JP2014057573A - Method for producing extract of papaya leaf and application to cigarette - Google Patents
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- 235000009467 Carica papaya Nutrition 0.000 title claims abstract description 52
- 241000219173 Carica Species 0.000 title claims abstract description 48
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 13
- 241000208125 Nicotiana Species 0.000 claims abstract description 36
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 238000003809 water extraction Methods 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims 1
- 230000000391 smoking effect Effects 0.000 abstract description 10
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- 238000012360 testing method Methods 0.000 abstract description 5
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- 238000011156 evaluation Methods 0.000 abstract description 4
- 230000005923 long-lasting effect Effects 0.000 abstract description 4
- 230000007794 irritation Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 description 7
- NPNUFJAVOOONJE-ZIAGYGMSSA-N β-(E)-Caryophyllene Chemical compound C1CC(C)=CCCC(=C)[C@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-ZIAGYGMSSA-N 0.000 description 6
- 240000006432 Carica papaya Species 0.000 description 5
- 239000000341 volatile oil Substances 0.000 description 5
- 239000011521 glass Substances 0.000 description 4
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 4
- NVEQFIOZRFFVFW-UHFFFAOYSA-N 9-epi-beta-caryophyllene oxide Natural products C=C1CCC2OC2(C)CCC2C(C)(C)CC21 NVEQFIOZRFFVFW-UHFFFAOYSA-N 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 3
- 235000006679 Mentha X verticillata Nutrition 0.000 description 3
- 235000002899 Mentha suaveolens Nutrition 0.000 description 3
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 3
- FAMPSKZZVDUYOS-UHFFFAOYSA-N alpha-Caryophyllene Natural products CC1=CCC(C)(C)C=CCC(C)=CCC1 FAMPSKZZVDUYOS-UHFFFAOYSA-N 0.000 description 3
- NPNUFJAVOOONJE-UHFFFAOYSA-N beta-cariophyllene Natural products C1CC(C)=CCCC(=C)C2CC(C)(C)C21 NPNUFJAVOOONJE-UHFFFAOYSA-N 0.000 description 3
- 229940117948 caryophyllene Drugs 0.000 description 3
- NPNUFJAVOOONJE-UONOGXRCSA-N caryophyllene Natural products C1CC(C)=CCCC(=C)[C@@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-UONOGXRCSA-N 0.000 description 3
- -1 damacenone Chemical compound 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 2
- LTMQZVLXCLQPCT-UHFFFAOYSA-N 1,1,6-trimethyltetralin Chemical compound C1CCC(C)(C)C=2C1=CC(C)=CC=2 LTMQZVLXCLQPCT-UHFFFAOYSA-N 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 2
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 2
- IMKHDCBNRDRUEB-UHFFFAOYSA-N Dihydroactinidiolide Natural products C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 description 2
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 2
- 235000003140 Panax quinquefolius Nutrition 0.000 description 2
- 206010036790 Productive cough Diseases 0.000 description 2
- KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 description 2
- 239000010634 clove oil Substances 0.000 description 2
- IMKHDCBNRDRUEB-LLVKDONJSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)O[C@@]21C IMKHDCBNRDRUEB-LLVKDONJSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000008434 ginseng Nutrition 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 235000001510 limonene Nutrition 0.000 description 2
- 229940087305 limonene Drugs 0.000 description 2
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229940041616 menthol Drugs 0.000 description 2
- 208000024794 sputum Diseases 0.000 description 2
- 210000003802 sputum Anatomy 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 1
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 208000000059 Dyspnea Diseases 0.000 description 1
- 206010013975 Dyspnoeas Diseases 0.000 description 1
- 239000001293 FEMA 3089 Substances 0.000 description 1
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 description 1
- 241000745768 Pluchea carolinensis Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000001754 anti-pyretic effect Effects 0.000 description 1
- 239000002221 antipyretic Substances 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 230000003177 cardiotonic effect Effects 0.000 description 1
