CN104026729A - Electronic cigarette liquid with scorch aroma - Google Patents

Electronic cigarette liquid with scorch aroma Download PDF

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Publication number
CN104026729A
CN104026729A CN201410287554.4A CN201410287554A CN104026729A CN 104026729 A CN104026729 A CN 104026729A CN 201410287554 A CN201410287554 A CN 201410287554A CN 104026729 A CN104026729 A CN 104026729A
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China
Prior art keywords
electronic cigarette
cigarette liquid
sugar
water
tobacco
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CN201410287554.4A
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Chinese (zh)
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CN104026729B (en
Inventor
赵国玲
黎艳玲
杨华武
黄建国
李亚白
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Abstract

The invention discloses an electronic cigarette liquid with scorch aroma. A preparation method of every 10-15mL of the electronic cigarette liquid includes: dissolving 20-40g of custer sugar or brown sugar, preferably the custer sugar, into 10-30mL of water, heating for 5-15min at the temperature of 80-150 DEG C, then adding 5-10g of tobacco powder or tobacco shreds, preferably the tobacco powder, heating up to 180-250 DEG C prior to performing reflux heating for 10-20min, dissolving a product after reflux heating into 10-50mL of mixed solution of glycerin, ethanol and water, or glycerin or propylene glycol, and filtering to obtain the electronic cigarette liquid. By the electronic cigarette liquid, intrinsic smoking quality of an electronic cigarette can be improved, and the electronic cigarette is enabled to be closer to cigarette in aroma and taste.

