CN104489901A - Tobacco taste electronic tobacco liquid - Google Patents

Tobacco taste electronic tobacco liquid Download PDF

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Publication number
CN104489901A
CN104489901A CN201410721776.2A CN201410721776A CN104489901A CN 104489901 A CN104489901 A CN 104489901A CN 201410721776 A CN201410721776 A CN 201410721776A CN 104489901 A CN104489901 A CN 104489901A
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CN
China
Prior art keywords
tobacco
ethanol
taste
propane diols
extract
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201410721776.2A
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Chinese (zh)
Other versions
CN104489901B (en
Inventor
张东豫
徐秀娟
黄光富
屈展
袁岐山
朱琦
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China Tobacco Henan Industrial Co Ltd
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China Tobacco Henan Industrial Co Ltd
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Publication date
Application filed by China Tobacco Henan Industrial Co Ltd filed Critical China Tobacco Henan Industrial Co Ltd
Priority to CN201410721776.2A priority Critical patent/CN104489901B/en
Publication of CN104489901A publication Critical patent/CN104489901A/en
Application granted granted Critical
Publication of CN104489901B publication Critical patent/CN104489901B/en
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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A24B15/26—Use of organic solvents for extraction

Abstract

The invention aims at providing tobacco taste electronic tobacco liquid. The tobacco taste electronic tobacco liquid is made of the following raw materials by weight percent: 5 to 50 percent of a tobacco extract light constituent, 5 to 10 percent of a tobacco essence, 0.5 to 2.0 percent of nicotine, 5 to 10 percent of deionized water, 100 to 20 percent of glycerol, and the balance of propylene glycol, wherein the tobacco extract light constituent is prepared by extracting tobacco material through solvent and then performing molecular distillation. As tobacco extract adopted by the electronic tobacco liquid adopts light constituent substance, the tobacco taste electronic tobacco liquid can ensure that the fragrance and taste of electronic tobacco are more close to that of the traditional tobacco and substance difficult to volatilize cannot be deposited on heating wires of the electronic tobacco, and can prolong the service life of the heating wires and improve the taste of electronic tobacco products.

