CN110338451A - A kind of preparation method of tobacco juice for electronic smoke - Google Patents
A kind of preparation method of tobacco juice for electronic smoke Download PDFInfo
- Publication number
- CN110338451A CN110338451A CN201810304045.6A CN201810304045A CN110338451A CN 110338451 A CN110338451 A CN 110338451A CN 201810304045 A CN201810304045 A CN 201810304045A CN 110338451 A CN110338451 A CN 110338451A
- Authority
- CN
- China
- Prior art keywords
- tobacco juice
- congruent melting
- electronic smoke
- melting solvent
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
- A24B15/243—Nicotine
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention proposes a kind of preparation methods of tobacco juice for electronic smoke, it is characterized in that, the following steps are included: (1) produces deep congruent melting solvent: choline chloride is reacted from different alcohols according to certain mol proportion, reaction temperature is 40~80 DEG C, reaction time is 1-6 hours, and the colourless transparent liquid of generation is deep congruent melting solvent；(2) 5~15wt% water the extraction of offal: is added in the deep congruent melting solvent in step (1), it mixes, then 1 part of deep congruent melting solvent aqueous solution is taken, 5~10%w/v offal is added, microwave abstracting 10~30 minutes, 0.22-0.45 μm of membrane filtration, gained clarified solution are tobacco juice for electronic smoke.It is an object of that present invention to provide amount of smoke when a kind of suction is big, increase the experience of smoker, saves charging ingredient, the preparation method for the tobacco juice for electronic smoke for being more nearly electronic cigarette aesthetic quality and traditional cigarette.
Description
Technical field
The present invention relates to a kind of electronic cigarette fields, more particularly to a kind of tobacco juice for electronic smoke for generating smog for electronic cigarette
Preparation method.
Background technique
" smoking and health " is people's question of common concern and tobacco business focus of attention.Traditional cigarette is taken out
Suction mode makes the substance being harmful to the human body containing there are many in the flue gas generated when cigarette burning, enters human body, meeting by sucking
Certain harm is generated to human body.In addition, the side-stream smoke generated can also make non-smokers' passive smoking.Therefore, public
It smokes increasingly by the criticism of various circles of society and limitation in place.Electronic cigarette is not due to without tar and CO, having " secondhand smoke " right
Harm and the pollution to environment caused by other people, therefore electronic cigarette becomes increasingly popular as a kind of for cigarette, smoking cessation product.Electronic cigarette
It comes out, indicates that smoking enters healthy epoch, and the response to " 12 " planning tobacco control smoking ban.Occur currently on the market
Electronic cigarette and its patent, mostly based on liquid tobacco tar.But this liquid tobacco tar can generate liquid in use and fall
Suction, leakage, the problems such as storage and transport are inconvenient, volatile aroma is fast.Also, when liquid smoke oil consumption needs replacing to the greatest extent, Yi Zao
It is exposed at liquid, dangerous, unhygienic.
In recent years, harm is brought in order to reduce smoking and secondhand smoke, new tobacco products has become tobacco business not
Come the vital task developed.Electronic cigarette, also known as electrospray cigarette, it is to transmit Buddhist nun to respiratory system by electronics heating means
The electronic device of Gu Ding.It is mounted with atomized liquid in electronic cigarette as tobacco juice, smoking effect is generated after tobacco juice materialization, electronic cigarette can be arranged
Except the biggish substance of conventional cigarette Poisoning, to have the substitution effect of tradition smoking.At present the atomized liquid of electronic cigarette be with
The liquid that the allotments such as propylene glycol, glycerine, nicotine, water, tobacco extract are formed, by gasifying after the atomizer heating of electronic cigarette
It is absorbed by the body.
In order to obtain tobacco flavor electronic cigarette, generally require that tobacco extract is added into tobacco juice for electronic smoke, and tobacco mentions
Take that object is needed by extracting, removal solvent, back extraction, removing solvent again etc., a series of processes can just obtain tobacco extract, preparation
Process is complicated, and not can avoid organic solvent use and medicinal extract in organic solvent residual, influence electronic cigarette and suck safety.
