CN104946390B - A kind of processing method of electronics natural perfume for cigarette - Google Patents
A kind of processing method of electronics natural perfume for cigarette Download PDFInfo
- Publication number
- CN104946390B CN104946390B CN201510286777.3A CN201510286777A CN104946390B CN 104946390 B CN104946390 B CN 104946390B CN 201510286777 A CN201510286777 A CN 201510286777A CN 104946390 B CN104946390 B CN 104946390B
- Authority
- CN
- China
- Prior art keywords
- extract
- natural perfume
- cigarette
- electronics
- processing method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Seasonings (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to tobacco juice for electronic smoke field, the processing method of specifically a kind of electronics natural perfume for cigarette, it is characterised in that：By natural perfume material water or ethanol solution (concentration is less than 30%) according to 1:1~1:4 dilution proportion, supernatant is detached by 0.22 ~ 0.45 μm of filter membrane first after centrifugation, then obtains molecular weight distribution in the component of 5 ~ 10kD, electronics natural perfume for cigarette that as treated by hyperfiltration technique.The great advantage of the present invention is to provide a kind of processing method of electronics natural perfume for cigarette, the high boiling substances such as polysaccharide, protein, pectin, the wax in natural perfume material can be removed with a stepization by this method, remain small molecule flavor component, treated that natural perfume material can be used in electronic cigarette blending for gained, solve the problems, such as that natural perfume material is also easy to produce when in use and be charred taste, and this method widened electronic cigarette can use fragrance use scope.
Description
Technical field
The invention belongs to tobacco juice for electronic smoke technical fields, and in particular to a kind of processing method of electronics natural perfume for cigarette.
Background technology
With《The Framework Convention on Tobacco Control》Come into effect, countries in the world public place smoking ban range gradually expand
Greatly, profound change just occurs for domestic and international tobacco consumption environment.The considerations of for factors such as health, some consumers are gradually mesh
Light turns to electronic cigarette, and in recent years, substitute of the electronic cigarette as traditional cigarette is fast-developing in the country such as America and Europe.Electronic cigarette is
A kind of electronic device transmitting nicotine to respiratory system by mode of heating, compared with traditional cigarette, without burning, thus
It has the following advantages：Without harmful components such as tar, CO, hydrogen cyanide；It not will produce secondhand smoke and do not generate cigarette ash and stub.
Tobacco aromaticss are divided into synthetic perfume and natural perfume material, are striven since people always exist the safety problem of synthetic perfume
View, thus its application is restricted.Compared with synthetic perfume, natural perfume material is with the rich of its note and the safety etc. used
Advantage, by more favors of tobacco productive corporation.But it is general all containing polysaccharide, protein, cellulose, fruit in natural perfume material
The wax components such as the macromolecular substances such as glue and long-chain fat hydrocarbon.The heating temperature of electronic cigarette is relatively low, these macromolecular substances exist
200 oC~250 oIt can not gasify under the heated condition of C, eventually be deposited on the heater strip of atomizer, generation is charred taste, increases
Sweet sense seriously affects the suction quality of electronic cigarette and the service life of atomizer.In addition, after using these fragrance, in tobacco juice
It is easy the insoluble wax of flowing, common separation method can not efficiently separate, and seriously affect the quality of tobacco juice, these tobacco juices
If in the electronic cigarette smoking set with transparent device for storing liquid, the sensory experience of consumer can be also influenced.These disadvantages or not
Foot causes use of the natural perfume material in tobacco juice for electronic smoke to be restricted.
It is more about the patent of tobacco juice for electronic smoke at present, such as a kind of tobacco juice for electronic smoke (CN prepared using strong-flavor tobacco leaf
103054172 A), it is a kind of it is effective reduce oral cavity sweet sense Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke (103989245 A of CN),
A kind of fragrant and sweet type tobacco juice for electronic smoke of coke (104026730 A of CN), a kind of tobacco juice for electronic smoke (CN rich in plant flavone
104068467 A), a kind of electronic cigarette atomization tobacco juice and preparation method (application number 201310686110.3), medicinal health type
Solid electronic aerosolization liquid and preparation method (101933653 B of CN), atomized liquid of electronic smoke (CN101461566 B) etc..For
Realization certain functions contain tobacco extract, absolute oil and natural plant extracts in these patent formulations more, and these cigarettes are used
Fragrance is direct use, and without any processing, this will seriously affect the organoleptic quality of tobacco juice for electronic smoke.
UF membrane is through film using selectivity as separating medium, using film to the difference of mixture each component permeance property,
Realize separation, purifying and the enrichment that physics is carried out to multicomponent mixture.According to molecular cut off difference, be divided into microfiltration membranes,
Ultrafiltration membrane, NF membrane and reverse osmosis membrane.The wherein relative molecular mass ranging from 5 × 10 of ultrafiltration membrane retention-3~5×10-5, naturally
The relative molecular mass of starch, protein, pectin, polysaccharide etc. is about 5 × 10 in fragrance and tobacco extract-4.It selects appropriate super
Filter membrane can effectively remove the macromolecular substances that negative interaction is played to electronic cigarette, retain effumability small molecule aroma substance, effectively
Improve the organoleptic quality of tobacco juice for electronic smoke.
Invention content
For the disadvantage for overcoming above-mentioned, the present invention provides a kind of processing method of electronics natural perfume for cigarette, and this method can incite somebody to action
The macromolecular substances such as polysaccharide, starch, protein, pectin, wax in natural perfume material disposably remove, and effectively widen electronic cigarette and use
The use scope of fragrance.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of processing method of electronics natural perfume for cigarette, includes the following steps：
Electronics natural perfume for cigarette is uniformly mixed, 1 ~ 4 times of amount water or ethanol solution is added（Concentration is less than 30%）, will be dilute
It releases liquid and stirs 10 ~ 40 min at a temperature of room temperature is to 50 C, after being cooled to room temperature, centrifuge supernatant (4000 ~ 6000
rpm, 10~30 min)；Supernatant is further detached by membrane separation plant, first with 0.22 ~ 0.45 μm of micro-filtrate membrane filtration,
Then with ultrafiltration membrane obtain molecular weight distribution 5 ~ 10kD component；It is concentrated under reduced pressure into the 1/4 ~ 1/2 of original volume；It can be obtained point
Son amount is distributed in the electronics natural perfume for cigarette of 5 ~ 10kD.
The electronics natural perfume for cigarette includes tobacco extract, maple maple extract, fenugreek extract, red bayberry extraction
Object, tamarind extract, cocoa extract, cocoa shell extract, coffee-extract, malt extract, Chinese date extract, hawthorn carry
Take object, attar of rose, mitoridining rude incense paste, Benzoinum extract, anise extract, apricot extract, cider, pear extract, black
Gallon extract, carob extract, tamarind extract, cherry extract, Flos Osmanthi Fragrantis extract, radix tarxaci solid extract,
One or more of licorice, vanilla extract, tea extract, chrysanthemum extract, Peru's extract exist
Form can be medicinal extract, tincture or absolute oil.
Compared with the existing technology, the present invention detaches natural perfume material using membrane separation technique, obtains molecular weight distribution
In the volatile aroma constituent of 5 ~ 10 kD, which has the following advantages：
Natural perfume material processing method of the present invention eliminates the more polysaccharide of content in natural perfume material, starch, fruit
The macromolecular substances such as glue, cellulose solve the problems, such as that these natural perfume materials easy to produce when in use and are charred taste, effectively open up
Wide tobacco juice for electronic smoke can use the use scope of fragrance.
Specific implementation mode
The present invention is described further with reference to embodiments, but is not intended to limit the present invention.
Embodiment 1
6 g fenugreek extracts, 10 g coffee-extracts, 5 g tea extracts and 8 g chrysanthemum concretes are uniformly mixed,
The dilution of 60 g water is added, is stirred 30 minutes under 50 C water bath conditions.Gained dilution is centrifuged into supernatant (4000
Rpm, 30min)；Subsequent supernatant passes through 0.22 μm of micro-filtrate membrane filtration；Filtrate passes through the Ultra filtration membrane of 8kD again after film；Filter
Liquid is concentrated under reduced pressure into the 1/2 of original volume, you can the electronics natural perfume for cigarette that obtains that treated.