Description

One grows tobacco taste tobacco juice for electronic smoke
Technical field
The invention belongs to tobacco juice for electronic smoke technical field, be specifically related to one and grow tobacco taste tobacco juice for electronic smoke.
Background technology
Along with coming into effect of socio-economic development and " Framework Convention on Tobacco Control ", just there is profound change in tobacco consumption environment, electronic cigarette goods, because it is not containing harmful components such as tar, CO, hydrogen cyanide, can not produces second-hand-cigarette and without features such as burnings, receive the favor of more and more people.But because the existing consumer group is mainly in countries such as America and Europes, the essence taste of electronic cigarette is generally heavier, and seldom has tobacco taste, does not therefore meet the taste of Chinese Consumer's.
At present, also there is the electronic cigarette patent of some tobacco tastes, the tobacco juice for electronic smoke utilizing flat-flavor tobacco leaf to prepare as a kind of (application number CN201310029544.6), a kind ofly effectively improve the tobacco juice for electronic smoke (application number CN201310029551.6) of electronic cigarette aesthetic quality, simple and elegant odor type electronic cigarette atomizing tobacco juice and preparation method thereof (application number CN201210457376.6), a kind of tobacco juice for electronic smoke (application number CN201310030063.7) utilizing strong-flavor tobacco leaf to prepare.But, operation principle due to electronic cigarette is that cigarette bullet drain enters atomizer, and battery energising makes the atomizer evaporation tobacco juice that generates heat nebulize particulate, if containing more volatile-resistant substance in tobacco juice, these materials final can be deposited on atomizer, affect the atomizer life-span and produce bad mouthfeel.These tobacco taste electronic cigarette products are all directly added with tobacco extract prepared by traditional handicraft, and in extract, the heavy constituent of difficult volatilization is more, directly can affect the quality of electronic cigarette.
Summary of the invention
One is the object of the present invention is to provide to grow tobacco taste tobacco juice for electronic smoke.
For achieving the above object, the present invention adopts following technical scheme:
One grows tobacco taste tobacco juice for electronic smoke, and mixed by the raw material of following percetage by weight and make: tobacco extract light component 5-50%, flavouring essence for tobacco 5%-10%, nicotine 0.5%-2.0%, deionized water 5%-10%, glycerine 10%-20%, surplus is propane diols; Wherein said tobacco extract light component is obtained by tobacco material molecular clock after solvent extraction; Wherein said solvent is 95vt% ethanol, 95vt% ethanol/ethyl acetate mixed solvent, 95vt% ethanol/mixed with propylene glycol solvent, propane diols, glycerine or propane diols/glycerine mixed solvent; Wherein in 95vt% ethanol/ethyl acetate mixed solvent, the mass ratio of 95vt% ethanol and ethyl acetate is (4-10): 1; In 95vt% ethanol/mixed with propylene glycol solvent, the mass ratio of 95vt% ethanol and propane diols is (4-10): 1.
In the present invention when tobacco material 95vt% ethanol, 95vt% ethanol/ethyl acetate mixed solvent or 95vt% ethanol/mixed with propylene glycol solvent extraction time, the preparation of tobacco extract light component specifically comprises the following steps: cross 80-100 mesh sieve after being pulverized by tobacco material, then tobacco material quality 4-10 solvent is doubly added, extract 1-3 h at 50 DEG C-80 DEG C, filter to get filtrate after being cooled to 20-30 DEG C; Concentrate filtrate to the 1/10-1 of tobacco material quality doubly, then-15--5 DEG C of freezing 5 h-15 h, filter and obtain tobacco material extract; Add quality 8-10 propane diols doubly in tobacco material extract again to dissolve, at 40 DEG C-200 DEG C, 10Pa-10 after filtration 5carry out molecular clock under Pa condition, obtain tobacco extract light component.
In the present invention when tobacco material propane diols, glycerine or propane diols/glycerine mixed solvent (mass ratio of propane diols and glycerine can be arbitrarily than) extraction, the preparation of tobacco extract light component specifically comprises the following steps: cross 80-100 mesh sieve after being pulverized by tobacco material, add tobacco material quality 2-10 propane diols doubly, 80 DEG C-150 DEG C are extracted 1-3 h, filter after being cooled to 20-30 DEG C; At 40 DEG C-200 DEG C, 10Pa-10 5under Pa condition, molecular clock is carried out to filtrate, obtain tobacco extract light component.
Described tobacco material is all kinds offal or tobacco leaf.
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 0.01%-0.3%, Megastigmatrienone 0.01%-0.5%, tree moss essential oil 0.01%-1%, ethyl maltol 0.1%-1%, guaiacol 0.01%-0.5%, methyl cyclopentenyl ketone 0.1%-2%, cocoa extract 1%-10%, ethanol 10%-30%, surplus are propane diols.
In order to make the application obtain good effect, described nicotine is natural nicotine, and in described cocoa extract, the content of theobromine is 10-20wt%.
Relative to prior art, the present invention has the following advantages:
(1) tobacco juice for electronic smoke of the present invention with tobacco extract light component for main component, can make the fragrance of electronic cigarette and traditional cigarette, mouthfeel closer to.
(2) tobacco extract that tobacco juice for electronic smoke of the present invention is used is light component material, and volatile-resistant substance can not be had to be deposited on the heater strip of electronic cigarette, can improve the life-span of tobacco taste electronic cigarette heater strip and the mouthfeel of electronic cigarette product.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated, but protection scope of the present invention is not limited in this.