Deep congruent melting solvent refers to the system using organic molecule and ionic compound composition.Deep congruent melting solvent has preparation
The characteristics such as at low cost, route is simple, biodegradable, Atom economy are a kind of novel green solvents.Since its is superior
Characteristic, deep congruent melting solvent have shown in fields such as active material extraction, reaction dissolvent, functional material and electrochemistry good
Application prospect.The deep congruent melting solvent that choline chloride and alcohols are formed is widely used to polyphenol, flavones, alkaloid, sterol, terpene
Among extraction.
Summary of the invention
Based on the above issues, it is an object of that present invention to provide amount of smoke when a kind of suction is big, increase the experience of smoker, save
Save charging ingredient, the preparation method for the tobacco juice for electronic smoke for being more nearly electronic cigarette aesthetic quality and traditional cigarette.
In view of the above problems, providing following technical solution: a kind of preparation method of tobacco juice for electronic smoke, which is characterized in that
The following steps are included:
(1) deep congruent melting solvent is produced: by 5~20wt% choline chloride or glycine betaine and ethyl alcohol, propylene glycol, propylene glycol, third
Three pure and mild mannitol, butanediol, polyethylene glycol, one or more of triethylene glycol, eight glycol, sorbierite, xylitol composition
Mixed liquor is reacted according to certain mol proportion, reaction temperature be 40~80 DEG C, the reaction time be 1-6 hours, generation it is colorless and transparent
Liquid is deep congruent melting solvent；
(2) extraction of offal: being added 5~15wt% water in the deep congruent melting solvent in step (1), mix, then take 1 part
Deep congruent melting solvent aqueous solution, addition 5~10%w/v offal, microwave abstracting 10~30 minutes, 0.22-0.45 μm of membrane filtration, institute
Obtaining clarified solution is tobacco juice for electronic smoke.
The present invention is further arranged to, and the butanediol in the step (1) is 1,2- butanediol, 1,3-BDO, 2,3-
The mixture of one or more of butanediol and 1,4-butanediol.
The present invention is further arranged to, the polyethylene glycol in the step (1) be polyethylene glycol 200, polyethylene glycol 400 and
The mixture of one or more of Macrogol 600.
Beneficial effects of the present invention: the present invention utilizes choline chloride and ethyl alcohol, ethylene glycol, propylene glycol, glycerine, sweet dew
Alcohol, butanediol, polyethylene glycol, triethylene glycol, eight glycol, sorbierite, one or more alcohols form deep congruent melting solvent in xylitol
It is used as tobacco juice for electronic smoke, nicotine and fragrance matter directly in extraction offal, directly as electronic cigarette after simple filtration filters
Tobacco juice uses, and solves to need additionally to add nicotine in the prior art very well and tobacco extract determines.
Amount of smoke is big when being aspirated using electronic cigarette made of above-mentioned preparation method, increases the experience of smoker, body of smoking
Test it is thick and solid, full, not dry do not moisten, it is with higher to suck comfort level；Containing tobacco flavor ingredient and nicotine etc. in extract, i.e.,
Charging ingredient can be saved, is more nearly electronic cigarette aesthetic quality with traditional cigarette, while being opened in tobacco juice for electronic smoke solvent
There is good application prospect in hair.
Specific embodiment
With reference to embodiment, the embodiment of the present invention is furthur described in detail.Following embodiment is used for
Illustrate the present invention, but is not intended to limit the scope of the invention.
Embodiment 1:
It takes choline chloride 10%, propylene glycol 70%, glycerine 20% to mix, stirs 4 hours, be cooled to room temperature at 80 DEG C,
Then the water of 5wt% is added, mixes；1 part of deep congruent melting solvent aqueous solution is taken, 10% (w/v) offal is added, microwave abstracting 15 divides
Clock, 0.22 μm of membrane filtration, gained clarified solution is tobacco juice for electronic smoke.
