/ms Analyser device of tree moss concrete molecular distillation fraction.
Result shows, the relative amount of the ter penoids such as alloaromadendrene, aromadendrene, ledene is 14.633%, higher
The ter penoids of content imparts the good delicate fragrance style of electronic cigarette liquid and volatility, it is ensured that flue gas has relatively
Good fresh and sweet sense, single aryl compound such as divaricatic acid ethyl ester, red star clothing acetoacetic ester, everninic acid ethyl ester
Relative amount is 74.986%, remains the tongue delicate fragrance aromatic style feature of tree moss concrete to greatest extent.
The composition of table 2 tree moss concrete molecular distillation fraction
The tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, each component of mass percentage is: tree moss concrete
Molecular distillation fraction 0.035%, tobacco extract 7.9%, malt extract 2.25%, geranyl acetate 1.25%,
Leaf Acetate 1.5%, menthyl acetate 0.85%, cinnamyl acetate 1.25%, the bread ketone 0.75% of 1%,
The damascone 1.235% of 1%, the 2，3，5-trimethylpyrazine 0.7% of 1%, the Oleum Pelargonii Graveolentis 2% of 1%, edible ethanol
3.28%, propylene glycol 47%, glycerol 30%.
Embodiment 3
Weigh tree moss concrete and dehydrated alcohol 200g altogether that mass ratio is 1:4, be dispersed into uniformly through refiner
System, by the feed liquid bottle adding wiped film molecular distillation device after ultrasonic for system degassing 4 minutes, opens cooling
Recirculated water, is set to 2 DEG C by the temperature of the first order and second level condensed water, and the third level uses liquid nitrogen condensation, adjusts
The parameter of device to vapo(u)rizing temperature is 80 DEG C, and blade applicator rotating speed is 200r/min, when absolute pressure is 2.5Pa
Start to feed with the speed of 3ml/min, collect the second level and third level fraction, and the second level and the third level are evaporated
Divide and mix according to mass ratio 5:1.
Table 3 gives the analysis result of the Gc/ms Analyser device of tree moss concrete molecular distillation fraction.
Result shows, the relative amount of the ter penoids such as alloaromadendrene, aromadendrene, ledene is 14.127%, higher
The ter penoids of content imparts the good delicate fragrance style of electronic cigarette liquid and volatility, it is ensured that flue gas has relatively
Good fresh and sweet sense, single aryl compound such as divaricatic acid ethyl ester, red star clothing acetoacetic ester, everninic acid ethyl ester
Relative amount is 76.737%, remains the tongue delicate fragrance aromatic style feature of tree moss concrete to greatest extent.
The composition of table 3 tree moss concrete molecular distillation fraction
The tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, each component of mass percentage is: tree moss concrete
Molecular distillation fraction 1.75%, tobacco extract 15%, malt extract 4.25%, geranyl acetate 1.75%,
Leaf Acetate 2%, menthyl acetate 1%, cinnamyl acetate 2%, the bread ketone 1% of 1%, the damascone of 1%
2.25%, the 2，3，5-trimethylpyrazine 1.2% of 1%, the Oleum Pelargonii Graveolentis 2.8% of 1%, edible ethanol 3%, propylene glycol
35%, glycerol 27%.
The above embodiment of the present invention is only for clearly demonstrating example of the present invention, not to the present invention
The restriction of embodiment.For those of ordinary skill in the field, on the basis of the above description also
Can make other changes in different forms.Here cannot all of embodiment be given exhaustive.All
It is belonging to obvious change that technical scheme extended out or the variation guarantor still in the present invention
Protect the row of scope.
Claims (7)
1. the tobacco juice for electronic smoke of a tongue delicate fragrance aromatic style feature, it is characterised in that by following percent mass
Each component composition of ratio: the molecular distillation fraction 0.005～5% of tree moss concrete, tobacco extract 1%～15%,
Malt extract 2～5%, geranyl acetate 0.2～2%, Leaf Acetate 0.5～2.5%, menthyl acetate 0.4～
2%, cinnamyl acetate 0.6～2.2%, the bread ketone 0.1～1.5% of 1%, the damascone 0.8～5% of 1%, 1%
2，3，5-trimethylpyrazine 0.2～1.5%, the Oleum Pelargonii Graveolentis 0.9～3% of 1%, edible ethanol 1～5%, the third two
Alcohol 20～60%, glycerol 10～40%.
2. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature as claimed in claim 1, it is characterised in that: institute
The molecular distillation fraction stating tree moss concrete is prepared by following steps:
Weigh tree moss concrete and dehydrated alcohol 200g altogether that mass ratio is 1:4, be dispersed into uniformly through refiner
System, by the feed liquid bottle adding wiped film molecular distillation device after ultrasonic for system degassing 4 minutes, opens cooling
Recirculated water, is set to 2 DEG C by the temperature of the first order and second level condensed water, and the third level uses liquid nitrogen condensation, adjusts
The parameter of device to vapo(u)rizing temperature is 50～100 DEG C, and blade applicator rotating speed is 50～300r/min, and absolute pressure is
Start when 0.1～30Pa to feed with the speed of 1～4ml/min, collect the second level and third level fraction, and by the
Two grades obtain according to after mass ratio 1-5:1 mixing with third level fraction.
3. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature as claimed in claim 1, it is characterised in that: institute
Stating the relative amount sum of single aryl compound in the molecular distillation fraction of tree moss concrete and be not less than 40%, tree moss soaks
In the molecular distillation fraction of cream, the relative amount of terpene compound is not less than 10%.
4. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, its feature as described in any one of claim 1-3
It is: described tobacco extract is that Zimbabwe's pure tobacco oil, cloud and mist absolute oil, Turkish tobaccos absolute oil, Sun cured tobacco are clean
One or more in oil, Dark sun-cured absolute oil.
5. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, its feature as described in any one of claim 1-3
It is: the bread ketone of described 1%, the damascone of 1%, the 2,3,5-trimethylpyrazine of 1% and the Oleum Pelargonii Graveolentis of 1%
Being respectively respective monomer essence mass fraction is the ethanol solution of 1%.
6. the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature, its feature as described in any one of claim 1-3
It is: formulated according to mass percent by following component: the molecular distillation fraction 0.01% of tree moss concrete,
Tobacco extract 7.5%, malt extract 2.24%, geranyl acetate 1.5%, Leaf Acetate 0.6%, acetic acid
Menthyl ester 0.5%, cinnamyl acetate 0.8%, the bread ketone 1% of 1%, the damascone 1.5% of 1%, the 2,3,5-of 1%
Trimethylpyrazine 0.6%, the Oleum Pelargonii Graveolentis 1.25% of 1%, edible ethanol 2.5%, propylene glycol 45%, glycerol 35%.
7. the preparation of the tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature described in an any one of claim 1-6
Method, it is characterised in that including:
Prepare the molecular distillation fraction of tree moss concrete, weigh tree moss concrete and dehydrated alcohol that mass ratio is 1:4
Altogether 200g, is dispersed into uniform system through refiner, ultrasonic for system degassing is added scraped film type after 4 minutes and divides
In the feed liquid bottle of sub-distilling apparatus, open cooling circulating water, the temperature of the first order and second level condensed water is set to
2 DEG C, the third level uses liquid nitrogen condensation, and the parameter of adjusting apparatus to vapo(u)rizing temperature is 50～100 DEG C, blade applicator
Rotating speed is 50～300r/min, and absolute pressure is to start when 0.1～30Pa to feed with the speed of 1～4ml/min,
Collect the second level and third level fraction, and after the second level and third level fraction are mixed according to mass ratio 1-5:1
Prepare the molecular distillation fraction of stand-by tree moss concrete；
The molecular distillation fraction preparing stand-by tree moss concrete is mixed to get with following mass percent: tree
The molecular distillation fraction 0.005～5% of tongue extractum, tobacco extract 1%～15%, malt extract 2～5%,
Geranyl acetate 0.2～2%, Leaf Acetate 0.5～2.5%, menthyl acetate 0.4～2%, cinnamyl acetate
0.6～2.2%, the bread ketone 0.1～1.5% of 1%, the damascone 0.8～5% of 1%, the 2 of 1%, 3,5-trimethyls
Pyrazine 0.2～1.5%, the Oleum Pelargonii Graveolentis 0.9～3% of 1%, edible ethanol 1～5%, propylene glycol 20～60%, sweet
Oil 10～40%.
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| CN106490674A (en) * | 2016-11-30 | 2017-03-15 | 湖北中烟工业有限责任公司 | A kind of electronics tobacco tar of fresh breath and preparation method thereof |
| CN106706794A (en) * | 2017-01-04 | 2017-05-24 | 江苏中烟工业有限责任公司 | Quantitative analysis method of main moss fragrance characteristics flavor component in fine cigarette mainstream smoke |
| CN108936791A (en) * | 2018-08-28 | 2018-12-07 | 云南恒罡科技有限公司 | A kind of method that high temperature pyrolysis prepares smoke condensate |
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| CN106706794A (en) * | 2017-01-04 | 2017-05-24 | 江苏中烟工业有限责任公司 | Quantitative analysis method of main moss fragrance characteristics flavor component in fine cigarette mainstream smoke |
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