embodiment 1
One tobacco juice for electronic smoke growing tobacco taste, obtained by the mixed raw material of following percentage by weight: tobacco extract light component 40%, natural nicotine 2%, deionized water 5%, flavouring essence for tobacco 7%, glycerine 15%, all the other are propane diols.
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 0.2%, Megastigmatrienone 0.2%, tree moss essential oil 1%, ethyl maltol 1%, guaiacol 0.2%, methyl cyclopentenyl ketone 0.5%, cocoa extract (content of theobromine is 15wt%) 5%, ethanol 20%, surplus are propane diols.
Tobacco extract light component is obtained by following methods: cross 100 mesh sieves after being pulverized by tobacco leaf, add the propane diols of quality of tobacco 8 times, and 130 DEG C are extracted 2h, filter after being cooled to 25 DEG C; 100 DEG C, molecular clock carried out to filtrate under 70Pa condition and get final product.
embodiment 2
One tobacco juice for electronic smoke growing tobacco taste, obtained by the mixed raw material of following percentage by weight: tobacco extract light component 5%, natural nicotine 1.2%, deionized water 5%, flavouring essence for tobacco 10%, glycerine 20%, all the other are propane diols.
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 0.05%, Megastigmatrienone 0.1%, tree moss essential oil 0.08%, ethyl maltol 0.5%, guaiacol 0.1%, methyl cyclopentenyl ketone 2%, cocoa extract (content of theobromine is 20wt%) 1%, ethanol 10%, surplus are propane diols.
Tobacco extract light component is obtained by following methods: cross 80 mesh sieves after being pulverized by tobacco material, then add the 95vt% ethanol of tobacco material quality 4 times, extract 1 h at 50 DEG C, filter to get filtrate after being cooled to 28 DEG C; Concentrate filtrate to 1/10 of tobacco material quality, then-15 DEG C of freezing 5 h, filter and obtain tobacco material ethanol extract; The propane diols adding quality 8 times in tobacco material ethanol extract again dissolves, after filtration 40 DEG C, carry out molecular clock under 10Pa condition and get final product; Wherein said tobacco material is offal.
embodiment 3
One tobacco juice for electronic smoke growing tobacco taste, obtained by the mixed raw material of following mass percent: tobacco extract light component 10%, natural nicotine 1.2%, deionized water 6%, flavouring essence for tobacco 10%, glycerine 10%, all the other are propane diols.
Described flavouring essence for tobacco is made up of the material of following mass percent: oxidation isophorone 0.07%, Megastigmatrienone 0.2%, tree moss essential oil 1%, ethyl maltol 1%, guaiacol 0.3%, methyl cyclopentenyl ketone 2%, cocoa extract (content of theobromine is 10wt%) 5%, ethanol 20%, surplus are propane diols.
Tobacco extract light component is obtained by following methods: offal is crossed 80 mesh sieves, then propane diols/glycerine the mixed solvent (mass ratio of propane diols and glycerine is 4:1) of tobacco material 6 times of quality is added, extract 2h at 150 DEG C, filter after being cooled to 23 DEG C and obtain filtrate; At 200 DEG C, 10 5carry out molecular clock under Pa condition and obtain tobacco extract light component.
embodiment 4
One tobacco juice for electronic smoke growing tobacco taste, obtained by the mixed raw material of following mass percent: tobacco extract light component 50%, natural nicotine 0.5%, deionized water 10%, flavouring essence for tobacco 8%, glycerine 15%, all the other are propane diols.
Described flavouring essence for tobacco is made up of the material of following mass percent: oxidation isophorone 0.01%, Megastigmatrienone 0.5%, tree moss essential oil 0.01%, ethyl maltol 0. 1%, guaiacol 0.01%, methyl cyclopentenyl ketone 0.1%, cocoa extract (content of theobromine is 15wt%) 10%, ethanol 30%, surplus are propane diols.
Tobacco extract light component is obtained by following methods: cross 100 mesh sieves after being pulverized by tobacco material, then the 95vt% ethanol/ethyl acetate mixed solvent (wherein the mass ratio of 95vt% ethanol and ethyl acetate is 4: 1) of tobacco material quality 10 times is added, extract 3h at 80 DEG C, filter to get filtrate after being cooled to 30 DEG C; Concentrate filtrate to 1/5 of tobacco material quality, then-5 DEG C of freezing 15 h, filter and obtain tobacco material extract; The propane diols adding quality 10 times in tobacco material extract again dissolves, at 100 DEG C, 10 after filtration 4carry out molecular clock under Pa condition and get final product; Wherein said tobacco material is offal.
embodiment 5
One tobacco juice for electronic smoke growing tobacco taste, obtained by the mixed raw material of following mass percent: tobacco extract light component 30%, natural nicotine 1.0%, deionized water 8%, flavouring essence for tobacco 8%, glycerine 16%, all the other are propane diols.
Described flavouring essence for tobacco is made up of the material of following mass percent: oxidation isophorone 0.1%, Megastigmatrienone 0.3%, tree moss essential oil 0.2%, ethyl maltol 0.5%, guaiacol 0.1%, methyl cyclopentenyl ketone 1.0%, cocoa extract (content of theobromine is 10wt%) 5%, ethanol 15%, surplus are propane diols.
Tobacco extract light component is obtained by following methods: cross 90 mesh sieves after being pulverized by tobacco material, then the 95vt% ethanol/mixed with propylene glycol solvent (wherein the mass ratio of 95vt% ethanol and propane diols is 8: 1) of tobacco material quality 9 times is added, extract 2h at 70 DEG C, filter to get filtrate after being cooled to 20 DEG C; Concentrate filtrate to 1 times of tobacco material quality, then-10 DEG C of freezing 10h, filter and obtain tobacco material extract; The propane diols adding quality 9 times in tobacco material extract again dissolves, at 150 DEG C, 10 after filtration 3carry out molecular clock under Pa condition and get final product; Wherein said tobacco material is tobacco leaf.

