CN104856216A - Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette - Google Patents
Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette Download PDFInfo
- Publication number
- CN104856216A CN104856216A CN201510286766.5A CN201510286766A CN104856216A CN 104856216 A CN104856216 A CN 104856216A CN 201510286766 A CN201510286766 A CN 201510286766A CN 104856216 A CN104856216 A CN 104856216A
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- China
- Prior art keywords
- extract
- electronic cigarette
- concrete
- absolute oil
- medicinal extract
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention provides a treatment method for concrete and absolute type natural extractive suitable for an electronic cigarette. According to the method, the frequently-used concrete, absolute type edible spice and absolute type spice for the cigarette are diluted through propylene glycol or glycerol (the mass ratio is 1:1-20:1), the molecular distillation is performed, and therefore light components are obtained and are products after treating the concrete and absolute type natural extractive suitable for the electronic cigarette. The treatment process is simple, treated natural extractive is dilution of the propylene glycol or glycerol and can be directly used for producing electronic cigarette liquid. Through treatment, high-boiling-point substances and a waxy component in the spice can be removed, the defect that high-boiling-point spice easily generates a charring smell is overcome, the extractive can be completely dissolved in the electronic cigarette liquid so that the electronic cigarette liquid can be clear and bright, the fragrance permeability is better, and the method can enlarge the selection range of the spice for the electronic cigarette.
Description
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind ofly be applicable to the medicinal extract of electronic cigarette, the processing method of absolute oil class natural extract.
Background technology
Along with socio-economic development, consumer are come into effect to the concern of health and various ban on opium-smoking and the opium trade regulations, the consumer environment of tobacco there occurs great changes.In recent years, various novel tobacco goods are constantly released, and receive the concern of more and more people.Wherein, electronic cigarette goods, because it is not containing harmful components such as tar, CO, hydrogen cyanide, can not produces second-hand-cigarette and without features such as burnings, receive the favor of more and more people.
Because electronic cigarette industry development is not also very perfect, tobacco juice for electronic smoke spices used is direct use flavoring essence and traditional flavouring essence for tobacco generally, is medicinal extract, absolute oil class natural extract greatly in these essence.But, due to medicinal extract, absolute oil class spices extraction process, in its composition, generally all contain the wax component such as the high boiling substance such as carbohydrate, protein and long-chain fat hydrocarbon.These compositions, being applied in electronic cigarette process, can produce a series of problem: one usually, and the general volatility of specific examples of such components is poor, can not have the effect in front to fragrance; Its two, high boiling substance can be deposited on atomizer, produce be charred taste, affect the suction quality of electronic cigarette and the service life of atomizer.Its three, wax component cannot dissolve each other in tobacco juice for electronic smoke, easily forms oily insoluble matter, having had a strong impact on the quality of tobacco juice, if these tobacco juices are for having in the electronic cigarette smoking set of transparent device for storing liquid, can have a strong impact on the sensory experience of consumer.Based on above reason, existing electronic cigarette product, or directly use synthetic perfume, or reduce the interpolation consumption of medicinal extract, absolute oil class natural extract as far as possible.But, relative to synthetic perfume, no matter natural extract is rich at note, or in security, there is very large advantage, if can process it, remove high boiling substance and wax, its application in electronic cigarette must be widened, and make the note of electronic cigarette more abundant, graceful.
At present, there is the more patent about tobacco juice for electronic smoke, as a kind of atomized liquid of electronic simulation cigarette (grant number CN 101731750 B), a kind of electronic cigarette atomization tobacco juice and preparation method's (application number 201310686110.3), atomized liquid of electronic smoke (grant number CN101461566 B), medicinal health type solid electronic aerosolization liquid and preparation method's (authorizing CN 101933653 B), all employ medicinal extract, absolute oil class spices in these patents, but all natural perfume material used is not processed.
Summary of the invention
Object of the present invention is just for the shortcoming existed in above-mentioned prior art, and a kind of medicinal extract of electronic cigarette, processing method of absolute oil class natural extract of being applicable to is provided, the method can remove high boiling substance in medicinal extract, absolute oil class natural extract and wax, and processing procedure is simple, the product after process can be directly used in the production of tobacco juice for electronic smoke.
