CN104026729B - A kind of electronic cigarette liquid with burnt odor fragrance - Google Patents

A kind of electronic cigarette liquid with burnt odor fragrance Download PDF

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Publication number
CN104026729B
CN104026729B CN201410287554.4A CN201410287554A CN104026729B CN 104026729 B CN104026729 B CN 104026729B CN 201410287554 A CN201410287554 A CN 201410287554A CN 104026729 B CN104026729 B CN 104026729B
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electronic cigarette
cigarette liquid
fragrance
dissolved
glycerine
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CN104026729A (en
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赵国玲
黎艳玲
杨华武
黄建国
李亚白
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Abstract

The present invention discloses a kind of electronic cigarette liquid with burnt odor fragrance, described in every 10-50mL, electronic cigarette liquid preparation is: by 20-40g white granulated sugar or brown sugar, preferred white granulated sugar is dissolved in the water of 10-30mL, 5-15min is heated under 80-150 DEG C of conditions, then 5-10g offal or pipe tobacco is added, preferred offal, be warming up to 180-250 DEG C of reflux heating 10-20min, product after reflux heating is dissolved in the mixed liquor of 10-50mL glycerine, second alcohol and water, or glycerine, or in propane diols, after filtration, namely obtain electronic cigarette liquid.Electronic cigarette liquid of the present invention can improve the inherent suction quality of electronic cigarette, makes electronic cigarette closer to fragrance, the taste of cigarette.