Claims (6)

1. one to grow tobacco taste tobacco juice for electronic smoke, it is characterized in that, be made up of the raw material of following percetage by weight: tobacco extract light component 5-50%, flavouring essence for tobacco 5%-10%, nicotine 0.5%-2.0%, deionized water 5%-10%, glycerine 10%-20%, surplus is propane diols; Wherein said tobacco extract light component is obtained by tobacco material molecular clock after solvent extraction; Wherein said solvent is 95vt% ethanol, 95vt% ethanol/ethyl acetate mixed solvent, 95vt% ethanol/mixed with propylene glycol solvent, propane diols, glycerine or propane diols/glycerine mixed solvent.
2. tobacco taste tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, when tobacco material 95vt% ethanol, 95vt% ethanol/ethyl acetate mixed solvent or 95vt% ethanol/mixed with propylene glycol solvent extraction time, the preparation of tobacco extract light component specifically comprises the following steps: cross 80-100 mesh sieve after being pulverized by tobacco material, then tobacco material quality 4-10 solvent is doubly added, extract 1-3 h at 50 DEG C-80 DEG C, filter to get filtrate after being cooled to 20-30 DEG C; Concentrate filtrate to the 1/10-1 of tobacco material quality doubly, then-15--5 DEG C of freezing 5 h-15 h, filter and obtain tobacco material extract; Add quality 8-10 propane diols doubly in tobacco material extract again to dissolve, at 40 DEG C-200 DEG C, 10Pa-10 after filtration 5carry out molecular clock under Pa condition, obtain tobacco extract light component.
3. tobacco taste tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, when tobacco material propane diols, glycerine or propane diols/glycerine mixed solvent extracts, the preparation of tobacco extract light component specifically comprises the following steps: cross 80-100 mesh sieve after being pulverized by tobacco material, add tobacco material quality 2-10 solvent doubly, 80 DEG C-150 DEG C are extracted 1-3 h, filter after being cooled to 20-30 DEG C; At 40 DEG C-200 DEG C, 10Pa-10 5under Pa condition, molecular clock is carried out to filtrate, obtain tobacco extract light component.
4. tobacco taste tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 0.01%-0.3%, Megastigmatrienone 0.01%-0.5%, tree moss essential oil 0.01%-1%, ethyl maltol 0.1%-1%, guaiacol 0.01%-0.5%, methyl cyclopentenyl ketone 0.1%-2%, cocoa extract 1%-10%, ethanol 10%-30%, surplus are propane diols.
5. the tobacco taste tobacco juice for electronic smoke as described in as arbitrary in claim 1-4, it is characterized in that, described nicotine is natural nicotine; Described tobacco material is offal or tobacco leaf.
6. tobacco taste tobacco juice for electronic smoke as claimed in claim 1 or 2, it is characterized in that, in 95vt% ethanol/ethyl acetate mixed solvent, the mass ratio of 95vt% ethanol and ethyl acetate is (4-10): 1; In 95vt% ethanol/mixed with propylene glycol solvent, the mass ratio of 95vt% ethanol and propane diols is (4-10): 1.
CN201410721776.2A 2014-12-03 2014-12-03 One grows tobacco taste tobacco juice for electronic smoke Active CN104489901B (en)