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- 238000013461 design Methods 0.000 description 1
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- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- HNZUNIKWNYHEJJ-FMIVXFBMSA-N geranyl acetone Chemical compound CC(C)=CCC\C(C)=C\CCC(C)=O HNZUNIKWNYHEJJ-FMIVXFBMSA-N 0.000 description 1
- HNZUNIKWNYHEJJ-UHFFFAOYSA-N geranyl acetone Natural products CC(C)=CCCC(C)=CCCC(C)=O HNZUNIKWNYHEJJ-UHFFFAOYSA-N 0.000 description 1
- 230000007407 health benefit Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229930002839 ionone Natural products 0.000 description 1
- 150000002499 ionone derivatives Chemical class 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000007721 medicinal effect Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229930003647 monocyclic monoterpene Natural products 0.000 description 1
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- 150000003233 pyrroles Chemical class 0.000 description 1
- 238000004451 qualitative analysis Methods 0.000 description 1
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- 238000007670 refining Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 208000013220 shortness of breath Diseases 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
【課題】パパイヤ葉抽出液の製造方法及び紙巻タバコへの応用の提供。
【解決手段】パパイヤ葉抽出液の製造方法及び紙巻タバコへの応用は、水抽出或いは異なる濃度のアルコール抽出によってパパイヤ葉の抽出液を取得し、作製済みの刻みタバコ重量の0.02〜5％のパパイヤ葉抽出液を前記刻みタバコの上に均等にスプレーしてタバコを作り出す。紙巻タバコ中にパパイヤ葉抽出液を添加した試験の評価分析結果から理解される通り、パパイヤ葉抽出液は、タバコの香りと調和し、香りの質を向上させ、タバコの香りが豊富で、香りは清々しくはっきりとし、性質は鮮明であり、柔らかくきめ細やかで、絶えることなく長く続く感じが良好であり、タバコ喫煙時の満足感を高め、刺激は明らかに減少し、タバコ喫煙の快適度を高め、余韻を楽しませ、煙の濃度及び勢いが適度である。
【選択図】なしA method for producing a papaya leaf extract and its application to cigarettes.
SOLUTION: A method for producing papaya leaf extract and its application to cigarettes is obtained by obtaining papaya leaf extract by water extraction or alcohol extraction of different concentrations, and 0.02-5% of the weight of the prepared cut tobacco. The leaf extract is sprayed evenly on the chopped tobacco to produce tobacco. As can be seen from the evaluation analysis results of the test with papaya leaf extract added to cigarettes, the papaya leaf extract harmonizes with the scent of tobacco, improves the quality of the scent, is rich in tobacco scent, Is clear and clear, has a clear character, is soft and fine, has a long lasting feeling, increases the satisfaction of smoking cigarettes, significantly reduces irritation and reduces the comfort of smoking High, entertaining lingering, moderate smoke concentration and momentum.
[Selection figure] None
Description
本発明はパパイヤ葉抽出液の製造方法及び紙巻タバコへの応用に関する。 The present invention relates to a method for producing papaya leaf extract and its application to cigarettes.
タバコと健康の問題が益々注目されるようになるに従い、紙巻タバコ喫煙の安全性、保健機能の向上、紙巻タバコの煙中の有害成分の低下が紙巻タバコの発展に必要な課題となった。よって、市場には朝鮮人参タバコやミントタバコ等が出現した。それは、刻みタバコの中に朝鮮人参やミント等の独特な保健効果を備えた質の高い物質を混入するものである。中国での研究の主なものは、パパイヤの化学成分の測定、医療方面に関するものであり、パパイヤをタバコに応用する報道はまだ見られない。 As tobacco and health issues have become increasingly focused, the safety of cigarette smoking, improved health functions, and the reduction of harmful components in cigarette smoke have become necessary issues for the development of cigarettes. Therefore, ginseng tobacco, mint tobacco, etc. appeared in the market. It is a mixture of high quality substances with unique health benefits such as ginseng and mint in chopped tobacco. The main research in China is related to the measurement of the chemical composition of papaya and the medical field, and there are no reports of papaya applied to tobacco.
パパイヤ(Carica papaya L)は華南及び台湾、福建と雲南の一部地区特有の熱帯、亜熱帯常緑果樹であり、その収穫量は多く、色が美しく美味で、しかも糖分とビタミンを豊富に含む。特に、パパウ(Papaw)は栄養価が非常に高い。また、パパイヤの葉は漢方材であり、強心作用、むくみを取り除く作用を備える。尚、パパイヤの葉の揮発油の化学成分及びタバコや紙巻タバコへの応用に関する報告はまだ見られない。 Papaya (Carica papaya L) is a tropical and subtropical evergreen fruit tree that is peculiar to some parts of South China and Taiwan, Fujian and Yunnan. It has a high yield, beautiful color, and is rich in sugar and vitamins. In particular, Papaw is very nutritious. Papaya leaves are Chinese medicine and have a cardiotonic effect and an effect of removing swelling. There are still no reports on the chemical composition of the volatile oil of papaya leaves and its application to tobacco and cigarettes.
GC×GC/TOF-MSによってパパイヤ葉揮発油の定性分析を行なったところ、相似度≧800の化学成分に、トータルイオンクロマトグラム、逆相似度、及び可能性データを結合し、整合度の高い化学成分383種を判定する(表1参照)。尚、アルコール37種、アルデヒド53種、酸21種、アルカン49種、アルケン20種、ケトン82種、エステル31種を含む。 Qualitative analysis of papaya leaf volatile oil by GC × GC / TOF-MS, combined with chemical components with similarity ≧ 800, combined with total ion chromatogram, reverse similarity and possibility data, and high consistency Determine 383 chemical components (see Table 1). In addition, 37 types of alcohol, 53 types of aldehyde, 21 types of acid, 49 types of alkane, 20 types of alkene, 82 types of ketone, and 31 types of ester are included.
パパイヤ葉抽出物中の一部化学成分には特殊な香りを有する特徴と薬効がある。パパイヤ葉揮発油の中には多くの成分が含まれる(表2参照)。例えば、カリオフィレン、ジヒドロアクチニジオリド、リナロール、メントール、ゲラニルアセトン、イオノン、ダマセノン、ピラジン及びピロール類化合物等はいずれも重要な香り成分である。そのうち、ジヒドロアクチニジオリドは強烈で新鮮な葉、草の香りがあるため、高貴な清らかな香りを有する香料と言われる。カリオフィレンにはチョウジ油とテレビン油の中間のような香りを備え、チョウジ油に似た辛い香りや木の香りを有し、若干の苦味がある。メントールはミントの清涼感を備え、爽やかで、甘く、クールである。拡散力は強いが持続力は弱い特徴がある。それに対し、パパイヤ葉揮発油の主な解熱成分には、甘い香り、フルーティな香り、タバコの香りを含むという特徴があり、これらの成分には紙巻タバコの香りを調和し増加させる作用、刺激を緩和する性質、汚れた空気を覆い隠し、タバコの風味を高める作用があり、紙巻タバコの香り増加に応用できる。 Some chemical components in papaya leaf extract have special scent characteristics and medicinal properties. Papaya leaf volatile oil contains many components (see Table 2). For example, caryophyllene, dihydroactinidiolide, linalool, menthol, geranylacetone, ionone, damacenone, pyrazine, and pyrrole compounds are all important fragrance components. Among them, dihydroactinidiolide is said to be a fragrance with a noble and clean fragrance because of its intense fresh leaf and grassy scent. Caryophyllene has a scent that is intermediate between clove oil and turpentine oil, has a spicy scent similar to clove oil and a wood scent, and has a slight bitter taste. Menthol is refreshing, sweet and cool with a refreshing mint feel. Diffusion is strong but sustainability is weak. On the other hand, the main antipyretic components of papaya leaf volatile oil are characterized by containing sweet scent, fruity scent, and tobacco scent. These components have the effect of stimulating and increasing the cigarette scent. It has an alleviating property, covers dirty air, and enhances the flavor of cigarettes. It can be applied to increase the scent of cigarettes.
パパイヤ葉揮発油中の一部成分である、イオネン、リモネン、オシメン、カリオフィレン等は、消炎、咳止め、息切れを抑え、痰を取り除く作用があり、臨床上では気管支炎の治療に用いる。リモネンは、単環式モノテルペン化合物であり、無色の油状液体であり、柑橘系の香りをもつ。咳の抑制、痰の除去、静菌作用を備える。これらの化学成分にはタバコによる呼吸器系の疾病を緩和させたり咳を抑える作用があるため、タバコの添加剤としての使用が可能であり、紙巻タバコ独特の香りをもつ特徴や薬効によって、喫煙時の安全性を高めることができる。 Ionene, limonene, osymene, caryophyllene, etc., which are some components in papaya leaf volatile oil, have anti-inflammatory, coughing, shortness of breath and action to remove sputum, and are clinically used to treat bronchitis. Limonene is a monocyclic monoterpene compound, is a colorless oily liquid, and has a citrus scent. Cough suppression, sputum removal, bacteriostatic action. These chemical ingredients can alleviate respiratory diseases caused by tobacco and suppress coughing, so they can be used as tobacco additives. The safety at the time can be increased.