Description

A kind of electronic cigarette liquid with burnt odor fragrance
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind of electronic cigarette liquid with burnt odor fragrance.
Background technology
In recent years, along with the sales volume of conventional smoke straw-made articles is stagnated even and declined in some developed country's markets appearance, and the continuing to increase of many states public places in Nan Chongs ban on opium-smoking and the opium trade dynamics, the novel tobacco goods such as low temperature cigarette, smoke-free tobacco product, electronic cigarette are just in rapid rising, and the transnational tobacco companies such as the Fei Mo world, BAT, Japan Tobacco also actively research and develop and promote novel tobacco goods from strategic height.Electronic cigarette profile is similar to common cigarette, is a kind ofly nicotine solution to be vaporized into the device of fog, smokes very by simulation, to smoker, brings excitement.It consists of elements such as lithium battery (chargeable), atomizer (heating element heater), cigarette bullets (cigarette holder of conventionally seeing).Electronic cigarette is by containing the solution atomization of nicotine, by pulmonary absorption, makes consumer obtain similar satisfaction of sucking traditional cigarette.
Electronic cigarette has reduced the injury to people's health in the custom that meets people's smoking.Generally, electronic cigarette has following principal characters: the one, do not need burning, and greatly reduce tar and the harmful components that produce because of burning, compare traditional cigarette harmfulness less; The 2nd, can not produce second-hand flue gas, can not exert an influence to PE, alleviated to a certain extent the contradiction of smoking and public place ban on opium-smoking and the opium trade; The 3rd, can adapt to a certain extent and meet consumer's physiological requirements.Electronic cigarette is through the development of several generations, and basically identical with traditional cigarette external form at present, taste can be realized variation, does not contain tar in electronic cigarette simultaneously, less to person injury.
The preparation method of the disclosed a kind of electronic cigarette liquid of Chinese patent CN201110184068.6, the tobacco leaf that takes the 5-20% of electronic cigarette liquid measure drops into extractor, the solvent preparing is joined and in extractor, soaks tobacco leaf 30-100 minute, be heated to 40-60 degree, 2-8 hour is got in temperature lixiviate, filter extract, the cocoa bean extract to adding the 1-10% of electronic cigarette liquid measure in filtrate, is uniformly mixed 20-40 minute; With propane diols or polyethylene glycol, supply 100% again.Although used leaf tobacco extract, but still be that simulated cigarette taste is with the product of leaf tobacco extract and the allotment of other essence and flavoring agents.Because increasing smoker starts to accept to use electronic cigarette to replace cigarette, also more and more obvious for the some shortcomings of the electronic cigarette liquid of these electronic cigarettes.Research according to investigations, electronic cigarette is compared with regular-size cigarette, although perceptual image cigarette such as shape, feel, smog, but the smog producing for these electronic cigarette liquids is aspect fragrance, taste, apart from larger, these deficiencies, have affected the quality of electronic cigarette greatly with real cigarette perceptual difference.Smoker generally reflects, electronic cigarette is compared with cigarette, although perceptual image cigarettes such as shape, feel, smog, but at aspects such as fragrance, tastes, larger with the perceptual difference distance of cigarette, the product being especially deployed into various essence and flavoring agents, they are difficult to accept or be accustomed to its fragrance and taste.These deficiencies have affected the quality of electronic cigarette greatly, are also restricting the universal and popular of electronic cigarette simultaneously.And traditional leaf tobacco extract is mainly by ethanol or water refluxing extraction at a certain temperature for tobacco leaf or pipe tobacco, be difficult to the burnt odor fragrance in tobacco leaf to extract.
Summary of the invention
The object of the invention is to for existing electronic cigarette liquid in the deficiency aspect the suction sensations such as fragrance, mouthfeel, it is raw material that a kind of white granulated sugar or brown sugar of utilizing is provided, carry out caramelization with offal or pipe tobacco at a certain temperature, the electronic cigarette liquid with burnt odor fragrance obtaining.
In order to achieve the above object, technical scheme provided by the invention is:
The electronic cigarette liquid preparation method described in every 10-50mL with burnt odor fragrance is as follows:
By 20-40g sugar, preferred white granulated sugar or brown sugar, more preferably white granulated sugar is dissolved in the water of 10-30mL, under 80-150 ℃ of conditions, heats 5-15min, then adds 5-10g offal or pipe tobacco, preferred offal, be warming up to 180-250 ℃ of reflux heating 10-20min, the product after reflux heating is dissolved in to the glycerine of 10-50mL, the mixed liquor of second alcohol and water, or glycerine, or in propane diols, after filtration, obtain electronic cigarette liquid.In general, the solvent of electronic cigarette liquid is 70% glycerine (mass percent), 20% ethanol (mass percent) and 10% water (mass percent), can dissolve the material of opposed polarity, solvent of the present invention can be the mixed solvent of glycerine, second alcohol and water, can be also only with glycerine or propane diols.
It is raw material that the present invention utilizes white granulated sugar or brown sugar, carries out caramelization at a certain temperature with offal, pipe tobacco or cigarette ash, obtains having the product of burnt odor fragrance.This odor type cause perfumery and in traditional cigarette combustion process, to produce burnt odor fragrance component similar, this electronic cigarette liquid with burnt odor odor type is after atomizer atomization, smoker feels that this electronic cigarette liquid is consistent with the impression in traditional cigarette combustion process, has the burnt odor in cigarette burning process.Electronic cigarette liquid of the present invention can improve the inherent suction quality of electronic cigarette, makes electronic cigarette more approach fragrance, the taste of cigarette.
The specific embodiment
embodiment 1
The described electronic cigarette liquid preparation method with burnt odor fragrance is as follows:
20g white granulated sugar is dissolved in the water of 10mL, under 150 ℃ of conditions, heats 10min, then add 7g Yunnan Shao to lead to B3F offal, be warming up to 180 ℃ of reflux heating 15min, the product after reflux heating is dissolved in the glycerine of 20mL, after filtration, obtain electronic cigarette liquid.
Get 1mL electronic cigarette liquid and add in atomizer, the personnel that smoke panel test that please be professional smoke panel test, and have Jiao of flue-cured tobacco fragrant and sweet, also have the baking of flue-cured tobacco fragrant simultaneously.
embodiment 2
The described electronic cigarette liquid preparation method with burnt odor fragrance is as follows:
25g white granulated sugar is dissolved in the water of 15mL, under 130 ℃ of conditions, heat 10min, then add 5g Sangzhi B3F offal, be warming up to 180 ℃ of reflux heating 20min, product after reflux heating is dissolved in the mixed liquor of 25mL mass percent is 10% water, mass percent is 70% glycerine, ethanol that mass percent is 20%, after filtration, obtains electronic cigarette liquid.
Get 1mL electronic cigarette liquid and add in atomizer, the personnel that smoke panel test that please be professional smoke panel test, and have Jiao of flue-cured tobacco fragrant and sweet.
 
embodiment 3
The described electronic cigarette liquid preparation method with burnt odor fragrance is as follows:
35g white granulated sugar is dissolved in the water of 30mL, under 140 ℃ of conditions, heats 10min, then add 8g Zimbabwe L1OF offal, be warming up to 180 ℃ of reflux heating 20min, the product after reflux heating is dissolved in the glycerine of 30mL, after filtration, obtain electronic cigarette liquid.
Get 1mL electronic cigarette liquid and add in atomizer, the personnel that smoke panel test that please be professional smoke panel test, and have Jiao of flue-cured tobacco fragrant and sweet.

Claims (2)

1. an electronic cigarette liquid with burnt odor fragrance, is characterized in that, electronic cigarette liquid preparation method is as follows described in every 10-50mL:
20-40g sugar is dissolved in the water of 10-30mL, under 80-150 ℃ of conditions, heat 5-15min, then add 5-10g offal or pipe tobacco, be warming up to 180-250 ℃ of reflux heating 10-20min, product after reflux heating is dissolved in to the glycerine of 10-50mL, the mixed liquor of second alcohol and water, or glycerine, or in propane diols, after filtration, obtain electronic cigarette liquid.
2. electronic cigarette liquid as claimed in claim 1, is characterized in that, described sugar is white granulated sugar or brown sugar.
CN201410287554.4A 2014-06-25 2014-06-25 A kind of electronic cigarette liquid with burnt odor fragrance Active CN104026729B (en)

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104432481A (en) * 2014-10-22 2015-03-25 浙江中烟工业有限责任公司 Electronic cigarette tobacco juice solvents utilizing polypropylene glycol and electronic cigarette tobacco juice and electronic cigarette prepared through electronic cigarette tobacco juice solvents
CN105433431A (en) * 2014-11-12 2016-03-30 湖南中烟工业有限责任公司 Electronic cigarette liquid and electronic cigarette
CN106947596A (en) * 2017-04-12 2017-07-14 安徽中烟工业有限责任公司 A kind of cigarette preparation method of maltose caramel spices
CN107692318A (en) * 2017-10-13 2018-02-16 上海烟草集团有限责任公司 A kind of tobacco juice for electronic smoke and preparation method
CN111254014A (en) * 2020-03-05 2020-06-09 四川中烟工业有限责任公司 Caramel aroma spice, preparation method and application method thereof
CN111248489A (en) * 2020-01-16 2020-06-09 四川中烟工业有限责任公司 Preparation method of scorched, sweet and scorched-aroma type cigar tobacco leaves
CN111411020A (en) * 2020-03-05 2020-07-14 四川中烟工业有限责任公司 Burnt sweet-fragrance bead-blasting oil, preparation method and application method
CN111588073A (en) * 2020-03-05 2020-08-28 四川中烟工业有限责任公司 Burnt sweet-fragrance electronic cigarette tobacco tar, preparation method and application method
CN111602838A (en) * 2020-06-12 2020-09-01 山东瑞博斯烟草有限公司 Feed liquid for increasing scorched and sweet aroma of tobacco leaves and method for treating tobacco leaves
CN112205659A (en) * 2020-09-28 2021-01-12 四川中烟工业有限责任公司 Composite burnt sweet aroma flavor, baking preparation method and application
CN112205663A (en) * 2020-09-28 2021-01-12 四川中烟工业有限责任公司 Composite burnt sweet aroma flavor, extrusion puffing preparation method and application method thereof
CN112369651A (en) * 2020-04-16 2021-02-19 湖北中烟工业有限责任公司 Tobacco-flavored electronic lampblack and preparation method thereof
CN114903196A (en) * 2022-05-11 2022-08-16 河北中烟工业有限责任公司 Coloring additive for tobacco, preparation method thereof and heated cigarette