Embodiment 2:
It takes glycine betaine 5%, propylene glycol 65%, triethylene glycol 10%, glycerine 20% to mix, is stirred 4 hours at 70 DEG C, it is cooling
To room temperature, the water of 10wt% is then added, mixes；1 part of deep congruent melting solvent aqueous solution is taken, 8% (w/v) offal, microwave extraction is added
It takes 30 minutes, 0.22 μm of membrane filtration, gained clarified solution is tobacco juice for electronic smoke.
Embodiment 3:
Take choline chloride 10%, 1,4-butanediol 15%, sorbierite 10%, polyethylene glycol 5%, propylene glycol 35%, the third three
Alcohol 25% mixes, and stirs 6 hours, is cooled to room temperature at 80 DEG C, and the water of 10wt% is then added, and mixes；Take 1 part of deep congruent melting solvent
8% (w/v) offal is added in aqueous solution, and microwave abstracting 20 minutes, 0.22 μm of membrane filtration, gained clarified solution was electronic cigarette
Liquid.
Comparative example:
It takes propylene glycol 65%, triethylene glycol 10%, glycerine 25% to mix, stirs 4 hours, be cooled to room temperature, so at 70 DEG C
The water of 10wt% is added afterwards, mixes；1 part of deep congruent melting solvent aqueous solution is taken, is added 8% (w/v) offal, microwave abstracting 30 minutes,
0.22 μm of membrane filtration, gained clarified solution are comparative example tobacco juice for electronic smoke.
Check problem: sample and check table are provided to 6 experts that smoke panel test, it is desirable that member of smoking requires to refer to items according to table
Mark is smoked panel test.
The product for the tobacco juice for electronic smoke that 1 embodiment of the present invention of table and comparative example obtain inhale result
| Sample | Amount of smoke | Comfort level | Tobacco is fragrant | Taste | Miscellaneous gas |
| Embodiment 1 | It is larger | Thick and solid, full, taste lubrication, pleasant impression are comfortably pure | It is sufficient | It is slightly sweet | It is relatively light |
| Embodiment 2 | It is larger | Thick and solid, full, taste lubrication, pleasant impression are comfortably pure | It is sufficient | It is slightly sweet | It is relatively light |
| Embodiment 3 | It is larger | Thick and solid, full, taste lubrication, pleasant impression are comfortably pure | It is sufficient | It is slightly sweet | It is relatively light |
| Comparative example | It is larger | It is slightly dry and astringent, do not blurt out, | It is very weak | It is slightly sweet | There is miscellaneous gas |
As shown in Table 1, tobacco juice for electronic smoke of the invention, product suction experience is thick and solid, full, mouthfeel is slightly sweet, the fragrant abundance of tobacco, miscellaneous
Gas is light, with higher to suck comfort level.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, several improvements and modifications can also be made, above-mentioned hypothesis these
Improvement and modification also should be regarded as protection scope of the present invention.
Claims (3)
1. a kind of preparation method of tobacco juice for electronic smoke, which comprises the following steps:
(1) deep congruent melting solvent is produced: by 5~20wt% choline chloride or glycine betaine and ethyl alcohol, propylene glycol, propylene glycol, glycerine
And mannitol, butanediol, polyethylene glycol, the mixing of one or more of triethylene glycol, eight glycol, sorbierite, xylitol composition
Liquid reaction, reaction temperature are 40~80 DEG C, and the reaction time is 1-6 hours, and the colourless transparent liquid of generation is deep congruent melting solvent；
(2) extraction of offal: being added 5~15wt% water in the deep congruent melting solvent in step (1), mixes, and then takes 1 part of depth total
Molten solvent aqueous solution, is added 5~10%w/v offal, and microwave abstracting 10~30 minutes, 0.22-0.45 μm of membrane filtration, gained was clear
Clear liquid is tobacco juice for electronic smoke.
2. a kind of preparation method of tobacco juice for electronic smoke according to claim 1, it is characterised in that: in the step (1)
Butanediol is the mixture of one or more of 1,2- butanediol, 1,3-BDO, 2,3-butanediol and 1,4-butanediol.