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Cited By (20)

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CN104856216A (en) * 2015-05-31 2015-08-26 中国烟草总公司郑州烟草研究院 Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette
CN104983063A (en) * 2015-05-31 2015-10-21 中国烟草总公司郑州烟草研究院 Improved preparation method for electronic cigarette smoke solution
CN105029681A (en) * 2015-07-14 2015-11-11 中国烟草总公司郑州烟草研究院 Natural perfume refining fluid suitable for cigarette fluid of electronic cigarettes and cigarette fluid and preparation method thereof
CN105054284A (en) * 2015-08-13 2015-11-18 深圳市施美乐科技股份有限公司 Fresh and elegant fragrance type electronic cigarette atomization liquid and preparation method thereof
CN105249527A (en) * 2015-10-31 2016-01-20 武汉纽威制药机械有限公司 Method for extracting tobacco aroma component through water jet comminution and centrifugal membrane vacuum low-temperature distillation
CN105433433A (en) * 2015-10-31 2016-03-30 武汉纽威晨创科技发展股份有限公司 Method for extracting tobacco aromatic components through water jet smashing and centrifugal membrane microwave distillation
CN105533793A (en) * 2016-02-24 2016-05-04 江西中烟工业有限责任公司 Preparation method for tobacco extract of dark sun-cured tobacco
CN105639718A (en) * 2016-02-29 2016-06-08 湖北中烟工业有限责任公司 Preparation method and application of tobacco extract easy to atomize at low temperature
CN105661625A (en) * 2016-02-29 2016-06-15 湖北中烟工业有限责任公司 Preparation method and application of tobacco extract for novel cigarettes
CN106307606A (en) * 2016-11-22 2017-01-11 中国烟草总公司郑州烟草研究院 Method for preparing high-fragrance tobacco extract
CN106433975A (en) * 2016-11-25 2017-02-22 中国烟草总公司郑州烟草研究院 Method for preparing low-As-content tree moss absolute by molecular distillation
CN107319637A (en) * 2016-04-28 2017-11-07 湖南中烟工业有限责任公司 A kind of extracting method of the electronic cigarette basic smoke raw material of tobacco source
CN108125277A (en) * 2018-03-21 2018-06-08 福建中烟工业有限责任公司 A kind of electronic cigarette and preparation method thereof
CN108887726A (en) * 2018-08-31 2018-11-27 湖北中烟工业有限责任公司 A kind of electric heating cigarette flavoring essence and its preparation method and application increasing this perfume of tobacco
CN109090699A (en) * 2018-08-28 2018-12-28 河北中烟工业有限责任公司 A kind of preparation method heating the tobacco product that do not burn
CN109998153A (en) * 2019-03-22 2019-07-12 河南中烟工业有限责任公司 A kind of tobacco juice for electronic smoke prepared using microbial fermentation tobacco leaf
CN110338451A (en) * 2018-04-04 2019-10-18 中国农业科学院烟草研究所 A kind of preparation method of tobacco juice for electronic smoke
CN111671131A (en) * 2020-06-22 2020-09-18 福建中烟工业有限责任公司 Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof
CN112369651A (en) * 2020-04-16 2021-02-19 湖北中烟工业有限责任公司 Tobacco-flavored electronic lampblack and preparation method thereof
CN112617272A (en) * 2019-10-09 2021-04-09 普济生物科技（台州）有限公司 Electronic cigarette tobacco tar of water matrix atomized liquid

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CN104983063A (en) * 2015-05-31 2015-10-21 中国烟草总公司郑州烟草研究院 Improved preparation method for electronic cigarette smoke solution
CN104856216A (en) * 2015-05-31 2015-08-26 中国烟草总公司郑州烟草研究院 Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette
CN105029681A (en) * 2015-07-14 2015-11-11 中国烟草总公司郑州烟草研究院 Natural perfume refining fluid suitable for cigarette fluid of electronic cigarettes and cigarette fluid and preparation method thereof
CN105054284A (en) * 2015-08-13 2015-11-18 深圳市施美乐科技股份有限公司 Fresh and elegant fragrance type electronic cigarette atomization liquid and preparation method thereof
CN105433433B (en) * 2015-10-31 2017-03-22 武汉纽威晨创科技发展股份有限公司 Method for extracting tobacco aromatic components through water jet smashing and centrifugal membrane microwave distillation
CN105249527A (en) * 2015-10-31 2016-01-20 武汉纽威制药机械有限公司 Method for extracting tobacco aroma component through water jet comminution and centrifugal membrane vacuum low-temperature distillation
CN105433433A (en) * 2015-10-31 2016-03-30 武汉纽威晨创科技发展股份有限公司 Method for extracting tobacco aromatic components through water jet smashing and centrifugal membrane microwave distillation
CN105533793A (en) * 2016-02-24 2016-05-04 江西中烟工业有限责任公司 Preparation method for tobacco extract of dark sun-cured tobacco
CN105533793B (en) * 2016-02-24 2016-12-28 江西中烟工业有限责任公司 A kind of preparation method of Dark sun-cured tobacco extract
CN105661625A (en) * 2016-02-29 2016-06-15 湖北中烟工业有限责任公司 Preparation method and application of tobacco extract for novel cigarettes
CN105639718A (en) * 2016-02-29 2016-06-08 湖北中烟工业有限责任公司 Preparation method and application of tobacco extract easy to atomize at low temperature
CN105661625B (en) * 2016-02-29 2017-06-30 湖北中烟工业有限责任公司 A kind of preparation method and application of the tobacco extract for new cigarette
CN107319637A (en) * 2016-04-28 2017-11-07 湖南中烟工业有限责任公司 A kind of extracting method of the electronic cigarette basic smoke raw material of tobacco source
CN106307606B (en) * 2016-11-22 2018-02-23 中国烟草总公司郑州烟草研究院 A kind of preparation method of high fragrance tobacco extract
CN106307606A (en) * 2016-11-22 2017-01-11 中国烟草总公司郑州烟草研究院 Method for preparing high-fragrance tobacco extract
CN106433975B (en) * 2016-11-25 2019-10-18 中国烟草总公司郑州烟草研究院 A method of utilizing the low As content tree moss absolute of molecular clock
CN106433975A (en) * 2016-11-25 2017-02-22 中国烟草总公司郑州烟草研究院 Method for preparing low-As-content tree moss absolute by molecular distillation
CN108125277A (en) * 2018-03-21 2018-06-08 福建中烟工业有限责任公司 A kind of electronic cigarette and preparation method thereof
CN110338451A (en) * 2018-04-04 2019-10-18 中国农业科学院烟草研究所 A kind of preparation method of tobacco juice for electronic smoke
CN109090699A (en) * 2018-08-28 2018-12-28 河北中烟工业有限责任公司 A kind of preparation method heating the tobacco product that do not burn
CN108887726A (en) * 2018-08-31 2018-11-27 湖北中烟工业有限责任公司 A kind of electric heating cigarette flavoring essence and its preparation method and application increasing this perfume of tobacco
CN109998153A (en) * 2019-03-22 2019-07-12 河南中烟工业有限责任公司 A kind of tobacco juice for electronic smoke prepared using microbial fermentation tobacco leaf
CN112617272A (en) * 2019-10-09 2021-04-09 普济生物科技（台州）有限公司 Electronic cigarette tobacco tar of water matrix atomized liquid
CN112369651A (en) * 2020-04-16 2021-02-19 湖北中烟工业有限责任公司 Tobacco-flavored electronic lampblack and preparation method thereof
CN112369651B (en) * 2020-04-16 2022-11-11 湖北中烟工业有限责任公司 Tobacco-flavored electronic lampblack and preparation method thereof
CN111671131A (en) * 2020-06-22 2020-09-18 福建中烟工业有限责任公司 Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof
CN111671131B (en) * 2020-06-22 2022-04-22 福建中烟工业有限责任公司 Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof

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