Embodiment 2
8 g mitoridining rude incense pastes, 10 g apricots extracts, 10 g red bayberries extracts and 12 g tamarind medicinal extract are uniformly mixed, are added
10% ethanol solution for entering 40g, stirs 20min at ambient temperature.By gained dilution centrifuge supernatant (6000 rpm,
10min)；Subsequent supernatant passes through 0.45 μm of micro-filtrate membrane filtration；Filtrate passes through the Ultra filtration membrane of 10 kD again after film；Filtrate
It is concentrated under reduced pressure into the 1/3 of original volume, you can the electronics natural perfume for cigarette that obtains that treated.
Embodiment 3
By 12g hawthorn extracts, 10g ciders, 6g cocoa extracts, 9g coffee-extracts, 8g licorices and mixing
Uniformly, 30% ethanol solution of 135g is added, is stirred 10 minutes under 50 C water bath conditions.Gained dilution is centrifuged
Clear liquid (5000 rpm, 20min)；Subsequent supernatant passes through 0.22 μm of micro-filtrate membrane filtration；Filtrate passes through the super of 5kD again after film
Filter membrane detaches, you can the electronics natural perfume for cigarette that obtains that treated.
Embodiment 4
50 g of date extract is weighed, 200 g water are added, 20 min are stirred under 40 C water bath conditions.By gained dilution
Centrifuge supernatant (4000 rpm, 20min)；Subsequent supernatant passes through 0.22 μm of micro-filtrate membrane filtration；Filtrate is led to again after film
Cross the Ultra filtration membrane of 5kD, you can the Chinese date extract that obtains that treated.
Claims (2)
1. a kind of processing method of electronics natural perfume for cigarette, it is characterised in that：Include the following steps：
Electronics natural perfume for cigarette is uniformly mixed, 1 ~ 4 times of amount water is added or concentration is less than 30% ethanol solution, dilution is existed
10 ~ 40 min are stirred at a temperature of room temperature to 50 C, after being cooled to room temperature, centrifuge supernatant, actual conditions are 4000 ~ 6000
Rpm, 10 ~ 30 min；Supernatant is further detached by membrane separation plant, first with 0.22 ~ 0.45 μm of micro-filtrate membrane filtration, with
Afterwards with ultrafiltration membrane obtain molecular weight distribution 5 ~ 10kD component, to remove the more polysaccharide of content in natural perfume material, starch, fruit
Glue, cellulose macromolecule substance, avoid the problem that natural perfume material using when easy to produce and be charred taste；It is concentrated under reduced pressure into original volume
1/4~1/2；Can be obtained molecular weight distribution 5 ~ 10kD electronics natural perfume for cigarette.
