CN101156712A - Perfume additive for natural tobacco and method for making same - Google Patents

Perfume additive for natural tobacco and method for making same Download PDF

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Publication number
CN101156712A
CN101156712A CNA2007100663048A CN200710066304A CN101156712A CN 101156712 A CN101156712 A CN 101156712A CN A2007100663048 A CNA2007100663048 A CN A2007100663048A CN 200710066304 A CN200710066304 A CN 200710066304A CN 101156712 A CN101156712 A CN 101156712A
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tobacco
natural tobacco
additive
natural
perfume additive
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CNA2007100663048A
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Chinese (zh)
Inventor
田玉红
黄天辉
邹克兴
周俊
刘政
李志华
刘远涛
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China Tobacco Guangxi Industrial Co Ltd
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China Tobacco Guangxi Industrial Co Ltd
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Priority to CNA2007100663048A priority Critical patent/CN101156712A/en
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Abstract

The invention relates to spicery additive used for natural tobacco and being capable of increasing the mellow as well as relieving the throat symptoms, the main raw material adopts star anise, cinnamon, and red river gum leaf with the weight ratio of 5.0-30.0:40.0-80.0:30.0. The invention adopts the preparation method that the monomer of the spicery additive used for the natural tobacco is prepared firstly, and then the monomer of the spicery additive is blended to be the spicery additive used for the natural tobacco. The spicery additive used for the natural tobacco of the invention ensures that the natural fragrant plants is blended reasonably and is added to tobacco thread samples after the natural fragrant plants are extracted and concentrated, thereby obviously enhancing the mellow of cigarettes, and improving the smoking quality of the tobacco, and leading the smoky flavor to be fragrant and elegant. The mouthfeel of the spicery additive is comfortable; the spicery additive can promote the saliva secretion in the oral cavity, reliever the throat uncomfortable symptoms, and achieve the effect that the harm from smoking is reduced.