Description

A kind of electronic cigarette liquid with burnt odor fragrance
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind of electronic cigarette liquid with burnt odor fragrance.
Background technology
In recent years, along with in some developed country markets, the sales volume of conventional tobacco products occurs that stagnation even declines, and the continuing to increase of many states public places in Nan Chongs ban on opium-smoking and the opium trade dynamics, the novel tobacco goods such as low temperature cigarette, smoke-free tobacco product, electronic cigarette are just in rapid rising, and the transnational tobacco companies such as the Fei Mo world, BAT, Japan Tobacco also actively research and develop from strategic height and promote novel tobacco goods.Electronic cigarette profile is similar to common cigarette, is a kind of device that nicotine solution can be vaporized into fog, smokes true, bring excitement to smoker by simulation.It is made up of elements such as lithium battery (chargeable), atomizer (heating element heater), cigarette bullets (cigarette holder usually seen).Electronic cigarette is by the solution atomization containing nicotine, by pulmonary absorption, makes consumer obtain similar satisfaction of sucking traditional cigarette.
Electronic cigarette decreases the injury of the health to people while the custom meeting people's smoking.Generally, electronic cigarette has following principal characters: one is do not need burning, greatly reduces the tar because burning produces and harmful components, compares traditional cigarette harmfulness less; Two is to produce second-hand flue gas, can not have an impact to PE, alleviates the contradiction of smoking and public place ban on opium-smoking and the opium trade to a certain extent; Three is the physiological requirements that can adapt to and meet consumer to a certain extent.Electronic cigarette is through the development of several generations, and basically identical with traditional cigarette external form at present, taste can realize variation, does not contain tar in electronic cigarette simultaneously, less to person injury.
A kind of preparation method of electronic cigarette liquid disclosed in Chinese patent CN201110184068.6, the tobacco leaf taking the 5-20% of electronic cigarette liquid measure drops into extractor, the solvent prepared is joined in extractor and soaks tobacco leaf 30-100 minute, be heated to 40-60 degree, 2-8 hour is got in temperature lixiviate, filter extract, in filtrate, add the cocoa bean extract of the 1-10% of electronic cigarette liquid measure, be uniformly mixed 20-40 minute; 100% is supplied again with propane diols or polyethylene glycol.Although employ leaf tobacco extract, but still it is the product that simulated cigarette taste is allocated with leaf tobacco extract and other essence and flavoring agents.Because increasing smoker starts to accept to use electronic cigarette to replace cigarette, the some shortcomings for the electronic cigarette liquid of these electronic cigarettes are also more and more obvious.Study according to investigations, electronic cigarette is compared with regular-size cigarette, although perceptual image cigarette such as shape, feel, smog, but the smog produced for these electronic cigarette liquids is in fragrance, taste, with real cigarette perceptual difference apart from comparatively large, these are not enough, greatly have impact on the quality of electronic cigarette.Smoker is generally reflected, electronic cigarette is compared with cigarette, although perceptual image cigarettes such as shape, feel, smog, but in fragrance, taste etc., larger with the perceptual difference distance of cigarette, especially with the product that various essence and flavoring agent is deployed into, they are difficult to accept or be accustomed to its fragrance and taste.These deficiencies have impact on the quality of electronic cigarette greatly, also govern the universal and popular of electronic cigarette simultaneously.And traditional leaf tobacco extract is mainly by tobacco leaf or pipe tobacco ethanol or water refluxing extraction at a certain temperature, is difficult to the burnt odor fragrance in tobacco leaf to extract.
Summary of the invention
The object of the invention is to for the deficiency of existing electronic cigarette liquid in the suction such as fragrance, mouthfeel sensation, one is provided to utilize white granulated sugar or brown sugar to be raw material, caramelization is carried out at a certain temperature, the electronic cigarette liquid with burnt odor fragrance obtained with offal or pipe tobacco.
In order to achieve the above object, technical scheme provided by the invention is:
The electronic cigarette liquid preparation method described in every 10-50mL with burnt odor fragrance is as follows:
By 20-40g sugar, preferred white granulated sugar or brown sugar, more preferably white granulated sugar is dissolved in the water of 10-30mL, heats 5-15min, then add 5-10g offal or pipe tobacco under 80-150 DEG C of conditions, preferred offal, be warming up to 180-250 DEG C of reflux heating 10-20min, the product after reflux heating be dissolved in the glycerine of 10-50mL, the mixed liquor of second alcohol and water, or glycerine, or in propane diols, after filtration, namely obtain electronic cigarette liquid.In general, the solvent of electronic cigarette liquid is 70% glycerine (mass percent), 20% ethanol (mass percent) and 10% water (mass percent), the material of opposed polarity can be dissolved, solvent of the present invention can be the mixed solvent of glycerine, second alcohol and water, also can be only with glycerine or propane diols.
The present invention utilizes white granulated sugar or brown sugar to be raw material, carries out caramelization at a certain temperature with offal, pipe tobacco or cigarette ash, obtains the product with burnt odor fragrance.This odor type cause perfumery and to produce burnt odor fragrance component in traditional cigarette combustion process similar, this electronic cigarette liquid with burnt odor odor type is after atomizer atomization, smoker feels that this electronic cigarette liquid is consistent with the impression in traditional cigarette combustion process, has the burnt odor in cigarette burning process.Electronic cigarette liquid of the present invention can improve the inherent suction quality of electronic cigarette, makes electronic cigarette closer to fragrance, the taste of cigarette.
Detailed description of the invention
embodiment 1
The described electronic cigarette liquid preparation method with burnt odor fragrance is as follows:
20g white granulated sugar is dissolved in the water of 10mL, under 150 DEG C of conditions, heats 10min, then add 7g Yunnan Shao and lead to B3F offal, be warming up to 180 DEG C of reflux heating 15min, the product after reflux heating be dissolved in the glycerine of 20mL, after filtration, namely obtain electronic cigarette liquid.
Getting 1mL electronic cigarette liquid adds in atomizer, and the personnel that smoke panel test that please be professional smoke panel test, and have Jiao of flue-cured tobacco fragrant and sweet, also has the baking of flue-cured tobacco fragrant simultaneously.
embodiment 2
The described electronic cigarette liquid preparation method with burnt odor fragrance is as follows:
25g white granulated sugar is dissolved in the water of 15mL, 10min is heated under 130 DEG C of conditions, then 5g Sangzhi B3F offal is added, be warming up to 180 DEG C of reflux heating 20min, product after reflux heating is dissolved in 25mL mass percent be 10% water, mass percent be 70% glycerine, mass percent be in the mixed liquor of the ethanol of 20%, namely obtain electronic cigarette liquid after filtration.
Getting 1mL electronic cigarette liquid adds in atomizer, and the personnel that smoke panel test that please be professional smoke panel test, and have Jiao of flue-cured tobacco fragrant and sweet.
embodiment 3
The described electronic cigarette liquid preparation method with burnt odor fragrance is as follows:
35g white granulated sugar is dissolved in the water of 30mL, under 140 DEG C of conditions, heats 10min, then add 8g Zimbabwe L1OF offal, be warming up to 180 DEG C of reflux heating 20min, the product after reflux heating be dissolved in the glycerine of 30mL, after filtration, namely obtain electronic cigarette liquid.
Getting 1mL electronic cigarette liquid adds in atomizer, and the personnel that smoke panel test that please be professional smoke panel test, and have Jiao of flue-cured tobacco fragrant and sweet.