2. the processing method of electronics natural perfume for cigarette according to claim 1, it is characterised in that：The electronic cigarette day
Right fragrance includes tobacco extract, maple maple extract, fenugreek extract, red bayberry extract, tamarind extract, can extract
Object, cocoa shell extract, coffee-extract, malt extract, Chinese date extract, haw thorn extract, attar of rose, mitoridining rude incense paste,
Benzoinum extract, anise extract, apricot extract, cider, pear extract, blackcurrant extract, carob extract,
Tamarind extract, cherry extract, Flos Osmanthi Fragrantis extract, radix tarxaci solid extract, licorice, vanilla extraction
One or more of object, tea extract, chrysanthemum extract, existence form are medicinal extract, tincture or absolute oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510286777.3A CN104946390B (en) | 2015-05-31 | 2015-05-31 | A kind of processing method of electronics natural perfume for cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510286777.3A CN104946390B (en) | 2015-05-31 | 2015-05-31 | A kind of processing method of electronics natural perfume for cigarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104946390A CN104946390A (en) | 2015-09-30 |
| CN104946390B true CN104946390B (en) | 2018-10-23 |
Family
ID=54161463
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510286777.3A Active CN104946390B (en) | 2015-05-31 | 2015-05-31 | A kind of processing method of electronics natural perfume for cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104946390B (en) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105542959A (en) * | 2015-12-17 | 2016-05-04 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette liquid flavor |
| CN105768198B (en) * | 2016-04-29 | 2017-09-19 | 江苏中烟工业有限责任公司 | Tobacco juice for electronic smoke of tongue delicate fragrance aromatic style feature and preparation method thereof |
| CN106165906B (en) * | 2016-07-25 | 2018-03-09 | 中国烟草总公司郑州烟草研究院 | Suitable for the burnt fragrant and sweet spices of the malt of cigarette products and the application tobacco product |
| CN106617266B (en) * | 2016-12-19 | 2018-05-29 | 深圳瀚星翔科技有限公司 | Tobacco juice for electronic smoke |
| CN108865438A (en) * | 2018-06-15 | 2018-11-23 | 广西中烟工业有限责任公司 | A kind of cigarette preparation method of Radix Angelicae Sinensis fragrance and the application in cigarette |
| CN108851209B (en) * | 2018-06-15 | 2020-10-23 | 广西中烟工业有限责任公司 | Tobacco Huai chrysanthemum perfume and preparation method and application of microcapsule thereof |
| CN108851210A (en) * | 2018-06-15 | 2018-11-23 | 广西中烟工业有限责任公司 | A kind of preparation method and application of cigarette mango fragrance and its microcapsules |
| CN108851173A (en) * | 2018-06-15 | 2018-11-23 | 广西中烟工业有限责任公司 | A kind of cigarette preparation method of mango fragrance and the application in cigarette |
| CN108851172A (en) * | 2018-06-15 | 2018-11-23 | 广西中烟工业有限责任公司 | A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette |
| CN108865437B (en) * | 2018-06-15 | 2020-10-23 | 广西中烟工业有限责任公司 | Preparation method of perilla seed spice for cigarettes and application of perilla seed spice in cigarettes |
| CN109082344B (en) * | 2018-07-03 | 2022-04-22 | 福建中烟工业有限责任公司 | Tobacco essence perfume, cigarette paper containing tobacco essence perfume and application of cigarette paper |
| CN109259296B (en) * | 2018-09-13 | 2021-10-26 | 云南中烟工业有限责任公司 | Electronic cigarette oil with tea baking fragrance and preparation method and application thereof |
| CN109259297B (en) * | 2018-09-25 | 2021-03-23 | 云南中烟工业有限责任公司 | Coffee roasted fragrant electronic tobacco tar and preparation method and application thereof |
| CN109259294B (en) * | 2018-09-25 | 2021-08-03 | 云南中烟工业有限责任公司 | Coffee roasted fragrant reconstituted tobacco and preparation method and application thereof |
| CN109984373A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Pear extract solution, pear electronics tobacco tar and preparation method thereof |
| CN111567850B (en) * | 2020-05-20 | 2022-06-24 | 云南瑞升烟草技术（集团）有限公司 | Refined preparation method of natural spice suitable for cigarette without burning under heating |
| CN111849632B (en) * | 2020-07-24 | 2023-06-20 | 云南养瑞科技集团有限公司 | Deep processing method of natural fragrant raw material for cigarettes and application of natural fragrant raw material in novel tobacco |
| CN111849639A (en) * | 2020-08-07 | 2020-10-30 | 江苏华祺生物科技有限公司 | Apricot liquid essence for cigarettes and production process thereof |