Description

A kind of perfume additive for natural tobacco and preparation method thereof
Technical field
The present invention relates to a kind of perfume additive for natural tobacco that increases sweet degree, alleviation throat symptom and preparation method thereof.
Background technology
Because the propaganda that Smoking is harmful to your health, the production of safe cigarette becomes the problem that cigarette industry extremely is concerned about already.One of its measure is the content that will reduce T/N in the flue gas, and this tends to cause smoke deficiency and fragrance to weaken.Therefore, under the prerequisite that reduces T/N, how to remedy the loss of fragrance and the task of raising smoke perfume quality, and about the perfuming problem of secondary tobacco leaf, expanded cut tobacco, tobacco leaf substitute etc., become an urgent demand that current tobacco industry is researched and proposed flavouring essence for tobacco, and promoting the raising and the development of development of cigarette odor additive and flavouring essence for tobacco meat flavor formulating technology thus.Comprise China, global tobacco business is all attached great importance to the development and utilization of essence spice for cigarette, and the technology that can produce high-quality essence and flavoring agent is used as oneself wuwa, to seek occupying perch in intense market competition.Assorted gas in the flue gas and flue gas all have much relations with the sucking quality of cigarette to the stimulation of oral cavity, throat, how effectively to reduce assorted gas in the flue gas, reduce flue gas to the stimulation of throat, reduce the flue gas drying sense, strengthen flue gas promote the production of body fluid sense, raising cigarette comfort level, alleviating the harm that smoking brings to health of smokers, is the work that the tobacco scientific workers are sticking at.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of perfume additive for natural tobacco that increases sweet degree, alleviation throat symptom and preparation method thereof.
The present invention solves the problems of the technologies described above with following technical scheme:
Preparing used primary raw material of this perfume additive for natural tobacco and consumption thereof is:
Anistree: Chinese cassia tree: the weight ratio of eucalyptus camaldulensis leaf is 5.0~30.0: 40.0~80.0: 5.0~30.0;
The preparation method of this perfume additive for natural tobacco is:
A, preparation perfume additive for natural tobacco monomer: after above-mentioned raw materials is crushed to a certain size, place the steam distillation device to distill extraction respectively, the distillation time of anise, Chinese cassia tree, eucalyptus camaldulensis leaf was respectively 0.5~8 hour, collect the distillation extract of anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively, obtain the raw material monomer of natural tobacco additive;
The allotment of b, perfume additive for natural tobacco: the extract of the anise that will extract, Chinese cassia tree, eucalyptus camaldulensis leaf, being dissolved in a certain amount of weight ratio is ethanol: propane diols=60~100: allocate in 0~40 the solvent, obtain perfume additive for natural tobacco.
The invention has the beneficial effects as follows that a natural perfume plant adds in the sample pipe tobacco after rationally compatibility, extraction concentrate, can obviously increase the sweet degree of cigarette, lifting cigarette perfume (or spice), can promote simultaneously the saliva of buccal cavity secretion, increase the humectation effect, the oral cavity that alleviation causes because of flue gas, the dry malaise symptoms of throat, thus harm of smoking alleviated.This perfume additive for natural tobacco is based on local resource, and preparation technology is simple, cost is low, has important market prospects.
The specific embodiment
This research is the advantage that makes full use of the distinctive natural perfume material resource in Guangxi, some had the natural perfume plant of special effect, through reasonable, scientific compatibility, be added on the pipe tobacco, can make cigarette increase the fragrant and sweet effect that promotes cigarette flavor of playing, can reduce the assorted gas in the flue gas, the malaise symptoms of alleviation throat again significantly, improve the cigarette quality.
The present invention adopts following method to prepare perfume additive for natural tobacco of the present invention:
A, preparation perfume additive for natural tobacco monomer: after above-mentioned raw materials is crushed to a certain size, place the steam distillation device to distill extraction respectively, the distillation time of anise, Chinese cassia tree, eucalyptus camaldulensis leaf was respectively 0.5~8 hour, collect the distillation extract of anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively, obtain the raw material monomer of perfume additive for natural tobacco;
The allotment of b, perfume additive for natural tobacco: the extract of the anise that will extract, Chinese cassia tree, eucalyptus camaldulensis leaf, being dissolved in a certain amount of weight ratio is ethanol: propane diols=60~100: allocate in 0~40 the solvent, obtain perfume additive for natural tobacco.
The perfume additive for natural tobacco that makes is used for the production of cigarette, cigarette, pipe tobacco, stem or reconstituted tobacoo by 0.05%~2% of pipe tobacco weight.
For ease of better understanding the present invention, enforcement of the present invention is illustrated especially exemplified by example.Present embodiment only is the explanation to most preferred embodiment of the present invention, not should be understood to limitation of the present invention.
Embodiment 1
(1) preparation perfume additive for natural tobacco monomer: get 50 gram Chinese anises, 300 gram Chinese cassia trees, 50 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 6 hours, Chinese cassia tree distillation 3 hours, the eucalyptus camaldulensis leaf distilled 1 hour, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 1 kilogram is an ethanol: allocate in the solvent of propane diols=80: 20, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 0.15% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Sensory evolution is the result show: clear of fragrance, comparatively coordinate with the delicate fragrance type cigarette, and can obviously increase the sweet degree of cigarette, improve tobacco and inhale flavor, make the fragrant saturating unstable ease of cigarette.Comfortable taste can promote the saliva of buccal cavity secretion, alleviates oral cavity, the dry malaise symptoms of throat, has reached the effect that alleviates harm of smoking.
Embodiment 2
(1) preparation perfume additive for natural tobacco monomer: get 100 gram Chinese anises, 200 gram Chinese cassia trees, 40 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 2 hours, Chinese cassia tree distillation 3 hours, the eucalyptus camaldulensis leaf distilled 3 hours, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 1.5 kilograms is an ethanol: allocate in the solvent of propane diols=70: 30, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 0.3% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 3
(1) preparation perfume additive for natural tobacco monomer: get 150 gram Chinese anises, 400 gram Chinese cassia trees, 50 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 6 hours, Chinese cassia tree distillation 2 hours, the eucalyptus camaldulensis leaf distilled 0.5 hour, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 25 kilograms is an ethanol: allocate in the solvent of propane diols=65: 35, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 2% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 4
(1) preparation perfume additive for natural tobacco monomer: get 30 gram Chinese anises, 500 gram Chinese cassia trees, 50 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 8 hours, Chinese cassia tree distillation 4 hours, the eucalyptus camaldulensis leaf distilled 1 hour, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 6.5 kilograms is an ethanol: allocate in the solvent of propane diols=60: 40, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 0.5% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 5