The object of the invention is to be achieved through the following technical solutions:
A kind ofly be applicable to the medicinal extract of electronic cigarette, the processing method of absolute oil class natural extract, this type of natural extract is added propane diols or glycol/propane triol (mass ratio 1:1 to the 20:1) dilution of 5-50 times of weight, dilution is stirred 10 ~ 120 minutes under normal temperature to 100 C temperature, after cooling, dilution molecular distillation equipment is at 40 DEG C ~ 200 DEG C, 10 pa ~ 10
5carry out molecular clock under pa condition, gained light component material is the medicinal extract, the product after the process of absolute oil class natural extract that are applicable to electronic cigarette of the present invention, and the natural extract after process is the dilution of propane diols or glycol/propane triol.
Described natural extract is that conventional medicinal extract, absolute oil class are edible, tobacco aromatics, can comprise
such as red date medicinal extract, plum medicinal extract, fenugreek concrete, tree moss concrete, Tolu concrete, maple extract, cocoa extract, tree moss absolute, malt extract, cherry extracts.
The present invention by medicinal extract, absolute oil class natural extract by propane diols or glycol/propane triol dilution, molecular clock two-step pretreatment, eliminate the high boiling substance in spices and wax, obtain the natural extract being applicable to electronic cigarette, the method has the following advantages:
(1) medicinal extract, absolute oil class natural extract first dilute with propane diols or glycol/propane triol by the present invention, can ensure when molecular clock, light component and heavy constituent all contain some solvent, there is certain mobility, solve natural extract medicinal extract, absolute oil is when being directly used in molecular clock, heavy constituent material easily sticks on rotor, hinders the problem of rotor turns, improves the operating efficiency of molecular clock.
(2) processing procedure of the present invention is comparatively simple, select propane diols or glycol/propane triol as solvent, natural extract light component after process is the dilution of propane diols or glycol/propane triol, Alevaire due to electronic cigarette is generally propane diols and glycerine, and therefore product can be directly used in the production of tobacco juice for electronic smoke.
(3) the method eliminates high boiling substance in spices and wax component, solves higher boiling spices and easily produces the shortcoming being charred taste, and it is bright that tobacco juice for electronic smoke is clarified, and the fragrance thoroughly property sent out is better.
(4) this method solve medicinal extract, problems when absolute oil class natural extract directly applies to electronic cigarette, the range of choice of electronics tobacco aromatics can be widened.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further, but does not limit the present invention.
embodiment 1
Get 50g red date medicinal extract, add 250g glycol/propane triol (mass ratio 7:3) dilution, stir 30 minutes under 50 C water bath condition.Gained dilution is crossed molecular clock, and distillation condition is set to 70 C, 100pa, obtain light component be process after red date extract glycol/propane triol dilution.
embodiment 2
Get 100g plum medicinal extract, add the dilution of 3000g propane diols, stir 120 minutes at ambient temperature.Gained dilution is crossed molecular clock, and distillation condition is set to 200 C, and 10
5pa, obtain light component be process after plum extract propane diols dilution.
embodiment 3
Get 100g tree moss absolute, add 1000g glycol/propane triol (mass ratio 1:1) dilution, stir 10 minutes at ambient temperature.Gained dilution is crossed molecular clock, and distillation condition is set to 40 C, 10pa, obtain light component be process after tree moss extract glycol/propane triol dilution.
Claims (3)
1. one kind is applicable to the medicinal extract of electronic cigarette, the processing method of absolute oil class natural extract, it is characterized in that: the propane diols or the dilution of glycol/propane triol that this type of natural extract are added 5-50 times of weight, mass ratio 1:1 to the 20:1 of glycol/propane triol, dilution is stirred 10 ~ 120 minutes under normal temperature to 100 C temperature, after cooling, dilution molecular distillation equipment is at 40 DEG C ~ 200 DEG C, 10 pa ~ 10
5carry out molecular clock under pa condition, gained light component material is the medicinal extract, the product after the process of absolute oil class natural extract that are applicable to electronic cigarette of the present invention.
2. be according to claim 1ly applicable to the medicinal extract of electronic cigarette, the processing method of absolute oil class natural extract, it is characterized in that: described natural extract is that conventional medicinal extract, absolute oil class are edible, tobacco aromatics.
3. be according to claim 2ly applicable to the medicinal extract of electronic cigarette, the processing method of absolute oil class natural extract, it is characterized in that: described conventional medicinal extract, absolute oil class are edible, tobacco aromatics comprises red date medicinal extract, plum medicinal extract, fenugreek concrete, tree moss concrete, Tolu concrete, maple extract, cocoa extract, tree moss absolute, malt extract, cherry extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510286766.5A CN104856216A (en) | 2015-05-31 | 2015-05-31 | Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510286766.5A CN104856216A (en) | 2015-05-31 | 2015-05-31 | Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104856216A true CN104856216A (en) | 2015-08-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510286766.5A Pending CN104856216A (en) | 2015-05-31 | 2015-05-31 | Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette |
Country Status (1)
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| CN (1) | CN104856216A (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105768198A (en) * | 2016-04-29 | 2016-07-20 | 江苏中烟工业有限责任公司 | Electronic cigarette juice with moss faint scent feature and preparation method thereof |
| CN106433975A (en) * | 2016-11-25 | 2017-02-22 | 中国烟草总公司郑州烟草研究院 | Method for preparing low-As-content tree moss absolute by molecular distillation |
| CN106522022A (en) * | 2016-10-26 | 2017-03-22 | 湖北中烟工业有限责任公司 | Additive for sheet cigarette paper of cigars as well as preparation method and application of additive |
| CN106638160A (en) * | 2016-10-14 | 2017-05-10 | 湖北中烟工业有限责任公司 | Additive for reducing woody gas in cigarette bobbin, preparation method and application thereof |
| CN106957723A (en) * | 2016-10-13 | 2017-07-18 | 武汉黄鹤楼香精香料有限公司 | A kind of cigarette preparation method of gillyflower extract |
| CN108192724A (en) * | 2018-01-10 | 2018-06-22 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of fermentation type tobacco cherry extract |
| CN109181877A (en) * | 2018-09-20 | 2019-01-11 | 云南中烟工业有限责任公司 | The high efficiency extraction and refining methd and purposes of a kind of tree moss absolute |
| CN109730366A (en) * | 2019-03-05 | 2019-05-10 | 铂德（深圳）科技有限公司 | Cherry extract solution, cherry electronics tobacco tar and preparation method thereof |
| CN111671131A (en) * | 2020-06-22 | 2020-09-18 | 福建中烟工业有限责任公司 | Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof |
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| CN104621705A (en) * | 2015-01-20 | 2015-05-20 | 川渝中烟工业有限责任公司 | Electronic cigarette juice comprising physalis pubescens extractive |
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| CN1400300A (en) * | 2001-08-01 | 2003-03-05 | 云南瑞升科技有限公司 | Method for deep-processing tobacco extract to prepare tobacco cleaned oil and enriched solanesol |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105768198B (en) * | 2016-04-29 | 2017-09-19 | 江苏中烟工业有限责任公司 | Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof |
| CN105768198A (en) * | 2016-04-29 | 2016-07-20 | 江苏中烟工业有限责任公司 | Electronic cigarette juice with moss faint scent feature and preparation method thereof |
| CN106957723A (en) * | 2016-10-13 | 2017-07-18 | 武汉黄鹤楼香精香料有限公司 | A kind of cigarette preparation method of gillyflower extract |
| CN106638160A (en) * | 2016-10-14 | 2017-05-10 | 湖北中烟工业有限责任公司 | Additive for reducing woody gas in cigarette bobbin, preparation method and application thereof |
| CN106522022A (en) * | 2016-10-26 | 2017-03-22 | 湖北中烟工业有限责任公司 | Additive for sheet cigarette paper of cigars as well as preparation method and application of additive |
| CN106433975B (en) * | 2016-11-25 | 2019-10-18 | 中国烟草总公司郑州烟草研究院 | A method of utilizing the low As content tree moss absolute of molecular clock |
| CN106433975A (en) * | 2016-11-25 | 2017-02-22 | 中国烟草总公司郑州烟草研究院 | Method for preparing low-As-content tree moss absolute by molecular distillation |
| CN108192724A (en) * | 2018-01-10 | 2018-06-22 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of fermentation type tobacco cherry extract |
| CN109181877A (en) * | 2018-09-20 | 2019-01-11 | 云南中烟工业有限责任公司 | The high efficiency extraction and refining methd and purposes of a kind of tree moss absolute |
| CN109181877B (en) * | 2018-09-20 | 2021-07-13 | 云南中烟工业有限责任公司 | Efficient extraction and refining method and application of tree moss absolute |
| CN109730366A (en) * | 2019-03-05 | 2019-05-10 | 铂德（深圳）科技有限公司 | Cherry extract solution, cherry electronics tobacco tar and preparation method thereof |
| CN111671131A (en) * | 2020-06-22 | 2020-09-18 | 福建中烟工业有限责任公司 | Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof |
| CN111671131B (en) * | 2020-06-22 | 2022-04-22 | 福建中烟工业有限责任公司 | Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof |
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Application publication date: 20150826 |