| KR102628986B1 (en) * | 2020-08-25 | 2024-01-24 | 주식회사 케이티앤지 | Flavor containing sheet comprising lm-pectin for smoking articles and smoking article comprising the same |
| CN113424980B (en) * | 2021-06-22 | 2023-03-17 | 云南中烟新材料科技有限公司 | Preparation method and application of coffee tobacco flavor |
| CN113349414B (en) * | 2021-07-13 | 2022-08-02 | 云南中烟工业有限责任公司 | Preparation of low-temperature fraction with aroma enhancement function applied to heated cigarette and application of low-temperature fraction in heated cigarette |
| CN113897242B (en) * | 2021-09-28 | 2024-05-14 | 深圳市真味生物科技有限公司 | Natural spice prepared from scorched malt and electronic atomized liquid |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101608144A (en) * | 2008-06-16 | 2009-12-23 | 湖北中烟工业有限责任公司 | A kind of preparation method of strawberry tobacco aromatics using |
| CN103497833A (en) * | 2013-09-11 | 2014-01-08 | 上海聚华科技股份有限公司 | Cigarette waxberry flavor preparation method |
| CN104489911A (en) * | 2014-12-17 | 2015-04-08 | 贵州中烟工业有限责任公司 | Tobacco juice of electronic cigarette |
-
2015
- 2015-05-31 CN CN201510286777.3A patent/CN104946390B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101608144A (en) * | 2008-06-16 | 2009-12-23 | 湖北中烟工业有限责任公司 | A kind of preparation method of strawberry tobacco aromatics using |
| CN103497833A (en) * | 2013-09-11 | 2014-01-08 | 上海聚华科技股份有限公司 | Cigarette waxberry flavor preparation method |
| CN104489911A (en) * | 2014-12-17 | 2015-04-08 | 贵州中烟工业有限责任公司 | Tobacco juice of electronic cigarette |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104946390A (en) | 2015-09-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104946390B (en) | A kind of processing method of electronics natural perfume for cigarette | |
| CN104839885B (en) | A kind of electronic cigarette liquid and preparation method thereof of improvement | |
| RU2761996C1 (en) | Method for manufacturing filtering rods from a pla bundle with low resistance to draw for reducing the smoking temperature | |
| CN105962426B (en) | Composition and tobacco juice for electronic smoke containing extra-strong tea extract | |
| JP2020114244A (en) | Protein-enriched tobacco-derived composition | |
| CN104403794A (en) | Preparation method and application of Pu'er tea extract to cigarettes | |
| CN103783660B (en) | The supercritical extraction method of flavor matter and application thereof in a kind of tobacco leaf fragment | |
| CN106307603A (en) | Method for preparing Maillard reactant for cigarettes by taking natural plant extract as raw material | |
| CN106037012B (en) | A kind of tobacco juice for electronic smoke | |
| CN104531353A (en) | Casing flavor for light flavor-style cigarettes | |
| KR20180068236A (en) | Liquid composition for eletronic cigarette and manufacture method thereof | |
| CN109156895A (en) | A kind of reduction cigarette smoking dry sensation and irritating filter stick additive, preparation method and the usage | |
| JP5005017B2 (en) | Production method of regenerated sliced bamboo leaf and its application in tobacco products | |
| CN107637858A (en) | A kind of plant for improving water extraction and alcohol precipitation method extraction causes perfumery and extracting method and application | |
| CN110226774A (en) | A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling | |
| CN101455442B (en) | Grape extractum and preparation method thereof and use thereof in cigarette performing | |
| CN108618192A (en) | A kind of 15 are formulated electronic cigarette tobacco tar and preparation method thereof | |
| CN108949347A (en) | Increase the essence and its preparation method and application for heating the new cigarette flue gas moist feeling that do not burn | |
| CN112716028A (en) | Additive for composite cigarette, preparation method and application | |
| CN104593150A (en) | Preparation method of mulberry extract and application of mulberry extract in cigarettes | |
| CN103222679A (en) | Method for preparing tobacco fragment extractives by high-pressure-puffing-flocculation and application of extractives | |
| CN114098141B (en) | Electronic atomized liquid containing borneol plant components and preparation method thereof | |
| CN104223351A (en) | Tea and chrysanthemum cigarette and preparing method thereof | |
| CN101322581B (en) | Mineral ether-extracted Pu'er cooked tea extract and preparation and use thereof | |
| CN107495463A (en) | A kind of preparation method of fruit cigarette |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |