CN103783658A - Preparation method of nicotine liquid perfume - Google Patents
Preparation method of nicotine liquid perfume Download PDFInfo
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- CN103783658A CN103783658A CN201410026777.5A CN201410026777A CN103783658A CN 103783658 A CN103783658 A CN 103783658A CN 201410026777 A CN201410026777 A CN 201410026777A CN 103783658 A CN103783658 A CN 103783658A
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Abstract
Disclosed is a preparation method of nicotine liquid perfume. The preparation method of the nicotine liquid perfume includes the steps of placing, by weight, 2.5 parts of methyl cyclopentenolone, 20 parts of L-proline and 200 parts of propylene glycol in a heating container for heating and stirring, rising temperature in the heating container to be 152-157 DEG C within 14-16min, stirring the mixture for 6-8min at the temperature of 152-157 DEG C, removing the heating container, cooling the mixture at the temperature of 7-10 DEG C, and obtaining claybank viscous liquid after cooling. The perfume prepared according to the method smells like sweet caramel and sweet popcorn, is used as the nicotine liquid perfume and greatly enhances the good taste of electronic cigarettes.
Description
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind of preparation method of electronic cigarette liquid spices.
Background technology
Along with the understanding of people to harmfulness of smoking, increasing people brings into use electronic cigarette product as an alternative, and the aesthetic quality after electronic cigarette suction is the key point of restriction electronic cigarette development always.Electronic cigarette liquid spices is the principal element that determines electronic cigarette mouthfeel, at present, always untapped go out a kind of electronic cigarette liquid spices that liked by vast electronic cigarette fan.
Summary of the invention
For solving the problems of the technologies described above, the present invention proposes a kind of preparation method of electronic cigarette liquid spices, the electronic cigarette liquid spices of producing according to this method, and the fragrance with sweet caramel has sweet puffed rice fragrance concurrently.Its technical scheme is as follows:
A kind of preparation method of electronic cigarette liquid spices, by weight, 200 parts of 2.5 parts of methyl cyclopentenyl ketones, 20 parts of L-proline and propane diols are placed in heating container, add thermal agitation, in 14-16 minute, the temperature in heating container is risen to 152-157 ℃, maintain and stir 6-8 minute at 152-157 ℃, remove firing equipment, be placed under 7-10 ℃ of environment coolingly, obtain brown color thick liquid after cooling.
Methyl cyclopentenyl ketone has caramel sample agreeable odor like coffee, has the sweet fragrance of maple maple sample, therefore there is the title of " maple maple lactone " when dilution.Be a kind of good fumet and low-calorie sweetener, can be widely used in the composition such as food, beverage.L-proline can be used as fragrance synergist, and propane diols is mainly used in the solvent of various spices, pigment, anticorrisive agent, the extractant of vanilla bean, roasted coffee grain, natural perfume material etc.Make us unexpected and surprised: the spices of producing according to this method, the fragrance with sweet caramel has sweet puffed rice fragrance concurrently, used as electronic cigarette liquid spices, has greatly strengthened the fine mouthfeel of electronic cigarette.
The specific embodiment
embodiment 1
200 grams of 2.5 grams of methyl cyclopentenyl ketones, 20 grams of L-proline and propane diols are placed in heating container, add thermal agitation, in 14 minutes, temperature in heating container is risen to 152 ℃, maintain and stir 6 minutes at 152 ℃, remove firing equipment, be placed under 7 ℃ of environment coolingly, obtain brown color thick liquid after cooling.
embodiment 2
200 parts of 2.5 parts of methyl cyclopentenyl ketones, 20 parts of L-proline and propane diols are placed in heating container, add thermal agitation, in 15 minutes, temperature in heating container is risen to 155 ℃, maintain and stir 7 minutes at 155 ℃, remove firing equipment, be placed under 8 ℃ of environment coolingly, obtain brown color thick liquid after cooling.
embodiment 3
200 parts of 2.5 parts of methyl cyclopentenyl ketones, 20 parts of L-proline and propane diols are placed in heating container, add thermal agitation, in 16 minutes, temperature in heating container is risen to 157 ℃, maintain and stir 8 minutes at 157 ℃, remove firing equipment, be placed under 10 ℃ of environment coolingly, obtain brown color thick liquid after cooling.
Claims (1)
1. the preparation method of an electronic cigarette liquid spices, it is characterized in that: by weight, 200 parts of 2.5 parts of methyl cyclopentenyl ketones, 20 parts of L-proline and propane diols are placed in heating container, add thermal agitation, in 14-16 minute, the temperature in heating container is risen to 152-157 ℃, maintain and stir 6-8 minute at 152-157 ℃, remove firing equipment, be placed under 7-10 ℃ of environment coolingly, obtain brown color thick liquid after cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410026777.5A CN103783658A (en) | 2014-01-21 | 2014-01-21 | Preparation method of nicotine liquid perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410026777.5A CN103783658A (en) | 2014-01-21 | 2014-01-21 | Preparation method of nicotine liquid perfume |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103783658A true CN103783658A (en) | 2014-05-14 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410026777.5A Pending CN103783658A (en) | 2014-01-21 | 2014-01-21 | Preparation method of nicotine liquid perfume |
Country Status (1)
| Country | Link |
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| CN (1) | CN103783658A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104026729A (en) * | 2014-06-25 | 2014-09-10 | 湖南中烟工业有限责任公司 | Electronic cigarette liquid with scorch aroma |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3920026A (en) * | 1972-03-07 | 1975-11-18 | Liggett & Myers Inc | Tobacco with flavor enhancer |
| CN1334031A (en) * | 2000-05-23 | 2002-02-06 | 雀巢制品公司 | Use of alpha-ketoenamine derivatives as adjuvants |
| CN101268867A (en) * | 2008-02-29 | 2008-09-24 | 修运强 | Electronic simulation cigarette and atomizing liquid |
| CN101787329A (en) * | 2010-03-10 | 2010-07-28 | 广东中烟工业有限责任公司 | Tobacco flavor as well as preparation method and application thereof |
| CN102140389A (en) * | 2011-01-28 | 2011-08-03 | 湖南中烟工业有限责任公司 | Ortho-hydroxyl ketone prepared essence and application thereof |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
-
2014
- 2014-01-21 CN CN201410026777.5A patent/CN103783658A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3920026A (en) * | 1972-03-07 | 1975-11-18 | Liggett & Myers Inc | Tobacco with flavor enhancer |
| CN1334031A (en) * | 2000-05-23 | 2002-02-06 | 雀巢制品公司 | Use of alpha-ketoenamine derivatives as adjuvants |
| CN101268867A (en) * | 2008-02-29 | 2008-09-24 | 修运强 | Electronic simulation cigarette and atomizing liquid |
| CN101787329A (en) * | 2010-03-10 | 2010-07-28 | 广东中烟工业有限责任公司 | Tobacco flavor as well as preparation method and application thereof |
| CN102140389A (en) * | 2011-01-28 | 2011-08-03 | 湖南中烟工业有限责任公司 | Ortho-hydroxyl ketone prepared essence and application thereof |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104026729A (en) * | 2014-06-25 | 2014-09-10 | 湖南中烟工业有限责任公司 | Electronic cigarette liquid with scorch aroma |
| CN104026729B (en) * | 2014-06-25 | 2015-11-04 | 湖南中烟工业有限责任公司 | A kind of electronic cigarette liquid with burnt odor fragrance |
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| C10 | Entry into substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20140514 |
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| RJ01 | Rejection of invention patent application after publication |