本発明は、製造したタバコの香りは清々しくはっきりし、喫煙時の満足感と快適度を高め、煙の濃度及び勢いを適度にし、パパイヤ葉抽出液の製造方法及び紙巻タバコへの応用を提供する。 The present invention provides a method for producing papaya leaf extract and its application to cigarettes, with a clear and clear scent of the tobacco produced, increasing the satisfaction and comfort level of smoking, moderate smoke concentration and momentum. To do.
パパイヤ葉抽出液の製造方法及び紙巻タバコへの応用は、水抽出或いは異なる濃度のアルコール抽出によってパパイヤ葉の抽出液を取得し、作製済みの刻みタバコ重量の0.02〜5％のパパイヤ葉抽出液を前記刻みタバコの上に均等にスプレーしてタバコを作り出す。 The method for producing papaya leaf extract and its application to cigarettes is to obtain papaya leaf extract by water extraction or alcohol extraction of different concentration, and use papaya leaf extract of 0.02-5% of the weight of the cut tobacco that has been prepared. Spray evenly onto the chopped tobacco to produce tobacco.
本発明は、紙巻タバコ中にパパイヤ葉抽出液を添加した試験の評価分析結果から理解される通り、パパイヤ葉抽出液はタバコの香りと調和し、香りの質を向上させ、香りが豊富で清々しくはっきりとし、柔らかくきめ細やかで、絶えることなく長く続く感じが良好であり、喫煙時の満足感を高め、刺激は明らかに減少し、喫煙の快適度を高め、煙の濃度及び勢いが適度である。 As is understood from the evaluation and analysis results of the test in which the papaya leaf extract was added to the cigarette, the present invention is harmonized with the scent of tobacco, improves the scent quality, is rich in scent and refreshed. Crisp, clear, soft and fine, with a long lasting feeling, increased smoking satisfaction, reduced irritation, increased smoking comfort, moderate smoke concentration and momentum is there.
次に、具体的な実施例を用いて本発明の詳細説明をする。尚、以下の実施例は、本発明を説明するために用いたものであり、本発明の実施範囲を制約するものではない。 Next, the present invention will be described in detail using specific examples. The following examples are used for explaining the present invention and do not limit the scope of the present invention.
パパイヤ葉抽出液の製造方法及び紙巻タバコへの応用の具体的実施例は次のとおりである。 Specific examples of the method for producing papaya leaf extract and its application to cigarettes are as follows.
まず、パパイヤ葉を細かく砕き、細かく砕いたパパイヤ葉の粉末20gを500mlのフラスコに入れ、120g、50％のエタノールを加え、60℃の恒温で6時間超音波抽出を行なう。その後、抽出液を高速遠心機を用いて遠心分離した後、上澄み液を濃縮してペースト状にし、茶褐色のガラス瓶に移し変えて密封し予備とする。
製造したパパイヤ葉のペースト状濃縮液を70％のエタノールを用いて溶解、希釈するとパパイヤ葉抽出液の溶液となる。次に、刻みタバコ100gに対し0.02％のパパイヤ葉抽出液(0.02g)を取り出す。希釈液を刻みタバコ上に均等にスプレーした後、スプレーの済んだ刻みタバコを温度22℃±1℃、RH60％±2％の恒温恒湿の箱の中に48時間放置し平衡させると、タバコが完成する。
紙巻タバコ中にパパイヤ葉抽出液を添加する試験の評価分析結果は次のとおりである。パパイヤ葉抽出液はタバコの香りと調和し、香りの質を向上させ、タバコの香りが豊富で、香りは清々しくはっきりと鮮明であり、柔らかくきめ細やかで、絶えることなく長く続く感じが良好であり、喫煙時の満足感を高め、刺激は明らかに減少し、喫煙の快適度を高め、余韻を楽しませ、煙の濃度及び勢いが適度である。
First, papaya leaves are finely crushed, 20 g of finely crushed papaya leaves powder is put into a 500 ml flask, 120 g, 50% ethanol is added, and ultrasonic extraction is performed at a constant temperature of 60 ° C. for 6 hours. Then, after the extract is centrifuged using a high-speed centrifuge, the supernatant is concentrated to a paste, transferred to a brown glass bottle, sealed, and used as a spare.