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US3920026A (en) * 1972-03-07 1975-11-18 Liggett & Myers Inc Tobacco with flavor enhancer
CN1106640A (en) * 1994-02-03 1995-08-16 锦州卷烟厂 Method for preparing health cigarette of reduced tar content
CN101461566A (en) * 2009-01-08 2009-06-24 华健 Atomized liquid of electronic smoke
CN101580757A (en) * 2009-06-02 2009-11-18 上海英华香精香料有限公司 Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method
CN103783658A (en) * 2014-01-21 2014-05-14 杨成云 Preparation method of nicotine liquid perfume
CN103849467A (en) * 2014-03-12 2014-06-11 河南中烟工业有限责任公司 Method for preparing tobacco flavor through maillard reaction with tobacco flower buds as raw material

Patent Citations (6)

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Publication number Priority date Publication date Assignee Title
US3920026A (en) * 1972-03-07 1975-11-18 Liggett & Myers Inc Tobacco with flavor enhancer
CN1106640A (en) * 1994-02-03 1995-08-16 锦州卷烟厂 Method for preparing health cigarette of reduced tar content
CN101461566A (en) * 2009-01-08 2009-06-24 华健 Atomized liquid of electronic smoke
CN101580757A (en) * 2009-06-02 2009-11-18 上海英华香精香料有限公司 Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method
CN103783658A (en) * 2014-01-21 2014-05-14 杨成云 Preparation method of nicotine liquid perfume
CN103849467A (en) * 2014-03-12 2014-06-11 河南中烟工业有限责任公司 Method for preparing tobacco flavor through maillard reaction with tobacco flower buds as raw material

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104432481A (en) * 2014-10-22 2015-03-25 浙江中烟工业有限责任公司 Electronic cigarette tobacco juice solvents utilizing polypropylene glycol and electronic cigarette tobacco juice and electronic cigarette prepared through electronic cigarette tobacco juice solvents
CN104432481B (en) * 2014-10-22 2016-03-30 浙江中烟工业有限责任公司 A kind ofly utilize the tobacco juice for electronic smoke solvent of polypropylene glycol and the tobacco juice for electronic smoke of preparation thereof and electronic cigarette
CN105433431A (en) * 2014-11-12 2016-03-30 湖南中烟工业有限责任公司 Electronic cigarette liquid and electronic cigarette
CN106947596A (en) * 2017-04-12 2017-07-14 安徽中烟工业有限责任公司 A kind of cigarette preparation method of maltose caramel spices
CN106947596B (en) * 2017-04-12 2020-12-25 安徽中烟工业有限责任公司 Preparation method of maltose caramel spice for cigarettes
CN107692318A (en) * 2017-10-13 2018-02-16 上海烟草集团有限责任公司 A kind of tobacco juice for electronic smoke and preparation method
CN111248489A (en) * 2020-01-16 2020-06-09 四川中烟工业有限责任公司 Preparation method of scorched, sweet and scorched-aroma type cigar tobacco leaves
CN111588073A (en) * 2020-03-05 2020-08-28 四川中烟工业有限责任公司 Burnt sweet-fragrance electronic cigarette tobacco tar, preparation method and application method
CN111411020A (en) * 2020-03-05 2020-07-14 四川中烟工业有限责任公司 Burnt sweet-fragrance bead-blasting oil, preparation method and application method
CN111254014A (en) * 2020-03-05 2020-06-09 四川中烟工业有限责任公司 Caramel aroma spice, preparation method and application method thereof
CN112369651A (en) * 2020-04-16 2021-02-19 湖北中烟工业有限责任公司 Tobacco-flavored electronic lampblack and preparation method thereof
CN112369651B (en) * 2020-04-16 2022-11-11 湖北中烟工业有限责任公司 Tobacco-flavored electronic lampblack and preparation method thereof
CN111602838A (en) * 2020-06-12 2020-09-01 山东瑞博斯烟草有限公司 Feed liquid for increasing scorched and sweet aroma of tobacco leaves and method for treating tobacco leaves
CN112205659A (en) * 2020-09-28 2021-01-12 四川中烟工业有限责任公司 Composite burnt sweet aroma flavor, baking preparation method and application
CN112205663A (en) * 2020-09-28 2021-01-12 四川中烟工业有限责任公司 Composite burnt sweet aroma flavor, extrusion puffing preparation method and application method thereof
CN114903196A (en) * 2022-05-11 2022-08-16 河北中烟工业有限责任公司 Coloring additive for tobacco, preparation method thereof and heated cigarette

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