(1) preparation perfume additive for natural tobacco monomer: get 100 gram Chinese anises, 200 gram Chinese cassia trees, 75 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 3 hours, Chinese cassia tree distillation 1 hour, the eucalyptus camaldulensis leaf distilled 6 hours, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 7 kilograms is an ethanol: allocate in the solvent of propane diols=75: 25, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 1% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 6
(1) preparation perfume additive for natural tobacco monomer: get 120 gram Chinese anises, 160 gram Chinese cassia trees, 120 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 6 hours, Chinese cassia tree distillation 0.5 hour, the eucalyptus camaldulensis leaf distilled 1 hour, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively;
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 1 kilogram is an ethanol: allocate in the solvent of propane diols=95: 5, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 0.15% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 7
(1) preparation perfume additive for natural tobacco monomer: get 100 gram Chinese anises, 200 gram Chinese cassia trees, 50 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 2 hours, Chinese cassia tree distillation 3 hours, the eucalyptus camaldulensis leaf distilled 8 hours, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 1.5 kilograms is an ethanol: allocate in the solvent of propane diols=100: 0, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 0.3% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 8
(1) preparation perfume additive for natural tobacco monomer: get 150 gram Chinese anises, 400 gram Chinese cassia trees, 50 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 8 hours, Chinese cassia tree distillation 2 hours, the eucalyptus camaldulensis leaf distilled 0.5 hour, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 25 kilograms is an ethanol: allocate in the solvent of propane diols=65: 35, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 2% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 9
(1) preparation perfume additive for natural tobacco monomer: get 30 gram Chinese anises, 500 gram Chinese cassia trees, 50 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 8 hours, Chinese cassia tree distillation 0.5 hour, the eucalyptus camaldulensis leaf distilled 1 hour, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 6.5 kilograms is an ethanol: allocate in the solvent of propane diols=60: 40, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 0.5% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
Embodiment 10
(1) preparation perfume additive for natural tobacco monomer: get 100 gram Chinese anises, 200 gram Chinese cassia trees, 75 gram eucalyptus camaldulensis leaves and be crushed to suitable particle respectively, Chinese anise is placed steam distillation device distillation 3 hours, Chinese cassia tree distillation 1 hour, the eucalyptus camaldulensis leaf distilled 8 hours, collected the distillation extract of Chinese anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively.
(2) allotment of perfume additive for natural tobacco: with the perfume additive for natural tobacco monomer that obtains, the weight ratio that is dissolved in 9.5 kilograms is an ethanol: allocate in the solvent of propane diols=90: 10, obtain perfume additive for natural tobacco.
With the perfume additive for natural tobacco that makes 1% ratio in pipe tobacco weight, be sprayed at according to the process of conventional perfuming and roll into cigarette on the sample pipe tobacco and prop up, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.Effect is with embodiment 1.
The effect of perfume additive for natural tobacco raw material of the present invention is:
(1) Chinese anise (Illicium verum Hook.f.)
Chinese anise is the dry fruit of Magnoliaceae Illicium plant Chinese anise, is the economic tree in China south important " integration of drinking and medicinal herbs ", mainly is distributed in the provinces and regions such as Guangxi, Guangdong, Yunnan of China.Chinese anise is the special product spice and the Chinese medicine of China, also is the condiment of herbal, in food processing industry and perfume industry extensive use.Contain aromatic oil about 5%~8% in the Chinese anise, the principal component of oil of badian is trans-anethole (content is 75%~85%), other main component also comprises anisaldehyde, γ-Song Youxi, α-terpinene, australene, nopinene, α-and β-phellandrene, the cis anethole, β-carypohyllene, to the allyl benzene methyl ether, citrene, chavicol methyl ether, anise ketone, laurene, anisoxide, terpinolene, 1, the 8-cineole, methyl-4-cumene, linalool, alpha-terpineol and terpinenol and benzoic acid, salicylic acid, palmitic acid, isoangelic acid and some other phenolic acid etc. [2-8]Oil of badian has characteristic perfume of Chinese anise and sweet taste, be generally used for engineered food essence, daily essence etc.,, be used for tobacco flavoring as drinks, beverage, candy, baked goods, chewing gum, cigarette etc., it is obvious to increase sweet removal of impurities effect, makes cigarette perfume (or spice) more elegant.
(2) Chinese cassia tree (Cinnamomum cassia Presl):
Chinese cassia tree is the dry bark of Lauraceae cinnamon xylocinnamomum, often claims cassia bark, integrates spices, medicinal material and uses material.Chinese cassia tree mainly is distributed in Guangxi, Guangdong in China, secondly is Hainan, Yunnan, Fujian.Chinese cassia tree, the sweet perfume (or spice) of distinguishing the flavor of, the hot temperature of property has warming meridians and promoting circulation of qi, the dry stomach of invigorating the spleen, the detumescence dampness removing, the function of sweating expelling pathogenic factors from muscles and skin, Chinese cassia tree is also with genseng, pilose antler, bird's nest and be called " ginseng and pilose antler swallow osmanthus ".Be rich in volatile oil in the Chinese cassia tree, oil yield is 1%~2%, and the main component in the oil is a cinnamic acid, and content reaches 75%~85%, and contains a small amount of cinnamyl alcohol, acetate cassia bark ester, cinnamic acid, benzaldehyde etc.Cinnamon oil also is widely used as commodity spices and foodstuff flavouring spices, the fragrance that contains sweetness and slightly stimulate, and hot sweet and warm is hot fragrant, be with burnt wooden cream perfume (or spice), smell is dense, uses in tobacco and can cover the assorted gas of earth, correct and inhale flavor, improve tobacco and inhale flavor, make the fragrant saturating unstable ease of cigarette.
(3) eucalyptus camaldulensis leaf (Eucalyptus camaldulensis)
The eucalyptus camaldulensis leaf is the blade of Myrtaceae eucalyptus plant eucalyptus camaldulensis.Folium eucalypti is in China or planting areas at other all is herbal medicine commonly used among the people.Be rich in volatile oil in the eucalyptus camaldulensis leaf, oil content is 2.5~2.8% (in the leaves that dry in the shade), and the main chemical compositions in the eucalyptus oil is 1, and 8-cineole (content is up to 50%~70%) secondly also has australene, globulol, terpinyl acetate and alpha-terpineol.1, the 8-cineole can be treated influenza, flu, bacillary dysentery, enteritis and various infection, can be used as the gas inhalant and is used for the treatment of breathing problem, alleviates the gentle spasm of separating of headache.Pharmacological evaluation shows that 1,8 cineole has gentle spread effect to nasal cavity and bronchial mucosa, can promote the mucus secretion, thereby the nasal cavity and the bronchus that help mediation to stop up, while saliva stimulating gland, promoting to salivate produces and secretion, keeps oral cavity and throat moistening.
The eucalyptus camaldulensis leaf oil still is a kind of blue or green fragrant perfume, and being used for the tobacco perfuming, can to increase on the one hand tobacco blue or green fragrant, on the other hand can the saliva stimulating gland, promote to salivate to reach the purpose of humectation, and alleviate oral cavity, throat's dry sensation that flue gas causes.

Claims (2)

1. perfume additive for natural tobacco that increases sweet degree, alleviates throat's symptom, its primary raw material is: anise: Chinese cassia tree: the weight ratio of eucalyptus camaldulensis leaf is 5.0~30.0: 40.0~80.0: 5.0~30.0.
2. a kind of preparation method who increases sweet degree, alleviates the perfume additive for natural tobacco of throat's symptom according to claim 1, described preparation process is:
A, preparation perfume additive for natural tobacco monomer: after above-mentioned raw materials is crushed to a certain size, place the steam distillation device to distill extraction respectively, the distillation time of anise, Chinese cassia tree, eucalyptus camaldulensis leaf was respectively 0.5~8 hour, collect the distillation extract of anise, Chinese cassia tree, eucalyptus camaldulensis leaf respectively, obtain the raw material monomer of natural tobacco additive;
The allotment of b, perfume additive for natural tobacco: the extract of the anise that will extract, Chinese cassia tree, eucalyptus camaldulensis leaf, being dissolved in a certain amount of weight ratio is ethanol: propane diols=60~100: allocate in 0~40 the solvent, obtain perfume additive for natural tobacco.
CNA2007100663048A 2007-10-18 2007-10-18 Perfume additive for natural tobacco and method for making same Pending CN101156712A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102396779A (en) * 2010-09-07 2012-04-04 何成钧 Chinese medicine environment-friendly cigarettes
RU2593093C1 (en) * 2015-04-20 2016-07-27 Олег Иванович Квасенков Method for production of hookah smoking composition
CN113088391A (en) * 2021-04-14 2021-07-09 云南中烟工业有限责任公司 Glutinous rice flavor type essence for cigarette and cigarette containing essence

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102396779A (en) * 2010-09-07 2012-04-04 何成钧 Chinese medicine environment-friendly cigarettes
CN102396779B (en) * 2010-09-07 2013-09-04 何成钧 Chinese medicine environment-friendly cigarettes
RU2593093C1 (en) * 2015-04-20 2016-07-27 Олег Иванович Квасенков Method for production of hookah smoking composition
CN113088391A (en) * 2021-04-14 2021-07-09 云南中烟工业有限责任公司 Glutinous rice flavor type essence for cigarette and cigarette containing essence

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