The prepared papaya leaf paste concentrate is dissolved and diluted with 70% ethanol to form a papaya leaf extract solution. Next, 0.02% of papaya leaf extract (0.02 g) is taken out per 100 g of chopped tobacco. After the diluted solution is sprayed evenly on the tobacco, the sprayed tobacco is allowed to stand in a constant temperature and humidity box at a temperature of 22 ° C ± 1 ° C and RH 60% ± 2% for 48 hours. Is completed.
The results of the evaluation analysis of the test of adding papaya leaf extract to cigarettes are as follows. The papaya leaf extract harmonizes with the scent of tobacco, improves the quality of the scent, is rich in the scent of tobacco, the scent is refreshingly clear and crisp, soft and fine, and has a long lasting feeling. Yes, it increases smoking satisfaction, irritation is clearly reduced, smoking comfort is enhanced, reverberation is enjoyed, smoke concentration and momentum are moderate.
まず、パパイヤ葉50g取り出し、2Lのフラスコに入れ、350g、65％のエタノールを加え、65℃の恒温水浴の中で8.5時間攪拌して抽出を行なう。抽出液を濾過して取得したパパイヤ葉抽出液を茶褐色のガラス瓶に移し変えて密封し予備とする。
まず、刻みタバコ100gを取り出した後、前記パパイヤ葉抽出液3.5gを取り出す。抽出液を取り出した刻みタバコ上に均等にスプレーした後、スプレーの済んだ刻みタバコを、温度22℃±1℃、RH60％±2％の恒温恒湿の箱内に48時間放置し平衡させると、タバコが完成する。
First, 50 g of papaya leaves are taken out, put into a 2 L flask, 350 g, 65% ethanol is added, and extraction is performed by stirring in a constant temperature water bath at 65 ° C. for 8.5 hours. The papaya leaf extract obtained by filtering the extract is transferred to a brown glass bottle and sealed for use as a reserve.
First, after removing 100 g of chopped tobacco, 3.5 g of the papaya leaf extract is taken out. After spraying the extracted liquid evenly on the chopped tobacco, the sprayed chopped tobacco is allowed to equilibrate for 48 hours in a constant temperature and humidity box at a temperature of 22 ℃ ± 1 ℃ and RH60% ± 2%. , Tobacco is completed.
まず、パパイヤ葉100gを取り出し、該パパイヤ葉を2Lのフラスコに入れ、1000gの水を加え、80℃の恒温水浴の中で8時間攪拌して抽出を行なう。その後、抽出液を濾過した後に、茶褐色のガラス瓶に移し変えて密封し予備とする。
刻みタバコ100gを取り出し、前記茶褐色のガラス瓶内に保存したパパイヤ葉抽出液4.5gを取り出し、該抽出液を刻みタバコ上に均等にスプレーする。スプレーの済んだ刻みタバコを温度22℃±1℃、RH60％±2％の恒温恒湿の箱内に48時間放置し平衡させると、タバコが完成する。
First, 100 g of papaya leaves are taken out, put into a 2 L flask, 1000 g of water is added, and extraction is performed by stirring for 8 hours in a constant temperature water bath at 80 ° C. Then, after the extract is filtered, it is transferred to a brown glass bottle and sealed for use as a spare.
100 g of chopped tobacco is taken out, 4.5 g of papaya leaf extract stored in the brown glass bottle is taken out, and the extract is sprayed evenly on the chopped tobacco. The sprayed chopped tobacco is left in a thermostatic and humidity box at a temperature of 22 ° C ± 1 ° C and RH 60% ± 2% for 48 hours to equilibrate.
紙巻タバコ中にパパイヤ葉抽出液を添加する試験の評価分析結果は次のとおりである。即ち、パパイヤ葉抽出液はタバコの香りと調和し、香りの質を向上させ、タバコの香りが豊富で清々しくはっきりとし、柔らかくきめ細やかで、絶えることなく長く続く感じが良好であり、喫煙時の満足感を高め、刺激は明らかに減少し、喫煙の快適度を高め、煙の濃度及び勢いが適度である。 The results of the evaluation analysis of the test of adding papaya leaf extract to cigarettes are as follows. That is, the papaya leaf extract harmonizes with the scent of tobacco, improves the quality of the scent, is rich in tobacco scent, is clear and clear, soft and fine, and has a long lasting feeling that is good when smoking , Comfort is clearly reduced, smoking comfort is increased, smoke concentration and momentum are moderate.
本発明の実施例１、実施例２、実施例３の相違点は、パパイヤ葉の試験量、精錬方式、抽出時間が異なる点にある。しかし、試料はいずれもパパイヤ葉である。 The difference between the first embodiment, the second embodiment, and the third embodiment of the present invention is that the papaya leaf test amount, the refining method, and the extraction time are different. However, all samples are papaya leaves.
前述は本発明の三つの具体的な実施例である。しかし、本発明の設計構想はこれに制約されないものである。よって、この構想を用いて、本発明に対して行なう非実質的な変更は全て本発明の保護範囲の侵害行為とみなすことをここに明記する。 The foregoing are three specific embodiments of the present invention. However, the design concept of the present invention is not limited to this. Thus, using this concept, it is explicitly stated here that all non-substantial changes made to the present invention are considered infringements of the protection scope of the present invention.
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| CN201210344626.5A CN103653238B (en) | 2012-09-17 | 2012-09-17 | The application of papaya leaf extract in cigarette |
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| CN111351889A (en) * | 2020-03-18 | 2020-06-30 | 福建中烟工业有限责任公司 | Method for separating and screening sweet and clear components in Sanming Youyi tobacco leaves |
| CN113604281A (en) * | 2021-08-13 | 2021-11-05 | 云南中烟新材料科技有限公司 | Preparation method and application of natural spice based on snake skin fruits |
| EP3820305A4 (en) * | 2018-07-12 | 2022-04-27 | International Flavors & Fragrances Inc. | Ligustrosidic acid and derivatives thereof for sweetness enhancement |
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| JP2008214299A (en) * | 2007-03-07 | 2008-09-18 | Innovatis Pharma Corp | Composition for prevention, treatment, or amelioration of cancer containing water-soluble extract constituents of carica papaya and hedyotis diffusa |
| JP2012000100A (en) * | 2010-06-18 | 2012-01-05 | China Tobacco Fujian Industrial Corp | Method for producing regenerated tobacco by using morinda root and use of morinda root regenerated tobacco produced thereby in tobacco product |
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| CN1142530A (en) * | 1996-05-03 | 1997-02-12 | 云南省烟草工业研究所 | Tobacco improving agent, preparation and application thereof |
| CN1298826C (en) * | 2004-07-04 | 2007-02-07 | 云南烟草科学研究院 | Method for preparing reactive mixture flavor and its use in tobacco |
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| JP2008505887A (en) * | 2004-07-06 | 2008-02-28 | 幾夫 森本 | A composition for preventing, treating or ameliorating cancer comprising papaya extract |
| JP2008214299A (en) * | 2007-03-07 | 2008-09-18 | Innovatis Pharma Corp | Composition for prevention, treatment, or amelioration of cancer containing water-soluble extract constituents of carica papaya and hedyotis diffusa |
| JP2012000100A (en) * | 2010-06-18 | 2012-01-05 | China Tobacco Fujian Industrial Corp | Method for producing regenerated tobacco by using morinda root and use of morinda root regenerated tobacco produced thereby in tobacco product |
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| EP3820305A4 (en) * | 2018-07-12 | 2022-04-27 | International Flavors & Fragrances Inc. | Ligustrosidic acid and derivatives thereof for sweetness enhancement |
| CN111351889A (en) * | 2020-03-18 | 2020-06-30 | 福建中烟工业有限责任公司 | Method for separating and screening sweet and clear components in Sanming Youyi tobacco leaves |
| CN113604281A (en) * | 2021-08-13 | 2021-11-05 | 云南中烟新材料科技有限公司 | Preparation method and application of natural spice based on snake skin fruits |
| CN113604281B (en) * | 2021-08-13 | 2023-04-21 | 云南中烟新材料科技有限公司 | Preparation method and application of natural spice based on snake skin fruits |
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| JP5781572B2 (en) | 2015-09-24 |
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