3. a kind of preparation method of tobacco juice for electronic smoke according to claim 1, it is characterised in that: in the step (1)
Polyethylene glycol is the mixture of one or more of polyethylene glycol 200, polyethylene glycol 400 and Macrogol 600.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810304045.6A CN110338451B (en) | 2018-04-04 | 2018-04-04 | Preparation method of electronic cigarette liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810304045.6A CN110338451B (en) | 2018-04-04 | 2018-04-04 | Preparation method of electronic cigarette liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110338451A true CN110338451A (en) | 2019-10-18 |
| CN110338451B CN110338451B (en) | 2022-12-02 |
Family
ID=68172956
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810304045.6A Active CN110338451B (en) | 2018-04-04 | 2018-04-04 | Preparation method of electronic cigarette liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110338451B (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111567851A (en) * | 2020-06-01 | 2020-08-25 | 中国农业科学院烟草研究所 | Smoke agent for promoting aroma release of heated non-combustible cigarettes and application thereof |
| CN113115982A (en) * | 2021-04-01 | 2021-07-16 | 中国烟草总公司郑州烟草研究院 | Cigarette filter stick capable of adsorbing harmful ingredients in smoke and cigarette |
| CN113331465A (en) * | 2021-06-17 | 2021-09-03 | 齐鲁工业大学 | Method for extracting sucrose ester in tobacco |
| CN113764713A (en) * | 2021-08-03 | 2021-12-07 | 江苏大学 | Flow battery based on ternary eutectic solvent |
| CN113956193A (en) * | 2020-06-12 | 2022-01-21 | 深圳市水槟榔生物科技有限公司 | Preparation method of arecoline extract |
| CN114271531A (en) * | 2022-01-06 | 2022-04-05 | 大连工业大学 | Electronic cigarette liquid and preparation method thereof |
| CN115715598A (en) * | 2022-12-01 | 2023-02-28 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing tobacco organic acid by deep eutectic solvent |
| WO2023170451A1 (en) * | 2022-03-10 | 2023-09-14 | Gerges Adnan Fayad | Process of solubilization of the smoke constituents in the vase of the water pipe using deep eutectic solvents |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103720030A (en) * | 2013-12-13 | 2014-04-16 | 浙江中烟工业有限责任公司 | Electronic cigarette liquid prepared from tobacco powder extractive and preparation method of electronic cigarette liquid |
| CN104489901A (en) * | 2014-12-03 | 2015-04-08 | 河南中烟工业有限责任公司 | Tobacco taste electronic tobacco liquid |
| US20150296872A1 (en) * | 2012-11-26 | 2015-10-22 | British American Tobacco (Investments) Limited | Treatment of tobacco material |
| CN107136560A (en) * | 2017-07-06 | 2017-09-08 | 中国烟草总公司郑州烟草研究院 | Natural eutectic solvent tobacco humectant and its preparation method and application |
-
2018
- 2018-04-04 CN CN201810304045.6A patent/CN110338451B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150296872A1 (en) * | 2012-11-26 | 2015-10-22 | British American Tobacco (Investments) Limited | Treatment of tobacco material |
| CN103720030A (en) * | 2013-12-13 | 2014-04-16 | 浙江中烟工业有限责任公司 | Electronic cigarette liquid prepared from tobacco powder extractive and preparation method of electronic cigarette liquid |
| CN104489901A (en) * | 2014-12-03 | 2015-04-08 | 河南中烟工业有限责任公司 | Tobacco taste electronic tobacco liquid |
| CN107136560A (en) * | 2017-07-06 | 2017-09-08 | 中国烟草总公司郑州烟草研究院 | Natural eutectic solvent tobacco humectant and its preparation method and application |
Non-Patent Citations (1)
| Title |
|---|
| 尚宪超等: "超声辅助深共熔溶剂提取两种烟草多酚的方法研究 ", 《中国烟草科学》 * |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111567851A (en) * | 2020-06-01 | 2020-08-25 | 中国农业科学院烟草研究所 | Smoke agent for promoting aroma release of heated non-combustible cigarettes and application thereof |