Claims (2)

1. have an electronic cigarette liquid for burnt odor fragrance, it is characterized in that, described in every 10-50mL, electronic cigarette liquid preparation method is as follows:
20-40g sugar is dissolved in the water of 10-30mL, 5-15min is heated under 80-150 DEG C of conditions, then 5-10g offal or pipe tobacco is added, be warming up to 180 DEG C of reflux heating 10-20min, product after reflux heating is dissolved in the glycerine of 10-50mL, the mixed liquor of second alcohol and water, or glycerine, or in propane diols, after filtration, namely obtain electronic cigarette liquid.
2. electronic cigarette liquid as claimed in claim 1, it is characterized in that, described sugar is white granulated sugar or brown sugar.
CN201410287554.4A 2014-06-25 2014-06-25 A kind of electronic cigarette liquid with burnt odor fragrance Active CN104026729B (en)

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Families Citing this family (13)

* Cited by examiner, † Cited by third party
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CN104432481B (en) * 2014-10-22 2016-03-30 浙江中烟工业有限责任公司 A kind ofly utilize the tobacco juice for electronic smoke solvent of polypropylene glycol and the tobacco juice for electronic smoke of preparation thereof and electronic cigarette
CN105433431B (en) * 2014-11-12 2018-12-07 湖南中烟工业有限责任公司 A kind of electronic cigarette liquid and electronic cigarette
CN106947596B (en) * 2017-04-12 2020-12-25 安徽中烟工业有限责任公司 Preparation method of maltose caramel spice for cigarettes
CN107692318A (en) * 2017-10-13 2018-02-16 上海烟草集团有限责任公司 A kind of tobacco juice for electronic smoke and preparation method
CN111248489A (en) * 2020-01-16 2020-06-09 四川中烟工业有限责任公司 Preparation method of scorched, sweet and scorched-aroma type cigar tobacco leaves
CN111588073A (en) * 2020-03-05 2020-08-28 四川中烟工业有限责任公司 Burnt sweet-fragrance electronic cigarette tobacco tar, preparation method and application method
CN111254014A (en) * 2020-03-05 2020-06-09 四川中烟工业有限责任公司 Caramel aroma spice, preparation method and application method thereof
CN111411020A (en) * 2020-03-05 2020-07-14 四川中烟工业有限责任公司 Burnt sweet-fragrance bead-blasting oil, preparation method and application method
CN112369651B (en) * 2020-04-16 2022-11-11 湖北中烟工业有限责任公司 Tobacco-flavored electronic lampblack and preparation method thereof
CN111602838A (en) * 2020-06-12 2020-09-01 山东瑞博斯烟草有限公司 Feed liquid for increasing scorched and sweet aroma of tobacco leaves and method for treating tobacco leaves
CN112205663A (en) * 2020-09-28 2021-01-12 四川中烟工业有限责任公司 Composite burnt sweet aroma flavor, extrusion puffing preparation method and application method thereof
CN112205659A (en) * 2020-09-28 2021-01-12 四川中烟工业有限责任公司 Composite burnt sweet aroma flavor, baking preparation method and application
CN114903196B (en) * 2022-05-11 2023-03-24 河北中烟工业有限责任公司 Coloring additive for tobacco, preparation method thereof and heated cigarette

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US3920026A (en) * 1972-03-07 1975-11-18 Liggett & Myers Inc Tobacco with flavor enhancer
CN1106640A (en) * 1994-02-03 1995-08-16 锦州卷烟厂 Method for preparing health cigarette of reduced tar content
CN101461566A (en) * 2009-01-08 2009-06-24 华健 Atomized liquid of electronic smoke
CN101580757A (en) * 2009-06-02 2009-11-18 上海英华香精香料有限公司 Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method
CN103783658A (en) * 2014-01-21 2014-05-14 杨成云 Preparation method of nicotine liquid perfume
CN103849467A (en) * 2014-03-12 2014-06-11 河南中烟工业有限责任公司 Method for preparing tobacco flavor through maillard reaction with tobacco flower buds as raw material

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3920026A (en) * 1972-03-07 1975-11-18 Liggett & Myers Inc Tobacco with flavor enhancer
CN1106640A (en) * 1994-02-03 1995-08-16 锦州卷烟厂 Method for preparing health cigarette of reduced tar content
CN101461566A (en) * 2009-01-08 2009-06-24 华健 Atomized liquid of electronic smoke
CN101580757A (en) * 2009-06-02 2009-11-18 上海英华香精香料有限公司 Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method
CN103783658A (en) * 2014-01-21 2014-05-14 杨成云 Preparation method of nicotine liquid perfume
CN103849467A (en) * 2014-03-12 2014-06-11 河南中烟工业有限责任公司 Method for preparing tobacco flavor through maillard reaction with tobacco flower buds as raw material

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