| CN113956193A (en) * | 2020-06-12 | 2022-01-21 | 深圳市水槟榔生物科技有限公司 | Preparation method of arecoline extract |
| CN113115982A (en) * | 2021-04-01 | 2021-07-16 | 中国烟草总公司郑州烟草研究院 | Cigarette filter stick capable of adsorbing harmful ingredients in smoke and cigarette |
| CN113331465A (en) * | 2021-06-17 | 2021-09-03 | 齐鲁工业大学 | Method for extracting sucrose ester in tobacco |
| CN113764713A (en) * | 2021-08-03 | 2021-12-07 | 江苏大学 | Flow battery based on ternary eutectic solvent |
| CN113764713B (en) * | 2021-08-03 | 2023-10-13 | 江苏大学 | Flow battery based on ternary eutectic solvent |
| CN114271531A (en) * | 2022-01-06 | 2022-04-05 | 大连工业大学 | Electronic cigarette liquid and preparation method thereof |
| WO2023170451A1 (en) * | 2022-03-10 | 2023-09-14 | Gerges Adnan Fayad | Process of solubilization of the smoke constituents in the vase of the water pipe using deep eutectic solvents |
| CN115715598A (en) * | 2022-12-01 | 2023-02-28 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing tobacco organic acid by deep eutectic solvent |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110338451B (en) | 2022-12-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110338451A (en) | A kind of preparation method of tobacco juice for electronic smoke | |
| RU2671775C1 (en) | Liquid composition for electronic cigarettes | |
| CN101461566B (en) | Atomized liquid of electronic smoke | |
| KR101208473B1 (en) | Composition of atomized solution for electronic cigarette | |
| WO2020239083A1 (en) | Aerosol generation or smoking system, or electronic cigarette and device thereof | |
| CN104026729B (en) | A kind of electronic cigarette liquid with burnt odor fragrance | |
| WO2021017137A1 (en) | Chewing gum, e-liquid and use thereof | |
| US20160366928A1 (en) | Solvent for electronic cigarette liquid and an electronic cigarette liquid | |
| US20160366927A1 (en) | A solvent for electronic cigarette liquid and an electronic cigarette liquid | |
| WO2021036122A1 (en) | Electronic cigarette liquid | |
| CN110506978A (en) | A kind of electronic cigarette oil solvent, electronic cigarette tobacco tar and preparation method comprising it | |
| KR20200056459A (en) | Aerosolizable formulations | |
| CN104397871A (en) | Electronic cigarette liquid containing tea extracts and preparation method of electronic cigarette liquid containing tea extracts | |
| CN108030143A (en) | A kind of peppermint tobacco composite electronic tobacco tar | |
| CN109549246A (en) | A kind of tobacco juice for electronic smoke and preparation method thereof of adjustable function of human body | |
| CN109619656A (en) | It is a kind of to have effects that the tobacco juice for electronic smoke of antiphlogistic antibacterial | |
| CN110584185A (en) | Flavor composition and electronic cigarette liquid containing same | |
| CN111000283A (en) | Electronic cigarette oil for aerosol device and preparation method and application thereof | |
| CN104970445B (en) | A kind of spacetabs type aerosol mouth cigarette | |
| CN111920079A (en) | Electronic atomization inhalant and preparation method thereof | |
| CN106418662A (en) | Electronic cigarette smoke solution and solvent for same | |
| CN108669635A (en) | The tobacco compositions of fruity style, smoke section and heating are not burnt cigarette cigarette stick | |
| CN105361237A (en) | Electronic cigarette tobacco juice with cholesterol reducing function and preparation method thereof | |
| CN108185539B (en) | Electronic cigarette with improved sensory quality and manufacturing method thereof | |
| KR20110023949A (en) | A assistance liquid matter for prohibition of smoking |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |